This study investigated the synthesis of zeolite from fly ash and its ability to remove Amido Black dye from wastewater through adsorption. Zeolite was synthesized from fly ash through a process involving calcination, fusion with sodium hydroxide, and aging. Experiments examined the adsorption of Amido Black dye onto zeolite. Results showed that dye removal efficiency increased with zeolite concentration up to 10 g/L, beyond which no significant improvement occurred. The optimal zeolite concentration for dye removal was 10 g/L. Adsorption capacity decreased as zeolite concentration increased, indicating too much zeolite is not effective. The study demonstrated that fly ash-based zeol
Name: - Thall ium(I I I ) Nit rate t rihydrate
• Abbreviat ion: - TTN
• Melt ing point : - 102-105 °C.
• Solubi lity: - water, organic solvents.
• General informat ion:-
o Oxidizing agent ; Lewis acid.
o All thall ium compounds are ext remely toxic to
inhalat ion, skin contact , and ingest ion. Toxicity is
cumulat ive. Ext reme caut ion should be used when
handling these materials. Use in a fume hood.
Thallium nitrate is a select ive and versat i le oxidizing agent ,
general ly accompanied by reduct ion of Tl(I I I ) to Tl(I ). Thallium
nitrate is elect rophil ic in character, so it reacts wi th alkenes &
alkynes to give addit ion products.
I t is very ef fect ive oxidizing agent because: -
(i ) Reduct ion potent ial of this half cell react ion is posit ive and
high.
(i i) Carbon-TI(I I I ) bond is very weak, so it undergo heterolyt ic
cleavage very readily and form carbocat ion easi ly.
(i ii ) Nit rate-ion is not a very good nucleophile, so the solvent
may part icipate select ively as nucleophile in the react ion.
Ionic Liquids : Green solvents for the futureMrudang Thakor
Ionic Liquids are entirely made up of Ions also known as Room Temperature Ionic Liquids (RTILs).
They are in demand because of their unmatchable uses and applications in the field of chemistry.
Zeolites (clinoptilolite) are volcanic tuff minerals,
which are formed when ash and lava from a volcano have a
chemical reaction with cool sea water, are naturally
negatively charged with a cage-like structure. The most
prominent features of Zeolites include the exchange of
cations and absorption of inorganic and organic molecules of
specific dimensions. Their high mechanical strength,
chemical stability,and abrasion values make Zeolites a
special material for water purifications and many more
applications. The negative chargesact as a magnet to attract
positively charged toxins and heavy metals to the Zeolites
Name: - Thall ium(I I I ) Nit rate t rihydrate
• Abbreviat ion: - TTN
• Melt ing point : - 102-105 °C.
• Solubi lity: - water, organic solvents.
• General informat ion:-
o Oxidizing agent ; Lewis acid.
o All thall ium compounds are ext remely toxic to
inhalat ion, skin contact , and ingest ion. Toxicity is
cumulat ive. Ext reme caut ion should be used when
handling these materials. Use in a fume hood.
Thallium nitrate is a select ive and versat i le oxidizing agent ,
general ly accompanied by reduct ion of Tl(I I I ) to Tl(I ). Thallium
nitrate is elect rophil ic in character, so it reacts wi th alkenes &
alkynes to give addit ion products.
I t is very ef fect ive oxidizing agent because: -
(i ) Reduct ion potent ial of this half cell react ion is posit ive and
high.
(i i) Carbon-TI(I I I ) bond is very weak, so it undergo heterolyt ic
cleavage very readily and form carbocat ion easi ly.
(i ii ) Nit rate-ion is not a very good nucleophile, so the solvent
may part icipate select ively as nucleophile in the react ion.
Ionic Liquids : Green solvents for the futureMrudang Thakor
Ionic Liquids are entirely made up of Ions also known as Room Temperature Ionic Liquids (RTILs).
They are in demand because of their unmatchable uses and applications in the field of chemistry.
Zeolites (clinoptilolite) are volcanic tuff minerals,
which are formed when ash and lava from a volcano have a
chemical reaction with cool sea water, are naturally
negatively charged with a cage-like structure. The most
prominent features of Zeolites include the exchange of
cations and absorption of inorganic and organic molecules of
specific dimensions. Their high mechanical strength,
chemical stability,and abrasion values make Zeolites a
special material for water purifications and many more
applications. The negative chargesact as a magnet to attract
positively charged toxins and heavy metals to the Zeolites
what is metal allyl complex
what is the definition of metal allyl complex
what are synthesis of metal allyl complex
what are reaction of metal allyl complex
summary of metal allyl complex
zeolites, types, nature, synthetic, processes, Deposits and properties;Physical characteristics of some naturally occurring zeolites; molecular sieves;Adsorption and related molecular sieving; zeolite catalysts
In these work, new nano and micro thermoplastic based composite is prepared with zeolite filler, The method involves using zeolite in powder form, the preparation of zeolite powder from ores by crushing it into small - sized granules. The characteristics of the zeolite powder are determined. The physical properties and chemical composition (XRD) are evaluated before impeding it into the thermoplastic. Thermoplastics powder are added to the zeolite powder as granules in different sizes, The particles sizes ranging from the size of a millimeter to nanometer. The manufacturing quality parameters are optimized at volume percentages of filler in the range 20 to 25 % , composite material is formed into molds. New Composite material is characterized by easy deformation into different shapes beside machine ability. The characteristics of new composite such as SEM, EDX,FTIR in absorption and transmission mode are evaluated and compared with the standard characteristics of Zeolite ores. The performance and characteristics of the new composite are completely different. The new composite is hard, solid and does not absorb water. The work end with list of recommendation about the new field and expected application of Zeolite when using it as filler in thermoplastic based micro and nano composites.
