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Effect of Surface Hardening
Technique and Case Depth on
Rolling Contact Fatigue
Behavior of Alloy Steels
1 BRP US, Inc. – Marine Propulsion Systems Division, Sturtevant, Wisconsin, USA
2 Center for Surface Engineering and Tribology, Northwestern University, Evanston, Illinois, USA
3 State Key Laboratory of Metal Matrix Composites, Shanghai Jiaotong University, Shanghai, China
4 Midwest Thermal-Vac, Kenosha, Wisconsin, USA
5 State Key Laboratory of Mechanical Transmission, Chongqing University, Chongqing, China
David Palmer1, Lechun Xie 2,3, Frederick Otto4, Zhanjiang Wang5,
Q. Jane Wang2
Introduction
Two-stroke outboard engine components
used in rolling contact fatigue (RCF)
2
 Crankshafts
 Connecting rods
 Driveshafts
 Propeller shafts
 Gears
 Bearings
 etc.
Introduction
Typical manufacturing process
Forging → Rough machining → Heat treatment
Straightening → Grinding
3
4
Surface hardening processes
Introduction
Atmosphere carburizing Induction hardening
Vacuum carburizing
(with or without
high-pressure gas
quenching)
5
Introduction
Carburizing vs. induction hardening
Jones et al (2010):
 Spiral bevel gears
 Induction hardened AISI 4340 had lower distortion
 Atmosphere carburized AISI 9310 had higher strength
Townshend et al (1995):
 Straight spur gears
 Induction hardened AISI 1552 had longer RCF life than
atmosphere carburized AISI 9310
 Carburized gears were ground after heat treatment; induction
hardened gears were not
6
Introduction
Atmosphere vs. vacuum carburizing
Lindell et al (2002):
 Helical spur gears
Atmosphere carburizing (with oil quench) vs. vacuum
carburizing (with gas quench) for AISI 8620
 Vacuum carburized AISI 8620 had:
 Higher surface hardness
 Higher surface compressive residual stress
 Greater depth of high hardness (>58 HRC) at same case
depth
7
Introduction
Case depth
 Traditionally measured as depth to 50 HRC (513 HV)
 May vary due to non-uniform heating, non-uniform carbon
pickup, and/or non-uniform stock removal during grinding
Introduction
Problems
 How do different surface hardening methods affect RCF life?
 Atmosphere carburizing with oil quenching
 Vacuum carburizing with oil quenching
 Vacuum carburizing with gas quenching
 Induction hardening
 What is the effect of case depth on RCF life?
 Can elasto-plastic modeling shed light on this problem?
8
Experimental
Design and
Procedure
9
10
RCF
life
Case
depth
Hardening
method
Alloy
Experimental Design
11
RCF
life
Case
depth
Hardening
method
Alloy
Experimental Design
AISI 8620
AISI 9310
AISI 4140
12
RCF
life
Case
depth
Hardening
method
Alloy
Experimental Design
Atmosphere carburize / oil quench
Vacuum carburize / oil quench
Vacuum carburize / gas quench
Induction harden / water quench
13
RCF
life
Case
depth
Hardening
method
Alloy
Experimental Design
Low (0.50 – 0.75 mm)
Medium (0.75 – 1.00 mm)
High (1.00 – 1.25 mm)
14
Procedure
Rough
machining
Heat
treatment
Centerless
grinding
RCF testing
(ball-on-rod)
Microhardness
/ case depth
Metallography
Elasto-plastic
modelling
AISI 8620, 9310, 4140
Vacuum degassed
Certified AQ per SAE AMS 2301
Materials
Material C Mn Si Ni Cr Mo Cu P S Al Fe
8620 0.21 0.83 0.24 0.48 0.54 0.21 0.12 0.008 0.010 0.031 Balance
9310 0.11 0.62 0.26 3.06 1.16 0.10 0.15 0.007 0.020 0.033 Balance
4140 0.41 0.90 0.25 0.06 0.99 0.22 0.07 0.007 0.019 0.030 Balance
15
Length: 3.00 ± .05” (76.2 ± 1.3 mm)
Diameter: 0.400 ± .005” (10.16 ± 0.13 mm) – before grind
Diameter: 0.3750 ± .0001” (9.525 ± 0.002 mm) – after grind
Surface finish: 2 – 4 µin. (0.05 – 0.10 µm)
16
Heat treatment
Carburizing
Temp. (°C)
Hold
Temp.
