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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
Analysis and Improvement of Distortion of Lathe Machine Main Spindle
B. Aditya Mani Sai
Pavan 1*
K.Madhusudhan1 Y. Pratapa Reddy 1 P V S Mohan
Kumar 2.
1 Assistant Professor(s) , Department of Mechanical Engineering, Vasireddy Venkatadri Institute
of Technology, Namburu (V), Guntur (Dt) -522 508, AP, India.
2 Professor, Department of Mechanical Engineering, Vasireddy Venkatadri Institute of Technology,
Namburu (V) , Guntur (Dt) -522 508, AP, India
---------------------------------------------------------------***----------------------------------------------------------------
Abstract: In lathe machine, main spindle is an important
component which is generally made with En353steel. It
undergoes distortion or bending due to high stresses and is
controlled by the heat treatment process called
carburizing. It is the process where the component is
heated to a specified temperature, generally above the
critical temperature and cooled for long period of time
such that the microstructure of the material gets changed
from austenite to martensite. Retained austenite reduces
the hardness, wear resistance and thermal conductivity of
steel and makes its dimensions unstable. A sub-zero
treatment has been devised to reduce the retained
austenite in hardened steel which is done by cooling the
metal to sub-zero temperature. This treatment is suitable
only when the temperature at which the martensite
transformation is completed is below zero. Due to this
change in material from austenite to martensite, the
material improves in its properties like change in
microstructure, hardness, carbon percentage and
composition of the material. Here, in this paper an
attempt is made to apply a heat treatment called sub-zero
treatment to check the changes in the material and results
are compared with conventional properties of specimen
material En353.
Key Words: lathe, main spindle, distortion, heat
treatment, sub-zero treatment, Austenite, Martensite
, hardness
1. INTRODUCTION
Lathe main spindle undergoes various types of
stresses, and bending stress is one of them. It is made up
of En353 material. It is made by following some
sequence of operations. Cryogenically treated high speed
steel tools which shows micro structural changes in the
material that can influence tool life and productivity. It
shows the improvements when using the cryogenically
treated HSS tools in industry [1], and a cooler fan drive
gears used in the MGB to cool the oil in the ALH
Helicopters. By the implementation of the fixture at time
of heat treatment and tested to see that distortion could
be reduced [2] and an example calculations using DANTE
software shows, it has very advanced features, and its
predictions were shown to agree in a relative sense
(within about 15%) with measurements reported on
heat treatment distortion on Navy-C rings made from
4140 and 8620 steel quenched in water and in oil [3],
and the optimum process parameter for XW-5 and XW-
42 were determined where XW-5 is recommended for
applications demanding maximum wear resistance and
XW-42 is a versatile tool steel used for cold work
applications like blanking and other processes [4]. A low
pressure carburizing (LPC) and high pressure gas
quenching (HPGQ) heat treatment processes reduces
distortion significantly and HPGQ provides a very
uniform heat transfer coefficient [5]. The ultimate tensile
strength and the yield strength decrease while the
elongation increases with an increase in tempering
temperature and tempering time of different tempered
specimen, when specimen of quenched, hardened
AISI1040 steel was tempered at temperature (650, 450
& 2500 C) for 60, 90 & 120 minutes to modify desired
properties [6] and the effects of cooling rate on the
microstructure and mechanical properties of AISI 1050
steel, was studied and find out that it varies by using
various quenching medium on the hardness of AISI 1050
Carbon steel [7], various types of heat treatment on
fracture toughness and hardness is analysed using UTM
with the help of sample specimens of low carbon steels
and Stainless Steels[8], and quenching produces a
martensitic microstructure characterized by significant
increase in material’s hardness and a significant
decrease in its impact energy when E110 case hardening
steel is subjected to different heat treatment
processes[9] and the cutting parameters that have the
highest influence on the dimensional changes are the
feed rate and the depth of cut. Residual stresses induced
by soft-machining lead to an increase of the ring
diameter, depending on the machining parameters [10].