Carbon Dioxide to Chemicals and Fuels Course Material.
National Centre for Catalysis Research (NCCR, IIT Madras), considered for the first on-line course the topic of Carbon dioxide to Chemicals and Fuels. NCCR has learnt many such lessons which are necessary for the researchers to understand and also have a complete comprehension of the limitations.
what is metal allyl complex
what is the definition of metal allyl complex
what are synthesis of metal allyl complex
what are reaction of metal allyl complex
summary of metal allyl complex
zeolites, types, nature, synthetic, processes, Deposits and properties;Physical characteristics of some naturally occurring zeolites; molecular sieves;Adsorption and related molecular sieving; zeolite catalysts
In these work, new nano and micro thermoplastic based composite is prepared with zeolite filler, The method involves using zeolite in powder form, the preparation of zeolite powder from ores by crushing it into small - sized granules. The characteristics of the zeolite powder are determined. The physical properties and chemical composition (XRD) are evaluated before impeding it into the thermoplastic. Thermoplastics powder are added to the zeolite powder as granules in different sizes, The particles sizes ranging from the size of a millimeter to nanometer. The manufacturing quality parameters are optimized at volume percentages of filler in the range 20 to 25 % , composite material is formed into molds. New Composite material is characterized by easy deformation into different shapes beside machine ability. The characteristics of new composite such as SEM, EDX,FTIR in absorption and transmission mode are evaluated and compared with the standard characteristics of Zeolite ores. The performance and characteristics of the new composite are completely different. The new composite is hard, solid and does not absorb water. The work end with list of recommendation about the new field and expected application of Zeolite when using it as filler in thermoplastic based micro and nano composites.
Carbon Dioxide to Chemicals and Fuels Course Material.
National Centre for Catalysis Research (NCCR, IIT Madras), considered for the first on-line course the topic of Carbon dioxide to Chemicals and Fuels. NCCR has learnt many such lessons which are necessary for the researchers to understand and also have a complete comprehension of the limitations.
2. Debido a que el ser humano ha deteriorado el medio ambiente de una manera casi irreparable, se han establecido ciertas medidas de cuidado hacia el medio ambiente, sin embargo; no se han obtenido buenos resultados y, el problema ahora afecta también a los seres vivos.
3. Es por ello que se ha estudiado un nuevo mineral que podria ayudarnos en varios aspectos de gran relevancia, como lo son el medio ambiente, la salud, la agricultura, etc.
4. Este mineral lleva el nombre de Zeolita, el cual proviene de las palabras Zeos (hervir) y Lithos (piedra), es decir «Piedra Hirviente».
5. ANTECEDENTES
En América Latina, y concretamente en Cuba, los primeros yacimientos de Zeolita fueron identificados a principios de los años 70.
6. A mediados de esa década se comenzaron sus estudios sobre posibles aplicaciones, obteniéndose resultados alentadores en aplicaciones agropecuarias y particularmente en alimentación animal.
7. Gracias a diferentes estudios e investigaciones, se han logrado obtener más aplicaciones para el uso de este mineral , tanto; que es sensato pensar que la zeolita podría convertirse en un gran recurso.
8. Es por ello que nos enfocamos en investigar los usos y aplicaciones en diferentes sectores y ámbitos para poder conocerla y aplicarla en nuestra vida diaria para detener o mejorar nuestro entorno.
9. DESARROLLO
Las zeolitas están compuestas por tetraedros formados por un catión y cuatro átomos de oxígenos, es decir TO4. El catión, T, puede ser silicio (Si),aluminio (Al) o incluso germanio (Ge).
10. Existen varios tipos de zeolita natural, que surgen en las rocas sedimentarias y que se encuentran constituidas por aluminio, silicio, hidrógeno, oxígeno, y un número variable de moléculas de agua.
11. Clasificación Por Grupo
12. Usos y Aplicaciones
13. Imagen
14. imagen
15. BIBLIOGRAFIA
Zeocat. (2008). Zeolitas y sus aplicaciones. 2010, de Zeocat Soluciones ecológicas S.L.U Sitio web: http://www.zeocat.es/index.htm
Cheng, Jun; Xu, Ruren; Yang, Guangdi (1991). «Synthesis, structure and characterization of a novel germanium dioxide with occluded tetramethylammonium hydroxide». Journal of the Chemical Society, Dalton Transactions (6): pp. 1537
Clean Air Technology Center. (1999). Zeolita un absorbente versatil de contaminantes de aire. 2013, de EPA Sitio web: http://www.epa.gov/ttn/catc/dir2/zeolits2.pdf
16. Coombs D S, Alberti A, Armbruster T, Artioli G, Colella C, Galli E, Grice J D, Liebau F, Mandarino J A, Minato H, Nickel E H, Passaglia E, Peacor D R, Quartieri S, Rinaldi R, Ross M, Sheppard R A, Tillmanns E, Vezzalini G, (1997) "Recommended nomenclature for zeolite minerals: report of the Subcommittee on Zeolites of the International Mineralogical Association, Commission on New Minerals and Mineral Names". The Canadian Mineralogist, 35, 1571-1606
Just basics of mesoporous materials!!The Break through came around 1992 by both Japanese and Mobil scientist on the soft template based synthesis of mesoporous materials
Abstract :
Although solutions to the challenge of binaural artificial recreation of audio specializations exist in the Computer Music domain, a review of the area suggests that a comprehensive, generic, accurate and efficient tool set is required; hence this paper/thesis will deal with automated sound creation using sound synthesis. The entire setup was implemented using Csound. Csound implements many synthesis techniques unavailable through other means, such as user-controlled physical modeling.
