I found no good source for extractive distillation on the internet.So i decided to make one myself.This ppt discusses about the technology,its working and benefits.It compares extractive distillation side by side to azeotropic distillation and counts the advantages.
Slides for the eLearning course Separation and purification processes in biorefineries (https://open-learn.xamk.fi) in IMPRESS project.
Section: Distillation
Subject: 1.1 Vapor Liquid Equilibrium
Mechanism of Distillation,simple distillation steam &fractional distillation...M Swetha
Distillation is a technique used to separate liquids based on their boiling points. It involves heating a liquid mixture so that the more volatile components vaporize and pass into a condenser where they condense. Simple distillation can separate two liquids with a boiling point difference of at least 70°C, while fractional distillation uses a column with multiple plates to separate very similar boiling points. Vacuum distillation uses reduced pressure to lower the boiling point of components. Steam distillation is used for heat-sensitive materials and allows distillation at lower temperatures.
The climbing film evaporator uses long, narrow steam-jacketed tubes to heat and evaporate liquid. As the preheated liquid rises through the tubes, bubbles form and coalesce into larger bubbles that trap liquid and rise as well. This forms a liquid film on the tube walls that rapidly vaporizes. The mixture of vapor and entrained liquid is then separated by an entrainment separator at the top, with vapor exiting and concentrated liquid collected below. Climbing film evaporators are well-suited for heat-sensitive and foaming liquids due to their short contact time and ability to break foam. However, they are also expensive to construct and maintain.
Distillation is a process that separates mixtures into individual components based on differences in their boiling points. It works by heating the mixture to vaporize components with lower boiling points, which are then cooled and condensed.
The key principles are that vapor pressure increases with temperature, allowing the lower boiling components to vaporize first. According to Raoult's law, the vapor produced will be enriched in the more volatile components compared to the liquid mixture.
There are several types of distillation including simple, fractional, vacuum, and azeotropic distillation. Simple distillation is used when components have very different boiling points while fractional distillation with multiple stages is needed for similar boiling points. Vacuum distillation lowers the
Vacuum distillation is used in oil refineries to further separate and refine the bottoms leftover from atmospheric distillation. It allows for distillation of compounds with high boiling points without thermal cracking by reducing the pressure and lowering the boiling points. Vacuum distillation units in refineries can have columns up to 14 meters wide and 50 meters tall, processing up to 25,400 cubic meters of feed per day. This additional refinement produces more valuable petroleum products from the heavier fractions of crude oil.
I found no good source for extractive distillation on the internet.So i decided to make one myself.This ppt discusses about the technology,its working and benefits.It compares extractive distillation side by side to azeotropic distillation and counts the advantages.
Slides for the eLearning course Separation and purification processes in biorefineries (https://open-learn.xamk.fi) in IMPRESS project.
Section: Distillation
Subject: 1.1 Vapor Liquid Equilibrium
Mechanism of Distillation,simple distillation steam &fractional distillation...M Swetha
Distillation is a technique used to separate liquids based on their boiling points. It involves heating a liquid mixture so that the more volatile components vaporize and pass into a condenser where they condense. Simple distillation can separate two liquids with a boiling point difference of at least 70°C, while fractional distillation uses a column with multiple plates to separate very similar boiling points. Vacuum distillation uses reduced pressure to lower the boiling point of components. Steam distillation is used for heat-sensitive materials and allows distillation at lower temperatures.
The climbing film evaporator uses long, narrow steam-jacketed tubes to heat and evaporate liquid. As the preheated liquid rises through the tubes, bubbles form and coalesce into larger bubbles that trap liquid and rise as well. This forms a liquid film on the tube walls that rapidly vaporizes. The mixture of vapor and entrained liquid is then separated by an entrainment separator at the top, with vapor exiting and concentrated liquid collected below. Climbing film evaporators are well-suited for heat-sensitive and foaming liquids due to their short contact time and ability to break foam. However, they are also expensive to construct and maintain.
Distillation is a process that separates mixtures into individual components based on differences in their boiling points. It works by heating the mixture to vaporize components with lower boiling points, which are then cooled and condensed.
The key principles are that vapor pressure increases with temperature, allowing the lower boiling components to vaporize first. According to Raoult's law, the vapor produced will be enriched in the more volatile components compared to the liquid mixture.