2. DISTORTION
Distortion is defined as an irreversible and
usually unpredictable dimensional change in the
component during processing by heat treatment due to
temperature variations in the material. The term
dimensional change is used to denote changes in both
size and shape. The heat-treatment distortion is
therefore a term often used by engineers to describe an
uncontrolled movement that has occurred in a
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 824
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
component as a result of heat-treatment operation. This
can be classified into two categories namely it is
apparent here that some steels such as case hardening
steels appreciable increase in size of about 0.2% after
hardening and tempering between 840 and 870°C and
180 - 200°C. This is sometimes called straightness or
angularity change. It is found particularly in non-
symmetrical components during heat treatment. From
the practical viewpoints, warpage in water- or oil-
hardening steels is normally of greater in magnitude
than in size distortion. Sub - zero literally means
"beneath zero" as such, it is usually used for negative
numbers, especially with regards to temperature. It also
known as cryogenic treatment, utilizes ultra-cold
temperatures to modify the micro-structure of metals
and other materials. It is part of heat treating operations
in manufacturing processes. This process requires
temperatures of at least -85°C to begin. For deep sub-
zero treatment the parts must be cooled to -185°C
where they are held for relatively long periods of time
and then slowly warmed back up. This type of heat-
treating production has been widely accepted as a cost
reduction process and performance enhancing
technology.
The Vickers test is often easier to use than other
hardness tests since the required calculations are
independent of the size of the indenter, and the indenter
can be used for all materials irrespective of hardness.
The basic principle, as with all common measures of
hardness, is to observe the questioned material's ability
to resist plastic deformation from a standard source. The
Vickers test can be used for all metals and has one of the
widest scales among hardness tests. The basic Vickers
Test principle with details of indenter is shown in Fig 2.1
Fig 2.1 Vickers Hardness Test nomenclature
3. METHODOLOGY
The general conventional procedure is applied
to make the main spindle of lathe machine is as follows:
 Selecting the material and cutting it to desired
size of length
 Forging
 Pre Turning
 Normalising
 Carburising and Annealing to 1.2-1.5 mm case
hardening
 Machining after heat treatment
 Hardening and Tempering.
In this analysis, two En 353 steel specimens are made by
conventional procedure mentioned above, which has a
carbon content of 0.171%. The samples of specimens are
shown in Figure 3.1(a), (b),(c) & (d ) used for analysis.
These specimens has undergone different heat treatment
processes like Case carburizing, Hardening & tempering.
(a) Specimen before case carburizing
(b) Specimen after case carburizing
(c) After Hardening process
(d) After tempering process
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 825
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
and the composition of material for En 353 which
are taken for analysis are mentioned in Table 3.1
Table 3.1 Properties of Material
Elements
Materials
present in %
Carbon 0.171 %
Manganese 0.56 %
Silicon 0.3 %
Sulphur 0.13 %,
Phosphorus 0.012 %
Chromium 0.953 %
Nickel 0.989 %
Molybdenum 0.16 %
By considering two samples of the material
En353 of sample size 60 mm each and one sample is
processed according to the conventional procedure. The
second sample is also made with same process but
processed with a heat treatment called sub-zero
treatment. Later the samples are tested with a hardness
tester (Vickers's Hardness test) and microstructures
are tested for both the samples and are compared.
4. RESULTS AND DISCUSSION
4.1 Results: The comparison of material composition is
shown in Table 4.1(a) and it shows that the Carbon
content increased from 1.171% to 1.20 %, and
Manganese increased from 0.56 to 0.70% but the
Sulphur, Chromium gets decreased. Nickel material also
increased from 0.99% to 1.15%, Silicon increased from
0.30% to 0.34 %, Phosphorus was increased to 0.01% to
0.03% in the material. Due to these variations the
hardness and strength were increased.
Table: 4.1.(a) Comparison results of material
composition
Elements
Present
in %
After
carburizing
Process in %
Carbon 0.171% 1.20%
Manganese 0.56% 0.70%
Silicon 0.30% 0.34%
Sulphur 0.13 %, 0.02%
Phosphorus 0.01% 0.03%
Chromium 0.95% 0.90%
Nickel 0.99% 1.15%
Molybdenum 0.16% 0.14%
4.2 Comparison of Microstructures: First the
specimen En353 steel is undergone a heat treatment
process of carburizing and it is annealed, hardened and
the un tempered martensite ranges between 15-20%
and the hardness lies in between 59-60HRC which is
shown in Fig 4.2.a.
