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Calibration of Instruments
E.Karolinekersin
Assistant professor
Calibration
• Calibration of the measuring instrument is the process in which the readings
obtained from the instrument are compared with the sub-standards in the
laboratory at several points along the scale of the instrument.
• The process of evaluating the measurements made by the instrument to be
calibrated against an instrument known to be making measurements that
surpass the suitable limits of precision and correctness is known as
instrument calibration.
2
contd..
• If any variation is found, then the instrument is calibrated so that it can give
exact readings and values.
• It is common for any instrument to lose its calibration after a long period of
usage.
• After the process of calibration, the instrument is good to use again.
3
Characteristics involved in the calibration
• Calibration range – the region between the within which a quantity is
measured, received or transmitted which is expressed by stating the lower
and upper range values.
• Zero value – the lower end of the calibration range
• Span – the difference between the upper and lower range
• Instrument range – the capability of the instrument; may be different than
the calibration range
4
• Accuracy - the ratio of the error to the full scale output or the ratio of the
error to the output, expressed in percent span or percent reading,
respectively.
• Tolerance - permissible deviation from a specified value; may be expressed
in measurement units, percent of span, or percent of reading.
5
• Traceability-the property of a result of a measurement whereby it can be
related to appropriate standards, generally national or international standards,
through an unbroken chain of comparisons.
6
Necessities of calibration
• A crucial measurement
• If the instrument has undergone adverse conditions and cannot give the
right reading.
• When the output does not match the stand-in instrument.
• Drastic change in weather
• Cyclic testing of instruments
7
Need of calibration
• To ensure the reliability of the instrument
• To determine the accuracy of the instrument
• To ensure the readings are consistent with other measurements.
8
Calibration of Measuring Instruments
• All the measuring instruments for measurement of length, pressure,
temperature etc should be calibrated against some standard scale at the
regular intervals as specified by the manufacturer.
• There are different methods or techniques of calibration, which are applied
depending on whether it is routine calibration or if it is for special purpose
where highly accurate calibration of the instruments is desired.
9
contd..
• In many cases different methods of calibration are applied for all the
individual instruments.
• The calibration of the instrument is done in the laboratory against the sub-
standard instruments, which are used very rarely for this sole purpose.
• These sub-standards are kept in highly controlled air-conditioned
atmosphere so that there their scale does not change with the external
atmospheric changes.
10
contd..
• To maintain the accuracy of the sub-standards, they are checked periodically
against some standard which is kept in the metrological laboratories under
highly secured, safe, clean and air conditioned atmosphere.
• Finally, standards can be checked against the absolute measurements of the
quantity, which the instruments are designed to measure.
11
contd..
• Methods of calibration depend on whether the instrument is calibrated
regularly or only occasionally for a special task where a highly calibrated
instrument is required.
• It is essential to get the instruments calibrated every now and then even if
they are in good condition to prevent wrong measurements of extremely
crucial measurements.
12
Types of calibration
The process of testing calibration can
be performed on a number of products
and types of equipment, across multiple
sectors.
Pressure calibration
Electric calibration
Mechanical calibration
Humidity and Temperature
calibration
13
Pressure calibration
This is a widely used calibration process in which gas and hydraulic pressure are measured
across a broad spectrum.
A number of pressure balances and calibrators are generally used, along with a variety of
pressure gages.
The ISO 17025 UKAS accreditation is often taken into consideration when calibrating
pressure and national standards must also generally be adhered to. Examples of pressure
equipment that can be tested for calibration include;
Barometers
Analogue and Digital Pressure Gauges
Digital Indicators
Transmitters 14
Electrical calibration
• This calibration service is used to measure voltage, current frequency and
resistance.
• Electrical calibration often has to adhere to UKAS accredited standards. The
process also monitors resistance and thermocouple simulation covering
process instrumentation.
15
Examples of electrical equipment that can be tested for calibration include;
• Multi-meters
• Counter timers
• Insulation Testers
• Loop Testers
• Clamp Meters
• RCD
• Data Logger
16
Mechanical calibration
A number of dimensional, mass, force, torque and vibration elements will be
calibrated during the testing process. Examples of mechanical equipment that can be
tested for calibration include
• Weight & Mass Sets
• Torque Wrenches & Screwdrivers
• Scales/Balances
• Micrometers, Verniers, Height Gauges
• Accelerometers
• Load Cells & Force Gauges
17
Temperature and Humidity Calibration
Temperature Calibration usually takes
place in a controlled environment.