There are several types of distillation including simple, fractional, vacuum, and azeotropic distillation. Simple distillation is used when components have very different boiling points while fractional distillation with multiple stages is needed for similar boiling points. Vacuum distillation lowers the
Vacuum distillation is used in oil refineries to further separate and refine the bottoms leftover from atmospheric distillation. It allows for distillation of compounds with high boiling points without thermal cracking by reducing the pressure and lowering the boiling points. Vacuum distillation units in refineries can have columns up to 14 meters wide and 50 meters tall, processing up to 25,400 cubic meters of feed per day. This additional refinement produces more valuable petroleum products from the heavier fractions of crude oil.
Definition
Roult’s law
Dalton’s law
Relative volatility
Methods of distillation
Types of distillation
► Simple or Differential distillation
► Flash or Equilibrium distillation
► Rectification or Fractionations
Reflux ratio
Application of distillation
This document discusses different types of solid-liquid and liquid-liquid extraction processes. Solid-liquid extraction, also called leaching, involves removing soluble components from an insolute matrix using a solvent. It occurs through diffusion of the solvent into the solid and diffusion of the dissolved components out of the solid into the solution. Common solid-liquid extraction techniques include maceration, percolation, digestion, and countercurrent extraction using equipment like diffusion batteries, rotocel extractors, and screw extractors. Liquid-liquid extraction relies on the partition of compounds between two immiscible liquid phases. Large-scale equipment used in extraction includes mixers, towers, spray towers, and agitated columns.
Distillation is a process that separates components of a liquid mixture based on differences in their volatilities in heating and cooling processes. It involves selectively boiling the more volatile components by heating the mixture and then condensing the vapor.
There are several types of distillation including simple distillation, fractional distillation, steam distillation and vacuum distillation. Simple distillation is used to separate components with large differences in volatility, while fractional distillation allows separation of mixtures with components of similar volatility by conducting multiple distillation steps. Distillation finds applications in purification of solvents, separation of essential oils, and production of alcoholic beverages and petroleum products among others. Key aspects of distillation systems include the still, condenser and
This document discusses different types of distillation processes including simple distillation and fractional distillation. Simple distillation involves a single vaporization and condensation cycle that produces an impure distillate. Fractional distillation uses a fractionating column containing packing materials between the distillation flask and head. This allows for multiple vaporization and condensation cycles, improving separation of components in the mixture. The document describes components of distillation columns like trays, packings, reboilers and condensers and how they facilitate fractional distillation.
Different settling methods in mechanical operations Jaydrath Sindhav
Its part of sedimentation which is covered under the Mechanical operations. It contains the gravity sedimentation, clarifier and classifiers, sink and float method, gravity and sorting classifiers, differential settling methods etc....
Its just gives basic concept of sedimentation.
An overview of distillation column design concepts and major design considerations. Explains distillation column design concepts, what you would provide to a professional distillation column designer, and what you can expect back from a distillation system design firm. To speak with an engineer about your distillation column project, call EPIC at 314-207-4250.
Full Distillation technique where you find about various terminologies, its principle in which raolt's law and henry's law, assembly, classification. Distillation apparatus with their principle, advantages and disadvantages and detailed abour steam distillation and azeotropic distillation.
The document discusses various methods of leaching, which is the process of extracting soluble constituents from a solid material using a liquid solvent. It describes several common leaching techniques used in industries like food processing, pharmaceuticals, and metals extraction. These include counter-current leaching systems that improve extraction efficiency, as well as equipment used for leaching like agitated vessels, thickeners, extractors, and the Kennedy and Bollman extractors.
Slides for the eLearning course Separation and purification processes in biorefineries (https://open-learn.xamk.fi) in IMPRESS project (https://www.spire2030.eu/impress).
Section: Distillation
Subject: 1.2 Flash distillation.
Distillation is a process that separates liquid mixtures into individual fractions based on differences in boiling points. It works by heating the mixture to vaporize components with lower boiling points. There are two main types of distillation columns - batch columns which process feed intermittently, and continuous columns which process a steady stream of feed. Distillation columns contain internals like trays or packings to enhance separation, a reboiler for vaporization, a condenser to cool vapors, and a reflux drum to collect condensed liquids and provide reflux. Separation occurs due to differences in vapor pressure and relative volatility between components in the mixture.
Liquid membranes can be either immobilized liquid membranes (ILM), also called supported liquid membranes (SLM), or emulsion liquid membranes (ELM). ILMs are made by immersing a thin porous solid film with a liquid, allowing molecules to diffuse through the liquid in the pores. ELMs contain small liquid globules of one liquid suspended in another liquid medium. Liquid membranes allow separation through passive diffusion, facilitated transport using a carrier molecule, or coupled transport where the carrier couples the flow of two species. Common applications include removal of specific ions, gases, and organic compounds.