Fig:4.2.a Specimen microstructure with un tempered
Martensite
Next another specimen of the same material En353 steel
is Case-carburized, 1.9 Hardened at 8400C and tempered
at 180 0 C and the tempered martensite can be seen with
15-20% retained martensite and the hardness lies in
between Case 59-60HRC and core has hardness of 30
HRC which is shown in Fig 4.2.b.
Fig 4.2.b. Specimen with case carburising and Hardened
with tempered Martensite
Another sample specimen of En353 steel is
carburized, Annealed and hardened followed by a heat
treatment process of sub-zero treatment and the un
tempered martensite is seen and the hardness increased
to 62 HRC and the temperature is taken as 9300 C where
the image is shown in Fig 4.2.c
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 826
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
Fig 4.2.c Specimen microstructurewith subzero
treatment and un tempered Martensite
For sub-zero treatment another specimen of the
same material En353 steel is Case-carburized to 1.8 mm
followed by sub-zero treatment, Hardened at 8400C and
tempered at - 80 0 C and the tempered martensite can be
seen with 2-3% with retained Austenite and the
hardness lies in between core 61-62 HRC and core has
hardness of 31 HRC which is shown in below Fig 4.2.d
Fig:4.2.d Specimen with case carburising and Hardened
with subzero treatment
After the sub-zero treatment conduced to the sample , it
shows lower hardness value which is 906 at 0.3 mm, 970
at 0.6mm and 862 at 1.1 mm etc., and the results
obtained from various points at surface level of material
are tabulated in the table : 4.2
Table 4.2 Comparison of Hardness of samples by Vickers
Method
Distance
on
surface
level
(in mm)
Vickers
Hardness
Values of
without Sub-
Zero Treated
Sample
(HV 0.5)
Vickers
Hardness
Values of Sub-
Zero Treated
Sample
(HV 0.5)
0.3 906 1030
0.6 970 1030
1.1 862 1030
1.3 906 1030
1.5 749 802
1.7 685 716
1.9 580 580
2.2 470 462
2.5 454 462
4.3 Graphical Comparison: The hardness values of both
specimens are compared in graph and shown in Graph
5.2(a) below.
Graph 4.3(a) Graphical Comparison
906
970862
906749
685
580
470
454
1030
1030
1030
1030
802
716
580462
462
-100
100
300
500
700
900
1100
1 2 3 4 5 6 7 8 9
Vickers
Hardness
Values of
without
Sub- Zero
Treated
Sample
(HV 0.5)
Vickers
Hardness
Values of
Sub- Zero
Treated
Sample
(HV 0.5)
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 827
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
4.4 CONCLUSIONS:
 Carbon potential is high 1.201 against 0.8 to 0.9 %
Max. hence formation of Retained Austenite has
increased.
 Effect of Hardening temperature can be reduced to
820oC to reduce Retained Austenite
 From above results it is been observed that
retained austenite of 15 -20 % is effecting
dimensional instability up to 30 to 50 microns for
the component of without sub-zero treated.
 It has been observed that retained austenite of 1 -2
% is improved dimensional stability up to 5
microns for the component with sub-zero
treatment.
 The Hardness of the specimen is decreased by Sub
Zero Treatment. The hardness value varied from
distance of 0.3 to 1.7mm at surface of the material.
 The hardness value remains same at distance of 1.9
mm from the surface.
REFERENCES
1. Flávio J. da Silva, Sinésio D. Franco, Álisson R.
Machado, Emmanuel O. Ezugwu, Antônio M. Souza
Jr., "Performance of cryogenically treated HSS tools" ,
Indian Journal of Science and Technology, Vol 9(9),
DOI: 10.17485/ijst/2015/v9i9/88738, November
2015.
2. Jeevan P. George1, Justin Koshy, Biju Cherian
Abraham, "Distortion Reduction in Gear Heat
Treatment Process by a Simple Fixture", International
Journal of Emerging Technology and Advanced
Engineering (IJETAE), Volume 4, Issue 11, November
2014.
3. R.A. Hardinand C. Beckermann"Simulation of Heat
Treatment Distortion” Proceedings of the 59th SFSA
Technical and Operating Conference, Paper No. 3.3,
Steel Founders' Society of America, Chicago, IL, 2005.
