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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 08 | Aug 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1309
Material characterization on Functionally Graded Al-Cu alloy
Fabricated using Centrifugal Technique
Manoj RM1 , Karthik S2 , Madhusudhan3
1,2BE student, Mechanical department, NMIT Bangalore
3 Professor, Mechanical department, NMIT Bangalore
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - Aluminum 2014 (Al-Cu) is one among the
strongest aluminum alloy and it is the functionally graded
material which has its application in the field of Aerospace
and Automotive Industries. An intensive study of this Cast
Aluminum family has been found in many literatures for
increasing the mechanical properties and grain refinement
of the aluminum alloys. The main objective of this work is to
study the properties of Al 2014 produced by Horizontal
Centrifugal Casting process at different rotating speeds
(400rpm 600rpm and 800rpm) wit fixed pouring
temperature (650°C). The mechanical properties such as
tensile strength and hardness were studied using Electronic
Tensometer and Brinell Hardness Tester. It was observed
that the tensile strength and hardness are increased with
the increase in rotary speed of the mold. Also, the
microstructure of the sample had very fine grain refinement
enhancing good property at higher Rotational speeds of the
mold.
Key Words: Al-Cu alloy, Tensile strength, Grain size,
Microstructure, Hardness.
1. INTRODUCTION
Functionally Graded Materials (FGMs) are the class of
engineering materials characterized by their spatial
variation of composition and microstructure aiming at
controlling corresponding functional properties (i.e.
mechanical, thermal, electrical, etc.). This material exhibits
steady progress in the microstructure as well as the
composition in a definite way, the presence of FGMs,
which prompts variety in useful execution inside the part
through micro structural control. [2] In castings
inhomogeneous distribution in composition, is a typical
defect although microsegregation usually between 10 and
100 μm can be minimized/eliminated by heat treatments
but macrosegregation (cm to m) is essentially unaffected
and this may influence the effects of heat treatment, result
in property variations and damage the quality of the final
product. [1]
Centrifugal casting is one of the promising processes
taking major role in the production of functionally graded
material. It is a process of producing hollow castings by
causing molten metal to solidify in rotating mould. The
operations include in centrifugal casting are rotation of
mold at a known speed, pouring the molten metal and
extraction of the casting from the mold. The solidification
is quite rapid and hence good metallurgical quality is
achieved as solidification starts from the inner surface of
the mold corresponding to casting outer surface, so low
melting point impurities are carried by the solidification
front to the casting inner surface and gas porosity is also
forced at the casting inner surface because of its low
density and also fine grain structures are formed.[5] On
Centrifugal casting the first melt that reaches the wall
surface of the mold will backing the income fresh metal
and hence forms nucleation sites hence promoted for fast
solidification fine grains[6]
The centrifugal process eliminates the mid wall effects
because the inner surface will completely be in the liquid
state during the solidification process which results in a
continuous feed of metal in the areas of contraction,
thereby ensuring the absence of trapped porosity.
2. EXPERIMENTAL PROCEDURE:
2.1 Material Selection: The increase in the demand for
the aluminum and its alloys in Aerospace and Automobile
industrial applications due to its favorable properties such
as high specific toughness, good strength, good
machinability and good wear properties. In this alloys
aluminum is the base and other materials such as Si, Mg,
Cu, Mn, Fe, Zn are the alloying elements. In this study Al
2014 (Al-Cu) has been taken because of its popularity
which is remarked as the strongest alloying elements.
Elemen
ts
C
r
C
u
F
e
M
g
M
n
Si Ti Zn Al
Percent
age
0.
1
5 0.
7
0.
8
1.
2
0.
5
0.1
5
0.2
5
Remain
ing
Chart-2.1 The chemical composition of Al 2014 (Al-Cu)
2.2 Methodology: The hollow cylindrical casting of outer
diameter 72mm and length 84mm with wall thickness of
8mm were produced by using Horizontal centrifugal
casting process which is shown in the fig . As mold
rotational speed is one of the process parameter which
influences the rate of solidification. The centrifugal casting
were produced at their rotational speed of the mold such
has 400rpm, 600rpm and 800rpm.The pouring
temperature is kept constant as 650°C, Due to the
centrifugal force which is acting away from the central axis
the denser metals in the alloy will be towards the wall of
the mold and lesser denser metals towards the central axis
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 08 | Aug 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1310
thus influencing the property of the metal. The casting
specimens are cut to prepare the specimen to conduct
various tests like Brinell Hardness Test, tensile test are
performed.