Presentation on Azeotropic and Extractive Distillation. Introduction about distillation, azeotropic and extractive distillation and the difference between them.
Filtration, cake filters & principles of cake filtration Karnav Rana
This document discusses filtration and cake filtration principles. Filtration is the separation of solids from a liquid suspension using a porous medium. In cake filtration, the suspended solids build up on the filter medium over time, forming a thicker cake with higher resistance. As the cake builds, the filtration rate decreases unless more pressure is applied. Common cake filters include filter presses, belt filters, and various types of vacuum filters that use a building cake to separate solids from liquids.
This document provides information on distillation, including definitions, applications, terminology, and different types of distillation methods. It defines distillation as a process of separating components of a liquid mixture through vaporization and condensation. Some key applications mentioned include separation of volatile oils, purification of organic solvents and drugs, and refining of petroleum products. Various distillation assembly equipment and concepts such as the still, condenser, receiver, and Raoult's law are also described. Finally, different classifications of distillation methods like simple distillation, fractional distillation, and steam distillation are briefly outlined.
Distillation is a method of separating mixtures based on differences in volatility. It involves heating a mixture to vaporize components with lower boiling points and then condensing the vapors. There are several types of distillation including simple distillation, fractional distillation, steam distillation, and destructive distillation. Fractional distillation uses a fractionating column with multiple theoretical plates to achieve high purity separations, while steam distillation uses steam to lower boiling points of heat-sensitive materials. Distillation is an important separation technique used in pharmacy, chemistry, and other fields.
Introduction to multicomponent distillationSujeet TAMBE
This document provides an introduction and overview of multicomponent distillation processes. It discusses key concepts like key components, distributed vs. undistributed components, and challenges in designing multicomponent distillation columns compared to binary systems. The document then outlines the steps of the Fenske-Underwood-Gilliland short cut design method for solving multicomponent distillation problems, including calculating the minimum number of stages, minimum reflux ratio, actual number of stages, and feed stage location.
Extraction theory involves removing soluble materials from insolids using liquid solvents. Liquid-liquid extraction is a useful method to separate components of a mixture based on differences in solubility between solvents. For example, sugar can be extracted from vegetable oil by shaking the mixture with water, as sugar is more soluble in water than oil. The partition coefficient K quantifies differences in solubility, with some compounds made more water-soluble by conversion to ionic salt forms using acid or base treatment. This allows separation of organic acid/base mixtures based on differing solubility properties.
Slides for the eLearning course Separation and purification processes in biorefineries (https://open-learn.xamk.fi) in IMPRESS project (https://www.spire2030.eu/impress).
Section: Mass transfer
Subject: 3.2 Equipment
This document provides information about different types of evaporators used to concentrate solutions. It discusses natural circulation, forced circulation, falling film, rising film, and plate evaporators. It covers key aspects like heat transfer, material and energy balances, capacity, economy, fouling, and multiple effect evaporation. The main types discussed are horizontal tube, short tube vertical, basket, long tube vertical, forced circulation, falling film, rising film, agitated thin film, and plate evaporators.
This document describes fractional distillation and cracking processes used to separate crude oil into its components. Fractional distillation uses differences in boiling points to separate a mixture by heating it into a distillation tower, where vapors condense into fractions of similar hydrocarbon chain lengths. Cracking processes like thermal cracking and catalytic cracking are then used to break larger hydrocarbon chains into more valuable shorter chains and alkenes.
Crude oil contains a mixture of hydrocarbons that can be separated using fractional distillation. This process involves heating the crude oil to vaporize the components and sending the vapor up a distillation column containing plates where the different components condense out at different temperatures based on their varying boiling points. The end result is separated fractions of useful products like gasoline, kerosene, and diesel fuel that are extracted from the crude oil.
Definition
Roult’s law
Dalton’s law
Relative volatility
Methods of distillation
Types of distillation
► Simple or Differential distillation
► Flash or Equilibrium distillation
► Rectification or Fractionations
Reflux ratio
Application of distillation
This document discusses different types of solid-liquid and liquid-liquid extraction processes. Solid-liquid extraction, also called leaching, involves removing soluble components from an insolute matrix using a solvent. It occurs through diffusion of the solvent into the solid and diffusion of the dissolved components out of the solid into the solution. Common solid-liquid extraction techniques include maceration, percolation, digestion, and countercurrent extraction using equipment like diffusion batteries, rotocel extractors, and screw extractors. Liquid-liquid extraction relies on the partition of compounds between two immiscible liquid phases. Large-scale equipment used in extraction includes mixers, towers, spray towers, and agitated columns.
