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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 28
OPTIMIZATION ON FRICTION WELDING OF DUPLEX STAINLESS
STEEL-S31803
R Arunprakash1, N. Thenammai2, P. Sundararaj3
1Dept. of metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India
2Asst .professor, Dept. of Metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India
3Head of the Dept. of Metallurgical Engineering, Government College of Engineering, Salem, Tamil Nadu, India
----------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - Friction welding is now well establishedasoneof
the most economical and highly productive methods in
joining similar and dissimilar metals. It is widely used in
automotive and aerospace industrial application. Friction
welding is often the only viable alternative in this field to
overcome the difficulties encountered in joining the
materials with widely varying physical characteristics. The
duplex stainless steel is superior to austenitic stainless steel
in corrosion resistant and strength. The aim of this study is
to do optimization on duplex stainless steel 2205 welded
specimens by using friction welding process. Based on the
trial weld run parameter valuesweldingisdoneandthenthe
microstructure analyses, hardness testing, were carriedout.
The mixture of re-crystallized grain in the weldment was
observed by microstructure analysis.Hardnesstestwasused
to find the hardness for the trial weld run parameter welded
specimen and it reveals that the hardness of the weld metal
zone of S31803 is less than that of the base metal zone.
Key Words: friction welding, Duplex stainless steel S31803,
tensile test, bending test, hardness test and macro & micro
structure.
1. INTRODUCTION
Solid state welding is a group of welding processes which
produces coalescence at temperatures essentially below the
melting point of the base materials being joined, without the
addition of brazing filler metal. Pressure may or may not be
used.Theseprocessesaresometimeserroneouslycalledsolid
state bonding processes: this group of welding processes
includes cold welding, diffusion welding, explosion welding,
forge welding, friction welding, hot pressure welding, roll
welding, and ultrasonic welding.
In all of these processes time, temperature, and pressure
individually or in combination produce coalescence of the
base metal without significant melting of the base metals.
Solid state welding includes some of the very oldest of the
welding processes and some of the very newest. Some of the
processes offer certain advantages since the base metal does
not melt and form a nugget. The metals being joined retain
their original properties without the heat-affected zone
problems involved when there is base metal melting. When
dissimilar metals are joined their thermal expansion and
conductivity is of much less importance with solid state
welding than with the arc welding processes.
Time, temperature, and pressure are involved; however, in
some processes the time element is extremely short, in the
microsecond range or up to a few seconds.Inothercases,the
time is extended to several hours. As temperature increases
time is usually reduced. Since one of these processes is
friction welding will be described the softened material is
squeezed out to form a flash. A forged structure is formed in
the joint. If desired, the flash can be removed by subsequent
machining action. Friction welding has been used to join
steel rod up to 80 mm in diameter and rod with outer
diameter upto 100 mm.
1.1 OBJECTIVE OF PROJECT
To study the characterization of Duplex stainless steel by
friction welding such as hardness test, tensile test, micro
structure, bending test
2. EXPERIMENTAL PROCEDURE
2.1 Material selection
Duplex 2205 is a duplex stainless steel, with a chemical
composition of nearly equal proportions of austenite and
ferrite. This combination allows the alloy to be strongerand
tougher than standard austenitic steels, they aremuchmore
resistant to stress corrosion cracking than standard
austenitic steels. It is also the strongest Duplex in welded
tubular products. Duplex 2205 grade has very high
mechanical strength and excellent seawater corrosion
resistance for use in some of themostdemandingoil andgas,
chemical process, desalination and geothermal power
applications
Table 1 Chemical Composition
2.2 Experimental of S31803 Duplex stainless steel
The welding process used in this project is solid state
welding process friction welding, which is used to weld the
ELE
MEN
TS
C Si M
n
P S Cr M
o
Ni Cu Fe
%
Wt
0.
03
1.
0
3.
0
0.
01
0.
01
23.
00
3.
50
4.
5
0.
24
Ba
l
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 29
S31803 stainless steel of diameter 20 mm, length of 80mm,
spindle speed of 1100 rpm.
12 specimens were prepared under different friction load
and forging load along with friction time and forging time.
Above diagram describes the friction welding of S31803
stainless steel, the welding has to be started from 81 mm
length and facing before 1 mm at the weld length of 80mm.
