This document describes an experiment on heat conduction using different specimen materials and shapes. Temperature data was collected as specimens cooled in air after being heated to an initial temperature in a water bath. The results were used to calculate dimensionless temperature, Fourier number, and Biot number to determine if the lumped capacitance method could be applied. For a stainless steel sphere specimen, the method yielded a heat transfer coefficient of 32.58 W/m2K, consistent with expected values. The experiment allowed students to analyze unsteady state heat transfer and compare heat transfer coefficients for different materials.