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Y.Bavaneethan.
Lecturer
Department of Food Technology
SLGTI. SriLanka.11/27/2017 Y.BAVANEETHAN 1
Pasteurization
 Pasteurisation is a relatively mild heat treatment, in
which food is heated to below 100ºC.
 In low acid foods (pH>4.5, for example milk) it is
used to minimize the hazards from pathogenic
micro-organisms and to extend the shelf life of
foods for severaldays.
 In acidic foods (pH< 4.5, for example bottled
fruit) it is used to extend the shelf life for several
months by destruction of pathogenic micro
organism and enzyme inactivation.
 In this method minimal changes are caused to
sensory characteristics or nutritive value.
11/27/2017 Y.BAVANEETHAN 2
• Sensible heat to raise liquid temperature
during pasteurisation:
• Q (W): specific rate of heat transfer,
• m (kg s-1): mass flow rate,
• c (kJ kg-1 ºC-1): specific heat capacity
• θA - θB (ºC): temperature change.
Theory
11/27/2017 Y.BAVANEETHAN 3
The extent of the heat treatment required to
stabilize the food.
– This is determined by the D value of the most heat-
resistant micro-organism
– For example milk pasteurisation - 12 logarithmic
cycle number (12D) reduction of C. burnetii
– liquid whole egg is treated to produce 9D reduction
in numbers of S. seftenberg.
Flavours, colours and vitamins of the
pasteurized food product also determined by D
values.
11/27/2017 Y.BAVANEETHAN 4
 High-temperature short-time (HTST) conditions
pasteurization method (71.8ºC for 15 s )is more
help to retention of nutritional and sensory quality.
– Example = Milk processing the lower-
temperature longer-time process operating at
63ºC for 30 min (Common process) causes
greater changes to flavour and loss of vitamins
than HTST processing at 71.8ºC for 15 s
 HTST method also called as Flash pasteurization.
 Direct estimation of pathogen numbers by
microbiological methods is expensive and time
consuming.
11/27/2017 Y.BAVANEETHAN 5
Different Methods of Pasteurization
Low-temperature hold method (LTH):
 conditions of 63oC for 30 min before cooled to
7oC
High-temperature short-time (HTST):
 conditions of 71.5oC for at least 15sec before
cooled to 10oC
Ultrahigh-temperature (UHT):
 138oC for at least 2 seconds
 extreme pasteurization
 kills all microorganisms
 keeping milk in a closed, sterile container at room
temperature
11/27/2017 Y.BAVANEETHAN 6
Estimation of Pathogenic Micro Organism in
Pasteurization
 Phosphatase activity test is simple test. Specially for
milk pasteurization.
– If phosphatase activity is found, it is assumed that
the heat treatment was inadequate to destroy the
pathogenic bacteria or
– Unpasteurized milk has contaminated the
pasteurized product.
 A similar test for the effectiveness of liquid-egg
pasteurization is based on residual -amylase activity.
11/27/2017 Y.BAVANEETHAN 7
Some examples of convention pasteurization treatments
Product Temperature Time Remark
Milk 62.8oC 30 min LTH
Milk 71.7oC 15 sec HTST
Milk 137.8oC 2 sec UHT
Ice-Cream 71.1oC 30 min LTH
Ice-Cream 82.2oC 16-20 sec HTST
Grape Wines* 82-85oC 1 min in bulk
Fruit Wines* 62.8oC depends bottled hot
Beer 60oC depends bottled hot
Dried fruits 65.6-85oC 30-90 min
Grape Juice* 76.7oC 30 min
Apple Juice* 85-87.8oC 30-60sec bottled in bulk
Carbonated Drinks* 65.6 30 min in common
Vinegar* 60-65.6 30 min in bulk
*depends on the acidity
11/27/2017 Y.BAVANEETHAN 8
11/27/2017 Y.BAVANEETHAN 9
11/27/2017 Y.BAVANEETHAN 10
11/27/2017 Y.BAVANEETHAN 11
Equipments
01. Pasteurization of Packaged Foods
 Some liquid foods are pasteurised after filling into
containers.
– Example => beers and fruit juices
 Hot water is normally used to packaged food.
 To reduce the risk of thermal shock of the container,
(fracture caused by rapid changes in temperature).