2.3 APPLICATIONS
Some of the major applications of grade S31803 stainless
steels include: seawater cooling pipes, oil transportation
pipes, gas scrubbing plants, paper processing industries,
acetic, phosphoric and sulphuric acid processing plants oil
refinery components, paper processing industries
3. Welding process
The duplex stainless steel are cut into 54 pieces with above
80 mm length pipe by grinding wheel cutting.Allthesamples
are subjected to facing operation in centre lathe machine on
both sides for better surface finishing. The welding process
chosen here is friction welding. At present duplex stainless
steel are welded using friction welding.
Fig 1 specimen dimension
4. Welded Specimen
Fig 4. welded specimen
The welding process used in this project is solid state
welding process friction welding, which is used to weld the
S31803 stainless steel of diameter 16 mm, length of 80mm,
spindle speed of 1100 rpm. 12 specimens were prepared
under different friction load and forging load along with
friction time and forging time. Above diagram describes the
friction welding of S31803 stainless steel, the weldinghasto
be started from 81 mm length and facing before 1 mm at the
weld length of 80mm.
5. Welding parameter
Exp no Friction
load kg
Friction
time sec
Forging
load kg
Forging time
sec
1 1200 22 1300 4
2 1100 20 1200 3
3 1000 18 1100 2
4 1200 22 1300 4
5 1100 20 1200 3
6 1000 18 1100 2
7 1200 22 1300 4
8 1100 20 1200 3
9 1000 18 1100 2
10 1200 22 1300 4
11 1100 20 1200 3
12 1000 18 1100 2
Table -5 welding parameter
6. RESULTS AND DISCUSSION
Hardness, Tensile Test, Impact Test, Bending Test,
Microstructure and Scanning Electron Microscopy (Sem)
6.1 VICKERS HARDNESS
Hardness is a characteristic of a material, not a fundamental
physical property. It is defined as the resistance to
indentation, and it is determined by measuring the
permanent depth of the indentation.
Table: 6.1 Vickers hardness
Base metal 156VHN
Heat affected zone 146VHN
Welding zone 136VHN
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 30
Fig 6.1 hardness test on surface
6.2 Tensile test
The welded joints are machined to the dimensions as per
ASTM guidelines are followed in preparing the tensile test
specimens. Tensile test is carried out on a 100 kN
electromechanical controlled universal testing machine. The
specimen is loaded at the rate of 1.5 kN per minutes
according to the ASTM specifications.
The tensile strength values are given with corresponding
friction welding process parameters in the Table 4.
Table -6.2: welding input parameters and corresponding
tensile strength
Exp
no
Friction
load kg
Friction
time sec
Forging
load kg
Forging
time sec
Tensile
strength
(TS) N/mm2
1 1300 20 1300 4 489
2 1300 20 1400 4 496
3 1300 25 1300 4 535
4 1400 20 1300 4 574
5 1400 20 1400 4 561
6 1450 20 1300 4 538
Table 6.2 friction welding parameter
6.3. Bending test
A bend test is a method for measuring stiffness and yield
properties of certain materials. Bend tests for ductility
provide a simple way to evaluate the quality of materials by
their ability to resist cracking or other surface irregularities
during one continuous bend
Table -6.3: welding input parameters and corresponding
tensile strength
GRADE
S31803
SPECIMEN
NO
LOAD
(MPa)
Length
(mm)
Time
(min)
1 5 956 15 1.56
2 6 1040 14 1.32
3 10 1125 12 1.45
Table 6.3 bending test
6.4 Impact test
Impact Testing of metals is performed to determine the
impact resistance or toughness of materials by calculating
the amount of energy absorbed during fracture. The impact
test is performed at various temperatures to uncover any
effects on impact energy
GRADE
S31803
SPECIMEN
NO
Parameter Toughness at
(RT)
1 7 Test result
(joules)
145
2 8 146
3 9 148
Average
(joules)
145
Table 6.4 impact test
6.5 Microstructure of S31803 stainless steel
Micro structural evaluation ranges from simple
determination of certain parameters such as grain size or
coating thickness through porosity and porestructuretofull
characterization of multi-component systems or evaluation
of degradation or failure mechanisms.