(°C)
Hold Time
(min.)
Quench
Temp (°C)
Tempering
Temp. (°C)
Tempering
Time
(hours)
Atmosphere 954 815 20 80 177 3
Vacuum 940 815 20 80 177 3
Carburizing
Temp. (°C)
Hold
Temp.
(°C)
Hold Time
(min.)
Quench
Pressure
(kPa)
Tempering
Temp. (°C)
Tempering
Time
(hours)
Vacuum 940 815 20 1500 177 3
AISI 8620
AISI 9310
17
RCF testing
Spring load:
310 N
Rotation speed:
3600 rpm
Lubrication:
0.3 mL/min TC-W3
Ball diameter:
0.500 in. (12.7 mm)
Ball material:
AISI 52100
18
Case depth measurement
Rough
machined
diameter Hardened
layer
Ground
diameter
19
Case depth measurement
Microhardness
traverse
Circumscribed
circle
Vickers scale
(500 g load)
Measurements
made every
.005” (.127 mm)
beginning from
surface
Eccentricity = distance
from specimen axis to
center of circumscribed
circle
Average case depth =
specimen radius – radius
of circumscribed circle
20
Elasto-plastic
Modelling
21
Elasto-plastic modelling
Elasto-plastic modelling for plastically-graded materials (Wang
et al, 2013)
Assumptions:
• Yield strength gradient based on experimentally-determined
hardness gradient
• Tabor approximation: H = 3σY0
• Isotropic strain hardening: σY = σY0(1+εp)n
• Strain hardening exponent:
n = 0.140 for AISI 8620
n = 0.035 for AISI 4140
n = 0.113 for AISI 9310
Values from AISI Bar
Steel Fatigue database
22
Results and
Discussion
23
Microhardness profiles
AISI 8620 – Atmosphere carburized
Hardness at 0.005”: 711 HV
Depth to 56 HRC: 0.54 mm
Depth to 50 HRC: 0.99 mm
24
Microhardness profiles
AISI 8620 – Vacuum carburized
Hardness at 0.005”: 819 HV
Depth to 56 HRC: 0.60 mm
Depth to 50 HRC: 1.02 mm
25
Microhardness profiles
AISI 9310 – Vacuum carburized
Hardness at 0.005”: 776 HV
Depth to 56 HRC: 0.78 mm
Depth to 50 HRC: 1.06 mm
26
Microhardness profiles
AISI 4140 – Induction hardened
Hardness at 0.005”: 639 HV
Depth to 56 HRC: 0.24 mm
Depth to 50 HRC: 1.05 mm
27
Surface hardness
Surface hardness vs. case depth
28
Surface hardness
Cycles to failure vs. surface hardness
29
Surface hardness
Cycles to failure vs. hardness at 0.005 in.
