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Presentation On
Importance of Salt Recovery Plant in
Textile Dyeing Industry
Submitted By:
Rajib Mia
Dept. of textile engineering,
Southeast University(SEU)
Gmail:mdrajibmia758@gmail.com
Phone: +8801774435305
SubmittedTo:
Israt zerin
Lecturer
Department of textile engineering
Southeast university(SEU)
Introduction:
Salt Recovery Plant (SRP) is such a plant which is related with betterment of environment issue of dying
sector as well as textile industry. Different projects have been done for recovering salt from dyed
solution. Textile industries mainly constitute large volume of fresh water and the effluent discharge are
heavily polluted with dissolve solid, organic and color. The advance treatment technologies and
processes, reducing concentration of the pollutants and also give scope for recovery and recycle of water
and salt from effluents, which help conserve natural sources.
In this study Chlorination, Ozonation, Reactor, Air Diffusion Tank, Flash Mixer, Pressure Sand Filter Feed
(PSF), Ultra Filtration, Reverse Osmosis (RO) processes used for treatment of waste water after dyeing
with reactive dye. After the treatment the saline water is used for dyeing fabric again and compared with
the dyed fabric using ground water.
Methodology :
The methodology is the general research strategy
that outlines the way in which research is to be
undertaken and identifies the methods to be
used in it.
Most of the salt concentration is contained in the
dye bath, In this study we have followed SRP
plant of Niagara Textiles Ltd. It has been
developed an innovative technology working
directly on dye-bath discharge or waste water. It
facilitates salt recovery reducing the quantity and
allowing its reuse, isolating the considerable
concentrate waste, treating it separately with the
treatment plant
•Raw Materials:
Chemical Has Been Used in This Plant Are –
 Hydro chloric acid
Chlorine
 Titanium (Ti)/Magnesium chloride Dye
 Poly aluminum chloride (PAC),
 Ozone gas
 Hydrogen
Process Flow Chart of SRP
 Bath Collection Tank
 Chlorination
 Ozonation
 Reactor
 Air Diffusion Tank
 Flash Mixer
 Pressure Sand Filter Feed (PSF)
 Ultra Filtration
 Reverse Osmosis (RO)
 cleaning tank.
• Dye Bath Collection Tank:
At first the waste water comes from dye bath to dye bath collection tank. Only the
water which contains 60g/l salt will be treated in salt recovery plant. This waste
water having a PH about 10-11 while coming in dye bath and then Hydro chloric
acid is added to reduce the pH level about 8.
Chlorination:
• Waste water runs for the further
process from dye bath and at a first
stage chlorination has been done
through the pipe. Water chlorination
is the process of adding chlorine or
hypochlorite to water. This method is
used to kill certain bacteria and other
microbes in tap water as chlorine is
highly toxic and in this process water
color is also reduced. When dissolved
in water, chlorine converts to an
equilibrium mixture of chlorine,
hypochlorous acid (HOCl), and
hydrochloric acid (HCl). [1]
Cl2 + H2O ⇌ HOCl + HCl
Ozonation:
• Ozone can eliminate a wide variety of
inorganic, organic and microbiological
problems and taste and odor problems.
The microbiological agents include
bacteria, viruses, and protozoans (such as
Guardia and Cryptosporidium). Ozone is a
powerful oxidant, leaves no residual
harmful product, no sludge disposal
problem and increases the DO content of
wastewater which helps further in the
degradation of residual pollutant. ozone
finds use in treatment of all types of
waste such as municipal waste water,
industrial waste water, contaminated
ground water, treatment of swimming
pool water.
Ozonation Tank.
Reactor:
After ozonation the water flows towards 6
boxes of reactors. The reactors are Ti and Mcl.
Which removes pathogens, color and wasted
raw materials present in water and works for
removing different types of toxic materials
from water.
Reactor tank.
Air Diffusion Tank:
After mixing with reactor the
water goes to the air diffusion
tank. Then air is passed to the
air diffusion tank by blower
Which increasing oxygen level
in the water.