Here we use the micro structural for the determination of
grain boundaries on the following three zones. Micro
examination is performed for a number of purposes most
commonly it is carried out to assess the structureofmaterial
for quality purposes: Ensures correct heat treatment is
employed Detectsunwanted phasesandinclusions Identifies
where excessive grain boundaries
Base metal fusion zone
HAZ zone
Fig 6.5 microstructure of S31803 Duplex stainless steel
7. CONCLUSIONS
In this study, Friction welding process parameters were
optimized by using response surface methodology. The
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 31
friction welding process was carried out as per the design of
experiments by central composite design. Tensile test was
carried out for friction welded samples and the results of the
tests are recorded. Based on the experimental results,
regression analysis has conducted. Based on the
experimentation and optimization the following conclusions
are stated:
[1] Specimen having high burnoff length has the high
Tensile strength
[2] The Microstructure of the specimen shows the
originated grain boundaries over Weld zone,HAZ,Base
metal the continuation on the welded area has the high
hard
[3] The empirical relations were developed to predict
the tensile strength of the friction welded superduplex
stainless steel incorporating process parameters at
85% confidence level.
The tensile tests showed that the friction processed joints
exhibited comparable strength with the base material and
joint strength decreased with an increase in thefrictiontime
REFERENCES
[1] T.Udayakumar et al, experimental investigation on
mechanical and metallurgical properties of super
duplex stainless steel joints using friction welding
process, Journal of Manufacturing Processes-188.
[2] Serdar Mercan et al, Effect of weldingparameterson
the fatigue properties of dissimilar AISI 2205- AISI
1020 joined by friction welding, International
Journal of Fatigue (2015).
[3] Nisarg Shete et al, A Review Paper on Rotary
Friction Welding, International ConferenceonIdeas,
Impact and Innovation in Mechanical Engineering
(ICIIIME 2017),vol : 5, pg : 1557-1560.
[4] D. Ananthapadmanaban et al, A study of mechanical
properties of friction welded mild steel to stainless
steel joints, Materials and Design 30 (2009) 2642–
2646.
[5] Vishnu P S et al, Optimization of Friction Welding
Parameters for Joining Medium Carbon Steels using
Response Surface Methodology, International
Journal of Engineering Research & Technology
(IJERT), Vol. 3 Issue 10, October- 2014.
[6] H.C. Dey et al, Joining of titanium to 304L stainless
steel by friction welding, Journal of Materials
Processing Technology 209 (2009) 5862–5870.
BIOGRAPHIES
R. Arunprakash
ME WELDING
TECHNOLOGY(2017-2019)
Dept. of metallurgical
Engineering, Government college
of Engineering, Salem, Tamil
Nadu, India
N. Thenammai
Asst. professor, Dept. of
Metallurgical Engineering,
Government college of
Engineering, Salem, Tamil Nadu,
India
P. Sundararaj
Head of the Dept. of Metallurgical
Engineering, Government college
of Engineering, Salem, Tamil
Nadu, India

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  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 28 OPTIMIZATION ON FRICTION WELDING OF DUPLEX STAINLESS STEEL-S31803 R Arunprakash1, N. Thenammai2, P. Sundararaj3 1Dept. of metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India 2Asst .professor, Dept. of Metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India 3Head of the Dept. of Metallurgical Engineering, Government College of Engineering, Salem, Tamil Nadu, India ----------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - Friction welding is now well establishedasoneof the most economical and highly productive methods in joining similar and dissimilar metals. It is widely used in automotive and aerospace industrial application. Friction welding is often the only viable alternative in this field to overcome the difficulties encountered in joining the materials with widely varying physical characteristics. The duplex stainless steel is superior to austenitic stainless steel in corrosion resistant and strength. The aim of this study is to do optimization on duplex stainless steel 2205 welded specimens by using friction welding process. Based on the trial weld run parameter valuesweldingisdoneandthenthe microstructure analyses, hardness testing, were carriedout. The mixture of re-crystallized grain in the weldment was observed by microstructure analysis.Hardnesstestwasused to find the hardness for the trial weld run parameter welded specimen and it reveals that the hardness of the weld metal zone of S31803 is less than that of the base metal zone. Key Words: friction welding, Duplex stainless steel S31803, tensile test, bending test, hardness test and macro & micro structure. 