4. Alias Mohd, Nurul Hazwani and Nor Bahiyah Baba
"Investigationon Hardness or Heat Treated
ASSABTool Steels", Indian Journal of Science and
Technology, Vol
(9),DOI:10.17485/ijst/2015/v9i9/88738, November
2015.
5. Dr. Volker Heuer and Dr. Klaus Löser, ALD Vacuum
Technologies GmbH, Donald R. Faron, General
Motors, and David Bolton, ALD-TT, "Low Distortion
Heat Treatment of Transmission Components",
AGMA Technical Paper, October 2010.
6. Ashish Verma, Pravin Kumar Singh,"Influence of Heat
Treatment on Mechanical Properties of Aisi1040
Steel", IOSR Journal of Mechanical and Civil
Engineering (IOSR-JMCE) , Volume 10, Issue 2, pp 32-
38 , Nov. - Dec, 2013.
7. Sanjeev Kumar Jaiswal, Dr. T. Sharma, Rajesh M,
"Study the Effect of Heat Treatment Processes on the
Hardness and the Microstructure of Medium Carbon
Steel", International Journal of Emerging Technology
and Advanced Engineering (IJETAE), Volume 5,
Special Issue 1, April 2015.
8. Devnath khunte, Gopal Sahu, Prakash Kumar Sen,
Ritesh Sharma, Shailendra Bohidar, " A Review On
Effect Of Heat Treatment On Steel," International
Journal of Research in Aeronautical and Mechanical
Engineering, Vol.3 Issue 11, pp: 91-99, November
2015.
9. Majid Tolouei-Rad, Erik Lichter"The Heat Treatment
Analysis of E110 Case Hardening Steel", Journal of
Engineering Science and Technology Vol. 11, No. 3 ,
pp:407 - 415, 2016.
10.Lutz Nowag, Jens Sӧlter , Ekkard Brinksmeier,
"Influence of turning parameters on distortion of
bearing rings" German Academic Society for
Production Engineering, Springer, Prod. Eng. Res.
Devel. 1:135–139,2007.
BIOGRAPHIES:
1. B. ADITYA MANI SAI PAVAN
, working as an Assistant Professor
in Mechanical Engineering
Department. VVIT. His areas of
interest are CAD/CAM, Strength of
Materials, design of Machine
Elements, FEM etc.,
2. K.MADHUSUDHANworking
as an Assistant Professor in
mechanical Engineering Department.
VVIT. His areas of interest are CAD
/CAM, Product Design, Metrology,
Automation.
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 828

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Analysis and Improvement of Distortion of Lathe Machine Main Spindle

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 Analysis and Improvement of Distortion of Lathe Machine Main Spindle B. Aditya Mani Sai Pavan 1* K.Madhusudhan1 Y. Pratapa Reddy 1 P V S Mohan Kumar 2. 1 Assistant Professor(s) , Department of Mechanical Engineering, Vasireddy Venkatadri Institute of Technology, Namburu (V), Guntur (Dt) -522 508, AP, India. 2 Professor, Department of Mechanical Engineering, Vasireddy Venkatadri Institute of Technology, Namburu (V) , Guntur (Dt) -522 508, AP, India ---------------------------------------------------------------***---------------------------------------------------------------- Abstract: In lathe machine, main spindle is an important component which is generally made with En353steel. It undergoes distortion or bending due to high stresses and is controlled by the heat treatment process called carburizing. It is the process where the component is heated to a specified temperature, generally above the critical temperature and cooled for long period of time such that the microstructure of the material gets changed from austenite to martensite. Retained austenite reduces the hardness, wear resistance and thermal conductivity of steel and makes its dimensions unstable. A sub-zero treatment has been devised to reduce the retained austenite in hardened steel which is done by cooling the metal to sub-zero temperature. This treatment is suitable only when the temperature at which the martensite transformation is completed is below zero. Due to this change in material from austenite to martensite, the material improves in its properties like change in microstructure, hardness, carbon percentage and composition of the material. Here, in this paper an attempt is made to apply a heat treatment called sub-zero treatment to check the changes in the material and results are compared with conventional properties of specimen material En353. Key Words: lathe, main spindle, distortion, heat treatment, sub-zero treatment, Austenite, Martensite , hardness 1. INTRODUCTION Lathe main spindle undergoes various types of stresses, and bending stress is one of them. It is made up of En353 material. It is made by following some sequence of operations. Cryogenically treated high speed steel tools which shows micro structural