Recent studies commissioned by UNICEF Kosovo show clearly that children are at significantly greater risk of poverty in Kosovo compared to the general population. Using the generally accepted consumption poverty line of €1.417 per person
per day, based on 2006/7 Household Budget Survey data, 46.2% of the Kosovo population is in poverty, whereas 48.6% of children aged 0-19 are in poverty. The highest risks of poverty are faced by children who live in households with three or more children; children aged 0-14; children of unemployed parents; children in households receiving social assistance; and children in households with low levels of education. Whilst the risk of poverty is lower for children where at least
one family member is employed, children in wage-earning households make up 36% of all children in poverty in Kosovo.
Operational parameters affecting the removal and recycling of direct blue ind...IJEAB
In this work the ability of “bleached” oil mill solid waste to reduce the dyestuff content in industrial textile wastewater was studied. Bleaching treatment consists in a preliminary oil mill solid waste management with NaOH and NaClO2 for obtaining cellulosic materials, mainly removing lignin from the waste surface. Thus, a novel bioadsorbent from agricultural residues, named bleached olive pomace (OP), was presented. Direct Blue 78 was studied as a model azoic dye. Experiments were planned to study the effect of different initial conditions on the adsorption processes: oil mill waste amount as grains and as a fine powder (OPP), solution temperature values, initial dye concentration, pH values and electrolytes influence. The results showed that the adsorption process using bleached oil mill waste determined an excellent degree of water color reduction, reaching the best work conditions when pH 2 and OPP were used. The presence of electrostatic interactions was also suggested. The adsorption appeared to be influenced by temperature values showing an endothermic character. Interestingly, to confirm the role of ionic interactions between dye and sorbent at pH 2, fashionable results were obtained. The adsorption process was verified also at pH 6 with 100% of dye removal in presence of both NaCl and Na2SO4 avoiding the aforementioned strong acid conditions. A very important aspect of this work is the recycle of both the dye and the adsorbent, with particular attention to the dye reuse for coloring cotton fabric.
Comparative Study for Adsorptive Removal of Coralene Blue BGFS Dye from Aqueo...IJERA Editor
Textile industries represent biggest impact on the environment due to high water consumption and waste water discharge as government control water pollution by setting strength regulation for waste water discharge, removal of color from waste water becomes more and more essential and attractive. Adsorption technology is very efficient in treatment of textile effluent. In this paper comparison of adsorption phenomena of textile dye Anthraquinone blue onto two different adsorbents MgO nano powder and Fe2O3 amorphous powder has been studied for removal of said dye from aqueous solutions. The adsorption of Anthraquinone blue on adsorbents occurs by studying the effects of adsorbent amount, dye concentration, contact time and pH of solution. All results found that MgO nano powder and Fe2O3 provide a fairly high dye adsorption capacity, which combined with their fulfilment of pollution control board’s standards, lack of pollution, lower environmental hazard and low-cost makes them promising for future applications. The present work also provides information on optimum value of different operating parameter for dye removal by two adsorbent.
International Refereed Journal of Engineering and Science (IRJES)irjes
International Refereed Journal of Engineering and Science (IRJES) is a leading international journal for publication of new ideas, the state of the art research results and fundamental advances in all aspects of Engineering and Science. IRJES is a open access, peer reviewed international journal with a primary objective to provide the academic community and industry for the submission of half of original research and applications
Treatment of Effluent from Granite Cutting Plant by Using Natural Adsorbents ...IJERD Editor
Granite cutting plant is one such industry that releases polluting and turbid effluent. The residue from all these processes is discharged with water as an effluent. The effluent mainly contains many solids that harm the environment. Hence it requires treatment techniques before disposal. Several conventional methods are available for removal of contaminants like coagulation, adsorption, polyelectrolyte methods and biological methods. Most of them are cost prohibitive. The reduction of solids concentration in the effluent before disposal by using the techniques, coagulation followed by adsorption using natural adsorbents, like rice husk carbon and saw dust carbon, in contrast to the usage of activated carbon as it is costly. From a local Granite cutting plant near Anantapur, the effluent is collected and its physico-chemical characteristics are estimated and found to be pH(7.5), TS(4240mg/l), TSS(21560mg/l), TDS(12373mg/l).Effluent obtained is subjected to coagulation by potash alum followed by adsorption using saw dust carbon and rice husk carbon.
Adsorptive Removal Of Dye From Industrial Dye Effluents Using Low-Cost Adsorb...IJERA Editor
Industrial, agricultural, and domestic activities of humans have affected the environmental system, resulting in drastic problems such as global warming and the generation of wastewater containing high concentration of pollutants. As water of good quality is a precious commodity and available in limited amounts, it has become highly imperative to treat wastewater for removal of pollutants. In addition, the rapid modernization of society has also led to the generation of huge amount of materials of little value that have no fruitful use. Such materials are generally considered as waste, and their disposal is a problem. The utilization of all such materials as low-cost adsorbents for the treatment of wastewater may make them of some value. An effort has been made to give a brief idea about the low-cost alternative adsorbents with a view to utilizing these waste/low-cost materials in the treatment of wastewater.
