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PRESENTED BY-
MOHIT RAM
CHEMICAL ENGINEERING
ROLL NO. 213
 Lubricating oils are used to reduce friction and wear , remove
heat generated by friction and prevents corrosion .
 Lubricating oils of various grades are manufactured by
mixing of selected lubricating oil and additives.
 Lubricating oil are produced from heavy waxy distillate
fractions obtained from vacuum distillation of atmospheric
residue.
 The straight run vacuum distillate fractions require further
treatment to bring them to the desired specification of
lubricating oil.
 The treatment involved depends on the properties such as
viscosity, conrandson carbon residue(CCR), viscosity index,
pour point and colour.
 High Vacuum Distillation Unit : To obtain various disstilate
fractions and vacuum residue.
 Solvent Deasphalting Unit : To remove asphalt from vacuum
residue.
 Solvent Extraction Unit : To remove undesirable napthenic
and aromatic hydrocarbons from the distillate fractions so as
to improve the viscosity index of lube oil base stocks.
 Solving Dewaxing Unit : To remove wax content of the soil so
as to improve the pour point of the lube oil.
 Hydrofinishing Unit : To improve colour , oxidation and
colour stability of finished lube oil.
 Kalol crude has little potential for high viscosity lube oil
because of low viscosity and high wax content .
 Since viscosity index of distillates from Naharkatia crude is
low , it is no not suitable for high viscosity index lube oils.
 Among three crudes NR crude oil has better potential for lube
oils .
 In vacuum distillation of long residue, feed is split into
various heavy waxy distillate fractions like spindle oil, light
oil, intermediate oil, heavy oil cuts and short residue.
 Fractionation of long residue is accomplished by distillation
under an appropriately high vacuum to prevent
decomposition of very high boiling components.
 Particular attention is paid to washing areas in the vacuum
column, in order to prevent any mechanical entrainment of
liquid.
 The reduced crude oil from the atmospheric column is further
heated and vaporized in the fired heater and charged to a
vacuum column.
 Typical flash temperature will be 390-400°C at 120 mm Hg
(absolute pressure).
 The required vacuum is maintained by a multistage steam
ejector system.
 Partial pressure of hydrocarbons in the vacuum column is
effectively reduced by the injection of steam at the bottom of
the column.
 The distillate fractions are steam stripped in strippers to
control the flash points. These fractions are then sent for
further processing.
Flash zone temperature,°C 385
Pressure (absolute), mm Hg,
(a)Top 23
(b)Flash zone 100
Fraction Yield, wt.% Kinematic viscosity at
98.9°C
Gas oil 5.0 1.55
Spindle oil 11.0 3.57
Light oil 18.5 4.15
Intermediate oil 12.0 11.1
Heavy oil 8.5 23.1
Short residue 45.0 1140.0
Lubricating Oils Production Process

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Lubricating Oils Production Process

  • 1. PRESENTED BY- MOHIT RAM CHEMICAL ENGINEERING ROLL NO. 213
  • 2.  Lubricating oils are used to reduce friction and wear , remove heat generated by friction and prevents corrosion .  Lubricating oils of various grades are manufactured by mixing of selected lubricating oil and additives.  Lubricating oil are produced from heavy waxy distillate fractions obtained from vacuum distillation of atmospheric residue.  The straight run vacuum distillate fractions require further treatment to bring them to the desired specification of lubricating oil.  The treatment involved depends on the properties such as viscosity, conrandson carbon residue(CCR), viscosity index, pour point and colour.
  • 3.  High Vacuum Distillation Unit : To obtain various disstilate fractions and vacuum residue.  Solvent Deasphalting Unit : To remove asphalt from vacuum residue.  Solvent Extraction Unit : To remove undesirable napthenic and aromatic hydrocarbons from the distillate fractions so as to improve the viscosity index of lube oil base stocks.  Solving Dewaxing Unit : To remove wax content of the soil so as to improve the pour point of the lube oil.  Hydrofinishing Unit : To improve colour , oxidation and colour stability of finished lube oil.
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  • 6.  Kalol crude has little potential for high viscosity lube oil because of low viscosity and high wax content .  Since viscosity index of distillates from Naharkatia crude is low , it is no not suitable for high viscosity index lube oils.  Among three crudes NR crude oil has better potential for lube oils .
  • 7.  In vacuum distillation of long residue, feed is split into various heavy waxy distillate fractions like spindle oil, light oil, intermediate oil, heavy oil cuts and short residue.  Fractionation of long residue is accomplished by distillation under an appropriately high vacuum to prevent decomposition of very high boiling components.  Particular attention is paid to washing areas in the vacuum column, in order to prevent any mechanical entrainment of liquid.
  • 8.  The reduced crude oil from the atmospheric column is further heated and vaporized in the fired heater and charged to a vacuum column.  Typical flash temperature will be 390-400°C at 120 mm Hg (absolute pressure).  The required vacuum is maintained by a multistage steam ejector system.  Partial pressure of hydrocarbons in the vacuum column is effectively reduced by the injection of steam at the bottom of the column.  The distillate fractions are steam stripped in strippers to control the flash points. These fractions are then sent for further processing.
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  • 10. Flash zone temperature,°C 385 Pressure (absolute), mm Hg, (a)Top 23 (b)Flash zone 100
  • 11. Fraction Yield, wt.% Kinematic viscosity at 98.9°C Gas oil 5.0 1.55 Spindle oil 11.0 3.57 Light oil 18.5 4.15 Intermediate oil 12.0 11.1 Heavy oil 8.5 23.1 Short residue 45.0 1140.0