changes in the material that can influence tool life and productivity. It shows the improvements when using the cryogenically treated HSS tools in industry [1], and a cooler fan drive gears used in the MGB to cool the oil in the ALH Helicopters. By the implementation of the fixture at time of heat treatment and tested to see that distortion could be reduced [2] and an example calculations using DANTE software shows, it has very advanced features, and its predictions were shown to agree in a relative sense (within about 15%) with measurements reported on heat treatment distortion on Navy-C rings made from 4140 and 8620 steel quenched in water and in oil [3], and the optimum process parameter for XW-5 and XW- 42 were determined where XW-5 is recommended for applications demanding maximum wear resistance and XW-42 is a versatile tool steel used for cold work applications like blanking and other processes [4]. A low pressure carburizing (LPC) and high pressure gas quenching (HPGQ) heat treatment processes reduces distortion significantly and HPGQ provides a very uniform heat transfer coefficient [5]. The ultimate tensile strength and the yield strength decrease while the elongation increases with an increase in tempering temperature and tempering time of different tempered specimen, when specimen of quenched, hardened AISI1040 steel was tempered at temperature (650, 450 & 2500 C) for 60, 90 & 120 minutes to modify desired properties [6] and the effects of cooling rate on the microstructure and mechanical properties of AISI 1050 steel, was studied and find out that it varies by using various quenching medium on the hardness of AISI 1050 Carbon steel [7], various types of heat treatment on fracture toughness and hardness is analysed using UTM with the help of sample specimens of low carbon steels and Stainless Steels[8], and quenching produces a martensitic microstructure characterized by significant increase in material’s hardness and a significant decrease in its impact energy when E110 case hardening steel is subjected to different heat treatment processes[9] and the cutting parameters that have the highest influence on the dimensional changes are the feed rate and the depth of cut. Residual stresses induced by soft-machining lead to an increase of the ring diameter, depending on the machining parameters [10]. 2. DISTORTION Distortion is defined as an irreversible and usually unpredictable dimensional change in the component during processing by heat treatment due to temperature variations in the material. The term dimensional change is used to denote changes in both size and shape. The heat-treatment distortion is therefore a term often used by engineers to describe an uncontrolled movement that has occurred in a © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 824
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 component as a result of heat-treatment operation. This can be classified into two categories namely it is apparent here that some steels such as case hardening steels appreciable increase in size of about 0.2% after hardening and tempering between 840 and 870°C and 180 - 200°C. This is sometimes called straightness or angularity change. It is found particularly in non- symmetrical components during heat treatment. From the practical viewpoints, warpage in water- or oil- hardening steels is normally of greater in magnitude than in size distortion. Sub - zero literally means "beneath zero" as such, it is usually used for negative numbers, especially with regards to temperature. It also known as cryogenic treatment, utilizes ultra-cold temperatures to modify the micro-structure of metals and other materials. It is part of heat treating operations in manufacturing processes. This process requires temperatures of at least -85°C to begin. For deep sub- zero treatment the parts must be cooled to -185°C where they are held for relatively long periods of time and then slowly warmed back up. This type of heat- treating production has been widely accepted as a cost reduction process and performance enhancing technology. The Vickers test is often easier to use than other hardness tests since the required calculations are independent of the size of the indenter, and the indenter can be used for all materials irrespective of hardness. The basic principle, as with all common measures of hardness, is to observe the questioned material's ability to resist plastic