Air Diffusion Tank
Flash Mixer:
Flash mixing is done in 4 tank. After air diffusion the water first
reserved in 1st tank. Then water goes to 2nd tank and there mix
with Poly Chloride (PC), Poly Aluminum Chloride (PAC). Which
removes color and pathogen from water. After that the water
enters into 3rd tank and mix with polymer. And then water flows
towards the 4th tank and there separation of water and sludge is
done. The 4th tank also called as clarifier tank. Titanium metal
contains on surface layer of titanium oxide that prevents
through chemical reactions. When the layer is damaged it is
usually restored rapidly. This not only occurs when it comes in
contact with air but also in contact with water. This reaction
forms both titanium oxide and highly flammable hydrogen gas
according to the following reaction mechanism.
Flash Mixer
Pressure Sand Filter Feed (PSF) :
From Clarifier tank water goes to the
PSF tank where water get recycled and
get filtered and then goes for another
process through the pipe.
Pressure Sand Filter Feed (PSF)
Ultra Filtration :
From PSF Feed the water
comes to the ultra filtration
feed tank. Feed tank water
goes to ultra filtration tower.
There pathogens are removed
and water get filtered and
recycled also.
Ultra Filtration Tank
• Reverse Osmosis (RO):
This is the last stage of Salt Recovery Plant. After ultra filtration water
goes to the two RO feed tank. From RO feed tank water flows toward
RO tower. In this process high air pressure is provided by a motor to the
RO tank and water recycled and creates saline water and fresh water.
Reverse Osmosis (RO)
• Cleaning Tank :
When ultra filtration tower and reverse osmosis tower deposits dirt,
this time cleaning is done by chlorine gas in cleaning tank. This process
is held after every twenty days.
Cleaning Tank
• Dyeing of Cotton Fabric Using Saline Water from SRP and Ground Water :
Cotton fabric dyed with reactive dyes with ground water and saline water from SRP. Gluber
Salt is added according to the calculation of extra salt needed prior to the salt content
remain in the saline water.
Recipe:
Jinjipi Super yellow-0.18%
Jinjipi Deep Red CD-2.3%
Dychufix Navy blue GG-0.15%
Gluber salt-60g/L
Soda ash-2.25g/L
Levelling Agent-0.6g/L
Sequestering Agent-0.5g/L
pH 10-11
Time 60min
Temperature 60°C
Liquor ratio 1:6
Comparison on Shade Variation:
The shade difference of the samples has been evaluated by Verivide light box.
Spectrophotometric Evaluation of Dyed Samples
Color co-ordinates values of dyed samples were compared by using spectrophotometer
“Spectro 600” (Spectro 600).
Color Fastness to Wash:
Washing fastness of dyed samples was tested according to ISO 105:CO3 method at 60°C
for 30 minutes.
Color Fastness to Rubbing :
This test is designed to determine the degree of color which may be transferred from the
surface of a colored fabric to a specific test cloth for rubbing (dry and wet), Method: ISO
105 /12 and M/c Name: Crock master has been used for rubbing test.
Salt Recovery Calculation :
Salt recovery proportion is calculated according to the capacity of the plant and
expressed as percentage.
Result & Discussions :
In this factory, As per recipe gluber salt =80 g/l needed for dyeing 1000kg fabric
When M:L=1:6
Total salt require=6*80=480 kg
With saline water salt covered=(1000*6)70/1000 =420 kg
salt save =(480-420)=60 kg
Daily, average gluber salt require=7000 kg
So salt recovery per day =2450 kg
Total salt recovery = (2450/7000)*100% =35%
So, 35% of total salt used is recovered by using salt recovery plant in Niagra Textiles
Limited.
Conclusion:
Now a day’s gradual increasing use of deep water in industries especially
in textile industries which is a big threat for our ecological balance &
environment. So considering the situation many textile industries of all
over the world should be implemented this plant because of the welfare
of our environment and maintain a hygienic nature by blowing out toxic-
free water from their industries waste by recycling waste into fresh
water & saline water.