In the present study, application of Amberlite FPA-98 was investigated for the removal of Acide
Orange 7 from aqueous solution using the continuous method and was optimized using Box–Behnken design
(BBD) and full factorial design (FFD). Fixed bed adsorption has become a frequently used in wastewater
treatment processes. In this work, the intention of the study was to explore the efficacy and feasibility for azo
dye, Acid Orange 7 (AO7) adsorption onto fixed bed column of Amberlite FPA-98. The effect of operating
parameters such as flow rate, initial dye concentration, and bed height was modeled by response surface
methodology (RSM). This study compares Box–Behnken design (BBD) and full factorial design (FFD) utility for
modeling and optimization by response surface methodology. The precision of the equation obtained by RSM
was confirmed by the analysis of variance (ANOVA)and calculation of correlation coefficient relating the
predicted and the experimental values of adsorption efficiency. The results revealed a good agreement between
the predicted values, as obtained by full factorial design (FFD) and the experimental values for AO7 (R2 =
0.987) . The optimum conditions proposed by Box–Behnken design (BBD) to reach the maximum dye removal
through adsorption process. Under the optimum conditions, the removal efficiency of AO7 were (R2 = 0.959).
The application of response surface methodology in order to optimize using Box–Behnken design (BBD) and full
factorial design (FFD). The research on modeling adsorption by RSM has been highly developed and The
Amberlite was shown to be suitable adsorbent for adsorption of AO7 using fixed-bed adsorption column.
IJERA (International journal of Engineering Research and Applications) is International online, ... peer reviewed journal. For more detail or submit your article, please visit www.ijera.com
Synthesis of Faujasite Zeolite (Z) For Adsorption of Cationic Dye from Textil...IJMREMJournal
The synthesis of Faujasite Zeolite from Locally available Erusu Kaolin clay sourced in Nigeria has been
attempted using standard procedures which have proven sufficient upon slight modifications and reported in
literature. The zeolite was characterized with Scanning Electron Microscopy, Fourier Transformed infrared
spectroscopy (FTIR), X-ray Diffractometer and BET surface area analyzer. Forthwith, Adsorption of the
hazardous cationic dye malachite green (MG) on the synthesized zeolite was investigated. Batch process
variables for the adsorption of MG by Zeolite were determined. The mechanisms involved in the adsorption of
MG by the sorbent were explored using isotherms models. The maximum equilibrium adsorption capacity was
found to be 108.26 mg/g at 30˚C. It is noteworthy that the adsorption of MG was reduced (about 45%) at low
pH (4) compared to that at high pH (12). Furthermore, among the other parameters affecting adsorption, a high
MG adsorption capacity (about 54%) was observed at a maximum initial MG dye concentration of 200 mg/L
compared to that at lower initial MG dye concentration (25 mg/L), indicating the dependency of sorption on the
initial adsorbate concentration (CO) in the solution. The MG adsorption data indicate multilayer adsorption
because the data were fit better by the Freundlich model (R2 >0.99) than by the Langmuir model. Surface
diffusion was found to be a possible mechanism for the adsorption of MG by Zeolite. The study shed light on the
potential of synthesized kaolinite derivative “Zeolite” as an efficient sorbent for cationic dye cleanup in
wastewater treatment.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
Removal of dye from polluted water using novel nano manganese oxide-based mat...Dr. Md. Aminul Islam
Dyes are priority pollutants, commonly found at significant concentrations in textile effluents. The presence of dyes stuffs in wastewater can cause severe problems to aquatic life and human beings. Therefore, the removal of dyes from wastewater is important in order to minimize their hazardous effects on the environment. One way of removing dyes is to use nanosized manganese oxides (MnOs). To date, there has been much work reported on the use of nanosized MnOs as sorbents for dyestuffs. They are promising sorbents for commercial use due to their amorphous nature, high specific surface areas (SSA), mesoporous structure, and low to the moderate point of zero charge (pHPZC). This review summarizes the toxicity and recent advances for removing dyes from wastewater using nanosized MnO sorbents. The article also describes the various experimental parameters necessary for adsorption optimization, such as adsorption time, pH, initial dye concentration, amount of sorbent and temperature. Adsorption mechanisms investigated by various modeling approaches are also discussed. In particular, it was observed that much work has been reported on the use of birnessite and its composites for dye removal. There are many papers reporting on the use of MnO in batch mode dye removal, but very few that report on the use of MnO in continuous column removal systems. Therefore, there is still a considerable need for further research to develop effective and economical large scale MnO column systems for commercial use.
Key Trends Shaping the Future of Infrastructure.pdfCheryl Hung
Keynote at DIGIT West Expo, Glasgow on 29 May 2024.
Cheryl Hung, ochery.com
Sr Director, Infrastructure Ecosystem, Arm.
The key trends across hardware, cloud and open-source; exploring how these areas are likely to mature and develop over the short and long-term, and then considering how organisations can position themselves to adapt and thrive.
Software Delivery At the Speed of AI: Inflectra Invests In AI-Powered QualityInflectra
In this insightful webinar, Inflectra explores how artificial intelligence (AI) is transforming software development and testing. Discover how AI-powered tools are revolutionizing every stage of the software development lifecycle (SDLC), from design and prototyping to testing, deployment, and monitoring.
Learn about:
• The Future of Testing: How AI is shifting testing towards verification, analysis, and higher-level skills, while reducing repetitive tasks.
• Test Automation: How AI-powered test case generation, optimization, and self-healing tests are making testing more efficient and effective.
• Visual Testing: Explore the emerging capabilities of AI in visual testing and how it's set to revolutionize UI verification.
• Inflectra's AI Solutions: See demonstrations of Inflectra's cutting-edge AI tools like the ChatGPT plugin and Azure Open AI platform, designed to streamline your testing process.
Whether you're a developer, tester, or QA professional, this webinar will give you valuable insights into how AI is shaping the future of software delivery.