• Thermometers/Thermocouples
• PRTs and Thermistors
• Thermal Cameras
• Infrared Meters
• Chambers/Furnaces
• Weather Stations
Humidity Calibration usually takes place
in a controlled environment.
• Humidity Recorders
• Humidity Generators
• Digital Indicators and Probes
• Transmitters
• Psychrometers
• Thermohygrographs
• Tinytag Sensors
18
Other calibration
• Waterflow Calibration
• Oilflow Calibration
• Air Velocity Calibration
• Air Flow Calibration
19
Methods of Calibration
• Data Calibration – This method is akin to accredited calibration except that
they are not accredited to the ISO standard and not supplemented by data with
doubtful measurements.
• Standard Calibration – This is the method used for instruments which are not
critical to quality or do not require accreditation. To make sure the standards are
operative, it is necessary to document the process.
20
contd..
• ISO 17025 Accredited Calibration – This is one of the most rigid forms
of calibration.
• An account of the measurement details is maintained.
• International Organization of Standardization is a benchmark which shows
that the company has maintained its standard rules and regulations to
maintain a level of quality.
21
Contd..
There are 4 things to achieve a level of quality
• Maintaining a Record
• Accurate list of Instruments
• Inspect the documentation
• Well –framed quality module
22
Contd ..
• Maintaining a Record – When an instrument is being calibrated it is
mandatory to maintain a record of every minute detail of the results before
and after the calibration.
• Accurate List of Instruments – It is necessary to maintain an updated list
of instruments if your company abides by ISO Standards. An ISO
certification is rejected if the instruments are in the list, but they are not
physically available.
23
Contd ..
Inspect the Documentation – Regular inspection of the calibration process is
mandatory other than just documenting the process.
• The changes can easily be detected if the calibration process is closely
audited every single time.
• It is necessary to document the changes as well as to get an ISO certification.
24
Well-framed Quality Module
• It is necessary to frame a module to keep the quality in check.
• The quality professionals need to follow the same code according to the
module to make sure there is regularity in the calibration processes.
• Only the companies with clear quality modules which is documented on a
regular basis will be eligible for ISO certification.
25
Procedure for calibration
• Firstly, the readings obtained from the scale of the instrument are compared
with the readings of the sub-standard and the calibration curve is formed
from the obtained values.
• In this procedure the instrument is fed with some known values (obtained
from the sub-standard).
• These are detected by the transducer parts of the instrument.
• The output obtained from the instrument is observed and compared against
the original value of the substandard.
26
Contd..
• A single point calibration is good enough if the system has been proved to
be linear (that is readings from instrument are linear with the substandard),
but if it is not, then readings will have to be taken at multiple points.
• In most of the cases the static input is applied to the instruments and its
dynamic response is based on the static calibration.
27
Contd..
• In some instruments it is not feasible to introduce the input quantity for the
calibration purpose like in bonded strain gauges.
• In such cases the spot calibration is done by the manufacturer.
• Calibrations of an instrument ensures precision, consistent measurements,
adheres to the government related standards which results in better and more
accurate reading.
28
Calibration Records
• Calibration, Analog: Stores information for linear or square root calibrations that
have a single input signal, a primary output, and an optional secondary output.
Examples of analog calibrations include gauges, flow, pressure, and temperature.
• Calibration, Discrete: Stores information for single-switch or dual-switch
instruments. Examples of discrete calibrations include flow, level, pressure,
temperature, vibration, and position switches.
• Calibration Weight Scale Setup: Stores information for weight scale calibrations.
29
• Calibration, Single Component Analyzer: Stores information for single
component calibrations. Examples of single component analyzer calibrations
include calibrating pH, in-situ oxygen, toxic gas, and combustible gas.
• Calibration, Multi-Component Analyzer: Stores information for comparing
standard gas values to test results from the analyzer. Examples of multi-component
analyzer calibrations include Mass Spectrometers and Process Gas Chromatographs.
• Calibration, Functional Test: Stores information for functional test calibrations.
An example of an instruction in a functional test is Describe the wires on the piece of
equipment.
30
Contd..
• Calibration, CMX: Stores information about calibrations that are received
from CMX software.
• When calibration data from CMX software is received , CMX record is
automatically created for the event.
