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Water Sampling
Its Purpose, Procedure, techniques &
equipments.
QUCEST,LARKANO, PAKISTAN
What is water Sampling?
The process of collecting a representative
portion of water, as from the natural
environment or from an industrial site, for the
purpose of analyzing it for constituents
The process of taking a portion of water for
analysis or other testing.
 e.g. drinking water to check that it complies,
or river water to check for pollutants, or
bathing water to check that it is safe.
Water Sampling Purpose:
The primary goal of water sampling is to observe
and measure how water quality changes over
time.
 An important premise to water sampling work is
that high acidity or high alkalinity (pH levels) in
the water might be normal for a given
environment or ecological region
water samples must be taken and analyzed
repeatedly over a period of weeks, months,
years, and decades to determine more precisely
how water conditions change.
Water Sampling Procedure:
1. If sampling a body of running water, point the
mouth of the bag upstream and your hands
downstream to avoid contamination.
2. If sampling from a water faucet, run the faucet
for 1 minute before obtaining a sample.
3. Rinse the bag twice with the sample water prior
to filling and closing.
4. Fill bag as full as possible. Half-filling the bottle
leaves more room for oxygen which will promote
degradation of your sample.
5. Collect data such as temperature and pH which
affect the solubility of many ions.
Sampling Flow Chart
Sampling
Planning
Water
Sampling
Preparation
Storage
Sampling at
the Sites
Transportation Analyses
Water Sampling Techniques
Systematic,
Random,
Judgmental (nonstatistical),
Stratified,
Haphazard
Sampling Methods
Systematic Sampling
For example,
The area to be analyzed may divided by a grid, and a
sample taken at each point of the grid.
For air pollution studies, an air sample might be taken at
fixed intervals of time, say every three hours.
Random Sampling
Judgmental Sampling
Stratified Sampling
Haphazard Sampling
A sampling location or sampling time is chosen arbitrarily.
This type of sampling is reasonable for a homogeneous
system.
Since most environmental systems have significant
spatial or temporal variability, haphazard sampling often
leads to biased results.
 However, this approach may be used as a preliminary
screening technique to identify a possible problem before a
full scale sampling is done.
Types Of Samples
Grab sample: A grab sample is a discrete sample which is
collected at a specific location at a certain point in time. If the
environmental medium varies spatially or temporally, then a
single grab sample is not representative and more samples
need to be collected.
Composite sample: A composite sample is made by
thoroughly mixing several grab samples. The whole composite
may be measured or random samples from the composites
may be withdrawn and measured.
Surface water Equipments
Rinse the sampling vessel with water on site 3~4 times. Care
must be taken to avoid contaminating water to be sampled
during rinsing.
Submerge the sampling vessel gently, fill it with the water
sample and close it tightly. If the collected water sample may
be frozen, leave some space for expansion equivalent to about
10% of the sampling vessel.
Water Sampling using Sampling Vessels
Simple Water Sampler
Buckets or Samplers with Shafts (Scoops)
Such instruments made of polyethylene are often used. A rope
can be attached to the bucket if required. Scoops with
adjustable shafts are convenient. Items made of synthetic
resins such as polypropylene can also be used. Samplers made
of stainless steel can be used provided they are not to be used
for tests on trace amounts of heavy metals.
Water Collection using Heyroth Water Sampler
Vandorn Water Sampler
Insulated Water Sampler
Ground Water Equipments
Bailer
A bailer in is a hollow tube used to retrieve groundwater
samples from monitoring wells. Bailers are tied to a piece of
rope or a piece of wire and lowered into the water column.
Once lowered, the bailer uses a simple ball check valve to seal
at the bottom in order to pull up a sample of the groundwater
table. Bailers can be disposable or reusable, and they are
made out of polyethylene, PVC, FEP or stainless steel.
Suction lift Pump
Suction-lift pumps create a vacuum
in the intake line that draws the
sample up to land surface.
Sampling is limited to situations
where water levels are within about
20 ft of the ground surface.
Vacuum effect can cause the water
to lose some dissolved gas.
Air-lift Samplers
The pump injects compressed air at the bottom
of the discharge pipe which is immersed in the
liquid. The compressed air mixes with the liquid
causing the air-water mixture to be less dense
than the rest of the liquid around it and
therefore is displaced upwards through the
discharge pipe by the surrounding liquid of
higher density. In general, this method is not an
appropriate method for acquisition of water
samples for detailed chemical analyses
because of degassing effect on the sample.
Oxygenation is impossible to avoid unless
elaborate precautions are taken.
Submersible Pump
The submersible pumps are multistage
centrifugal pumps operating in a vertical
position. Produced liquids, after being
subjected to great centrifugal forces caused
by the high rotational speed of the impeller,
lose their kinetic energy in the diffuser where a
conversion of kinetic to pressure energy takes
place. This is the main operational mechanism
of radial and mixed flow pumps.