Transcript: Selling digital books in 2024: Insights from industry leaders - T...BookNet Canada
The publishing industry has been selling digital audiobooks and ebooks for over a decade and has found its groove. What’s changed? What has stayed the same? Where do we go from here? Join a group of leading sales peers from across the industry for a conversation about the lessons learned since the popularization of digital books, best practices, digital book supply chain management, and more.
Link to video recording: https://bnctechforum.ca/sessions/selling-digital-books-in-2024-insights-from-industry-leaders/
Presented by BookNet Canada on May 28, 2024, with support from the Department of Canadian Heritage.
JMeter webinar - integration with InfluxDB and GrafanaRTTS
Watch this recorded webinar about real-time monitoring of application performance. See how to integrate Apache JMeter, the open-source leader in performance testing, with InfluxDB, the open-source time-series database, and Grafana, the open-source analytics and visualization application.
In this webinar, we will review the benefits of leveraging InfluxDB and Grafana when executing load tests and demonstrate how these tools are used to visualize performance metrics.
Length: 30 minutes
Session Overview
-------------------------------------------
During this webinar, we will cover the following topics while demonstrating the integrations of JMeter, InfluxDB and Grafana:
- What out-of-the-box solutions are available for real-time monitoring JMeter tests?
- What are the benefits of integrating InfluxDB and Grafana into the load testing stack?
- Which features are provided by Grafana?
- Demonstration of InfluxDB and Grafana using a practice web application
To view the webinar recording, go to:
https://www.rttsweb.com/jmeter-integration-webinar
LF Energy Webinar: Electrical Grid Modelling and Simulation Through PowSyBl -...DanBrown980551
Do you want to learn how to model and simulate an electrical network from scratch in under an hour?
Then welcome to this PowSyBl workshop, hosted by Rte, the French Transmission System Operator (TSO)!
During the webinar, you will discover the PowSyBl ecosystem as well as handle and study an electrical network through an interactive Python notebook.
PowSyBl is an open source project hosted by LF Energy, which offers a comprehensive set of features for electrical grid modelling and simulation. Among other advanced features, PowSyBl provides:
- A fully editable and extendable library for grid component modelling;
- Visualization tools to display your network;
- Grid simulation tools, such as power flows, security analyses (with or without remedial actions) and sensitivity analyses;
The framework is mostly written in Java, with a Python binding so that Python developers can access PowSyBl functionalities as well.
What you will learn during the webinar:
- For beginners: discover PowSyBl's functionalities through a quick general presentation and the notebook, without needing any expert coding skills;
- For advanced developers: master the skills to efficiently apply PowSyBl functionalities to your real-world scenarios.
Generating a custom Ruby SDK for your web service or Rails API using Smithyg2nightmarescribd
Have you ever wanted a Ruby client API to communicate with your web service? Smithy is a protocol-agnostic language for defining services and SDKs. Smithy Ruby is an implementation of Smithy that generates a Ruby SDK using a Smithy model. In this talk, we will explore Smithy and Smithy Ruby to learn how to generate custom feature-rich SDKs that can communicate with any web service, such as a Rails JSON API.
The Art of the Pitch: WordPress Relationships and SalesLaura Byrne
Clients don’t know what they don’t know. What web solutions are right for them? How does WordPress come into the picture? How do you make sure you understand scope and timeline? What do you do if sometime changes?
All these questions and more will be explored as we talk about matching clients’ needs with what your agency offers without pulling teeth or pulling your hair out. Practical tips, and strategies for successful relationship building that leads to closing the deal.
Kubernetes & AI - Beauty and the Beast !?! @KCD Istanbul 2024Tobias Schneck
As AI technology is pushing into IT I was wondering myself, as an “infrastructure container kubernetes guy”, how get this fancy AI technology get managed from an infrastructure operational view? Is it possible to apply our lovely cloud native principals as well? What benefit’s both technologies could bring to each other?
Let me take this questions and provide you a short journey through existing deployment models and use cases for AI software. On practical examples, we discuss what cloud/on-premise strategy we may need for applying it to our own infrastructure to get it to work from an enterprise perspective. I want to give an overview about infrastructure requirements and technologies, what could be beneficial or limiting your AI use cases in an enterprise environment. An interactive Demo will give you some insides, what approaches I got already working for real.
DevOps and Testing slides at DASA ConnectKari Kakkonen
My and Rik Marselis slides at 30.5.2024 DASA Connect conference. We discuss about what is testing, then what is agile testing and finally what is Testing in DevOps. Finally we had lovely workshop with the participants trying to find out different ways to think about quality and testing in different parts of the DevOps infinity loop.
Builder.ai Founder Sachin Dev Duggal's Strategic Approach to Create an Innova...Ramesh Iyer
In today's fast-changing business world, Companies that adapt and embrace new ideas often need help to keep up with the competition. However, fostering a culture of innovation takes much work. It takes vision, leadership and willingness to take risks in the right proportion. Sachin Dev Duggal, co-founder of Builder.ai, has perfected the art of this balance, creating a company culture where creativity and growth are nurtured at each stage.
Slack (or Teams) Automation for Bonterra Impact Management (fka Social Soluti...Jeffrey Haguewood
Sidekick Solutions uses Bonterra Impact Management (fka Social Solutions Apricot) and automation solutions to integrate data for business workflows.
We believe integration and automation are essential to user experience and the promise of efficient work through technology. Automation is the critical ingredient to realizing that full vision. We develop integration products and services for Bonterra Case Management software to support the deployment of automations for a variety of use cases.
This video focuses on the notifications, alerts, and approval requests using Slack for Bonterra Impact Management. The solutions covered in this webinar can also be deployed for Microsoft Teams.