30
Case depth
Cycles to failure vs. case depth
31
Case depth
Cycles to failure vs. depth to 56 HRC
RCF life
Material
Surface
treatment
Average life
(cycles)
Average
case depth
(mm)
Eccentricity
(mm)
Depth to
56 HRC
(mm)
Hardness at
0.005”
(HV)
8620 vacuum 2,300,400 0.813 0.066 0.484 777
8620 vacuum 29,095,200 1.083 0.075 0.718 812
8620 vacuum 37,778,400 1.500 0.066 0.942 866
8620 atmosphere 2,049,300 0.578 0.067 0.287 693
8620 atmosphere 8,812,800 1.009 0.093 0.545 716
8620 atmosphere 21,772,800 1.332 0.141 0.560 673
9310 vacuum 26,568,000 0.677 0.030 0.470 749
9310 vacuum 43,372,800 1.078 0.033 0.793 782
9310 vacuum 52,401,600 1.257 0.027 0.931 793
4140 induction 237,600 0.502 0.041 0.080 605
4140 induction 410,400 0.720 0.060 0.342 631
4140 induction 604,800 1.115 0.086 0.465 635
32
Average cycles to failure
33
Metallography
AISI 8620 atmosphere carburized
Case depth: 1.03 mm
Cycles to failure: 5,248,880
Dark etching area: 0.99 mm wide × 0.15 mm deep
34
Metallography
AISI 8620 vacuum carburized
Case depth: 1.14 mm
Cycles to failure: 29,872,800
Dark etching area: 0.49 mm wide × 0.15 mm deep
35
Metallography
AISI 9310 vacuum carburized
Case depth: 1.10 mm
Cycles to failure: 51,256,800
Dark etching area: 0.44 mm wide × 0.16 mm deep
36
Metallography
AISI 4140 induction hardened
Case depth: 1.17 mm
Cycles to failure: 874,800
Light etching area: 0.78 mm wide × 0.28 mm deep
37
Stress and plastic deformation
Maximum von Mises stress:
3638 MPa at 0.148 mm
depth (0.006”)
38
Stress and plastic deformation
Material
Surface
treatment
Case
depth
Maximum
von Mises
stress (MPa)
Depth of
maximum
stress (mm)
Volume of plastic
deformation zone
(mm³)
Average life
(cycles)
8620 vacuum low 3566 0.138 0.065 2,300,400
8620 vacuum medium 3603 0.148 0.056 29,095,200
8620 vacuum high 3653 0.148 0.042 37,778,400
8620 atmosphere low 3279 0.128 0.113 2,049,300
8620 atmosphere medium 3356 0.138 0.085 8,812,800
8620 atmosphere high 3229 0.128 0.093 21,772,800
9310 vacuum low 3556 0.138 0.078 26,568,000
9310 vacuum medium 3638 0.148 0.057 43,372,800
9310 vacuum high 3647 0.148 0.057 52,401,600
4140 induction low 3531 0.128 0.189 237,600
4140 induction medium 3665 0.148 0.148 410,400
4140 induction high 3636 0.189 0.120 604,800
Maximum stress and plastic zone size
39
Conclusions
Conclusions
(1.) Longest RCF lives: vacuum carburized 8620 and
9310
Shortest RCF lives: induction hardened 4140
More than 2 orders of magnitude!
(2.) Higher surface hardness → longer RCF life
(except for atmosphere carburized 8620)
(3.) More important than surface hardness:
hardness at depth of maximum von Mises stress
(in this case, approximately 0.13 mm)
40
41
Conclusions
(4.) RCF life correlates more closely with depth of
high hardness (>56 HRC) than with case depth
as traditionally defined (>50 HRC)
(5.) Vacuum carburizing → greater depth of high
hardness → smaller plastic deformation zone →
longer RCF life
(6.) Metallographically light- and dark-etching areas
correspond with plastic deformation zones as
predicted by elasto-plastic simulation
42
Dissemination activities
STLE Annual Meeting & Exhibition
Lake Buena Vista, Florida
May 22, 2014
Design News
“Understanding Case Hardening of Steel”
September 4, 2014
Tribology Transactions
Volume 58, Issue 1
2015 (forthcoming)
Acknowledgements
• BRP US, Inc. – Marine Propulsion Systems Division, Sturtevant,
Wisconsin, USA
• Center for Surface Engineering and Tribology, Northwestern
University, Evanston, Illinois, USA
• Midwest Thermal Vac., Kenosha, Wisconsin, USA
• China Scholarship Council (No. 2011623074), Beijing, China
• Shanghai Jiao Tong University, Shanghai, China
• Chongqing University, Chongqing, China
43
References
Jones, K.T., et al. (2010), "Gas Carburizing vs. Contour
Induction Hardening in Bevel Gears," Gear Solutions 8 (82),
pp. 38-44, 51, 54.
Lindell, G.D, et al. (2002), "Selecting the Best Carburizing
Method for the Heat Treatment of Gears (AGMA Technical
Paper 02FTM7)," American Gear Manufacturers
Association, Alexandria, VA, ISBN 1 55589 807 6.
Townsend, D.P., et al. (1995), "The Surface Fatigue Life of
Induction Hardened AISI 1552 Gears (AGMA Technical Paper
95FTM5)," American Gear Manufacturers Association,
Arlington, VA, ISBN 1 55589 654 5.