deformation from a standard source. The Vickers test can be used for all metals and has one of the widest scales among hardness tests. The basic Vickers Test principle with details of indenter is shown in Fig 2.1 Fig 2.1 Vickers Hardness Test nomenclature 3. METHODOLOGY The general conventional procedure is applied to make the main spindle of lathe machine is as follows:  Selecting the material and cutting it to desired size of length  Forging  Pre Turning  Normalising  Carburising and Annealing to 1.2-1.5 mm case hardening  Machining after heat treatment  Hardening and Tempering. In this analysis, two En 353 steel specimens are made by conventional procedure mentioned above, which has a carbon content of 0.171%. The samples of specimens are shown in Figure 3.1(a), (b),(c) & (d ) used for analysis. These specimens has undergone different heat treatment processes like Case carburizing, Hardening & tempering. (a) Specimen before case carburizing (b) Specimen after case carburizing (c) After Hardening process (d) After tempering process © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 825
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 and the composition of material for En 353 which are taken for analysis are mentioned in Table 3.1 Table 3.1 Properties of Material Elements Materials present in % Carbon 0.171 % Manganese 0.56 % Silicon 0.3 % Sulphur 0.13 %, Phosphorus 0.012 % Chromium 0.953 % Nickel 0.989 % Molybdenum 0.16 % By considering two samples of the material En353 of sample size 60 mm each and one sample is processed according to the conventional procedure. The second sample is also made with same process but processed with a heat treatment called sub-zero treatment. Later the samples are tested with a hardness tester (Vickers's Hardness test) and microstructures are tested for both the samples and are compared. 4. RESULTS AND DISCUSSION 4.1 Results: The comparison of material composition is shown in Table 4.1(a) and it shows that the Carbon content increased from 1.171% to 1.20 %, and Manganese increased from 0.56 to 0.70% but the Sulphur, Chromium gets decreased. Nickel material also increased from 0.99% to 1.15%, Silicon increased from 0.30% to 0.34 %, Phosphorus was increased to 0.01% to 0.03% in the material. Due to these variations the hardness and strength were increased. Table: 4.1.(a) Comparison results of material composition Elements Present in % After carburizing Process in % Carbon 0.171% 1.20% Manganese 0.56% 0.70% Silicon 0.30% 0.34% Sulphur 0.13 %, 0.02% Phosphorus 0.01% 0.03% Chromium 0.95% 0.90% Nickel 0.99% 1.15% Molybdenum 0.16% 0.14% 4.2 Comparison of Microstructures: First the specimen En353 steel is undergone a heat treatment process of carburizing and it is annealed, hardened and the un tempered martensite ranges between 15-20% and the hardness lies in between 59-60HRC which is shown in Fig 4.2.a. Fig:4.2.a Specimen microstructure with un tempered Martensite Next another specimen of the same material En353 steel is Case-carburized, 1.9 Hardened at 8400C and tempered at 180 0 C and the tempered martensite can be seen with 15-20% retained martensite and the hardness lies in between Case 59-60HRC and core has hardness of 30 HRC which is shown in Fig 4.2.b. Fig 4.2.b. Specimen with case carburising and Hardened with tempered Martensite Another sample specimen of En353 steel is carburized, Annealed and hardened followed by a heat treatment process of sub-zero treatment and the un tempered martensite is seen and the hardness increased to 62 HRC and the temperature is taken as 9300 C where the image is shown in Fig 4.2.c © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 826
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 Fig 4.2.c Specimen microstructurewith subzero treatment and un tempered Martensite For sub-zero treatment another specimen of the same material En353 steel is Case-carburized to 1.8 mm followed by sub-zero treatment, Hardened at 8400C and tempered at - 80 0 C and the tempered martensite can be seen with 2-3% with retained Austenite and the hardness lies in between core 61-62 HRC and core has hardness of 31 HRC which is shown in below Fig 4.2.d Fig:4.2.d Specimen with case carburising and Hardened with subzero treatment After the sub-zero treatment conduced to the sample , it shows lower hardness value which is 906 at 0.3 mm, 970 at 0.6mm and 862 at 1.1 mm etc., and the results obtained from various