– Keep maximum temperature differences between the
container and water are 20ºC for heating and 10ºC for
cooling.
11/27/2017 Y.BAVANEETHAN 12
Packaged food …..
 Finally packaged food is cooled to approximately 40ºC
– to evaporate surface water that help to minimize external
corrosion to the container and
– to accelerate the label adhesives.
 Hot-water pasteurizers may be batch or continuous
operation.
 The batch equipment consists a water bath.
– packaged food are heated to a set temperature and held
this to required length of time.
– Cold water is pumped in to cool the product.
 The continuous version consists a long narrow
conveyor belt to carry containers through heating and
cooling sections.
11/27/2017 Y.BAVANEETHAN 13
Packaged Food - Tunnel pasteurizer
 Tunnel divided into a number of heating zones.
 Very fine hot water sprays are used to heat the container
– Packaged food pass through each zone of the
conveyer. ( 1st & 2nd per heater, pasteurizer)
– Incrementaly rises in temperature until pasteurization
is achieved.
 Cool water spray is used to cool the containers through
the tunnel.
 Temperatures in the heating zones are gradually
increased by reducing the amount of air in the steam–air
mixtures.
11/27/2017 Y.BAVANEETHAN 14
Tunnel pasteurizer
11/27/2017 Y.BAVANEETHAN 15
02. Pasteurization of Unpackaged Food
 Two main heat exchangers is commonly used for
unpackaged food pasteurization.
1. Plate heat exchangers
2. Tubular heat exchangers
 Large scale pasteurization of low viscosity liquids,
– milk, milk products, fruit juices, liquid egg, beers
and wines
– usually treated through Plate heat exchangers.
 Food is sprayed into a vacuum chamber and dissolved
air is removed by a vacuum pump, prior to
pasteurization.
11/27/2017 Y.BAVANEETHAN 16
01. Plate heat exchanger
11/27/2017 Y.BAVANEETHAN 17
Plate heat exchanger .....
 Food is pumped from a balance tank to a ‘regeneration’
section.
– where it is pre-heated by food that has already been
pasteurized.
 It is then heated to pasteurizing temperature in a
heating section.
– Hold until achieve the pasteurization temperature.
 If the pasteurizing temperature is not reached,
– flow diversion valve automatically returns the food to the
balance tank to be re-pasteurized.
.
11/27/2017 Y.BAVANEETHAN 18
Plate heat exchanger .....
 The pasteurized product is then cooled in the
regeneration section. And
– then further cooled by cold water.
– If necessary, chilled water also use in the cooling
section.
 The regeneration of heat in this way leads to
substantial savings in energy and up to 97% of the
heat can be recovered.
11/27/2017 Y.BAVANEETHAN 19
11/27/2017 Y.BAVANEETHAN 20
If the pasteurising temperature is not reached
– a flow diversion valve automatically returns food to
balance tank to be re-pasteurised
• θ1 (ºC): inlet temperature,
• θ2 (ºC): pre-heating temperature
• θ3 (ºC): pasteurisation temperature
11/27/2017 Y.BAVANEETHAN 21
Advantages of heat exchangers (HE)
Advantages of HEs over in-bottle processing:
– more uniform heat treatment
– simpler equipment & lower maintenance costs
– lower space & labour costs
– greater flexibility for different products
– greater control over pasteurization conditions.
11/27/2017 Y.BAVANEETHAN 22
Concentric tube HE
 For more viscous foods;
• dairy products, mayonnaise, tomato ketchup & baby
foods.
 Number of concentric stainless steel coils
• each made from double- or triple-walled tube.
 Food passes through the tube
• heating or cooling water is re-circulated through the tube
walls.
 Liquid food is passed from one coil to next for heating &
cooling
• heat is regenerated to reduce energy costs.
• Pasteurised food is immediately filled into bottles& sealed.
11/27/2017 Y.BAVANEETHAN 23
11/27/2017 Y.BAVANEETHAN 24
02. Shell and tubular or multi-tube heat
exchanger
 Important and so widely used in modern food
processing industries.
 Designed - various standards and codes,
– Standards of the Tubular Exchanger
Manufacturers Association (TEMA)
– American Society of Mechanical Engineers.
