Fluid Solutions
Your partner in planning and manufacturing
    latest state of the art grease plants




             www.fluid-solutions.de          -2-
LUBRICATING GREASE - DEFINITION




LUBRICATING GREASE *) IS A SOLID TO SEMI-FLUID PRODUCT
   OF DISPERSION OF A THICKENING AGENT IN A LIQUID
  LUBRICANT … OTHER INGREDIENTS IMPARTING SPECIAL
            PROPERTIES MAY BE PRESENT




*) A.S.T.M. STANDARD DEFINITION OF TERMS OF PETROLEUM, 1959



                      www.fluid-solutions.de                  3
LUBRICATING GREASE
General composition:



      Base Oil           +        Thickener            +        Additives                 =          Grease
Conventional Oil             Metallic Soaps (-salts)       Surface active                     Grade of goods
- Raffinate                  - Lithium soap                - High pressure/abrasive           - Multi purpose grease
                             - Calcium soap                  protection                       - High temperature grease
Unconventional Oil           - Sodium soap                 - Corrosion-/rust protection       - Lubricating grease
- Hydrocrack Oil             - Aluminum soap               - Solids                           - Semi-fluid grease
  (HC synthesis)             - Lead soap                                                      - Gel grease
- Synthetical Volatile       - Barium soap                 Grease protective                  - Polyurea grease
  Organic Compounds                                        - Age protection                   - Bentonite grease
  (VOC)                      Other thickeners
- Synthetical Esters         - Gels                                                           Performance classes
                             - Polyurethane                                                   - Acc. to automotive
Herbal Oil                   - Bentonite                                                         regulations
- Rape seed oil
                                                                                              Identification
                                                                                              - Acc. DIN 51502

                                                                                              Consistency classes
                                                                                              - Acc. NLGI code




                                           www.fluid-solutions.de                                                    4
LUBRICATING GREASE
Classification acc. to NLGI classes:

                      classification                                               applications




                                                                                                                      Roller bearing
                                                                                                        Water pumps
                                                                                        Slide bearing
                                                      Block grease
                                   penetration
                    NLGI-class




                                                                     lubricating
                                   (mm/10




                                                                     Gear
                                   full-
               000               445 – 475                             
               00                400 – 430                             
               0                 355 – 385                             
               1                 310 – 340                                                                          
               2                 265 – 295                                                                           
               3                 220 – 250                                                                           
               4                 175 – 205                                                                           
               5                 130 – 160                                                              
               6                 85 – 115             


                                                 www.fluid-solutions.de                                                                5
LUBRICATING GREASE
Classification acc. DIN 51502:
  K PF 2 K - 30
                  Lower operating temperature (°C)
                  Upper operating temperature, behavior in contact with water3

                  NLGI-class

                  Additional letter(s) for base oil type and additive2
                  Lubricating grease for1

  1)Lubricating grease for                  3)                           Behavior
                                                     Upper temperature                        Test temperature
                                                                         with water
  G    Closed gears (DIN 51826)
                                                 C         60°C           0 oder 1                    40°C
  OG Open gears
                                                 D                        2 oder 3
  K    Ball bearing
  M    Slide bearing and gaskets                 E         80°C           0 oder 1                    40°C

                                                 F                        2 oder 3

  2)                                             G        100°C           0 oder 1                    90°C
    Additional
                                                 H                        2 oder 3
  G    Closed gears (DIN 51826)
  OG Open gears                                  K        120°C           0 oder 1                    90°C

  K    Ball bearing                              M                        2 oder 3

  M    Slide bearing                             N        140°C

  P    Additives                                 P        160°C

  F    Solids (e.g. MoS2)                        R        180°C
                                                                                     By arrangement
                                                 S        200°C                                                  0 = no modification
                                                                                                                 1 = slight modification
                                                 T        220°C
                                                                                                                 2 = moderate modification
                                                 U        > 220°C                                                3 = strong modification


                                            www.fluid-solutions.de                                                                           6
LUBRICATING GREASE
Applications:
      Industrial Lubricating Grease
      - Roller- and bush bearing lubrication
      - Central lube system
      - Strand casting systems, breaker and mill lubrication
                                                                                      Roller Bearings
      Special- and Biodegradable Greases
      - Lubrication of high performance precision bearing
      - High speed bearings (railway wheels)

      Industrial Semi-Fluid Grease
      - Highly stressed roller bearings e.g. cylinder- and taper roller bearing
      - Gear motor, drives, couplings, chain drive systems
      - Gear semi-fluid grease

      Drill Rods Grease                                                                Wheel Bearing
      - Thread grease

      Automotive Lubricating Grease
      - Wheel bearing, ball joints, roller bearing
      - Bush and antifriction bearing
      - Steering linkage, wheel suspension

      Automotive Semi-Fluid Grease
      - Chassis lubrication
      - Central lubricating systems
                                                                                  Drill Rod Lubrication