THE END
THANK YOU

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Importance of Salt Recovery Plant in Textile Dyeing Industry.

  • 1. Welcome To Our Presentation Presentation On Importance of Salt Recovery Plant in Textile Dyeing Industry Submitted By: Rajib Mia Dept. of textile engineering, Southeast University(SEU) Gmail:mdrajibmia758@gmail.com Phone: +8801774435305 SubmittedTo: Israt zerin Lecturer Department of textile engineering Southeast university(SEU)
  • 2. Introduction: Salt Recovery Plant (SRP) is such a plant which is related with betterment of environment issue of dying sector as well as textile industry. Different projects have been done for recovering salt from dyed solution. Textile industries mainly constitute large volume of fresh water and the effluent discharge are heavily polluted with dissolve solid, organic and color. The advance treatment technologies and processes, reducing concentration of the pollutants and also give scope for recovery and recycle of water and salt from effluents, which help conserve natural sources. In this study Chlorination, Ozonation, Reactor, Air Diffusion Tank, Flash Mixer, Pressure Sand Filter Feed (PSF), Ultra Filtration, Reverse Osmosis (RO) processes used for treatment of waste water after dyeing with reactive dye. After the treatment the saline water is used for dyeing fabric again and compared with the dyed fabric using ground water.
  • 3. Methodology : The methodology is the general research strategy that outlines the way in which research is to be undertaken and identifies the methods to be used in it. Most of the salt concentration is contained in the dye bath, In this study we have followed SRP plant of Niagara Textiles Ltd. It has been developed an innovative technology working directly on dye-bath discharge or waste water. It facilitates salt recovery reducing the quantity and allowing its reuse, isolating the considerable concentrate waste, treating it separately with the treatment plant
  • 4. •Raw Materials: Chemical Has Been Used in This Plant Are –  Hydro chloric acid Chlorine  Titanium (Ti)/Magnesium chloride Dye  Poly aluminum chloride (PAC),  Ozone gas  Hydrogen
  • 5. Process Flow Chart of SRP  Bath Collection Tank  Chlorination  Ozonation  Reactor  Air Diffusion Tank  Flash Mixer  Pressure Sand Filter Feed (PSF)  Ultra Filtration  Reverse Osmosis (RO)  cleaning tank.
  • 6. • Dye Bath Collection Tank: At first the waste water comes from dye bath to dye bath collection tank. Only the water which contains 60g/l salt will be treated in salt recovery plant. This waste water having a PH about 10-11 while coming in dye bath and then Hydro chloric acid is added to reduce the pH level about 8.
  • 7. Chlorination: • Waste water runs for the further process from dye bath and at a first stage chlorination has been done through the pipe. Water chlorination is the process of adding chlorine or hypochlorite to water. This method is used to kill certain bacteria and other microbes in tap water as chlorine is highly toxic and in this process water color is also reduced. When dissolved in water, chlorine converts to an equilibrium mixture of chlorine, hypochlorous acid (HOCl), and hydrochloric acid (HCl). [1] Cl2 + H2O ⇌ HOCl + HCl
  • 8. Ozonation: • Ozone can eliminate a wide variety of inorganic, organic and microbiological problems and taste and odor problems. The microbiological agents include bacteria, viruses, and protozoans (such as Guardia and Cryptosporidium). Ozone is a powerful oxidant, leaves no residual harmful product, no sludge disposal problem and increases the DO content of wastewater which helps further in the degradation of residual pollutant. ozone finds use in treatment of all types of waste such as municipal waste water, industrial waste water, contaminated ground water, treatment of swimming pool water. Ozonation Tank.
  • 9. Reactor: After ozonation the water flows towards 6 boxes of reactors. The reactors are Ti and Mcl. Which removes pathogens, color and wasted raw materials present in water and works for removing different types of toxic materials from water. Reactor tank.
