The document summarizes different methods for synthesizing cadmium sulfide (CdS) nanoparticles. It describes an aqueous precipitation method using cadmium nitrate and sodium sulfide precursors that produces yellow CdS precipitate. It also outlines a sol-gel method using cadmium acetate, diaminobenzene, and thioacetamide precursors that generates a CdS sol and gel. Additionally, it mentions a hydrothermal method using cadmium nitrate, thiourea, and hexamethylenetetramine precursors under high temperature and pressure that can control CdS morphology. The document provides an overview of various preparation techniques for CdS nanoparticles.
With the increasing researches in the field of nanotechnology, various nanoparticles have become a source of interest among the nano technologists because of their great properties, like the optical properties of Cadmium Sulfide Nanoparticles are amazing and also easy to synthesize, but to make sure its quality it is equally essential to make out characterize it, this file will do the same in a lucid way!!
It's simple to understand the synthesis. Hydrothermal method is a chemical reaction in water in a sealed pressure vessel, which is in fact a type of reaction at both high temperature and pressure.
With the increasing researches in the field of nanotechnology, various nanoparticles have become a source of interest among the nano technologists because of their great properties, like the optical properties of Cadmium Sulfide Nanoparticles are amazing and also easy to synthesize, but to make sure its quality it is equally essential to make out characterize it, this file will do the same in a lucid way!!
It's simple to understand the synthesis. Hydrothermal method is a chemical reaction in water in a sealed pressure vessel, which is in fact a type of reaction at both high temperature and pressure.
This includes what is Quantum Dots and their properties ,types of synthesis methods of nano materials such as top down, bottom up etc.It includes few things about Carbon Quantum Dots.
Perovskite: introduction, classification, structure of perovskite, method to synthesis, characterization by XRD and UV- vis spectroscopy , lambert beer's law, material properties and advantage and application.
Synthesis of ZnO Nanoparticles using wet chemical method and its characteriza...Govind Soni
This is very intersting power point on ZnO NPs synthesized by me GOVIND SONI and my lab partnes KAUSHAL ,SANEHA & DINESH under the guidance of our PhD scholar Mr.SAHIL & Ms.KIRTI in the CYRSTAL LAB of DR.BINAY KUMAR in Department of Physics & Astrophysics .This presentation basically covers the Introduction to Nanoscience and Nanotechnology and synthesis of Zinc oxide nanoparticles using wet chemical method . its characterization has been done in Msc finals Nanoscience lab using X-Ray Diffraction and Particle size Analyzer.This presentation also contains an advance topic on introduction to Spintronics which is basically the study of internsic spin of electronics and its magnetic moment.I hope it will be an important tool to know about Nanoworld .
Just basics of mesoporous materials!!The Break through came around 1992 by both Japanese and Mobil scientist on the soft template based synthesis of mesoporous materials
Growth and characterization of cd s doped kdp single crystalseSAT Journals
Abstract Pure and CdS added potassium dihydrogen phosphate (KDP) single crystals (a total of six) have been grown by the slow evaporation method at room temperature. Powder X-ray diffraction, atomic absorption spectroscopic and Fourier transform infrared spectral measurements were done to characterize the grown crystals structurally and chemically. Thermal and mechanical stabilities were understood by making respectively the thermogravimetric and microhardness measurements. The optical transmittance and second harmonic generation efficiency were understood by making respectively the UV-Vis-NIR spectral and nonlinear optical measurements. The AC and DC electrical measurements made on all the six grown single crystals indicate a normal dielectric behaviour. The electrical parameters, viz. dielectric constant, dielectric loss factor and AC and DC electrical conductivities are found to increase with the increase in temperature in the range (40 – 150oC ) considered in the present study. The estimated AC and DC activation energies are found to vary nonlinearly with the impurity concentration. Keywords: Crystal growth, Doped crystals, KDP crystals, Physical properties, X-ray diffraction.
This includes what is Quantum Dots and their properties ,types of synthesis methods of nano materials such as top down, bottom up etc.It includes few things about Carbon Quantum Dots.
Perovskite: introduction, classification, structure of perovskite, method to synthesis, characterization by XRD and UV- vis spectroscopy , lambert beer's law, material properties and advantage and application.