                                         www.fluid-solutions.de                                      7
Grease Manufacturing Process
Calculation of typical plant size
Required capacity:                               2.000 to per year
Working time:                                    250 days per year
                                                8 to per day in total (1 shift, with 8 hrs batchtime)*

With 2 Finishing vessels:        8 to per day in total
                                              4 to per day (Batch) each
                                              4,5 m³ per day in total (1 shift)
                                              5 m³ working capacity of each finishing vessel*

Process vessel:                                 half size of finishing kettle
                                                3 m³ working capacity
                                                2,7 to per Batch with batchtime 8 h (1 shift)*



            Key Equipment for grease plants
            Total required capacity            Working capacity          Working capacity
            of grease                          Process kettle*           Finishing kettle*
            2.000 to/year                              3 m³                      2 x 5 m³

            4.000 to/year                              6 m³                      2 x 10 m³

            8.000 to/year                             2 x 6 m³                   4 x 10 m³
            *depending on grease formulation




                                                   www.fluid-solutions.de                                 8
Grease Manufacturing Process
                                      Sketch
                                      Manufacturing Process




             www.fluid-solutions.de                           9
Grease Manufacturing Process
Process Flow Diagram




                       www.fluid-solutions.de   10
Grease Manufacturing Process
Key Equipment – Mixing Equipment

                                    • Grease kettles are heated with hot oil to
                                      as much as 250°C or more
                                    • Kettle capacities generally range up to 10
                                      tons
                                    • Kettles could be pressured up to 6bar as
                                      option if required
                                    • Kettles could have counter rotating
                                      paddles which force the grease in
                                      opposite directions to improve mixing
                                      efficiency and temperature
                                      transportation
                                    • Kettles also have a homogenization unit
                                      to provide additional (vertical) mixing &
                                      homogenization action and to transport
                                      the grease to other processing
                                      equipment such as a colloid mill.

                         www.fluid-solutions.de                             11
Grease Manufacturing Process
Key Equipment – Homogenization/Filtration/Dearation




    P&i diagram HFD unit




                           HFD unit


                             www.fluid-solutions.de   12
Grease Manufacturing Process
Key Equipment – Homogenization/Filtration/Dearation
                                                                Mixing/Scraper
                                                                Equipment




Tank farm




            CIP elements                     Cooking vessel during assembly
                           www.fluid-solutions.de                                13
Grease Manufacturing Process
Layout




   Grease production unit
   as skid-mounted unit


                            www.fluid-solutions.de   14
Grease Manufacturing Process
Layout




     Vertical grease production unit

                           www.fluid-solutions.de   15
Grease Manufacturing Process
Automation System




 Control the interactions between thickener and
 lubricant (Base Oil + Additive) together with the
 manufacturing process by process automation

                             www.fluid-solutions.de   16
Grease Manufacturing Process
Automation System




   Overview
                    Tank farm
                                             Cooking kettle




                    www.fluid-solutions.de                    17
Our expertise in Grease Production




   • High quality Engineering for the
     complete grease plant
   • Definition of working and delivery
     packages in the project
   • Available for a wide range of grease
     production applications
   • Pressurized processes possible
   • Available in a wide range of
     production sizes from pilot plants up
     to commercial plants