Interested in deploying notification automations for Bonterra Impact Management? Contact us at sales@sidekicksolutionsllc.com to discuss next steps.
State of ICS and IoT Cyber Threat Landscape Report 2024 previewPrayukth K V
The IoT and OT threat landscape report has been prepared by the Threat Research Team at Sectrio using data from Sectrio, cyber threat intelligence farming facilities spread across over 85 cities around the world. In addition, Sectrio also runs AI-based advanced threat and payload engagement facilities that serve as sinks to attract and engage sophisticated threat actors, and newer malware including new variants and latent threats that are at an earlier stage of development.
The latest edition of the OT/ICS and IoT security Threat Landscape Report 2024 also covers:
State of global ICS asset and network exposure
Sectoral targets and attacks as well as the cost of ransom
Global APT activity, AI usage, actor and tactic profiles, and implications
Rise in volumes of AI-powered cyberattacks
Major cyber events in 2024
Malware and malicious payload trends
Cyberattack types and targets
Vulnerability exploit attempts on CVEs
Attacks on counties – USA
Expansion of bot farms – how, where, and why
In-depth analysis of the cyber threat landscape across North America, South America, Europe, APAC, and the Middle East
Why are attacks on smart factories rising?
Cyber risk predictions
Axis of attacks – Europe
Systemic attacks in the Middle East
Download the full report from here:
https://sectrio.com/resources/ot-threat-landscape-reports/sectrio-releases-ot-ics-and-iot-security-threat-landscape-report-2024/
State of ICS and IoT Cyber Threat Landscape Report 2024 preview
Paper on synthesis of zeolite and application
1. Chemical and Process Engineering Research www.iiste.org
ISSN 2224-7467 (Paper) ISSN 2225-0913 (Online)
Vol 2, 2012
A Study on Synthesis of Zeolite and Removal of Amido Black
dye by adsorption with Zeolite
Ameen Sayal*, Vijaya Kumar Bulasara, Sanghamitra Barman
Department of Chemical Engineering, Thapar University, Patiala
ameen.sayal@gmail.com
Abstract
Investigations have been undertaken to determine whether cheap, commercially available materials (natural
zeolite and bentonite) hold promise in the treatment of wastewaters from the textile industry. The initial
findings indicate that zeolite synthesized from fly ash has high adsorptive capacity for dyes and it is
relatively cheap. The adsorption of two basic dyes (Amido Black and Thionine) onto granular activated
carbon as well as zeolite from fly ash and bentonite has to be studied as single equilibrium isotherms. The
effectiveness of each adsorbent has to be measured in terms of its adsorption capacity towards individual
constituents of the effluent. The adsorption isotherm would be described by the Langmuir and Freundlich
isotherm equations. The parameters in the adsorption isotherms will be estimated from the experimental
equilibrium data using non-linear regression analysis. Using these data, the selection of the best adsorbent
can be done for design purposes.
Keywords: Natural Zeolite, bentonite, Amido Black, Thionine, Langmuir, Freundlich, granular activated
carbon
1. Introduction
Adsorption has been found to be superior to other techniques for water re-use in terms of initial cost,
simplicity of design, ease of operation and insensitivity to toxic substances. Activated carbon is the most
popular adsorbent and has been used with great success, but is expensive [6]. A full description of low cost
adsorbents for waste and wastewater treatment: a review has been presented by S.J.T. Pollard et al (2007)
[11]. A number of studies have been reported with regard to the adsorption equilibrium of dye removal
processes using various adsorbents. In most adsorption systems of dyestuffs-adsorbent, Langmuir [3,9,10],
Freundlich [2,9,10], and Redlich-Peterson [1,6,7,8,10] isotherms have been applied to describe equilibrium
between liquid–solid phases. Two intra-particle diffusion mechanisms are involved in the adsorption rate
(a) diffusion within the pore volume known as pore diffusion, and (b) diffusion along the surface of pores
known as surface diffusion [13]. Some of the investigators have applied the pore diffusion model with and
without film resistance [3]. McKay has developed homogeneous solid phase diffusion model to describe
systems dyes on bagasse pith (2011) [7]. The homogeneous solid phase diffusion model has been
developed based on external mass transfer and surface diffusion by M.S.El-Geundi [1]. He has applied this
model for adsorption of basic dyes onto natural clay in a batch adsorber. The branched pore kinetic model
was used to describe the adsorption of cobalt phthalocyanine dye onto active carbon and basic dyes onto
natural clay [2].
Research has already been carried out using different treatment technologies e.g. chemical coagulation-
flocculation [2], different types of oxidation processes [3], biological processes [4], membrane based
separation processes [5–7], adsorption [8] etc. for the removal of colored dye from wastewater. Research is
focused on the use of low-cost, reusable, locally available, biodegradable adsorbents made from natural
sources. Natural and modified clays, zeolite from fly ash and bentonite are being considered as alternative
low-cost adsorbents. Adsorption of organic molecules to an adsorbent depends on various factors like
temperature, pH of the solution, the structure and concentration of the adsorbing molecule, the ionic
strength of the suspension, and the structure of the adsorbent. Experimental investigations have been
carried out to adsorb Amido Black dye from aqueous medium using zeolite as an adsorbent.
Characterization of zeolite is to be done by measuring
Particle size distribution using particle size analyzer
BET surface area using BET surface analyzer
Structural analysis using X-ray diffractometer
Microscopic analysis using scanning electron microscope.
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The effects of initial dye concentration, contact time, zeolite loading, stirring speed, pH, and
temperature are to be studied for the adsorption of Amido Black in batch mode.
