IR spectroscopy analyzes molecular vibrations and rotations that are excited by infrared light. When the frequency of infrared light matches the natural vibrational frequency of a molecule, absorption occurs. Different functional groups absorb characteristic frequencies allowing IR spectroscopy to determine a molecule's structure. A proper sampling technique like mulling or using a liquid cell is required to obtain an IR spectrum. An IR spectrometer consists of an infrared source, monochromator, sample holder, detector, and recorder. Common detectors include bolometers and pyroelectric detectors which convert the infrared absorption into electrical signals.
In this slide contains Interference In Atomic Absorption Spectroscopy and applications.
Presented by: Shaik Gouse ul azam. ( department of pharmaceutical analysis.)
RIPER, anantpur.
In this slide contains Interference In Atomic Absorption Spectroscopy and applications.
Presented by: Shaik Gouse ul azam. ( department of pharmaceutical analysis.)
RIPER, anantpur.
Various factor affecting vibrational frequency in IR spectroscopy.vishvajitsinh Bhati
various factor affecting vibrational frequency in IR,
• Coupled vibrations
• Fermi resonance
• Electronic effects
• Hydrogen bonding
and their examples
Various factor affecting vibrational frequency in IR spectroscopy.vishvajitsinh Bhati
various factor affecting vibrational frequency in IR,
• Coupled vibrations
• Fermi resonance
• Electronic effects
• Hydrogen bonding
and their examples
Infrared spectroscopy (IR spectroscopy) is the spectroscopy that deals with the infrared
region of the electromagnetic spectrum, that is light with a longer wavelength and
lower frequency than visible light.
Infrared Spectroscopy is the analysis of infrared light interacting with a molecule.
IR spectroscopy (which is short for infrared spectroscopy) deals with the infrared region of the electromagnetic spectrum, i.e. light having a longer wavelength and a lower frequency than visible light. Infrared Spectroscopy generally refers to the analysis of the interaction of a molecule with infrared light.
Gout is a common and complex form of arthritis that can affect anyone. It's characterized by sudden, severe attacks of pain, swelling, redness and tenderness in one or more joints, most often in the big toe
Typhoid fever is a life-threatening infection caused by the bacterium Salmonella Typhi. It is usually spread through contaminated food or water. Once Salmonella Typhi bacteria are ingested, they multiply and spread into the bloodstream
Tuberculosis (TB) is an infectious disease that most often affects the lungs and is caused by a type of bacteria. It spreads through the air when infected people cough, sneeze or spit. Tuberculosis is preventable and curable. About a quarter of the global population is estimated to have been infected with TB bacteria
It includes Defination,Classification of powders.Special Types of Powders like effervesent,effloroscent,Eutectic mixture.Fomulation of powder with mixing technique of powder.
Two-dimensional nuclear magnetic resonance spectroscopy (2D NMR) is a set of nuclear magnetic resonance spectroscopy (NMR) methods which give data plotted in a space defined by two frequency axes rather than one.
Types of 2D NMR include correlation spectroscopy (COSY), J-spectroscopy, exchange spectroscopy (EXSY), and nuclearOverhauser effect spectroscopy (NOESY).
The prostate is an exocrine gland of the male mammalian reproductive system
It is a walnut-sized gland that forms part of the male reproductive system and is located in front of the rectum and just below the urinary bladder
Function is to store and secrete a clear, slightly alkaline fluid that constitutes 10-30% of the volume of the seminal fluid that along with the spermatozoa, constitutes semen
A healthy human prostate measures (4cm-vertical, by 3cm-horizontal, 2cm ant-post ).
It surrounds the urethra just below the urinary bladder. It has anterior, median, posterior and two lateral lobes
It’s work is regulated by androgens which are responsible for male sex characteristics
Generalised disease of the prostate due to hormonal derangement which leads to non malignant enlargement of the gland (increase in the number of epithelial cells and stromal tissue)to cause compression of the urethra leading to symptoms (LUTS
Couples presenting to the infertility clinic- Do they really have infertility...Sujoy Dasgupta
Dr Sujoy Dasgupta presented the study on "Couples presenting to the infertility clinic- Do they really have infertility? – The unexplored stories of non-consummation" in the 13th Congress of the Asia Pacific Initiative on Reproduction (ASPIRE 2024) at Manila on 24 May, 2024.