points at surface level of material are tabulated in the table : 4.2 Table 4.2 Comparison of Hardness of samples by Vickers Method Distance on surface level (in mm) Vickers Hardness Values of without Sub- Zero Treated Sample (HV 0.5) Vickers Hardness Values of Sub- Zero Treated Sample (HV 0.5) 0.3 906 1030 0.6 970 1030 1.1 862 1030 1.3 906 1030 1.5 749 802 1.7 685 716 1.9 580 580 2.2 470 462 2.5 454 462 4.3 Graphical Comparison: The hardness values of both specimens are compared in graph and shown in Graph 5.2(a) below. Graph 4.3(a) Graphical Comparison 906 970862 906749 685 580 470 454 1030 1030 1030 1030 802 716 580462 462 -100 100 300 500 700 900 1100 1 2 3 4 5 6 7 8 9 Vickers Hardness Values of without Sub- Zero Treated Sample (HV 0.5) Vickers Hardness Values of Sub- Zero Treated Sample (HV 0.5) © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 827
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 4.4 CONCLUSIONS:  Carbon potential is high 1.201 against 0.8 to 0.9 % Max. hence formation of Retained Austenite has increased.  Effect of Hardening temperature can be reduced to 820oC to reduce Retained Austenite  From above results it is been observed that retained austenite of 15 -20 % is effecting dimensional instability up to 30 to 50 microns for the component of without sub-zero treated.  It has been observed that retained austenite of 1 -2 % is improved dimensional stability up to 5 microns for the component with sub-zero treatment.  The Hardness of the specimen is decreased by Sub Zero Treatment. The hardness value varied from distance of 0.3 to 1.7mm at surface of the material.  The hardness value remains same at distance of 1.9 mm from the surface. REFERENCES 1. Flávio J. da Silva, Sinésio D. Franco, Álisson R. Machado, Emmanuel O. Ezugwu, Antônio M. Souza Jr., "Performance of cryogenically treated HSS tools" , Indian Journal of Science and Technology, Vol 9(9), DOI: 10.17485/ijst/2015/v9i9/88738, November 2015. 2. Jeevan P. George1, Justin Koshy, Biju Cherian Abraham, "Distortion Reduction in Gear Heat Treatment Process by a Simple Fixture", International Journal of Emerging Technology and Advanced Engineering (IJETAE), Volume 4, Issue 11, November 2014. 3. R.A. Hardinand C. Beckermann"Simulation of Heat Treatment Distortion” Proceedings of the 59th SFSA Technical and Operating Conference, Paper No. 3.3, Steel Founders' Society of America, Chicago, IL, 2005. 4. Alias Mohd, Nurul Hazwani and Nor Bahiyah Baba "Investigationon Hardness or Heat Treated ASSABTool Steels", Indian Journal of Science and Technology, Vol (9),DOI:10.17485/ijst/2015/v9i9/88738, November 2015. 5. Dr. Volker Heuer and Dr. Klaus Löser, ALD Vacuum Technologies GmbH, Donald R. Faron, General Motors, and David Bolton, ALD-TT, "Low Distortion Heat Treatment of Transmission Components", AGMA Technical Paper, October 2010. 6. Ashish Verma, Pravin Kumar Singh,"Influence of Heat Treatment on Mechanical Properties of Aisi1040 Steel", IOSR Journal of Mechanical and Civil Engineering (IOSR-JMCE) , Volume 10, Issue 2, pp 32- 38 , Nov. - Dec, 2013. 7. Sanjeev Kumar Jaiswal, Dr. T. Sharma, Rajesh M, "Study the Effect of Heat Treatment Processes on the Hardness and the Microstructure of Medium Carbon Steel", International Journal of Emerging Technology and Advanced Engineering (IJETAE), Volume 5, Special Issue 1, April 2015. 8. Devnath khunte, Gopal Sahu, Prakash Kumar Sen, Ritesh Sharma, Shailendra Bohidar, " A Review On Effect Of Heat Treatment On Steel," International Journal of Research in Aeronautical and Mechanical Engineering, Vol.3 Issue 11, pp: 91-99, November 2015. 9. Majid Tolouei-Rad, Erik Lichter"The Heat Treatment Analysis of E110 Case Hardening Steel", Journal of Engineering Science and Technology Vol. 11, No. 3 , pp:407 - 415, 2016. 10.Lutz Nowag, Jens Sӧlter , Ekkard Brinksmeier, "Influence of turning parameters on distortion of bearing rings" German Academic Society for Production Engineering, Springer, Prod. Eng. Res. Devel. 1:135–139,2007. BIOGRAPHIES: 1. B. ADITYA MANI SAI PAVAN , working as an Assistant Professor in Mechanical Engineering Department. VVIT. His areas of interest are CAD/CAM, Strength of Materials, design of Machine Elements, FEM etc., 2. K.MADHUSUDHANworking as an Assistant Professor in mechanical Engineering Department. VVIT. His areas of interest are CAD /CAM, Product Design, Metrology, Automation. © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 828