This document describes the identification of various textile fibers through burn, microscopic, and solubility tests. It provides details on the properties of cotton, silk, wool, linen, polyester, nylon, rayon, and acetate fibers when subjected to these standard tests. Key identifying features include how each fiber burns and any beads, ash, or odor produced; its appearance under a microscope; and whether it dissolves in various solvents like acetone or acids. The tests allow differentiation between natural fibers like cotton and silk from synthetic or manufactured fibers.
3. Burn Test.
Is a cellulose fiber. It burns and may flare up when lit.
No melted bead is left by it. After burning, it
continues to glow. It gives out smell like that of a
burning paper. The smoke is gray or white. The ash is
fine, soft that can be easily crumbled.
4. Microscopic Test
The cotton fiber is a single elongated cell. Under a
microscope, it looks like flat, spirally twisted ribbon
like tube with rough granular surface.
However, mercerized cotton doesn't have natural
twist. The finishing process makes them swollen,
straight, smooth and round with a shining surface.
7. Burn Test
A protein fiber which burns slowly and curls away from
the flame. It leaves dark bead which can be easily
crushed. It is self-extinguishing and leaves ash that is
dark, gritty, fine powder. It smells like burned hair or
charred meat. It gives out a little or no smoke and the
fume has no hazard.
8. Microscopic Test
Raw silk fiber, composed of two filaments, has elliptical
shape under the microscope. The two fine and lustrous
filaments are shown clearly looking like transparent
rods with triangular shape. Wild silk or tussah fiber has
different appearance than the cultivated silk. It is
flattened, coarse, thick and broader fiber having fine,
wavy lines all across its surface whereas cultivated silk
is narrower fiber with no marks on it.
11. Burn Test
Is a protein fiber which burns slowly. It sizzles and curls
away from flame and may curl back onto fingernail. It
leaves beads that are brittle, dark, and easily crushed.
It is self-extinguishing and leaves harsh ash from
crushed bead. It gives out a strong odor of burning hair
or feathers. It gives out dark smoke and moderate
fume.
12. Microscopic Test
Wool fiber has irregular, roughly cylindrical, multi
cellular structure with tapered ends. Under a
microscope, three basic layers are shown- epidermis
(outer layer), cortex (middle layer) and medulla (inner
layer). Medulla is seen only in coarse and medium wool
fibers and that too under a highly powerful microscope.
15. Burn Test
A cellulose fiber, it takes longer to ignite. It is easily
extinguished by blowing on it. Burns quickly with bright
flame. It leaves no melted bead and after burning no
sign of flame is seen but it does not melts. It smells like
burning leaves or wood. The ash is gray and smoke has
no fume hazard.
16. Microscopic Test
Linen fiber, under a microscope, looks like having
multiple sided cylindrical filaments with fine pointed
edges. The filaments show nodes at intervals. It, in fact,
looks like a bamboo stick having joints that results into
a little unevenness.
19. Burn Test
It burns quickly and shrinks away from flame, may also
flare up. It leaves hard, dark, and round beads. After
the flame, it burns slowly and is not always self-
extinguishing. It has a slightly sweet chemical odor. It
leaves no ash but its black smoke and fume are
hazardous.
20. Microscopic Test
Generally, polyester fiber is smooth, straight. It looks
round cross sectionally. However, with various finishing
processes, its appearance changes in context of texture
and luster.
23. Burn Test
Due to their fabric finish, they quickly burn and shrink
to flame. The beads are hard, grayish and uncrushable.
After flame, they burn slowly and melt. They are self-
extinguishing but drip dangerously. Their odor is like
celery and they leave no ash but the fume is very
hazardous.
24. Microscopic Test
There are many variants of nylon fiber. However,
generally it appears fine, round, smooth and
translucent. Sometimes it has shiny appearance. If it
looks dull, it will also be dotted under the microscope.
27. Burn Test
It burns without flame or melting and may flare up.
Unless there is a fabric finish, it doesn't leave any bead.
After the flame is removed, it may glow a bit longer
than cotton. It smells like burning paper and leaves
soft, gray ash. It's smoke is a little hazardous.
28. Microscopic Test
Rayon fiber has uniform diameter with glass like
shine. If delustered then rayon fiber shows
marks similar to pepper, when viewed cross
sectionally. Viscose fiber of rayon looks irregular
when viewed cross sectionally.
31. Burn Test
Is a protein fiber which burns quickly and can flare even
after flame is removed. The bead is hard, brittle, and
can't be crushed. It melts into very hot bead and drips
very dangerously. No ash is left by it and the smell is
like hot vinegar or burning pepper. It gives out black
smoke and the fume is hazardous.
32. Microscopic Test
Acetate fiber looks lesser irregular than viscose rayon
when viewed cross sectionally. It has indentations that
look like occasional marks when viewed longitudinally.