• This record contains an event ID, details of the equipment that was
calibrated, calibration strategy used, and the result of the calibration (i.e.,
whether the calibration passed or failed
31
Thank you

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Calibration of Instruments

  • 2. Calibration • Calibration of the measuring instrument is the process in which the readings obtained from the instrument are compared with the sub-standards in the laboratory at several points along the scale of the instrument. • The process of evaluating the measurements made by the instrument to be calibrated against an instrument known to be making measurements that surpass the suitable limits of precision and correctness is known as instrument calibration. 2
  • 3. contd.. • If any variation is found, then the instrument is calibrated so that it can give exact readings and values. • It is common for any instrument to lose its calibration after a long period of usage. • After the process of calibration, the instrument is good to use again. 3
  • 4. Characteristics involved in the calibration • Calibration range – the region between the within which a quantity is measured, received or transmitted which is expressed by stating the lower and upper range values. • Zero value – the lower end of the calibration range • Span – the difference between the upper and lower range • Instrument range – the capability of the instrument; may be different than the calibration range 4
  • 5. • Accuracy - the ratio of the error to the full scale output or the ratio of the error to the output, expressed in percent span or percent reading, respectively. • Tolerance - permissible deviation from a specified value; may be expressed in measurement units, percent of span, or percent of reading. 5
  • 6. • Traceability-the property of a result of a measurement whereby it can be related to appropriate standards, generally national or international standards, through an unbroken chain of comparisons. 6
  • 7. Necessities of calibration • A crucial measurement • If the instrument has undergone adverse conditions and cannot give the right reading. • When the output does not match the stand-in instrument. • Drastic change in weather • Cyclic testing of instruments 7
  • 8. Need of calibration • To ensure the reliability of the instrument • To determine the accuracy of the instrument • To ensure the readings are consistent with other measurements. 8
  • 9. Calibration of Measuring Instruments • All the measuring instruments for measurement of length, pressure, temperature etc should be calibrated against some standard scale at the regular intervals as specified by the manufacturer. • There are different methods or techniques of calibration, which are applied depending on whether it is routine calibration or if it is for special purpose where highly accurate calibration of the instruments is desired. 9
  • 10. contd.. • In many cases different methods of calibration are applied for all the individual instruments. • The calibration of the instrument is done in the laboratory against the sub- standard instruments, which are used very rarely for this sole purpose. • These sub-standards are kept in highly controlled air-conditioned atmosphere so that there their scale does not change with the external atmospheric changes. 10
  • 11. contd.. • To maintain the accuracy of the sub-standards, they are checked periodically against some standard which is kept in the metrological laboratories under highly secured, safe, clean and air conditioned atmosphere. • Finally, standards can be checked against the absolute measurements of the quantity, which the instruments are designed to measure. 11
  • 12. contd.. • Methods of calibration depend on whether the instrument is calibrated regularly or only occasionally for a special task where a highly calibrated instrument is required. • It is essential to get the instruments calibrated every now and then even if they are in good condition to prevent wrong measurements of extremely crucial measurements. 12
  • 13. Types of calibration The process of testing calibration can be performed on a number of products and types of equipment, across multiple sectors. Pressure calibration Electric calibration Mechanical calibration Humidity and Temperature calibration 13
  • 14. Pressure calibration This is a widely used calibration process in which gas and hydraulic pressure are measured across a broad spectrum. A number of pressure balances and calibrators are generally used, along with a variety of pressure gages. The ISO 17025 UKAS accreditation is often taken into consideration when calibrating pressure and national standards must also generally be adhered to. Examples of pressure equipment that can be tested for calibration include; Barometers Analogue and Digital Pressure Gauges Digital Indicators Transmitters 14
  • 15. Electrical calibration • This calibration service is used to measure voltage, current frequency and resistance. • Electrical calibration often has to adhere to UKAS accredited standards. The process also monitors resistance and thermocouple simulation covering process instrumentation. 15
  • 16. Examples of electrical equipment that can be tested for calibration include; • Multi-meters • Counter timers • Insulation Testers • Loop Testers • Clamp Meters • RCD • Data Logger 16
  • 17. Mechanical calibration A number of dimensional, mass, force, torque and vibration elements will be calibrated during the testing process. Examples of mechanical equipment that can be tested for calibration include • Weight & Mass Sets • Torque Wrenches & Screwdrivers • Scales/Balances • Micrometers, Verniers, Height Gauges • Accelerometers • Load Cells & Force Gauges 17