Fig-2.1 Experimental setup of horizontal centrifugal
casting
Fig-2.2 Mold formed after centrifugal casting
3. RESULTS AND DISCUSSION:
3.1 Microstructural Analysis: The figure shows the
microstructure obtained from the castings Produced at
different Rotational speeds of the mold.
Inner Middle Outer
Fig-3.1a Microstructure of Al-Cu Specimen-1 (650°C
temperature at 400rpm speed)
Inner Middle Outer
Fig-3.1b Microstructure of Al-Cu Specimen-2 (650°C
temperature at 600rpm speed)
Inner Middle Outer
Fig-3.1c Microstructure of Al-Cu Specimen-3 (650°C
temperature at 800rpm speed)
3.2 Hardness test:
The graph shows the variation of hardness along the radial
direction among three specimens which was
experimented at different rotary speeds.
Chart-3.2 Variation of Brinell Hardnesss number from
inner to outer region
It shows similar variation in rate of solidification of the
casting along the radial direction. The cast shows higher
hardness number at the outer and inner region due to the
rapid solidification of the casts. The outer surface is harder
due to the chilling effect where the molten metal is
contacted to the mold surface. The lower hardness
number at the middle region indicates that the metal takes
more time to solidify compared to inner and outer radius.
spru
e Rotating
mold
Motor
Dial
Indicator
Speed
Indicator
0
10
20
30
40
50
Inner Middle Outer
400rpm
600rpm
800rpm
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 08 | Aug 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1311
3.3 Tensile test:
The pictures show the tensile specimen before and after
fracture
Fig-3.3 Tensile specimen before and after breaking
Chart-3.3 Variation of Break Load at different speeds
The tensile test specimen of the Indian standards was
tested using Electronic Tensometer with the uniform load
applied to the specimen to undergo fracture; The Fig.
shows the tensile strength of centrifugally cast specimen
at three different rotational speeds of the mold. It shows
higher tensile strength for casting produced at the higher
rotational speed compared to the casting produced at
lower rotational speed.
4. CONCLUSIONS:
The main Conclusions of this work are:
 The Centrifugal casting is one of the methods to
produce functionally graded materials with
variation in hardness along the radial direction in
the casting.
 At higher rotational speeds of the mold fine grains
will be formed with improved mechanical
properties and at lower rotational speeds coarse
grains will be formed with lower mechanical
properties.
 The results show the variation in hardness along
the radial direction with slightly higher hardness
values at inner and outer radii.
 The tensile strength is also observed higher for
the casting produced at the 800rpm compared to
that of 400rpm.
5. REFERENCE:
[1] Yisen Hu1, Gang Wang, Qing Jiang, Wenfeng Xiao,
Yiming Rong, “Precipitation strengthening behaviour of
Al-Cu-Mn alloys with the effect of casting segregation”
Contributed Papers from Materials Science and
Technology 2017 (MS&T17)
[2] Mallikarjun, Sukruth M, Chethan KS and Dr. Kiran
Aithal, “Study of Functionally Graded Al-Si Alloy
Fabricated by Centrifuge Casting Technique” International
Journal of Advances in Scientific Research and Engineering
(ijasre)
[3] Sani A Salihu, Aliyu Isah, Polycarp Evarastics,
“Influence of Magnesium Addition on Mechanical
Properties and Microstructure of Al-Cu-Mg Alloy” IOSR
Journal of Pharmacy and Biological Sciences (IOSR-JPBS)
ISSN: 2278-3008. Volume 4, Issue 5 (Nov. – Dec. 2012), PP
15-20
[4] Maria Eduarda Farinaa*, Pedro Bella, Carlos Raimundo
Frick Ferreirab, Berenice Anina Dedavida, “Effects of
Solidification Rate in the Microstructure of Al-Si5Cu3
Aluminum Cast Alloy” Materials Research. 2017; 20(Suppl.
2): 273-278
[5] Madhusudhan, Narendranath S, G C Mohan Kumar,
“Experimental Study on Cooling Rate of Centrifugal
Casting Based on Grain Size” International Journal of
Scientific & Engineering Research, Volume 3, Issue 1,
January-2012 1 ISSN 2229-5518
[6] S. R. CHANG, J. M. KIM and C. P. HONG, “Numerical
Simulation of Microstructure Evolution of Al Alloys in
Centrifugal Casting” ISIJ International, Vol. 41 (2001), No.