1. INTRODUCTION Solid state welding is a group of welding processes which produces coalescence at temperatures essentially below the melting point of the base materials being joined, without the addition of brazing filler metal. Pressure may or may not be used.Theseprocessesaresometimeserroneouslycalledsolid state bonding processes: this group of welding processes includes cold welding, diffusion welding, explosion welding, forge welding, friction welding, hot pressure welding, roll welding, and ultrasonic welding. In all of these processes time, temperature, and pressure individually or in combination produce coalescence of the base metal without significant melting of the base metals. Solid state welding includes some of the very oldest of the welding processes and some of the very newest. Some of the processes offer certain advantages since the base metal does not melt and form a nugget. The metals being joined retain their original properties without the heat-affected zone problems involved when there is base metal melting. When dissimilar metals are joined their thermal expansion and conductivity is of much less importance with solid state welding than with the arc welding processes. Time, temperature, and pressure are involved; however, in some processes the time element is extremely short, in the microsecond range or up to a few seconds.Inothercases,the time is extended to several hours. As temperature increases time is usually reduced. Since one of these processes is friction welding will be described the softened material is squeezed out to form a flash. A forged structure is formed in the joint. If desired, the flash can be removed by subsequent machining action. Friction welding has been used to join steel rod up to 80 mm in diameter and rod with outer diameter upto 100 mm. 1.1 OBJECTIVE OF PROJECT To study the characterization of Duplex stainless steel by friction welding such as hardness test, tensile test, micro structure, bending test 2. EXPERIMENTAL PROCEDURE 2.1 Material selection Duplex 2205 is a duplex stainless steel, with a chemical composition of nearly equal proportions of austenite and ferrite. This combination allows the alloy to be strongerand tougher than standard austenitic steels, they aremuchmore resistant to stress corrosion cracking than standard austenitic steels. It is also the strongest Duplex in welded tubular products. Duplex 2205 grade has very high mechanical strength and excellent seawater corrosion resistance for use in some of themostdemandingoil andgas, chemical process, desalination and geothermal power applications Table 1 Chemical Composition 2.2 Experimental of S31803 Duplex stainless steel The welding process used in this project is solid state welding process friction welding, which is used to weld the ELE MEN TS C Si M n P S Cr M o Ni Cu Fe % Wt 0. 03 1. 0 3. 0 0. 01 0. 01 23. 00 3. 50 4. 5 0. 24 Ba l
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 29 S31803 stainless steel of diameter 20 mm, length of 80mm, spindle speed of 1100 rpm. 12 specimens were prepared under different friction load and forging load along with friction time and forging time. Above diagram describes the friction welding of S31803 stainless steel, the welding has to be started from 81 mm length and facing before 1 mm at the weld length of 80mm. 2.3 APPLICATIONS Some of the major applications of grade S31803 stainless steels include: seawater cooling pipes, oil transportation pipes, gas scrubbing plants, paper processing industries, acetic, phosphoric and sulphuric acid processing plants oil refinery components, paper processing industries 3. Welding process The duplex stainless steel are cut into 54 pieces with above 80 mm length pipe by grinding wheel cutting.Allthesamples are subjected to facing operation in centre lathe machine on both sides for better surface finishing. The welding process chosen here is friction welding. At present duplex stainless steel are welded using friction welding. Fig 1 specimen dimension 4. Welded Specimen Fig 4. welded specimen The welding process used in this project is solid state welding process friction welding, which is used to weld the S31803 stainless steel of diameter 16 mm, length of 80mm, spindle speed of 1100 rpm. 12 specimens were prepared under different friction load and forging load along with friction time and forging time. Above diagram describes the friction welding of S31803 stainless steel, the weldinghasto be started from 81 mm length and facing before 1 mm at the weld length of 80mm. 5. Welding parameter Exp no Friction load kg Friction time sec Forging load kg Forging time sec 1 1200 22 1300 4 2 1100 20 1200 3 3 1000 18 1100 2 4 1200 22 1300 4 5 1100 20 1200 3 6 1000 18 1100 2 7 1200 22 1300 4 8 1100 20 1200 3 9 1000 18 1100 2 10 1200 22 1300 4 11 1100 20 1200 3 12 1000 18 1100 2 Table -5 welding parameter 6. RESULTS AND DISCUSSION Hardness, Tensile Test, Impact Test, Bending Test, Microstructure and Scanning Electron Microscopy (Sem) 6.1 VICKERS HARDNESS Hardness is a characteristic of a material, not a fundamental physical property. It is defined as the resistance to indentation, and it is determined by measuring the permanent depth of the indentation. Table: 6.1 Vickers hardness Base metal 156VHN Heat affected zone 146VHN Welding zone 136VHN