Synthesis of ZnO Nanoparticles using wet chemical method and its characteriza...Govind Soni
This is very intersting power point on ZnO NPs synthesized by me GOVIND SONI and my lab partnes KAUSHAL ,SANEHA & DINESH under the guidance of our PhD scholar Mr.SAHIL & Ms.KIRTI in the CYRSTAL LAB of DR.BINAY KUMAR in Department of Physics & Astrophysics .This presentation basically covers the Introduction to Nanoscience and Nanotechnology and synthesis of Zinc oxide nanoparticles using wet chemical method . its characterization has been done in Msc finals Nanoscience lab using X-Ray Diffraction and Particle size Analyzer.This presentation also contains an advance topic on introduction to Spintronics which is basically the study of internsic spin of electronics and its magnetic moment.I hope it will be an important tool to know about Nanoworld .
Just basics of mesoporous materials!!The Break through came around 1992 by both Japanese and Mobil scientist on the soft template based synthesis of mesoporous materials
Growth and characterization of cd s doped kdp single crystalseSAT Journals
Abstract Pure and CdS added potassium dihydrogen phosphate (KDP) single crystals (a total of six) have been grown by the slow evaporation method at room temperature. Powder X-ray diffraction, atomic absorption spectroscopic and Fourier transform infrared spectral measurements were done to characterize the grown crystals structurally and chemically. Thermal and mechanical stabilities were understood by making respectively the thermogravimetric and microhardness measurements. The optical transmittance and second harmonic generation efficiency were understood by making respectively the UV-Vis-NIR spectral and nonlinear optical measurements. The AC and DC electrical measurements made on all the six grown single crystals indicate a normal dielectric behaviour. The electrical parameters, viz. dielectric constant, dielectric loss factor and AC and DC electrical conductivities are found to increase with the increase in temperature in the range (40 – 150oC ) considered in the present study. The estimated AC and DC activation energies are found to vary nonlinearly with the impurity concentration. Keywords: Crystal growth, Doped crystals, KDP crystals, Physical properties, X-ray diffraction.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
— CdTe quantum dots (QDs)/Poly (diallyldimethylammonium chloride) (PDDA) multilayer films (QDMF) have been self-assembled by layer-by-layer (LBL) technique. CdTe quantum dots (QDs) were synthesized by using Te, NaBH 4 , and CdCl 2 as precursors and mercaptopropionic acid (MPA) as stabilizer. The as-prepared composites were characterized by transmission electron microscope (TEM), Fourier transform infrared spectroscopy (FTIR), UV-vis adsorption spectrum(UV-vis), and Fluorescence spectrum(FS), respectively. It was shown that the self-assembled QDMF in this study could be used as gaseous sensors for detecting organic gases, such as ammonia, acetone, methanol and formaldehyde. The quenching mechanism of CdTe QDs multilayer films by formaldehyde was studied in detail and The detection limit was 10-236ppm.
International Journal of Engineering Research and Applications (IJERA) is an open access online peer reviewed international journal that publishes research and review articles in the fields of Computer Science, Neural Networks, Electrical Engineering, Software Engineering, Information Technology, Mechanical Engineering, Chemical Engineering, Plastic Engineering, Food Technology, Textile Engineering, Nano Technology & science, Power Electronics, Electronics & Communication Engineering, Computational mathematics, Image processing, Civil Engineering, Structural Engineering, Environmental Engineering, VLSI Testing & Low Power VLSI Design etc.
Some studies on ceria–zirconia reinforced solvothermally synthesized cordieri...Abhinav Srivastava
Nanostructured cordierite and 12 mol% ceria stabilized zirconia were chemically prepared separately. Pure cordierite was synthesized solvothermally, whereas [(Zr)0.88(Ce)0.12O2] termed as CeSZ was processed with gelation and co-precipitation method. The evolution of crystalline phases and the microstructures have been studied using X-ray diffractometer, and FE-SEM with EDX. Varying contents (0–20 weight%) of CeSZ were then mixed with cordierite to form sample blocks of desired shapes. These nano-composite blocks were fired at 1100–1400 C for a soaking time of 3 h to observe their thermomechanical, micro-structural and physical properties. Results indicate that ceria not only acts as a stabilizer in zirconia ceramics but it also acts as a sintering aid in cordierite formation. CeO2 also improves
compressibility and structural properties of nano-composites. Sintering temperature also plays an important role in the behavior of nano-composite blocks. All properties show a major improvement than previous reported data’s.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
International Journal of Engineering Research and Applications (IJERA) is an open access online peer reviewed international journal that publishes research and review articles in the fields of Computer Science, Neural Networks, Electrical Engineering, Software Engineering, Information Technology, Mechanical Engineering, Chemical Engineering, Plastic Engineering, Food Technology, Textile Engineering, Nano Technology & science, Power Electronics, Electronics & Communication Engineering, Computational mathematics, Image processing, Civil Engineering, Structural Engineering, Environmental Engineering, VLSI Testing & Low Power VLSI Design etc.