7, pp. 738–747
1950
2000
2050
2100
2150
2200
750 rpm 850 rpm 950 rpm
Break Load (N)
Break Load (N)

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IRJET- Material Characterization on Functionally Graded AL-CU Alloy Fabricated using Centrifugal Technique

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 08 | Aug 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1309 Material characterization on Functionally Graded Al-Cu alloy Fabricated using Centrifugal Technique Manoj RM1 , Karthik S2 , Madhusudhan3 1,2BE student, Mechanical department, NMIT Bangalore 3 Professor, Mechanical department, NMIT Bangalore ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - Aluminum 2014 (Al-Cu) is one among the strongest aluminum alloy and it is the functionally graded material which has its application in the field of Aerospace and Automotive Industries. An intensive study of this Cast Aluminum family has been found in many literatures for increasing the mechanical properties and grain refinement of the aluminum alloys. The main objective of this work is to study the properties of Al 2014 produced by Horizontal Centrifugal Casting process at different rotating speeds (400rpm 600rpm and 800rpm) wit fixed pouring temperature (650°C). The mechanical properties such as tensile strength and hardness were studied using Electronic Tensometer and Brinell Hardness Tester. It was observed that the tensile strength and hardness are increased with the increase in rotary speed of the mold. Also, the microstructure of the sample had very fine grain refinement enhancing good property at higher Rotational speeds of the mold. Key Words: Al-Cu alloy, Tensile strength, Grain size, Microstructure, Hardness. 1. INTRODUCTION Functionally Graded Materials (FGMs) are the class of engineering materials characterized by their spatial variation of composition and microstructure aiming at controlling corresponding functional properties (i.e. mechanical, thermal, electrical, etc.). This material exhibits steady progress in the microstructure as well as the composition in a definite way, the presence of FGMs, which prompts variety in useful execution inside the part through micro structural control. [2] In castings inhomogeneous distribution in composition, is a typical defect although microsegregation usually between 10 and 100 μm can be minimized/eliminated by heat treatments but macrosegregation (cm to m) is essentially unaffected and this may influence the effects of heat treatment, result in property variations and damage the quality of the final product. [1] Centrifugal casting is one of the promising processes taking major role in the production of functionally graded material. It is a process of producing hollow castings by causing molten metal to solidify in rotating mould. The operations include in centrifugal casting are rotation of mold at a known speed, pouring the molten metal and extraction of the casting from the mold. The solidification is quite rapid and hence good metallurgical quality is achieved as solidification starts from the inner surface of the mold corresponding to casting outer surface, so low melting point impurities are carried by the solidification front to the casting inner surface and gas porosity is also forced at the casting inner surface because of its low density and also fine grain structures are formed.[5] On Centrifugal casting the first melt that reaches the wall surface of the mold will backing the income fresh metal and hence forms nucleation sites hence promoted for fast solidification fine grains[6] The centrifugal process eliminates the mid wall effects because the inner surface will completely be in the liquid state during the solidification process which results in a continuous feed of metal in the areas of contraction, thereby ensuring the absence of trapped porosity. 2. EXPERIMENTAL PROCEDURE: 2.1 Material Selection: The increase in the demand for the aluminum and its alloys in Aerospace and Automobile industrial applications due to its favorable properties such as high specific toughness, good strength, good machinability and good wear properties. In this alloys aluminum is the base and other materials such as Si, Mg, Cu, Mn, Fe, Zn are the alloying elements. In this study Al 2014 (Al-Cu) has been taken because of its popularity which is remarked as the strongest alloying elements. Elemen ts C r C u F e M g M n Si Ti Zn Al Percent age 0. 1 5 0. 7 0. 8 1. 2 0. 5 0.1 5 0.2 5 Remain ing Chart-2.1 The chemical composition of Al 2014 (Al-Cu) 2.2 Methodology: The hollow cylindrical casting of outer diameter 72mm and length 84mm with wall thickness of 8mm were produced by using Horizontal centrifugal casting process which is shown in the fig . As mold rotational speed is one of the process parameter which influences the rate of solidification. The centrifugal casting were produced at their rotational speed of the mold such has 400rpm, 600rpm and 800rpm.The pouring temperature is kept constant as 650°C, Due to the centrifugal force which is acting away from the central axis the denser metals in the alloy will be towards the wall of the mold and lesser denser metals towards the central axis