44
45
References
Wang, Z.J., et al. (2013), “An Efficient Numerical Method
With a Parallel Computation Strategy for Solving Arbitrarily
Shaped Inclusions in Elasto-Plastic Contact Problems,"
ASME Journal of Tribology 135 (3), pp. 031401.

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Effect of Surface Hardening Technique and Case Depth on Rolling Contact Fatigue Behavior of Alloy Steels

  • 1. Effect of Surface Hardening Technique and Case Depth on Rolling Contact Fatigue Behavior of Alloy Steels 1 BRP US, Inc. – Marine Propulsion Systems Division, Sturtevant, Wisconsin, USA 2 Center for Surface Engineering and Tribology, Northwestern University, Evanston, Illinois, USA 3 State Key Laboratory of Metal Matrix Composites, Shanghai Jiaotong University, Shanghai, China 4 Midwest Thermal-Vac, Kenosha, Wisconsin, USA 5 State Key Laboratory of Mechanical Transmission, Chongqing University, Chongqing, China David Palmer1, Lechun Xie 2,3, Frederick Otto4, Zhanjiang Wang5, Q. Jane Wang2
  • 2. Introduction Two-stroke outboard engine components used in rolling contact fatigue (RCF) 2  Crankshafts  Connecting rods  Driveshafts  Propeller shafts  Gears  Bearings  etc.
  • 3. Introduction Typical manufacturing process Forging → Rough machining → Heat treatment Straightening → Grinding 3
  • 4. 4 Surface hardening processes Introduction Atmosphere carburizing Induction hardening Vacuum carburizing (with or without high-pressure gas quenching)
  • 5. 5 Introduction Carburizing vs. induction hardening Jones et al (2010):  Spiral bevel gears  Induction hardened AISI 4340 had lower distortion  Atmosphere carburized AISI 9310 had higher strength Townshend et al (1995):  Straight spur gears  Induction hardened AISI 1552 had longer RCF life than atmosphere carburized AISI 9310  Carburized gears were ground after heat treatment; induction hardened gears were not
  • 6. 6 Introduction Atmosphere vs. vacuum carburizing Lindell et al (2002):  Helical spur gears Atmosphere carburizing (with oil quench) vs. vacuum carburizing (with gas quench) for AISI 8620  Vacuum carburized AISI 8620 had:  Higher surface hardness  Higher surface compressive residual stress  Greater depth of high hardness (>58 HRC) at same case depth
  • 7. 7 Introduction Case depth  Traditionally measured as depth to 50 HRC (513 HV)  May vary due to non-uniform heating, non-uniform carbon pickup, and/or non-uniform stock removal during grinding
  • 8. Introduction Problems  How do different surface hardening methods affect RCF life?  Atmosphere carburizing with oil quenching  Vacuum carburizing with oil quenching  Vacuum carburizing with gas quenching  Induction hardening  What is the effect of case depth on RCF life?  Can elasto-plastic modeling shed light on this problem? 8
  • 12. 12 RCF life Case depth Hardening method Alloy Experimental Design Atmosphere carburize / oil quench Vacuum carburize / oil quench Vacuum carburize / gas quench Induction harden / water quench
  • 13. 13 RCF life Case depth Hardening method Alloy Experimental Design Low (0.50 – 0.75 mm) Medium (0.75 – 1.00 mm) High (1.00 – 1.25 mm)
  • 15. AISI 8620, 9310, 4140 Vacuum degassed Certified AQ per SAE AMS 2301 Materials Material C Mn Si Ni Cr Mo Cu P S Al Fe 8620 0.21 0.83 0.24 0.48 0.54 0.21 0.12 0.008 0.010 0.031 Balance 9310 0.11 0.62 0.26 3.06 1.16 0.10 0.15 0.007 0.020 0.033 Balance 4140 0.41 0.90 0.25 0.06 0.99 0.22 0.07 0.007 0.019 0.030 Balance 15 Length: 3.00 ± .05” (76.2 ± 1.3 mm) Diameter: 0.400 ± .005” (10.16 ± 0.13 mm) – before grind Diameter: 0.3750 ± .0001” (9.525 ± 0.002 mm) – after grind Surface finish: 2 – 4 µin. (0.05 – 0.10 µm)
