This document summarizes a study that used Taguchi methodology to optimize parameters for maximum biodiesel production from linseed oil through transesterification. The parameters investigated were molar ratio of methanol to triglyceride, reaction temperature, reaction time, and catalyst concentration. Experiments were conducted according to an L9 orthogonal array. ANOVA results showed that reaction temperature had the greatest effect on yield, contributing most to variation in yield. The optimal conditions found were a molar ratio of 6:1, reaction temperature of 60°C, reaction time of 60 minutes, and catalyst concentration of 1%, which yielded 95% biodiesel. Further work could utilize other experimental designs like factorial or response surface methodology.