International Journal of Engineering Research and Applications (IJERA) is an open access online peer reviewed international journal that publishes research and review articles in the fields of Computer Science, Neural Networks, Electrical Engineering, Software Engineering, Information Technology, Mechanical Engineering, Chemical Engineering, Plastic Engineering, Food Technology, Textile Engineering, Nano Technology & science, Power Electronics, Electronics & Communication Engineering, Computational mathematics, Image processing, Civil Engineering, Structural Engineering, Environmental Engineering, VLSI Testing & Low Power VLSI Design etc.
Multi-source connectivity as the driver of solar wind variability in the heli...Sérgio Sacani
The ambient solar wind that flls the heliosphere originates from multiple
sources in the solar corona and is highly structured. It is often described
as high-speed, relatively homogeneous, plasma streams from coronal
holes and slow-speed, highly variable, streams whose source regions are
under debate. A key goal of ESA/NASA’s Solar Orbiter mission is to identify
solar wind sources and understand what drives the complexity seen in the
heliosphere. By combining magnetic feld modelling and spectroscopic
techniques with high-resolution observations and measurements, we show
that the solar wind variability detected in situ by Solar Orbiter in March
2022 is driven by spatio-temporal changes in the magnetic connectivity to
multiple sources in the solar atmosphere. The magnetic feld footpoints
connected to the spacecraft moved from the boundaries of a coronal hole
to one active region (12961) and then across to another region (12957). This
is refected in the in situ measurements, which show the transition from fast
to highly Alfvénic then to slow solar wind that is disrupted by the arrival of
a coronal mass ejection. Our results describe solar wind variability at 0.5 au
but are applicable to near-Earth observatories.
Earliest Galaxies in the JADES Origins Field: Luminosity Function and Cosmic ...Sérgio Sacani
We characterize the earliest galaxy population in the JADES Origins Field (JOF), the deepest
imaging field observed with JWST. We make use of the ancillary Hubble optical images (5 filters
spanning 0.4−0.9µm) and novel JWST images with 14 filters spanning 0.8−5µm, including 7 mediumband filters, and reaching total exposure times of up to 46 hours per filter. We combine all our data
at > 2.3µm to construct an ultradeep image, reaching as deep as ≈ 31.4 AB mag in the stack and
30.3-31.0 AB mag (5σ, r = 0.1” circular aperture) in individual filters. We measure photometric
redshifts and use robust selection criteria to identify a sample of eight galaxy candidates at redshifts
z = 11.5 − 15. These objects show compact half-light radii of R1/2 ∼ 50 − 200pc, stellar masses of
M⋆ ∼ 107−108M⊙, and star-formation rates of SFR ∼ 0.1−1 M⊙ yr−1
. Our search finds no candidates
at 15 < z < 20, placing upper limits at these redshifts. We develop a forward modeling approach to
infer the properties of the evolving luminosity function without binning in redshift or luminosity that
marginalizes over the photometric redshift uncertainty of our candidate galaxies and incorporates the
impact of non-detections. We find a z = 12 luminosity function in good agreement with prior results,
and that the luminosity function normalization and UV luminosity density decline by a factor of ∼ 2.5
from z = 12 to z = 14. We discuss the possible implications of our results in the context of theoretical
models for evolution of the dark matter halo mass function.
Richard's aventures in two entangled wonderlandsRichard Gill
Since the loophole-free Bell experiments of 2020 and the Nobel prizes in physics of 2022, critics of Bell's work have retreated to the fortress of super-determinism. Now, super-determinism is a derogatory word - it just means "determinism". Palmer, Hance and Hossenfelder argue that quantum mechanics and determinism are not incompatible, using a sophisticated mathematical construction based on a subtle thinning of allowed states and measurements in quantum mechanics, such that what is left appears to make Bell's argument fail, without altering the empirical predictions of quantum mechanics. I think however that it is a smoke screen, and the slogan "lost in math" comes to my mind. I will discuss some other recent disproofs of Bell's theorem using the language of causality based on causal graphs. Causal thinking is also central to law and justice. I will mention surprising connections to my work on serial killer nurse cases, in particular the Dutch case of Lucia de Berk and the current UK case of Lucy Letby.