  • 16. 16 Heat treatment Carburizing Temp. (°C) Hold Temp. (°C) Hold Time (min.) Quench Temp (°C) Tempering Temp. (°C) Tempering Time (hours) Atmosphere 954 815 20 80 177 3 Vacuum 940 815 20 80 177 3 Carburizing Temp. (°C) Hold Temp. (°C) Hold Time (min.) Quench Pressure (kPa) Tempering Temp. (°C) Tempering Time (hours) Vacuum 940 815 20 1500 177 3 AISI 8620 AISI 9310
  • 17. 17 RCF testing Spring load: 310 N Rotation speed: 3600 rpm Lubrication: 0.3 mL/min TC-W3 Ball diameter: 0.500 in. (12.7 mm) Ball material: AISI 52100
  • 18. 18 Case depth measurement Rough machined diameter Hardened layer Ground diameter
  • 19. 19 Case depth measurement Microhardness traverse Circumscribed circle Vickers scale (500 g load) Measurements made every .005” (.127 mm) beginning from surface Eccentricity = distance from specimen axis to center of circumscribed circle Average case depth = specimen radius – radius of circumscribed circle
  • 21. 21 Elasto-plastic modelling Elasto-plastic modelling for plastically-graded materials (Wang et al, 2013) Assumptions: • Yield strength gradient based on experimentally-determined hardness gradient • Tabor approximation: H = 3σY0 • Isotropic strain hardening: σY = σY0(1+εp)n • Strain hardening exponent: n = 0.140 for AISI 8620 n = 0.035 for AISI 4140 n = 0.113 for AISI 9310 Values from AISI Bar Steel Fatigue database
  • 23. 23 Microhardness profiles AISI 8620 – Atmosphere carburized Hardness at 0.005”: 711 HV Depth to 56 HRC: 0.54 mm Depth to 50 HRC: 0.99 mm
  • 24. 24 Microhardness profiles AISI 8620 – Vacuum carburized Hardness at 0.005”: 819 HV Depth to 56 HRC: 0.60 mm Depth to 50 HRC: 1.02 mm
  • 25. 25 Microhardness profiles AISI 9310 – Vacuum carburized Hardness at 0.005”: 776 HV Depth to 56 HRC: 0.78 mm Depth to 50 HRC: 1.06 mm
  • 26. 26 Microhardness profiles AISI 4140 – Induction hardened Hardness at 0.005”: 639 HV Depth to 56 HRC: 0.24 mm Depth to 50 HRC: 1.05 mm
  • 28. 28 Surface hardness Cycles to failure vs. surface hardness
  • 29. 29 Surface hardness Cycles to failure vs. hardness at 0.005 in.
  • 30. 30 Case depth Cycles to failure vs. case depth
  • 31. 31 Case depth Cycles to failure vs. depth to 56 HRC
  • 32. RCF life Material Surface treatment Average life (cycles) Average case depth (mm) Eccentricity (mm) Depth to 56 HRC (mm) Hardness at 0.005” (HV) 8620 vacuum 2,300,400 0.813 0.066 0.484 777 8620 vacuum 29,095,200 1.083 0.075 0.718 812 8620 vacuum 37,778,400 1.500 0.066 0.942 866 8620 atmosphere 2,049,300 0.578 0.067 0.287 693 8620 atmosphere 8,812,800 1.009 0.093 0.545 716 8620 atmosphere 21,772,800 1.332 0.141 0.560 673 9310 vacuum 26,568,000 0.677 0.030 0.470 749 9310 vacuum 43,372,800 1.078 0.033 0.793 782 9310 vacuum 52,401,600 1.257 0.027 0.931 793 4140 induction 237,600 0.502 0.041 0.080 605 4140 induction 410,400 0.720 0.060 0.342 631 4140 induction 604,800 1.115 0.086 0.465 635 32 Average cycles to failure
  • 33. 33 Metallography AISI 8620 atmosphere carburized Case depth: 1.03 mm Cycles to failure: 5,248,880 Dark etching area: 0.99 mm wide × 0.15 mm deep
  • 34. 34 Metallography AISI 8620 vacuum carburized Case depth: 1.14 mm Cycles to failure: 29,872,800 Dark etching area: 0.49 mm wide × 0.15 mm deep