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 30 Fig 6.1 hardness test on surface 6.2 Tensile test The welded joints are machined to the dimensions as per ASTM guidelines are followed in preparing the tensile test specimens. Tensile test is carried out on a 100 kN electromechanical controlled universal testing machine. The specimen is loaded at the rate of 1.5 kN per minutes according to the ASTM specifications. The tensile strength values are given with corresponding friction welding process parameters in the Table 4. Table -6.2: welding input parameters and corresponding tensile strength Exp no Friction load kg Friction time sec Forging load kg Forging time sec Tensile strength (TS) N/mm2 1 1300 20 1300 4 489 2 1300 20 1400 4 496 3 1300 25 1300 4 535 4 1400 20 1300 4 574 5 1400 20 1400 4 561 6 1450 20 1300 4 538 Table 6.2 friction welding parameter 6.3. Bending test A bend test is a method for measuring stiffness and yield properties of certain materials. Bend tests for ductility provide a simple way to evaluate the quality of materials by their ability to resist cracking or other surface irregularities during one continuous bend Table -6.3: welding input parameters and corresponding tensile strength GRADE S31803 SPECIMEN NO LOAD (MPa) Length (mm) Time (min) 1 5 956 15 1.56 2 6 1040 14 1.32 3 10 1125 12 1.45 Table 6.3 bending test 6.4 Impact test Impact Testing of metals is performed to determine the impact resistance or toughness of materials by calculating the amount of energy absorbed during fracture. The impact test is performed at various temperatures to uncover any effects on impact energy GRADE S31803 SPECIMEN NO Parameter Toughness at (RT) 1 7 Test result (joules) 145 2 8 146 3 9 148 Average (joules) 145 Table 6.4 impact test 6.5 Microstructure of S31803 stainless steel Micro structural evaluation ranges from simple determination of certain parameters such as grain size or coating thickness through porosity and porestructuretofull characterization of multi-component systems or evaluation of degradation or failure mechanisms. Here we use the micro structural for the determination of grain boundaries on the following three zones. Micro examination is performed for a number of purposes most commonly it is carried out to assess the structureofmaterial for quality purposes: Ensures correct heat treatment is employed Detectsunwanted phasesandinclusions Identifies where excessive grain boundaries Base metal fusion zone HAZ zone Fig 6.5 microstructure of S31803 Duplex stainless steel 7. CONCLUSIONS In this study, Friction welding process parameters were optimized by using response surface methodology. The
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 04 | Apr 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 31 friction welding process was carried out as per the design of experiments by central composite design. Tensile test was carried out for friction welded samples and the results of the tests are recorded. Based on the experimental results, regression analysis has conducted. Based on the experimentation and optimization the following conclusions are stated: [1] Specimen having high burnoff length has the high Tensile strength [2] The Microstructure of the specimen shows the originated grain boundaries over Weld zone,HAZ,Base metal the continuation on the welded area has the high hard [3] The empirical relations were developed to predict the tensile strength of the friction welded superduplex stainless steel incorporating process parameters at 85% confidence level. The tensile tests showed that the friction processed joints exhibited comparable strength with the base material and joint strength decreased with an increase in thefrictiontime REFERENCES [1] T.Udayakumar et al, experimental investigation on mechanical and metallurgical properties of super duplex stainless steel joints using friction welding process, Journal of Manufacturing Processes-188. [2] Serdar Mercan et al, Effect of weldingparameterson the fatigue properties of dissimilar AISI 2205- AISI 1020 joined by friction welding, International Journal of Fatigue (2015). [3] Nisarg Shete et al, A Review Paper on Rotary Friction Welding, International ConferenceonIdeas, Impact and Innovation in Mechanical Engineering (ICIIIME 2017),vol : 5, pg : 1557-1560. [4] D. Ananthapadmanaban et al, A study of mechanical properties of friction welded mild steel to stainless steel joints, Materials and Design 30 (2009) 2642– 2646. [5] Vishnu P S et al, Optimization of Friction Welding Parameters for Joining Medium Carbon Steels using Response Surface Methodology, International Journal of Engineering Research & Technology (IJERT), Vol. 3 Issue 10, October- 2014. [6] H.C. Dey et al, Joining of titanium to 304L stainless steel by friction welding, Journal of Materials Processing Technology 209 (2009) 5862–5870. BIOGRAPHIES R. Arunprakash ME WELDING TECHNOLOGY(2017-2019) Dept. of metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India N. Thenammai Asst. professor, Dept. of Metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India P. Sundararaj Head of the Dept. of Metallurgical Engineering, Government college of Engineering, Salem, Tamil Nadu, India