Comparison of adsorption capacity of zeolite with other adsorbent such as activated carbon
The aim of this work is to study the ability of zeolite synthesized from fly ash to remove the acidic dye
Amido Black from aqueous solutions. This adsorbent was chosen because of its cheapness and abundance.
II Description of Materials
A. ZEOLITES
The types of zeolites formed on treatment are very much selective to reaction parameters and also the raw
material compositions. The synthesis of various zeolites from fly ash and their properties mainly depend on
the effect of reaction time, reaction
temperature, alkalinity and fly ash composition.
Zeolites are crystalline, micro-porous, hydrated aluminosilicates that are built from an infinitely extending
three-dimensional network of [SiO4]4- and [AlO4]4- tetrahedral linked to each other by the sharing of oxygen
atom. Generally, their structure can be considered as inorganic polymer built from tetrahedral TO 4 units,
where T is Si4+ or Al3+ ion. Each oxygen (O) atom is shared between two T atoms.
Mx/n[(AlO2x(SiO2)y]· 2O, where M is an alkali or alkaline earth cation, n is the valence of the cation, w
wH
is the number of water molecules per unit cell, x and y are the total number of tetrahedra per unit cell, and
the ratio y/x usually has values of 1 to 5, though for the silica zeolite, y/x can be raging from 10 to 100.
The adsorption of dyes onto zeolites has been extensively investigated by some researcher but only a few
studies have been reported about the adsorption of dye onto fly ash-based zeolites .A comparison of the
adsorption capabilities of Amido Black with other larger dyes over zeolites and activated carbon will
provide valuable information about adsorption mechanisms and the structure of the zeolites. The structure
of zeolite is given in fig.1.
Adsorption and adsorption processes are important fields of study in physical chemistry. They form the
basis for understanding phenomena such as heterogeneous catalysis, chromatographic analysis, dyeing of
textiles, and clarification of various effluents.
Dyes are defined as colored substances which when applied to fibers give them a permanent color, i.e.
resistant to action of light, water and soap. Practically every dyestuff is made from either one or more of
the compounds obtained by the distillation of the coal tar. The chief of these are Benzene (C6H6), Toluene
(C6H5.CH3), Naphthalene (C10H8), Anthracene (C14H10), Phenol (C6H5OH), Cresol (C7H7OH), Acridine
(C13H9N), and Quinoline (C9H7N). Wastewaters from dyeing and finishing operations in the textile industry
are generally high in both color and organic content. Color removal from textile effluent has been the target
of great attention in the last few years, not only because of its potential toxicity, but also mainly due to its
visibility problems. Recent estimate indicates that 20% of dyes enter the environment through effluent that
result from the treatment of industrial wastewater. The existing technologies have certain efficiency in the
removal of dyes but their initial and operational costs are very high. On the other hand, low cost
technologies do not allow the desired degree of color removal or have certain disadvantage. Oxidation and
adsorption are two major technologies that are used for wastewater treatment in the textile industry. Among
oxidation methods, UV/Ozone and UV/H2O2 treatments are technologies for decolorizing wastewater.
Adsorption is rapidly becoming a prominent method of treating
aqueous effluents and it has been extensively used in industrial processes for a variety of separation and
purification purposes. Adsorption of dyes by zeolites has evolved into one of the most effective physical
process for the decolorization of textile wastewater. This process has been found to be superior to other
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techniques for water re-use in terms of initial cost, simplicity of design, ease of operation and insensitivity
to toxic substances.
B. TYPES OF ZEOLITE
The following table presents the most common types of zeolites in table 1.
C. AMIDO BLACK DYE
Amido black 10B is an amino acid staining diazo dye. Its molecular formula is C22H14N6Na2O9S2. Amido
Black 10B is a synthetic acid dye containing both NN and CC chromophore groups (pyrazolone dye). It is a
dark red to black powder soluble in water and used as a stain for protein-containings. Its chemical
designation is 4-amino-5-hydroxy- 3-[(4-nitrophenyl) azo]- 6-(phenylazo)- 2,7-naphthalene disulfonic acid
disodium salt. Acid dyes are water-soluble dyes employed mostly in the form of sodium salts of the
sulfonic or carboxylic acids. They are anionic which attach strongly to cationic groups in the fibre directly.
They can be applicable to all kind of natural fibres
like wool, cotton and silk as well as to synthetics like polyesters, acrylic and rayon. However, they are not
substantive to cellulosic fibres. They are also used in paints, inks, plastics and leather. Chemical structure
of Amido Black dye is shown in fig.2.
III. Experimental Methodology
Process flow diagram for synthesis of zeolite from fly ash is shown in fig.3.
A. ZEOLITE SYNTHESIS:
Before any treatment, the raw fly ash samples were first screened through a BSS Tyler sieve of 80-mesh
size to eliminate the larger particles. The unburnt carbon (4–6%) along with other volatile materials present
in fly ash were removed by calcination at 800 (± 10) ° for 2 h.Mixture of sodium hydroxide and fly ash
C
(calcined and HCl treated) in a pre-determined ratio, was milled and fused in a stainless steel tray at
different temperatures ranging from 500–650° for 1 h. The sodium hydroxideto fly ash ratio (by weight)
C
was varied from 1× 0–1× The resultant fused mixture was then cooled to room temperature, ground
5.
further and added to water (10 g fly ash/100 ml water). The slurry thus obtained was agitated mechanically
in a glass beaker for several hours. It was then kept at around 90° for 6 h without any disturbance. The
C
flow diagram of the synthesis process is shown in figure 3.