  • 35. 35 Metallography AISI 9310 vacuum carburized Case depth: 1.10 mm Cycles to failure: 51,256,800 Dark etching area: 0.44 mm wide × 0.16 mm deep
  • 36. 36 Metallography AISI 4140 induction hardened Case depth: 1.17 mm Cycles to failure: 874,800 Light etching area: 0.78 mm wide × 0.28 mm deep
  • 37. 37 Stress and plastic deformation Maximum von Mises stress: 3638 MPa at 0.148 mm depth (0.006”)
  • 38. 38 Stress and plastic deformation Material Surface treatment Case depth Maximum von Mises stress (MPa) Depth of maximum stress (mm) Volume of plastic deformation zone (mm³) Average life (cycles) 8620 vacuum low 3566 0.138 0.065 2,300,400 8620 vacuum medium 3603 0.148 0.056 29,095,200 8620 vacuum high 3653 0.148 0.042 37,778,400 8620 atmosphere low 3279 0.128 0.113 2,049,300 8620 atmosphere medium 3356 0.138 0.085 8,812,800 8620 atmosphere high 3229 0.128 0.093 21,772,800 9310 vacuum low 3556 0.138 0.078 26,568,000 9310 vacuum medium 3638 0.148 0.057 43,372,800 9310 vacuum high 3647 0.148 0.057 52,401,600 4140 induction low 3531 0.128 0.189 237,600 4140 induction medium 3665 0.148 0.148 410,400 4140 induction high 3636 0.189 0.120 604,800 Maximum stress and plastic zone size
  • 40. Conclusions (1.) Longest RCF lives: vacuum carburized 8620 and 9310 Shortest RCF lives: induction hardened 4140 More than 2 orders of magnitude! (2.) Higher surface hardness → longer RCF life (except for atmosphere carburized 8620) (3.) More important than surface hardness: hardness at depth of maximum von Mises stress (in this case, approximately 0.13 mm) 40
  • 41. 41 Conclusions (4.) RCF life correlates more closely with depth of high hardness (>56 HRC) than with case depth as traditionally defined (>50 HRC) (5.) Vacuum carburizing → greater depth of high hardness → smaller plastic deformation zone → longer RCF life (6.) Metallographically light- and dark-etching areas correspond with plastic deformation zones as predicted by elasto-plastic simulation
  • 42. 42 Dissemination activities STLE Annual Meeting & Exhibition Lake Buena Vista, Florida May 22, 2014 Design News “Understanding Case Hardening of Steel” September 4, 2014 Tribology Transactions Volume 58, Issue 1 2015 (forthcoming)
  • 43. Acknowledgements • BRP US, Inc. – Marine Propulsion Systems Division, Sturtevant, Wisconsin, USA • Center for Surface Engineering and Tribology, Northwestern University, Evanston, Illinois, USA • Midwest Thermal Vac., Kenosha, Wisconsin, USA • China Scholarship Council (No. 2011623074), Beijing, China • Shanghai Jiao Tong University, Shanghai, China • Chongqing University, Chongqing, China 43
  • 44. References Jones, K.T., et al. (2010), "Gas Carburizing vs. Contour Induction Hardening in Bevel Gears," Gear Solutions 8 (82), pp. 38-44, 51, 54. Lindell, G.D, et al. (2002), "Selecting the Best Carburizing Method for the Heat Treatment of Gears (AGMA Technical Paper 02FTM7)," American Gear Manufacturers Association, Alexandria, VA, ISBN 1 55589 807 6. Townsend, D.P., et al. (1995), "The Surface Fatigue Life of Induction Hardened AISI 1552 Gears (AGMA Technical Paper 95FTM5)," American Gear Manufacturers Association, Arlington, VA, ISBN 1 55589 654 5. 44
  • 45. 45 References Wang, Z.J., et al. (2013), “An Efficient Numerical Method With a Parallel Computation Strategy for Solving Arbitrarily Shaped Inclusions in Elasto-Plastic Contact Problems," ASME Journal of Tribology 135 (3), pp. 031401.