The pump shaft is connected to the gas
separator or the protector by a mechanical
coupling at the bottom of the pump. When
fluids enter the pump through an intake screen
and are lifted by the pump stages..
Thank
you 

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Water sampling , procedure, purpose , techniques and equipments

  • 1. Water Sampling Its Purpose, Procedure, techniques & equipments. QUCEST,LARKANO, PAKISTAN
  • 2. What is water Sampling? The process of collecting a representative portion of water, as from the natural environment or from an industrial site, for the purpose of analyzing it for constituents The process of taking a portion of water for analysis or other testing.  e.g. drinking water to check that it complies, or river water to check for pollutants, or bathing water to check that it is safe.
  • 3. Water Sampling Purpose: The primary goal of water sampling is to observe and measure how water quality changes over time.  An important premise to water sampling work is that high acidity or high alkalinity (pH levels) in the water might be normal for a given environment or ecological region water samples must be taken and analyzed repeatedly over a period of weeks, months, years, and decades to determine more precisely how water conditions change.
  • 4. Water Sampling Procedure: 1. If sampling a body of running water, point the mouth of the bag upstream and your hands downstream to avoid contamination. 2. If sampling from a water faucet, run the faucet for 1 minute before obtaining a sample. 3. Rinse the bag twice with the sample water prior to filling and closing. 4. Fill bag as full as possible. Half-filling the bottle leaves more room for oxygen which will promote degradation of your sample. 5. Collect data such as temperature and pH which affect the solubility of many ions.
  • 8. Systematic Sampling For example, The area to be analyzed may divided by a grid, and a sample taken at each point of the grid. For air pollution studies, an air sample might be taken at fixed intervals of time, say every three hours.
  • 12. Haphazard Sampling A sampling location or sampling time is chosen arbitrarily. This type of sampling is reasonable for a homogeneous system. Since most environmental systems have significant spatial or temporal variability, haphazard sampling often leads to biased results.  However, this approach may be used as a preliminary screening technique to identify a possible problem before a full scale sampling is done.
  • 13. Types Of Samples Grab sample: A grab sample is a discrete sample which is collected at a specific location at a certain point in time. If the environmental medium varies spatially or temporally, then a single grab sample is not representative and more samples need to be collected. Composite sample: A composite sample is made by thoroughly mixing several grab samples. The whole composite may be measured or random samples from the composites may be withdrawn and measured.
  • 15. Rinse the sampling vessel with water on site 3~4 times. Care must be taken to avoid contaminating water to be sampled during rinsing. Submerge the sampling vessel gently, fill it with the water sample and close it tightly. If the collected water sample may be frozen, leave some space for expansion equivalent to about 10% of the sampling vessel. Water Sampling using Sampling Vessels
  • 17. Buckets or Samplers with Shafts (Scoops) Such instruments made of polyethylene are often used. A rope can be attached to the bucket if required. Scoops with adjustable shafts are convenient. Items made of synthetic resins such as polypropylene can also be used. Samplers made of stainless steel can be used provided they are not to be used for tests on trace amounts of heavy metals.
  • 18. Water Collection using Heyroth Water Sampler
  • 22. Bailer A bailer in is a hollow tube used to retrieve groundwater samples from monitoring wells. Bailers are tied to a piece of rope or a piece of wire and lowered into the water column. Once lowered, the bailer uses a simple ball check valve to seal at the bottom in order to pull up a sample of the groundwater table. Bailers can be disposable or reusable, and they are made out of polyethylene, PVC, FEP or stainless steel.
  • 23. Suction lift Pump Suction-lift pumps create a vacuum in the intake line that draws the sample up to land surface. Sampling is limited to situations where water levels are within about 20 ft of the ground surface. Vacuum effect can cause the water to lose some dissolved gas.
  • 24. Air-lift Samplers The pump injects compressed air at the bottom of the discharge pipe which is immersed in the liquid. The compressed air mixes with the liquid causing the air-water mixture to be less dense than the rest of the liquid around it and therefore is displaced upwards through the discharge pipe by the surrounding liquid of higher density. In general, this method is not an appropriate method for acquisition of water samples for detailed chemical analyses because of degassing effect on the sample. Oxygenation is impossible to avoid unless elaborate precautions are taken.
  • 25. Submersible Pump The submersible pumps are multistage centrifugal pumps operating in a vertical position. Produced liquids, after being subjected to great centrifugal forces caused by the high rotational speed of the impeller, lose their kinetic energy in the diffuser where a conversion of kinetic to pressure energy takes place. This is the main operational mechanism of radial and mixed flow pumps. The pump shaft is connected to the gas separator or the protector by a mechanical coupling at the bottom of the pump. When fluids enter the pump through an intake screen and are lifted by the pump stages..