Tom Selleck Health: A Comprehensive Look at the Iconic Actor’s Wellness Journeygreendigital
Tom Selleck, an enduring figure in Hollywood. has captivated audiences for decades with his rugged charm, iconic moustache. and memorable roles in television and film. From his breakout role as Thomas Magnum in Magnum P.I. to his current portrayal of Frank Reagan in Blue Bloods. Selleck's career has spanned over 50 years. But beyond his professional achievements. fans have often been curious about Tom Selleck Health. especially as he has aged in the public eye.
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Introduction
Many have been interested in Tom Selleck health. not only because of his enduring presence on screen but also because of the challenges. and lifestyle choices he has faced and made over the years. This article delves into the various aspects of Tom Selleck health. exploring his fitness regimen, diet, mental health. and the challenges he has encountered as he ages. We'll look at how he maintains his well-being. the health issues he has faced, and his approach to ageing .
Early Life and Career
Childhood and Athletic Beginnings
Tom Selleck was born on January 29, 1945, in Detroit, Michigan, and grew up in Sherman Oaks, California. From an early age, he was involved in sports, particularly basketball. which played a significant role in his physical development. His athletic pursuits continued into college. where he attended the University of Southern California (USC) on a basketball scholarship. This early involvement in sports laid a strong foundation for his physical health and disciplined lifestyle.
Transition to Acting
Selleck's transition from an athlete to an actor came with its physical demands. His first significant role in "Magnum P.I." required him to perform various stunts and maintain a fit appearance. This role, which he played from 1980 to 1988. necessitated a rigorous fitness routine to meet the show's demands. setting the stage for his long-term commitment to health and wellness.
Fitness Regimen
Workout Routine
Tom Selleck health and fitness regimen has evolved. adapting to his changing roles and age. During his "Magnum, P.I." days. Selleck's workouts were intense and focused on building and maintaining muscle mass. His routine included weightlifting, cardiovascular exercises. and specific training for the stunts he performed on the show.
Selleck adjusted his fitness routine as he aged to suit his body's needs. Today, his workouts focus on maintaining flexibility, strength, and cardiovascular health. He incorporates low-impact exercises such as swimming, walking, and light weightlifting. This balanced approach helps him stay fit without putting undue strain on his joints and muscles.
Importance of Flexibility and Mobility
In recent years, Selleck has emphasized the importance of flexibility and mobility in his fitness regimen. Understanding the natural decline in muscle mass and joint flexibility with age. he includes stretching and yoga in his routine. These practices help prevent injuries, improve posture, and maintain mobilit
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micro teaching on communication m.sc nursing.pdfAnurag Sharma
Microteaching is a unique model of practice teaching. It is a viable instrument for the. desired change in the teaching behavior or the behavior potential which, in specified types of real. classroom situations, tends to facilitate the achievement of specified types of objectives.
Ethanol (CH3CH2OH), or beverage alcohol, is a two-carbon alcohol
that is rapidly distributed in the body and brain. Ethanol alters many
neurochemical systems and has rewarding and addictive properties. It
is the oldest recreational drug and likely contributes to more morbidity,
mortality, and public health costs than all illicit drugs combined. The
5th edition of the Diagnostic and Statistical Manual of Mental Disorders
(DSM-5) integrates alcohol abuse and alcohol dependence into a single
disorder called alcohol use disorder (AUD), with mild, moderate,
and severe subclassifications (American Psychiatric Association, 2013).
In the DSM-5, all types of substance abuse and dependence have been
combined into a single substance use disorder (SUD) on a continuum
from mild to severe. A diagnosis of AUD requires that at least two of
the 11 DSM-5 behaviors be present within a 12-month period (mild
AUD: 2–3 criteria; moderate AUD: 4–5 criteria; severe AUD: 6–11 criteria).
The four main behavioral effects of AUD are impaired control over
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effects (tolerance, withdrawal). This chapter presents an overview
of the prevalence and harmful consequences of AUD in the U.S.,
the systemic nature of the disease, neurocircuitry and stages of AUD,
comorbidities, fetal alcohol spectrum disorders, genetic risk factors, and
pharmacotherapies for AUD.
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Report Back from SGO 2024: What’s the Latest in Cervical Cancer?bkling
Are you curious about what’s new in cervical cancer research or unsure what the findings mean? Join Dr. Emily Ko, a gynecologic oncologist at Penn Medicine, to learn about the latest updates from the Society of Gynecologic Oncology (SGO) 2024 Annual Meeting on Women’s Cancer. Dr. Ko will discuss what the research presented at the conference means for you and answer your questions about the new developments.
New Directions in Targeted Therapeutic Approaches for Older Adults With Mantl...i3 Health
i3 Health is pleased to make the speaker slides from this activity available for use as a non-accredited self-study or teaching resource.
