This document outlines the standard procedure for validating new analytical test methods according to ASTM International (ASTM). The validation process involves 5 phases: design, development, validation, evaluation, and conclusion. During the validation phase, studies are conducted to establish selectivity, calibration, repeatability, bias, and ruggedness. An inter-laboratory study with multiple matrices is also required before a new method can be approved. The document provides an example validation study conducted for a new ASTM nitrate-nitrite test method according to these procedures.