                        www.fluid-solutions.de   18

Presentation grease 2012

  • 2.
    Fluid Solutions Your partnerin planning and manufacturing latest state of the art grease plants www.fluid-solutions.de -2-
  • 3.
    LUBRICATING GREASE -DEFINITION LUBRICATING GREASE *) IS A SOLID TO SEMI-FLUID PRODUCT OF DISPERSION OF A THICKENING AGENT IN A LIQUID LUBRICANT … OTHER INGREDIENTS IMPARTING SPECIAL PROPERTIES MAY BE PRESENT *) A.S.T.M. STANDARD DEFINITION OF TERMS OF PETROLEUM, 1959 www.fluid-solutions.de 3
  • 4.
    LUBRICATING GREASE General composition: Base Oil + Thickener + Additives = Grease Conventional Oil Metallic Soaps (-salts) Surface active Grade of goods - Raffinate - Lithium soap - High pressure/abrasive - Multi purpose grease - Calcium soap protection - High temperature grease Unconventional Oil - Sodium soap - Corrosion-/rust protection - Lubricating grease - Hydrocrack Oil - Aluminum soap - Solids - Semi-fluid grease (HC synthesis) - Lead soap - Gel grease - Synthetical Volatile - Barium soap Grease protective - Polyurea grease Organic Compounds - Age protection - Bentonite grease (VOC) Other thickeners - Synthetical Esters - Gels Performance classes - Polyurethane - Acc. to automotive Herbal Oil - Bentonite regulations - Rape seed oil Identification - Acc. DIN 51502 Consistency classes - Acc. NLGI code www.fluid-solutions.de 4
  • 5.
    LUBRICATING GREASE Classification acc.to NLGI classes: classification applications Roller bearing Water pumps Slide bearing Block grease penetration NLGI-class lubricating (mm/10 Gear full- 000 445 – 475  00 400 – 430  0 355 – 385  1 310 – 340    2 265 – 295   3 220 – 250   4 175 – 205   5 130 – 160  6 85 – 115  www.fluid-solutions.de 5
  • 6.
    LUBRICATING GREASE Classification acc.DIN 51502: K PF 2 K - 30 Lower operating temperature (°C) Upper operating temperature, behavior in contact with water3 NLGI-class Additional letter(s) for base oil type and additive2 Lubricating grease for1 1)Lubricating grease for 3) Behavior Upper temperature Test temperature with water G Closed gears (DIN 51826) C 60°C 0 oder 1 40°C OG Open gears D 2 oder 3 K Ball bearing M Slide bearing and gaskets E 80°C 0 oder 1 40°C F 2 oder 3 2) G 100°C 0 oder 1 90°C Additional H 2 oder 3 G Closed gears (DIN 51826) OG Open gears K 120°C 0 oder 1 90°C K Ball bearing M 2 oder 3 M Slide bearing N 140°C P Additives P 160°C F Solids (e.g. MoS2) R 180°C By arrangement S 200°C 0 = no modification 1 = slight modification T 220°C 2 = moderate modification U > 220°C 3 = strong modification www.fluid-solutions.de 6
  • 7.
    LUBRICATING GREASE Applications: Industrial Lubricating Grease - Roller- and bush bearing lubrication - Central lube system - Strand casting systems, breaker and mill lubrication Roller Bearings Special- and Biodegradable Greases - Lubrication of high performance precision bearing - High speed bearings (railway wheels) Industrial Semi-Fluid Grease - Highly stressed roller bearings e.g. cylinder- and taper roller bearing - Gear motor, drives, couplings, chain drive systems - Gear semi-fluid grease Drill Rods Grease Wheel Bearing - Thread grease Automotive Lubricating Grease - Wheel bearing, ball joints, roller bearing - Bush and antifriction bearing - Steering linkage, wheel suspension Automotive Semi-Fluid Grease - Chassis lubrication - Central lubricating systems Drill Rod Lubrication www.fluid-solutions.de 7
  • 8.
    Grease Manufacturing Process Calculationof typical plant size Required capacity: 2.000 to per year Working time: 250 days per year  8 to per day in total (1 shift, with 8 hrs batchtime)* With 2 Finishing vessels: 8 to per day in total  4 to per day (Batch) each  4,5 m³ per day in total (1 shift)  5 m³ working capacity of each finishing vessel* Process vessel:  half size of finishing kettle  3 m³ working capacity  2,7 to per Batch with batchtime 8 h (1 shift)* Key Equipment for grease plants Total required capacity Working capacity Working capacity of grease Process kettle* Finishing kettle* 2.000 to/year 3 m³ 2 x 5 m³ 4.000 to/year 6 m³ 2 x 10 m³ 8.000 to/year 2 x 6 m³ 4 x 10 m³ *depending on grease formulation www.fluid-solutions.de 8
  • 9.
    Grease Manufacturing Process Sketch Manufacturing Process www.fluid-solutions.de 9
  • 10.
    Grease Manufacturing Process ProcessFlow Diagram www.fluid-solutions.de 10
  • 11.
    Grease Manufacturing Process KeyEquipment – Mixing Equipment • Grease kettles are heated with hot oil to as much as 250°C or more • Kettle capacities generally range up to 10 tons • Kettles could be pressured up to 6bar as option if required • Kettles could have counter rotating paddles which force the grease in opposite directions to improve mixing efficiency and temperature transportation • Kettles also have a homogenization unit to provide additional (vertical) mixing & homogenization action and to transport the grease to other processing equipment such as a colloid mill. www.fluid-solutions.de 11
  • 12.
    Grease Manufacturing Process KeyEquipment – Homogenization/Filtration/Dearation P&i diagram HFD unit HFD unit www.fluid-solutions.de 12
  • 13.
    Grease Manufacturing Process KeyEquipment – Homogenization/Filtration/Dearation Mixing/Scraper Equipment Tank farm CIP elements Cooking vessel during assembly www.fluid-solutions.de 13
  • 14.
    Grease Manufacturing Process Layout Grease production unit as skid-mounted unit www.fluid-solutions.de 14
  • 15.
    Grease Manufacturing Process Layout Vertical grease production unit www.fluid-solutions.de 15
  • 16.
    Grease Manufacturing Process AutomationSystem Control the interactions between thickener and lubricant (Base Oil + Additive) together with the manufacturing process by process automation www.fluid-solutions.de 16
  • 17.
    Grease Manufacturing Process AutomationSystem Overview Tank farm Cooking kettle www.fluid-solutions.de 17
  • 18.
    Our expertise inGrease Production • High quality Engineering for the complete grease plant • Definition of working and delivery packages in the project • Available for a wide range of grease production applications • Pressurized processes possible • Available in a wide range of production sizes from pilot plants up to commercial plants www.fluid-solutions.de 18