This slide deck presented by Dr. Kami Maddocks, Professor-Clinical in the Division of Hematology and
Associate Division Director for Ambulatory Operations
The Ohio State University Comprehensive Cancer Center, will provide insight into new directions in targeted therapeutic approaches for older adults with mantle cell lymphoma.
STATEMENT OF NEED
Mantle cell lymphoma (MCL) is a rare, aggressive B-cell non-Hodgkin lymphoma (NHL) accounting for 5% to 7% of all lymphomas. Its prognosis ranges from indolent disease that does not require treatment for years to very aggressive disease, which is associated with poor survival (Silkenstedt et al, 2021). Typically, MCL is diagnosed at advanced stage and in older patients who cannot tolerate intensive therapy (NCCN, 2022). Although recent advances have slightly increased remission rates, recurrence and relapse remain very common, leading to a median overall survival between 3 and 6 years (LLS, 2021). Though there are several effective options, progress is still needed towards establishing an accepted frontline approach for MCL (Castellino et al, 2022). Treatment selection and management of MCL are complicated by the heterogeneity of prognosis, advanced age and comorbidities of patients, and lack of an established standard approach for treatment, making it vital that clinicians be familiar with the latest research and advances in this area. In this activity chaired by Michael Wang, MD, Professor in the Department of Lymphoma & Myeloma at MD Anderson Cancer Center, expert faculty will discuss prognostic factors informing treatment, the promising results of recent trials in new therapeutic approaches, and the implications of treatment resistance in therapeutic selection for MCL.
Target Audience
Hematology/oncology fellows, attending faculty, and other health care professionals involved in the treatment of patients with mantle cell lymphoma (MCL).
Learning Objectives
1.) Identify clinical and biological prognostic factors that can guide treatment decision making for older adults with MCL
2.) Evaluate emerging data on targeted therapeutic approaches for treatment-naive and relapsed/refractory MCL and their applicability to older adults
3.) Assess mechanisms of resistance to targeted therapies for MCL and their implications for treatment selection
These lecture slides, by Dr Sidra Arshad, offer a quick overview of physiological basis of a normal electrocardiogram.
Learning objectives:
1. Define an electrocardiogram (ECG) and electrocardiography
2. Describe how dipoles generated by the heart produce the waveforms of the ECG
3. Describe the components of a normal electrocardiogram of a typical bipolar leads (limb II)
4. Differentiate between intervals and segments
5. Enlist some common indications for obtaining an ECG
Study Resources:
1. Chapter 11, Guyton and Hall Textbook of Medical Physiology, 14th edition
2. Chapter 9, Human Physiology - From Cells to Systems, Lauralee Sherwood, 9th edition
3. Chapter 29, Ganong’s Review of Medical Physiology, 26th edition
4. Electrocardiogram, StatPearls - https://www.ncbi.nlm.nih.gov/books/NBK549803/
5. ECG in Medical Practice by ABM Abdullah, 4th edition
6. ECG Basics, http://www.nataliescasebook.com/tag/e-c-g-basics
ARTIFICIAL INTELLIGENCE IN HEALTHCARE.pdfAnujkumaranit
Artificial intelligence (AI) refers to the simulation of human intelligence processes by machines, especially computer systems. It encompasses tasks such as learning, reasoning, problem-solving, perception, and language understanding. AI technologies are revolutionizing various fields, from healthcare to finance, by enabling machines to perform tasks that typically require human intelligence.
Lung Cancer: Artificial Intelligence, Synergetics, Complex System Analysis, S...Oleg Kshivets
RESULTS: Overall life span (LS) was 2252.1±1742.5 days and cumulative 5-year survival (5YS) reached 73.2%, 10 years – 64.8%, 20 years – 42.5%. 513 LCP lived more than 5 years (LS=3124.6±1525.6 days), 148 LCP – more than 10 years (LS=5054.4±1504.1 days).199 LCP died because of LC (LS=562.7±374.5 days). 5YS of LCP after bi/lobectomies was significantly superior in comparison with LCP after pneumonectomies (78.1% vs.63.7%, P=0.00001 by log-rank test). AT significantly improved 5YS (66.3% vs. 34.8%) (P=0.00000 by log-rank test) only for LCP with N1-2. Cox modeling displayed that 5YS of LCP significantly depended on: phase transition (PT) early-invasive LC in terms of synergetics, PT N0—N12, cell ratio factors (ratio between cancer cells- CC and blood cells subpopulations), G1-3, histology, glucose, AT, blood cell circuit, prothrombin index, heparin tolerance, recalcification time (P=0.000-0.038). Neural networks, genetic algorithm selection and bootstrap simulation revealed relationships between 5YS and PT early-invasive LC (rank=1), PT N0—N12 (rank=2), thrombocytes/CC (3), erythrocytes/CC (4), eosinophils/CC (5), healthy cells/CC (6), lymphocytes/CC (7), segmented neutrophils/CC (8), stick neutrophils/CC (9), monocytes/CC (10); leucocytes/CC (11). Correct prediction of 5YS was 100% by neural networks computing (area under ROC curve=1.0; error=0.0).