11/27/2017 Y.BAVANEETHAN 25
11/27/2017 Y.BAVANEETHAN 26
Shell and tube or multi-tube heat exchanger
11/27/2017 Y.BAVANEETHAN 27
Multi-tubular heat exchanger
 Liquid food product pass through the multi tube
chamber.
 Outer tube carrying heating liquid to opposite
direction of liquid food.
– Heating medium hot steam or hot water.
 This flow direction is called as “ counter flow”.
 Counter flow direction is more efficient method than
parallel flow method.
 Cooling with chilled water or brine ( counter flow)
11/27/2017 Y.BAVANEETHAN 28
 Multi-tubular heat exchanger is well efficient method
compare with single tubular heater.
– Heating surface area of food is high
– Complete and time efficiency pasteurization. (No
cold point effect)
– Retention of more sensory characters ( aroma,
flavour).
 To increase heat absorption efficient, the outer tubular
chamber insulate with heat resistant materials.(reduce
heat loss to environment)
 Tubular heat exchanger can be cleaned by through
methods (usually 1 % HNO3 and 1 % NaOH).
 Problem is deposits on the heating surfaces cannot be
seen and hardly removable by mechanical.
11/27/2017 Y.BAVANEETHAN 29
11/27/2017 Y.BAVANEETHAN 30
Effect on foods
 Pasteurization is,
– mild heat treatment
– minor changes to nutritional and sensorial
characteristics
 shelf life: few days or weeks
Effect: Colour, flavour and aroma
 Fruit juices
– Main problem is colour deterioration by enzymic
browning (poly phenol oxidase).
– This browning reaction promoted by the presence of
oxygen.
– In fruit juice industries, fruits are involve to de-
aerated prior to pasteurization process. There for
retain natural fruit colour.11/27/2017 Y.BAVANEETHAN 31
Whiteness of raw milk & pasteurised milk differs
– due to homogenisation
Pasteurization has no measurable effect on
– the colour of milk.
Pigments in plant & animal products are
mostly unaffected.
Small loss of volatile aroma compounds during
pasteurisation of juices.
Volatile recovery used to produce high quality
juices.
11/27/2017 Y.BAVANEETHAN 32
Effect: Vitamin loss
• In fruit juices,
– losses of vitamin C & carotene are minimized
• Changes to milk,
– 5% loss of serum proteins &
– small changes to vitamin content.
11/27/2017 Y.BAVANEETHAN 33
11/27/2017 Y.BAVANEETHAN 34
11/27/2017 Y.BAVANEETHAN 35
11/27/2017 Y.BAVANEETHAN 36

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Pasteurization

  • 1. Y.Bavaneethan. Lecturer Department of Food Technology SLGTI. SriLanka.11/27/2017 Y.BAVANEETHAN 1
  • 2. Pasteurization  Pasteurisation is a relatively mild heat treatment, in which food is heated to below 100ºC.  In low acid foods (pH>4.5, for example milk) it is used to minimize the hazards from pathogenic micro-organisms and to extend the shelf life of foods for severaldays.  In acidic foods (pH< 4.5, for example bottled fruit) it is used to extend the shelf life for several months by destruction of pathogenic micro organism and enzyme inactivation.  In this method minimal changes are caused to sensory characteristics or nutritive value. 11/27/2017 Y.BAVANEETHAN 2
  • 3. • Sensible heat to raise liquid temperature during pasteurisation: • Q (W): specific rate of heat transfer, • m (kg s-1): mass flow rate, • c (kJ kg-1 ºC-1): specific heat capacity • θA - θB (ºC): temperature change. Theory 11/27/2017 Y.BAVANEETHAN 3
  • 4. The extent of the heat treatment required to stabilize the food. – This is determined by the D value of the most heat- resistant micro-organism – For example milk pasteurisation - 12 logarithmic cycle number (12D) reduction of C. burnetii – liquid whole egg is treated to produce 9D reduction in numbers of S. seftenberg. Flavours, colours and vitamins of the pasteurized food product also determined by D values. 11/27/2017 Y.BAVANEETHAN 4
  • 5.  High-temperature short-time (HTST) conditions pasteurization method (71.8ºC for 15 s )is more help to retention of nutritional and sensory quality. – Example = Milk processing the lower- temperature longer-time process operating at 63ºC for 30 min (Common process) causes greater changes to flavour and loss of vitamins than HTST processing at 71.8ºC for 15 s  HTST method also called as Flash pasteurization.  Direct estimation of pathogen numbers by microbiological methods is expensive and time consuming. 11/27/2017 Y.BAVANEETHAN 5