Cancer cell metabolism: special Reference to Lactate PathwayAADYARAJPANDEY1
Normal Cell Metabolism:
Cellular respiration describes the series of steps that cells use to break down sugar and other chemicals to get the energy we need to function.
Energy is stored in the bonds of glucose and when glucose is broken down, much of that energy is released.
Cell utilize energy in the form of ATP.
The first step of respiration is called glycolysis. In a series of steps, glycolysis breaks glucose into two smaller molecules - a chemical called pyruvate. A small amount of ATP is formed during this process.
Most healthy cells continue the breakdown in a second process, called the Kreb's cycle. The Kreb's cycle allows cells to “burn” the pyruvates made in glycolysis to get more ATP.
The last step in the breakdown of glucose is called oxidative phosphorylation (Ox-Phos).
It takes place in specialized cell structures called mitochondria. This process produces a large amount of ATP. Importantly, cells need oxygen to complete oxidative phosphorylation.
If a cell completes only glycolysis, only 2 molecules of ATP are made per glucose. However, if the cell completes the entire respiration process (glycolysis - Kreb's - oxidative phosphorylation), about 36 molecules of ATP are created, giving it much more energy to use.
IN CANCER CELL:
Unlike healthy cells that "burn" the entire molecule of sugar to capture a large amount of energy as ATP, cancer cells are wasteful.
Cancer cells only partially break down sugar molecules. They overuse the first step of respiration, glycolysis. They frequently do not complete the second step, oxidative phosphorylation.
This results in only 2 molecules of ATP per each glucose molecule instead of the 36 or so ATPs healthy cells gain. As a result, cancer cells need to use a lot more sugar molecules to get enough energy to survive.
Unlike healthy cells that "burn" the entire molecule of sugar to capture a large amount of energy as ATP, cancer cells are wasteful.
Cancer cells only partially break down sugar molecules. They overuse the first step of respiration, glycolysis. They frequently do not complete the second step, oxidative phosphorylation.
This results in only 2 molecules of ATP per each glucose molecule instead of the 36 or so ATPs healthy cells gain. As a result, cancer cells need to use a lot more sugar molecules to get enough energy to survive.
introduction to WARBERG PHENOMENA:
WARBURG EFFECT Usually, cancer cells are highly glycolytic (glucose addiction) and take up more glucose than do normal cells from outside.
Otto Heinrich Warburg (; 8 October 1883 – 1 August 1970) In 1931 was awarded the Nobel Prize in Physiology for his "discovery of the nature and mode of action of the respiratory enzyme.
WARNBURG EFFECT : cancer cells under aerobic (well-oxygenated) conditions to metabolize glucose to lactate (aerobic glycolysis) is known as the Warburg effect. Warburg made the observation that tumor slices consume glucose and secrete lactate at a higher rate than normal tissues.
Professional air quality monitoring systems provide immediate, on-site data for analysis, compliance, and decision-making.
Monitor common gases, weather parameters, particulates.
A brief information about the SCOP protein database used in bioinformatics.
The Structural Classification of Proteins (SCOP) database is a comprehensive and authoritative resource for the structural and evolutionary relationships of proteins. It provides a detailed and curated classification of protein structures, grouping them into families, superfamilies, and folds based on their structural and sequence similarities.
Seminar of U.V. Spectroscopy by SAMIR PANDASAMIR PANDA
Spectroscopy is a branch of science dealing the study of interaction of electromagnetic radiation with matter.
Ultraviolet-visible spectroscopy refers to absorption spectroscopy or reflect spectroscopy in the UV-VIS spectral region.
Ultraviolet-visible spectroscopy is an analytical method that can measure the amount of light received by the analyte.
This pdf is about the Schizophrenia.
For more details visit on YouTube; @SELF-EXPLANATORY;
https://www.youtube.com/channel/UCAiarMZDNhe1A3Rnpr_WkzA/videos
Thanks...!