  • 10. Air Diffusion Tank: After mixing with reactor the water goes to the air diffusion tank. Then air is passed to the air diffusion tank by blower Which increasing oxygen level in the water. Air Diffusion Tank
  • 11. Flash Mixer: Flash mixing is done in 4 tank. After air diffusion the water first reserved in 1st tank. Then water goes to 2nd tank and there mix with Poly Chloride (PC), Poly Aluminum Chloride (PAC). Which removes color and pathogen from water. After that the water enters into 3rd tank and mix with polymer. And then water flows towards the 4th tank and there separation of water and sludge is done. The 4th tank also called as clarifier tank. Titanium metal contains on surface layer of titanium oxide that prevents through chemical reactions. When the layer is damaged it is usually restored rapidly. This not only occurs when it comes in contact with air but also in contact with water. This reaction forms both titanium oxide and highly flammable hydrogen gas according to the following reaction mechanism. Flash Mixer
  • 12. Pressure Sand Filter Feed (PSF) : From Clarifier tank water goes to the PSF tank where water get recycled and get filtered and then goes for another process through the pipe. Pressure Sand Filter Feed (PSF)
  • 13. Ultra Filtration : From PSF Feed the water comes to the ultra filtration feed tank. Feed tank water goes to ultra filtration tower. There pathogens are removed and water get filtered and recycled also. Ultra Filtration Tank
  • 14. • Reverse Osmosis (RO): This is the last stage of Salt Recovery Plant. After ultra filtration water goes to the two RO feed tank. From RO feed tank water flows toward RO tower. In this process high air pressure is provided by a motor to the RO tank and water recycled and creates saline water and fresh water. Reverse Osmosis (RO)
  • 15. • Cleaning Tank : When ultra filtration tower and reverse osmosis tower deposits dirt, this time cleaning is done by chlorine gas in cleaning tank. This process is held after every twenty days. Cleaning Tank
  • 16. • Dyeing of Cotton Fabric Using Saline Water from SRP and Ground Water : Cotton fabric dyed with reactive dyes with ground water and saline water from SRP. Gluber Salt is added according to the calculation of extra salt needed prior to the salt content remain in the saline water. Recipe: Jinjipi Super yellow-0.18% Jinjipi Deep Red CD-2.3% Dychufix Navy blue GG-0.15% Gluber salt-60g/L Soda ash-2.25g/L Levelling Agent-0.6g/L Sequestering Agent-0.5g/L pH 10-11 Time 60min Temperature 60°C Liquor ratio 1:6
  • 17. Comparison on Shade Variation: The shade difference of the samples has been evaluated by Verivide light box. Spectrophotometric Evaluation of Dyed Samples Color co-ordinates values of dyed samples were compared by using spectrophotometer “Spectro 600” (Spectro 600). Color Fastness to Wash: Washing fastness of dyed samples was tested according to ISO 105:CO3 method at 60°C for 30 minutes. Color Fastness to Rubbing : This test is designed to determine the degree of color which may be transferred from the surface of a colored fabric to a specific test cloth for rubbing (dry and wet), Method: ISO 105 /12 and M/c Name: Crock master has been used for rubbing test. Salt Recovery Calculation : Salt recovery proportion is calculated according to the capacity of the plant and expressed as percentage.
  • 18. Result & Discussions : In this factory, As per recipe gluber salt =80 g/l needed for dyeing 1000kg fabric When M:L=1:6 Total salt require=6*80=480 kg With saline water salt covered=(1000*6)70/1000 =420 kg salt save =(480-420)=60 kg Daily, average gluber salt require=7000 kg So salt recovery per day =2450 kg Total salt recovery = (2450/7000)*100% =35% So, 35% of total salt used is recovered by using salt recovery plant in Niagra Textiles Limited.
  • 19. Conclusion: Now a day’s gradual increasing use of deep water in industries especially in textile industries which is a big threat for our ecological balance & environment. So considering the situation many textile industries of all over the world should be implemented this plant because of the welfare of our environment and maintain a hygienic nature by blowing out toxic- free water from their industries waste by recycling waste into fresh water & saline water.