  • 6. Different Methods of Pasteurization Low-temperature hold method (LTH):  conditions of 63oC for 30 min before cooled to 7oC High-temperature short-time (HTST):  conditions of 71.5oC for at least 15sec before cooled to 10oC Ultrahigh-temperature (UHT):  138oC for at least 2 seconds  extreme pasteurization  kills all microorganisms  keeping milk in a closed, sterile container at room temperature 11/27/2017 Y.BAVANEETHAN 6
  • 7. Estimation of Pathogenic Micro Organism in Pasteurization  Phosphatase activity test is simple test. Specially for milk pasteurization. – If phosphatase activity is found, it is assumed that the heat treatment was inadequate to destroy the pathogenic bacteria or – Unpasteurized milk has contaminated the pasteurized product.  A similar test for the effectiveness of liquid-egg pasteurization is based on residual -amylase activity. 11/27/2017 Y.BAVANEETHAN 7
  • 8. Some examples of convention pasteurization treatments Product Temperature Time Remark Milk 62.8oC 30 min LTH Milk 71.7oC 15 sec HTST Milk 137.8oC 2 sec UHT Ice-Cream 71.1oC 30 min LTH Ice-Cream 82.2oC 16-20 sec HTST Grape Wines* 82-85oC 1 min in bulk Fruit Wines* 62.8oC depends bottled hot Beer 60oC depends bottled hot Dried fruits 65.6-85oC 30-90 min Grape Juice* 76.7oC 30 min Apple Juice* 85-87.8oC 30-60sec bottled in bulk Carbonated Drinks* 65.6 30 min in common Vinegar* 60-65.6 30 min in bulk *depends on the acidity 11/27/2017 Y.BAVANEETHAN 8
  • 12. Equipments 01. Pasteurization of Packaged Foods  Some liquid foods are pasteurised after filling into containers. – Example => beers and fruit juices  Hot water is normally used to packaged food.  To reduce the risk of thermal shock of the container, (fracture caused by rapid changes in temperature). – Keep maximum temperature differences between the container and water are 20ºC for heating and 10ºC for cooling. 11/27/2017 Y.BAVANEETHAN 12
  • 13. Packaged food …..  Finally packaged food is cooled to approximately 40ºC – to evaporate surface water that help to minimize external corrosion to the container and – to accelerate the label adhesives.  Hot-water pasteurizers may be batch or continuous operation.  The batch equipment consists a water bath. – packaged food are heated to a set temperature and held this to required length of time. – Cold water is pumped in to cool the product.  The continuous version consists a long narrow conveyor belt to carry containers through heating and cooling sections. 11/27/2017 Y.BAVANEETHAN 13
  • 14. Packaged Food - Tunnel pasteurizer  Tunnel divided into a number of heating zones.  Very fine hot water sprays are used to heat the container – Packaged food pass through each zone of the conveyer. ( 1st & 2nd per heater, pasteurizer) – Incrementaly rises in temperature until pasteurization is achieved.  Cool water spray is used to cool the containers through the tunnel.  Temperatures in the heating zones are gradually increased by reducing the amount of air in the steam–air mixtures. 11/27/2017 Y.BAVANEETHAN 14
  • 16. 02. Pasteurization of Unpackaged Food  Two main heat exchangers is commonly used for unpackaged food pasteurization. 1. Plate heat exchangers 2. Tubular heat exchangers  Large scale pasteurization of low viscosity liquids, – milk, milk products, fruit juices, liquid egg, beers and wines – usually treated through Plate heat exchangers.  Food is sprayed into a vacuum chamber and dissolved air is removed by a vacuum pump, prior to pasteurization. 11/27/2017 Y.BAVANEETHAN 16
  • 17. 01. Plate heat exchanger 11/27/2017 Y.BAVANEETHAN 17
  • 18. Plate heat exchanger .....  Food is pumped from a balance tank to a ‘regeneration’ section. – where it is pre-heated by food that has already been pasteurized.  It is then heated to pasteurizing temperature in a heating section. – Hold until achieve the pasteurization temperature.  If the pasteurizing temperature is not reached, – flow diversion valve automatically returns the food to the balance tank to be re-pasteurized. . 11/27/2017 Y.BAVANEETHAN 18