  • 18. Temperature and Humidity Calibration Temperature Calibration usually takes place in a controlled environment. • Thermometers/Thermocouples • PRTs and Thermistors • Thermal Cameras • Infrared Meters • Chambers/Furnaces • Weather Stations Humidity Calibration usually takes place in a controlled environment. • Humidity Recorders • Humidity Generators • Digital Indicators and Probes • Transmitters • Psychrometers • Thermohygrographs • Tinytag Sensors 18
  • 19. Other calibration • Waterflow Calibration • Oilflow Calibration • Air Velocity Calibration • Air Flow Calibration 19
  • 20. Methods of Calibration • Data Calibration – This method is akin to accredited calibration except that they are not accredited to the ISO standard and not supplemented by data with doubtful measurements. • Standard Calibration – This is the method used for instruments which are not critical to quality or do not require accreditation. To make sure the standards are operative, it is necessary to document the process. 20
  • 21. contd.. • ISO 17025 Accredited Calibration – This is one of the most rigid forms of calibration. • An account of the measurement details is maintained. • International Organization of Standardization is a benchmark which shows that the company has maintained its standard rules and regulations to maintain a level of quality. 21
  • 22. Contd.. There are 4 things to achieve a level of quality • Maintaining a Record • Accurate list of Instruments • Inspect the documentation • Well –framed quality module 22
  • 23. Contd .. • Maintaining a Record – When an instrument is being calibrated it is mandatory to maintain a record of every minute detail of the results before and after the calibration. • Accurate List of Instruments – It is necessary to maintain an updated list of instruments if your company abides by ISO Standards. An ISO certification is rejected if the instruments are in the list, but they are not physically available. 23
  • 24. Contd .. Inspect the Documentation – Regular inspection of the calibration process is mandatory other than just documenting the process. • The changes can easily be detected if the calibration process is closely audited every single time. • It is necessary to document the changes as well as to get an ISO certification. 24
  • 25. Well-framed Quality Module • It is necessary to frame a module to keep the quality in check. • The quality professionals need to follow the same code according to the module to make sure there is regularity in the calibration processes. • Only the companies with clear quality modules which is documented on a regular basis will be eligible for ISO certification. 25
  • 26. Procedure for calibration • Firstly, the readings obtained from the scale of the instrument are compared with the readings of the sub-standard and the calibration curve is formed from the obtained values. • In this procedure the instrument is fed with some known values (obtained from the sub-standard). • These are detected by the transducer parts of the instrument. • The output obtained from the instrument is observed and compared against the original value of the substandard. 26
  • 27. Contd.. • A single point calibration is good enough if the system has been proved to be linear (that is readings from instrument are linear with the substandard), but if it is not, then readings will have to be taken at multiple points. • In most of the cases the static input is applied to the instruments and its dynamic response is based on the static calibration. 27
  • 28. Contd.. • In some instruments it is not feasible to introduce the input quantity for the calibration purpose like in bonded strain gauges. • In such cases the spot calibration is done by the manufacturer. • Calibrations of an instrument ensures precision, consistent measurements, adheres to the government related standards which results in better and more accurate reading. 28
  • 29. Calibration Records • Calibration, Analog: Stores information for linear or square root calibrations that have a single input signal, a primary output, and an optional secondary output. Examples of analog calibrations include gauges, flow, pressure, and temperature. • Calibration, Discrete: Stores information for single-switch or dual-switch instruments. Examples of discrete calibrations include flow, level, pressure, temperature, vibration, and position switches. • Calibration Weight Scale Setup: Stores information for weight scale calibrations. 29
  • 30. • Calibration, Single Component Analyzer: Stores information for single component calibrations. Examples of single component analyzer calibrations include calibrating pH, in-situ oxygen, toxic gas, and combustible gas. • Calibration, Multi-Component Analyzer: Stores information for comparing standard gas values to test results from the analyzer. Examples of multi-component analyzer calibrations include Mass Spectrometers and Process Gas Chromatographs. • Calibration, Functional Test: Stores information for functional test calibrations. An example of an instruction in a functional test is Describe the wires on the piece of equipment. 30
  • 31. Contd.. • Calibration, CMX: Stores information about calibrations that are received from CMX software. • When calibration data from CMX software is received , CMX record is automatically created for the event. • This record contains an event ID, details of the equipment that was calibrated, calibration strategy used, and the result of the calibration (i.e., whether the calibration passed or failed 31