Slide 1: Title Slide
Extrachromosomal Inheritance
Slide 2: Introduction to Extrachromosomal Inheritance
Definition: Extrachromosomal inheritance refers to the transmission of genetic material that is not found within the nucleus.
Key Components: Involves genes located in mitochondria, chloroplasts, and plasmids.
Slide 3: Mitochondrial Inheritance
Mitochondria: Organelles responsible for energy production.
Mitochondrial DNA (mtDNA): Circular DNA molecule found in mitochondria.
Inheritance Pattern: Maternally inherited, meaning it is passed from mothers to all their offspring.
Diseases: Examples include Leber’s hereditary optic neuropathy (LHON) and mitochondrial myopathy.
Slide 4: Chloroplast Inheritance
Chloroplasts: Organelles responsible for photosynthesis in plants.
Chloroplast DNA (cpDNA): Circular DNA molecule found in chloroplasts.
Inheritance Pattern: Often maternally inherited in most plants, but can vary in some species.
Examples: Variegation in plants, where leaf color patterns are determined by chloroplast DNA.
Slide 5: Plasmid Inheritance
Plasmids: Small, circular DNA molecules found in bacteria and some eukaryotes.
Features: Can carry antibiotic resistance genes and can be transferred between cells through processes like conjugation.
Significance: Important in biotechnology for gene cloning and genetic engineering.
Slide 6: Mechanisms of Extrachromosomal Inheritance
Non-Mendelian Patterns: Do not follow Mendel’s laws of inheritance.
Cytoplasmic Segregation: During cell division, organelles like mitochondria and chloroplasts are randomly distributed to daughter cells.
Heteroplasmy: Presence of more than one type of organellar genome within a cell, leading to variation in expression.
Slide 7: Examples of Extrachromosomal Inheritance
Four O’clock Plant (Mirabilis jalapa): Shows variegated leaves due to different cpDNA in leaf cells.
Petite Mutants in Yeast: Result from mutations in mitochondrial DNA affecting respiration.
Slide 8: Importance of Extrachromosomal Inheritance
Evolution: Provides insight into the evolution of eukaryotic cells.
Medicine: Understanding mitochondrial inheritance helps in diagnosing and treating mitochondrial diseases.
Agriculture: Chloroplast inheritance can be used in plant breeding and genetic modification.
Slide 9: Recent Research and Advances
Gene Editing: Techniques like CRISPR-Cas9 are being used to edit mitochondrial and chloroplast DNA.
Therapies: Development of mitochondrial replacement therapy (MRT) for preventing mitochondrial diseases.
Slide 10: Conclusion
Summary: Extrachromosomal inheritance involves the transmission of genetic material outside the nucleus and plays a crucial role in genetics, medicine, and biotechnology.
Future Directions: Continued research and technological advancements hold promise for new treatments and applications.
Slide 11: Questions and Discussion
Invite Audience: Open the floor for any questions or further discussion on the topic.
2. 1nm- One thousandth of a micron (10–9m) (or) a billionth of a meter
Semiconductor nanoparticles
• An important class of nanostructured
materials that have a larger number of
interesting physical, chemical,
mechanical, optical, & electronic,
properties
• Semiconductor nanoparticles(10-
100nm) /semiconductor nanocrystals
(or) quantum dots (2-7nm), which can
emit monochrome & tunable fluorescent
light based on their sizes &
compositions
Compound semiconductor Nanoparticles
Binary compounds- Combination of two elements
Group II-VI, III-V, IV-VI, E.g., GaAs, GAP, CdS
Ternary compounds- Alloy semiconductors
Group III-VxV1-x or IIIxIII1-xV, E.g., Ga0.7Al0.3As,
GaAsxP1-x
Quaternary compounds- Combination of many
binary and ternary compounds
Group III-VxV1-x or IIIxIII1-xV, E.g., Cu2ZnSnS4,
Ag2ZnSnSe4
3. Covers the IR to ultraviolet range could be
the basis for a variety of efficient light–
emitting devices spanning the entire range