CONCLUSIONS: 5YS of LCP after radical procedures significantly depended on: 1) PT early-invasive cancer; 2) PT N0--N12; 3) cell ratio factors; 4) blood cell circuit; 5) biochemical factors; 6) hemostasis system; 7) AT; 8) LC characteristics; 9) LC cell dynamics; 10) surgery type: lobectomy/pneumonectomy; 11) anthropometric data. Optimal diagnosis and treatment strategies for LC are: 1) screening and early detection of LC; 2) availability of experienced thoracic surgeons because of complexity of radical procedures; 3) aggressive en block surgery and adequate lymph node dissection for completeness; 4) precise prediction; 5) adjuvant chemoimmunoradiotherapy for LCP with unfavorable prognosis.
Lung Cancer: Artificial Intelligence, Synergetics, Complex System Analysis, S...
Ir spectroscopy
1. IR SPECTROSCOPY
Mr. Shinde GANESH SHASHIKANT
PRAVARA RURAL COLLEGE OF PHARMACY, PRAVARANAGAR
Department of Pharmaceutical Chemistry
2. Spectroscopy
• Method of “Seeing the unseeable”
• using electromagnetic radiation to obtain
information about atoms and molecules that are
too small to see.
Atoms
Molecules
3. Spectroscopy is an instrumentally aided study of
the interactions between matter (sample being
analyzed) and energy (any portion of the
electromagnetic spectrum)
EMR ANALYTE SPECTROPHOTOGRAPH
1.UV-Visible radiations--------excitation of electrons---------UV-visible spectrum
2.IR-radiations------------------vibration changes in electrons--------IR spectrum
3.Radio frequency---------------spin rotational changes-------------N.M.R spectrum
Conc. should be lower
4. IR spectrophotometry
Energy of molecule = Electronic energy+ Vibrational
energy + Rotational energy
• IR spectroscopy is concerned with the study of
absorption of infrared radiation, which causes
vibrational transition in the molecule.
Hence, IR spectroscopy also known as Vibrational
spectroscopy.
• IR spectra mainly used in structure elucidation to
determine the functional groups.
5.
6. • IR region:
Most of the analytical applications are confined to the
middle IR region because absorption of organic
molecules are high in this region.
Sub divided into
Near infrared region 0.8-2.5 µ(12,500-4000 cm-1)
Main infrared region 2.5-15 µ(4000-667cm-1)
Far infrared region 15-200 µ(667-50 cm-1)
7. Principle of IR spectroscopy
• Molecules are made up of atoms linked by chemical
bonds. The movement of atoms and the chemical
bonds like like spring and balls (vibration)
• This characteristic vibration are called Natural
frequency of vibration.
8. • When energy in the form of infrared radiation is
applied then it causes the vibration between the
atoms of the molecules and when,
Applied infrared frequency = Natural frequency of
vibration
Then, Absorption of IR radiation takes place and a
peak is observed.
Different functional groups absorb characteristic
frequencies of IR radiation. Hence gives the
characteristic peak value.
Therefore, IR spectrum of a chemical substance is a
finger print of a molecule for its identification.
9. Criteria for a compound to absorb
IR radiation
1. Correct wavelength of radiation
2. Change in dipole moment
1. Correct wavelength of radiation:
A molecule to absorb IR radiation, the natural
frequency of vibrations of some part of a
molecule is the same as the frequency of
incident radiation.
10. 2. Change in dipole moment
• A molecule can only absorb IR radiation when
its absorption cause a change in its electric
dipole
• A molecule is said to have an electric dipole
when there is a slight positive and a slight
negative charge on its component of atoms.