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 08 | Aug 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1310 thus influencing the property of the metal. The casting specimens are cut to prepare the specimen to conduct various tests like Brinell Hardness Test, tensile test are performed. Fig-2.1 Experimental setup of horizontal centrifugal casting Fig-2.2 Mold formed after centrifugal casting 3. RESULTS AND DISCUSSION: 3.1 Microstructural Analysis: The figure shows the microstructure obtained from the castings Produced at different Rotational speeds of the mold. Inner Middle Outer Fig-3.1a Microstructure of Al-Cu Specimen-1 (650°C temperature at 400rpm speed) Inner Middle Outer Fig-3.1b Microstructure of Al-Cu Specimen-2 (650°C temperature at 600rpm speed) Inner Middle Outer Fig-3.1c Microstructure of Al-Cu Specimen-3 (650°C temperature at 800rpm speed) 3.2 Hardness test: The graph shows the variation of hardness along the radial direction among three specimens which was experimented at different rotary speeds. Chart-3.2 Variation of Brinell Hardnesss number from inner to outer region It shows similar variation in rate of solidification of the casting along the radial direction. The cast shows higher hardness number at the outer and inner region due to the rapid solidification of the casts. The outer surface is harder due to the chilling effect where the molten metal is contacted to the mold surface. The lower hardness number at the middle region indicates that the metal takes more time to solidify compared to inner and outer radius. spru e Rotating mold Motor Dial Indicator Speed Indicator 0 10 20 30 40 50 Inner Middle Outer 400rpm 600rpm 800rpm
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 08 | Aug 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1311 3.3 Tensile test: The pictures show the tensile specimen before and after fracture Fig-3.3 Tensile specimen before and after breaking Chart-3.3 Variation of Break Load at different speeds The tensile test specimen of the Indian standards was tested using Electronic Tensometer with the uniform load applied to the specimen to undergo fracture; The Fig. shows the tensile strength of centrifugally cast specimen at three different rotational speeds of the mold. It shows higher tensile strength for casting produced at the higher rotational speed compared to the casting produced at lower rotational speed. 4. CONCLUSIONS: The main Conclusions of this work are:  The Centrifugal casting is one of the methods to produce functionally graded materials with variation in hardness along the radial direction in the casting.  At higher rotational speeds of the mold fine grains will be formed with improved mechanical properties and at lower rotational speeds coarse grains will be formed with lower mechanical properties.  The results show the variation in hardness along the radial direction with slightly higher hardness values at inner and outer radii.  The tensile strength is also observed higher for the casting produced at the 800rpm compared to that of 400rpm. 5. REFERENCE: [1] Yisen Hu1, Gang Wang, Qing Jiang, Wenfeng Xiao, Yiming Rong, “Precipitation strengthening behaviour of Al-Cu-Mn alloys with the effect of casting segregation” Contributed Papers from Materials Science and Technology 2017 (MS&T17) [2] Mallikarjun, Sukruth M, Chethan KS and Dr. Kiran Aithal, “Study of Functionally Graded Al-Si Alloy Fabricated by Centrifuge Casting Technique” International Journal of Advances in Scientific Research and Engineering (ijasre) [3] Sani A Salihu, Aliyu Isah, Polycarp Evarastics, “Influence of Magnesium Addition on Mechanical Properties and Microstructure of Al-Cu-Mg Alloy” IOSR Journal of Pharmacy and Biological Sciences (IOSR-JPBS) ISSN: 2278-3008. Volume 4, Issue 5 (Nov. – Dec. 2012), PP 15-20 [4] Maria Eduarda Farinaa*, Pedro Bella, Carlos Raimundo Frick Ferreirab, Berenice Anina Dedavida, “Effects of Solidification Rate in the Microstructure of Al-Si5Cu3 Aluminum Cast Alloy” Materials Research. 2017; 20(Suppl. 2): 273-278 [5] Madhusudhan, Narendranath S, G C Mohan Kumar, “Experimental Study on Cooling Rate of Centrifugal Casting Based on Grain Size” International Journal of Scientific & Engineering Research, Volume 3, Issue 1, January-2012 1 ISSN 2229-5518 [6] S. R. CHANG, J. M. KIM and C. P. HONG, “Numerical Simulation of Microstructure Evolution of Al Alloys in Centrifugal Casting” ISIJ International, Vol. 41 (2001), No. 7, pp. 738–747 1950 2000 2050 2100 2150 2200 750 rpm 850 rpm 950 rpm Break Load (N) Break Load (N)