The resultant precipitate was then repeatedly washed with distilled water to remove excess sodium
hydroxide, filtered and dried. The sodium hydroxide added to the fly ash not only works as an activator, but
also adjusts the sodium content in the starting material.
IV. Results and Discussion
A. DETERMINATION OF λmax FOR AMIDO BLACK DYE SOLUTION
To determine the wavelength that corresponds to maximum absorbance (λmax), a standard solution of
Amido Black in distilled water was scanned through a wavelength range of 200–700 nm using a UV–
Visible spectrophotometer. Maximum absorbance value was noticed at a wavelength of 618 nm (Figure 1).
The same value was also used in several literatures (Qiu et al., 2009). Therefore, λmax for amido black was
taken as 618 nm. A plot of absorbance versus wavelength for Amido Black dye solution is given in fig.4.
B. CALIBRATION CURVE FOR AMIDO BLACK DYE SOLUTION
Absorbance values were determined at various known concentrations of the dye solution to obtain a
calibration curve for Amido Black dye solution. As shown in figure 2, a linear fit to the observed data
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(absorbance versus dye concentration) yielded a straight line with a slope of 0.0658. This calibration curve
can be used for the determination of unknown dye concentration in the solution after adsorption with
zeolite. A calibration curve for amido black dye solution is shown in fig 5.
C. ADSORPTION EXPERIMENTS
The adsorption experiments were carried out for 6 h under continuous agitation at 120 rpm and 20C. The
experimental scheme is as follows.
Six different concentrations of the adsorbent (zeolite) were studied to obtain the optimal concentration of
the zeolite for effective removal of the dye from its aqueous solution.
D. CALCULATION OF REMOVAL EFFICIENCY
Dye removal efficiency was determined from the dye concentration in the solution before and after
adsorption with zeolite.
Ci C f
Removal efficiency, R 100
Ci (1)
Ci C f
Adsorption capacity, q t
Cz (2)
Here,
Ci = initial dye concentration in the solution, mg/L
Cf = dye concentration in the solution after adsorption with zeolite, mg/L
Cz = zeolite loading (adsorbent dosage), g/L
qt = amount of dye adsorbed per unit weight of zeolite, mg/g
The values of dye removal efficiency and adsorption capacity of zeolite evaluated using the above formulae
(Eq. 1–2) for various concentrations of zeolite were presented in table 3.
A plot of dye removal efficiency versus zeolite concentration yielded a non-linear profile as shown in
figure 3. From this figure, it can be observed that the removal efficiency increased with increasing the
zeolite concentration up to 10 g/L and no significant improvement in the removal efficiency values was
observed beyond this value. Hence, the optimal zeolite concentration for Hence, the optimal zeolite
concentration for the removal of Amido Black dye was chosen to be 10 g/L. A variation of dye removal
efficiency with zeolite concentration is given in fig.6.
As can be seen from figure 5, the adsorption capacity of the zeolite (determined by Eq. (2)) decreased with
increasing the zeolite concentration. This observation is also in good agreement with the literature [xx]. It
indicates that the adsorption capacity of a zeolite decreases with increasing the zeolite dosage. Hence, it can
be concluded that too much of zeolite concentration in the solution is not effective for adsorption and it is
also not economical. A variation of adsorption capacity with zeolite concentration is given in fig.7.
Zeolitized fly ash product is successfully used as low cost adsorbent for this anionic dye. Equilibrium and
kinetic results obtained in this study may be useful for designing a treatment plant for dye removal from
industrial colored effluents.
V. Conclusions
The following conclusions have been derived from the experimental analysis carried out so far.
Zeolite has been synthesized from low-cost raw material, i.e. fly ash.
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The prepared zeolite has been successfully applied for the adsorptive removal of Amido Black dye
from its aqueous solutions.
The prepared fly ash based zeolite is found to be more effective than the natural zeolite
clinoptilolite presented in the literature (Qiu et al., 2009).
The optimum zeolite concentration obtained from the experimental studies for Amido Black is 10
g/L.
λmax for Amido Black 10B dye solution was found to be 618 nm.
Most important observation in this work is that the zeolite synthesized from fly ash could act as a very
effective adsorbent for the removal of Amido Black dye. The removal efficiency increased with increasing
the zeolite concentration significantly and reached a value as high as 74% at lower concentrations (up to 10
g/L) where as no significant change was observed at higher concentrations.
Work done so far includes the preparation of zeolite and studying the effect of zeolite loading on the
removal of Amido Black dye by varying the zeolite concentration from 0 to 15 g/L.
VI. Acknowledgement
This work was supported by Thapar University under Research Fellowship Programme.
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List of Table
Table Title Page No.
1 Typical oxide formula of some synthetic zeolites 09
2 Calculation of absorbance of amido black dye from dye concentration 09
3 Calculation of adsorption capacity using solutin concentration 09
4 Calculation of dye removal efficiency from Zeolite concentration 10
List of Figures
Figure Title Page No.
1 Primary building unit of zeolite structure 10
2 Structure of Amido Black 10B dye 10
3 Flow sheet of synthesis of Zeolite from fly ash 11
4 A plot of absorbance versus wavelength for Amido Black dye solution 11
5 Calibration curve for amido black dye solution 12
6 12
Variation of dye removal efficiency with zeolite concentration
7 12
Variation of adsorption capacity with zeolite concentration
Tables
Table 1
Zeolites Typical oxide formula
Zeolites A Na2O.Al2O3.2SiO2.4.5H2O
Zeolites X Na2O.Al2O3.2.5SiO2.6H2O
Zeolites Y Na2O.Al2O3.4.8SiO2.8.9H2O
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