of the visible spectrum such as blue–
green lasers
Top of the VB and the bottom of the CB occur at
the same value of electron momentum
Maximum energy of the VB occurs at a
different value of momentum to the
minimum in the CB energy
Direct Indirect Bandgap
Minimum energy difference between the top of the VB and the bottom of the CB
Band gap
4. 4
II–VI semiconductors
ME (M = Cd, Zn, Hg; E = S, Se, Te)
Comprising elements of Groups II and VI of the Periodic Table
Bonding in II–VI compounds is a mixture of covalent and ionic types
Good candidates for optical and optoelectronic devices because of their direct bandgap
• Cadmium selenide (CdSe)
• Cadmium sulfide (CdS)
• Cadmium telluride (CdTe)
• Zinc selenide (ZnSe)
• Zinc sulfide (ZnS)
• Zinc telluride (ZnTe)
5. 5
CdS Nanoparticles Properties
• CdS yellow in color
• II-VI group element
• Direct Bandgap-2.42eV
• Remarkable electrical, optical
and surface properties
• Polymorphs: hexagonal greenlockite
& cubic hawleyite
Applications
▪ solar cells
▪ optical detectors
▪ optoelectronic devices
6. Preparation of CdS Nanoparticles
6
Method chosen:
Aqueous precipitation method
Precursors Used:
Cadmium Nitrate (Cd(NO3)2.4H2O)
Sodium sulfide (Na2S)
Diethylene Glycol DEG
(size of nanoparticles effectively controlled
by adding small amount of protecting agent)
METHODOLOGY
20ml 0.1M(Cd(NO3)2.4H2O
+
10ml DEG
After stirring 3 hrs,
yellow precipitate of
CdS formed, washed
with ethanol and acetone
and dried at room
temperature
3 2( ) 2 ( ) ( ) 3 2( )
( ) 2 ( )
aq aq s aq
Cd NO Na S CdS Na NO
+ → +
7. Precursors
Cadmium acetate hydrate
Diaminobenzene
Thioacetamide
Deionized (DI) water
A sol is a colloidal or molecular suspension of solid
particles of ions in a solvent. Dispersed phase is so
small that gravitational forces do not exist;
only van der Waals forces and surface charges are
present
A gel is a semirigid mass that forms when the solvent
from the sol begins to evaporate, and the particles or
ions left behind begin to join in a continuous network
After a drying process, the liquid phase is removed
from the gel. Then a thermal treatment may be
performed in order to favor further poly condensation
and enhance mechanical properties
• Dissolve Cadmium acetate hydrate and
diaminobenzene in deionized (DI)
water and stirrer 4 h
• Add thioacetamide to the solution and
stirrer for another 4 h
• Centrifuge with 3000 rpm to collect the
precipitate and wash down with
numerous times of DI water and then
dry in a desiccators
METHODOLOGY
Synthesis of CdS nanoparticle by sol-gel method as low temperature NO sensor 2 Rakesh K. Sonker, B.C. Yadav, Vinay Gupta, Monika Tomar, https://doi.org/10.1016/j, Materials Chemistry
and Physics , 2019
Preparation of CdS Nanoparticles Sol-gel method
8. Preparation of CdS Nanoparticles Hydrothermal method
Precursors
▪ Cadmium nitrate tetrahydrate (Cd(NO3)2·4H2O)
▪ Thiourea (CH4N2S)
▪ Capping agent hexamethylenetetramine [(CH2)6N4), HMT]
▪ Deionized water
(Cd(NO3)2·4H2O) : CH4N2S) : [(CH2)6N4), HMT
1:1:0 - dendritic-like CdS (D-CdS),
1:3:1 - branched-like CdS (B-CdS),
1:1:1- petaloid-like CdS (P-CdS)
• The mixture is transferred to a teflon-lined stainless-steel
autoclave, (sealed and kept at 200 ℃ for 12 hours)
• Cooled to room temperature
• Washed several times with ultrapure water and ethanol,
• Vacuum-dried and preserved for further Characterization
Preparation of CdS semiconductor nanomaterials with different morphologies Haiyan Fu1,2, Hui Ou1,2*, Yongping Luo1,2, Zonghu Xiao1,2, Ping Huang1,2 , Lishuigen1,2 and Chen Liu1, 2020 3rd
International Conference on Chemistry and Energy Research IOP Conf. Series: Earth and Environmental Science 639 (2021) 012010 IOP Publishing doi:10.1088/1755-1315/639/1/012010 1
Hydrothermal method is a chemical
reaction in water in a sealed pressure
vessel, which is in fact a type of reaction at
both high temperature and pressure.
METHODOLOGY