  • 19. Plate heat exchanger .....  The pasteurized product is then cooled in the regeneration section. And – then further cooled by cold water. – If necessary, chilled water also use in the cooling section.  The regeneration of heat in this way leads to substantial savings in energy and up to 97% of the heat can be recovered. 11/27/2017 Y.BAVANEETHAN 19
  • 21. If the pasteurising temperature is not reached – a flow diversion valve automatically returns food to balance tank to be re-pasteurised • θ1 (ºC): inlet temperature, • θ2 (ºC): pre-heating temperature • θ3 (ºC): pasteurisation temperature 11/27/2017 Y.BAVANEETHAN 21
  • 22. Advantages of heat exchangers (HE) Advantages of HEs over in-bottle processing: – more uniform heat treatment – simpler equipment & lower maintenance costs – lower space & labour costs – greater flexibility for different products – greater control over pasteurization conditions. 11/27/2017 Y.BAVANEETHAN 22
  • 23. Concentric tube HE  For more viscous foods; • dairy products, mayonnaise, tomato ketchup & baby foods.  Number of concentric stainless steel coils • each made from double- or triple-walled tube.  Food passes through the tube • heating or cooling water is re-circulated through the tube walls.  Liquid food is passed from one coil to next for heating & cooling • heat is regenerated to reduce energy costs. • Pasteurised food is immediately filled into bottles& sealed. 11/27/2017 Y.BAVANEETHAN 23
  • 25. 02. Shell and tubular or multi-tube heat exchanger  Important and so widely used in modern food processing industries.  Designed - various standards and codes, – Standards of the Tubular Exchanger Manufacturers Association (TEMA) – American Society of Mechanical Engineers. 11/27/2017 Y.BAVANEETHAN 25
  • 27. Shell and tube or multi-tube heat exchanger 11/27/2017 Y.BAVANEETHAN 27
  • 28. Multi-tubular heat exchanger  Liquid food product pass through the multi tube chamber.  Outer tube carrying heating liquid to opposite direction of liquid food. – Heating medium hot steam or hot water.  This flow direction is called as “ counter flow”.  Counter flow direction is more efficient method than parallel flow method.  Cooling with chilled water or brine ( counter flow) 11/27/2017 Y.BAVANEETHAN 28
  • 29.  Multi-tubular heat exchanger is well efficient method compare with single tubular heater. – Heating surface area of food is high – Complete and time efficiency pasteurization. (No cold point effect) – Retention of more sensory characters ( aroma, flavour).  To increase heat absorption efficient, the outer tubular chamber insulate with heat resistant materials.(reduce heat loss to environment)  Tubular heat exchanger can be cleaned by through methods (usually 1 % HNO3 and 1 % NaOH).  Problem is deposits on the heating surfaces cannot be seen and hardly removable by mechanical. 11/27/2017 Y.BAVANEETHAN 29
  • 31. Effect on foods  Pasteurization is, – mild heat treatment – minor changes to nutritional and sensorial characteristics  shelf life: few days or weeks Effect: Colour, flavour and aroma  Fruit juices – Main problem is colour deterioration by enzymic browning (poly phenol oxidase). – This browning reaction promoted by the presence of oxygen. – In fruit juice industries, fruits are involve to de- aerated prior to pasteurization process. There for retain natural fruit colour.11/27/2017 Y.BAVANEETHAN 31
  • 32. Whiteness of raw milk & pasteurised milk differs – due to homogenisation Pasteurization has no measurable effect on – the colour of milk. Pigments in plant & animal products are mostly unaffected. Small loss of volatile aroma compounds during pasteurisation of juices. Volatile recovery used to produce high quality juices. 11/27/2017 Y.BAVANEETHAN 32
  • 33. Effect: Vitamin loss • In fruit juices, – losses of vitamin C & carotene are minimized • Changes to milk, – 5% loss of serum proteins & – small changes to vitamin content. 11/27/2017 Y.BAVANEETHAN 33