11. Molecular vibrations
There are 2 types of vibrations:
1. Stretching vibrations
2. Bending vibrations
1. Stretching vibrations:
Vibration or oscillation along the line of bond
Change in bond length
Occurs at higher energy: 4000-1500 cm-1 (1250 cm-1 )
2 types:
a) Symmetrical stretching
b) Asymmetrical stretching
13. b) Asymmetrical stretching
• In Asymmetrical Stretching , one bond length is
increased and other is decreased.
H
H
C
14. 2. Bending vibrations
• Vibration or oscillation not along the line of
bond
• These are also called as deformations
• In this, bond angle is altered
• Occurs at low energy: 1400-666 cm-1
• 2 types:
a) In plane bending: scissoring, rocking
b) Out plane bending: wagging, twisting
15. a) In plane bending
i. Scissoring:
• This is an in plane blending
• 2 atoms approach each other
• Bond angles are decrease
H
H
CC
17. b) Out plane bending
i. Wagging:
• 2 atoms move to one side of the plane. They move
up and down the plane.
ii. Twisting:
• One atom moves above the plane and another
atom moves below the plane.
H
H
CC
H
H
CC
18. • Types of Molecular Vibrations
• Stretching Vibrations: in which bond length changes
that require more energy.
• Bending Vibrations: in which bond angle changes
that require less energy.
Asymmetrical stretchingSymmetrical stretching
Rocking ScissoringTwisting Wagging
22. Sampling techniques
• Sample preparation is the most important part
in IR spectral analysis, Sample should be
transparent to IR radiations so it allows the
radiations to pass through them
• Hence the salts like KBr, NaCl, AgCl are used
for mixing of sample in order to obtain the
accurate IR spectrum of a sample with good
intensity, sharp peaks and high resolution.
23. 1) Solid samples:
• Mull technique
• Pressed pellet technique
• Solids run in solutions
• Solid film
2) Liquid samples
3) Gaseous sample
23
Sampling techniques
24. Mull technique
• Grinding 2-5mg of sample in smooth agitate
mortar.
• Powdered sample + Nujol oil (mineral oil) paste
• Paste between the two plates of salt.
• The oil has few absorption bands at 2857, 1449
and 1389 cm-1
• The particle size must 1 -2 micron.
• Nujol agent (mineral oil) used in this techniques are : High boiling
petroleum, Halocarbon oil, perfluorokerosene
24
25. Pressed pellet technique:
• In this technique, a small amount of finely
ground solid sample is mixed with 100 times its
weight of potassium bromide and compressed
into a thin transparent pellet using a hydraulic
press. These pellets are transparent to IR
radiation and it is used for analysis.
• 1mg Sample+ 100mg KBr powder
25
26. Solids films:
• Amorphous solid samples melted between salt
plates allowed to form solid film.
• For qualitative purpose.
Solids run in solution
• Solid + suitable solvent 🡪 solution
• Kept in cells for liquids
• Solvents- non associated
solvents- CS2, CCl4,
26
28. Liquid sample:
• Liquid samples are usually handled pure without mixing them with
any solvent because all solvents have their own characteristics
absorption spectra.
• For liquid samples highly polished salt (NaCl, KBr or AgCl) plates
are used.
• A drop of liquid sample is placed on the face first plate and the
second plate is placed on the top to form a uniform film of a sample
wipe off the excees liquid spilled from the edge of the plate then
place the plates in the sample compartment of spectrophotometer
and run the spectrum.
28
29. Gaseous sample:
• Vapors in specially designed cells.
• End walls made up of Sodium chloride.
• A special sample cell is used for the
gaseous sample made up of NaCl, KBr
with long path length i.e 5 to 10 cm
• The vapors of gas are placed into the cell
and directly place in the path of Infrared
radiation
29
31. The main parts of IR spectrometer are as follows:
• RADIATION SOURCE
• SAMPLE CELLS AND SAMPLING OF SUBSTANCES
• MONOCHROMATORS
• DETECTORS
• RECORDER
32. IR instruments require a source of radiant energy
which emit IR radiation which must be:
Sufficient
intensity
Continuous Stable
33. Globar source
• Rod of sintered silicon carbide. (5cm x 5mm).
• Positive coefficient of resistance.
• Self starting and electrically heated
• Enclosed in water cooled brass tube
• Less intense.
• Emit Radiation at 5200 cm-1
33
34. Nernst glower
• Composed of rare earth oxides- zirconium, yttrium and thorium
• Hollow tube (2-5cm x 1-3mm)
• Platinum leads at one end
• Large negative temp. coefficient.
• Emit radiation 7100 cm-1 over wide range and remains steady over a
long period.
Disadvantages:
• Fragile
• Auxiliary heater
• Over heating
34
35. Incandescent wire loop
• Tightly wound spiral of Nichrome wire.
• No water cooling
• Less maintenance
• Less intense than other sources.
Tungsten filament lamp
• Tightly wound spiral of tungsten wire.
• For near IR
• Emit radiation 667-4000 cm-1
35
36. Mercury arc
• For far IR region
• High pressure Hg arc, enclosed in quartz
jacketed tube, at 1 atm
• Passage of electricity through vapor 🡪 internal
plasma sourc IR radiation
• Emit radiation less than 667 cm-1
36
38. Sample holders
• Constructed of rock salt.
• Path length is adjusted with Teflon.
• Filled and emptied with hypodermic needles.
• Foggy due to moisture.
Care:
▫ Moisture free samples
▫ Fingers should not be come in contact
▫ Prevent contamination with silicones
38
44. Bolometer is derived from a Greek word
(bolometron)
Bolo = for something thrown
Metron = measure
It was invented in 1878 by the American
astronomer Samuel Pierpont Langley
45. Construction
• A bolometer consists of an absorptive element,
such as a thin layer of metal or thermister .
• Most bolometers use semiconductor or
superconductor absorptive elements rather than
metals.
46. Working
Thin layer of
metal
connected to a
reservoir
Any radiation on the
absorptive element
raises its
temperature above
that of the reservoir.
The temperature
change can be
measured directly
with an attached
thermometer.
47. Temperature changes Potential difference
changes
Thermocouples consist of a pair of junctions of different metals; for
example, two pieces of bismuth fused to either end of a piece of
antimony.
48. Thermopile detectors are voltage-generating
devices, which can be thought of as
miniature arrays of thermocouple junctions.
Cold junction(t2)is kept const. temp and not
exposed IR but other junction hot when
exposed IR cause increase temp of junction
and generatre P.D due to incident IR
radiation fall on hot junction .
49. PYRO ELECTRIC DETECTOR
Construction:
• Single crystalline
wafer of a pyro electric
material, such as
triglycerine sulphate.
• Pyro electric Infrared
Detectors (PIR)
convert the changes in
incoming infrared light
to electric signals.
50. Below curie temperature
Pyro electric materials exhibit electrical polarization.
Temperature is altered, the polarization changes.
Observed as an electrical signal
(if electrodes are placed on opposite faces of a thin slice of the
material to form a capacitor)
51. Construction:
• Small metal cylinder
• Flexible silvered diaphragm
• Whole chamber is filled with xenon gas.
52. I.R radiations
Metal cylinder and flexible diaphragm
Temperature increases
Gas is expended and diaphragm deforms
detect as a signal
57. 57
INTRODUCTION
• Absorption of IR radiation by sample, result in
vibration transition.
• Infrared radiation lies between the tfisible and
microwave portions of the electromagnetic
spectrum.
• Infrared waves have wavelengths longer than
visible and shorter than microwave and have
frequencies which arelower than visible and higher
than microwaves.
• IR spectra aremainly used in structure elucidation
to determine the groups.
58. PRINCIPLE
TheBeamSplitter Divides the beamandtransmits half of the incomingradiation
to the fixed mirrorandthe otherhalf to the movablemirror .
• Upon reflectionfromthe fixed andthe movablemirrorthe light is
recombinedat the beamsplitter.
• Therecombinationof the radiationis then directthroughthe sampleand focused
onthe detectoronthe detector(Pyroelectric detector).
• When the path differenceis ZERO, allthe spectralcomponentsarein phase
andthe output is at a MAXIMUM.
60. • Sources:Nernst Glower, GlobalSource,Tungsten Lamp, Mercuryarc.
• BeamSplitter: It ismadeupof materialwhichismadeupof refractiveindex
1. ForFarInfrared: Mylar film sandwichedbetween halideplateof low
refractiveindexsolid used.
2. FormiddleIR :Thin film of germaniumorsilicondepositedonCsIorCsBror
KClor NaCl.
3. ForNearIR: Thin film of ferricoxidedepositedoncalciumchloride
• Detector:PyroelectricDetectoris used
61. • It consist of two perpendicularmirrors,oneof which is
Stationary mirrorand the other is amovable mirror.
• ThePosition of movablemirror is controlledby HeNe Laser.
(632.8 nm)
• Between these two mirrors , set abeamsplitter at 45
degreefrom initial positon of the movable mirror.
• A parallelbeamof radiation fromIR sourceis passedon
the mirrorsthroughthe beam splitter