Distillation is a process that separates components of a liquid mixture based on differences in their volatilities in heating and cooling processes. It involves selectively boiling the more volatile components by heating the mixture and then condensing the vapor.
There are several types of distillation including simple distillation, fractional distillation, steam distillation and vacuum distillation. Simple distillation is used to separate components with large differences in volatility, while fractional distillation allows separation of mixtures with components of similar volatility by conducting multiple distillation steps. Distillation finds applications in purification of solvents, separation of essential oils, and production of alcoholic beverages and petroleum products among others. Key aspects of distillation systems include the still, condenser and
This document discusses different types of distillation processes including simple distillation and fractional distillation. Simple distillation involves a single vaporization and condensation cycle that produces an impure distillate. Fractional distillation uses a fractionating column containing packing materials between the distillation flask and head. This allows for multiple vaporization and condensation cycles, improving separation of components in the mixture. The document describes components of distillation columns like trays, packings, reboilers and condensers and how they facilitate fractional distillation.
Different settling methods in mechanical operations Jaydrath Sindhav
Its part of sedimentation which is covered under the Mechanical operations. It contains the gravity sedimentation, clarifier and classifiers, sink and float method, gravity and sorting classifiers, differential settling methods etc....
Its just gives basic concept of sedimentation.
An overview of distillation column design concepts and major design considerations. Explains distillation column design concepts, what you would provide to a professional distillation column designer, and what you can expect back from a distillation system design firm. To speak with an engineer about your distillation column project, call EPIC at 314-207-4250.
Full Distillation technique where you find about various terminologies, its principle in which raolt's law and henry's law, assembly, classification. Distillation apparatus with their principle, advantages and disadvantages and detailed abour steam distillation and azeotropic distillation.
The document discusses various methods of leaching, which is the process of extracting soluble constituents from a solid material using a liquid solvent. It describes several common leaching techniques used in industries like food processing, pharmaceuticals, and metals extraction. These include counter-current leaching systems that improve extraction efficiency, as well as equipment used for leaching like agitated vessels, thickeners, extractors, and the Kennedy and Bollman extractors.
Slides for the eLearning course Separation and purification processes in biorefineries (https://open-learn.xamk.fi) in IMPRESS project (https://www.spire2030.eu/impress).
Section: Distillation
Subject: 1.2 Flash distillation.
Distillation is a process that separates liquid mixtures into individual fractions based on differences in boiling points. It works by heating the mixture to vaporize components with lower boiling points. There are two main types of distillation columns - batch columns which process feed intermittently, and continuous columns which process a steady stream of feed. Distillation columns contain internals like trays or packings to enhance separation, a reboiler for vaporization, a condenser to cool vapors, and a reflux drum to collect condensed liquids and provide reflux. Separation occurs due to differences in vapor pressure and relative volatility between components in the mixture.
Liquid membranes can be either immobilized liquid membranes (ILM), also called supported liquid membranes (SLM), or emulsion liquid membranes (ELM). ILMs are made by immersing a thin porous solid film with a liquid, allowing molecules to diffuse through the liquid in the pores. ELMs contain small liquid globules of one liquid suspended in another liquid medium. Liquid membranes allow separation through passive diffusion, facilitated transport using a carrier molecule, or coupled transport where the carrier couples the flow of two species. Common applications include removal of specific ions, gases, and organic compounds.
Presentation on Azeotropic and Extractive Distillation. Introduction about distillation, azeotropic and extractive distillation and the difference between them.
Filtration, cake filters & principles of cake filtration Karnav Rana
This document discusses filtration and cake filtration principles. Filtration is the separation of solids from a liquid suspension using a porous medium. In cake filtration, the suspended solids build up on the filter medium over time, forming a thicker cake with higher resistance. As the cake builds, the filtration rate decreases unless more pressure is applied. Common cake filters include filter presses, belt filters, and various types of vacuum filters that use a building cake to separate solids from liquids.
This document provides information on distillation, including definitions, applications, terminology, and different types of distillation methods. It defines distillation as a process of separating components of a liquid mixture through vaporization and condensation. Some key applications mentioned include separation of volatile oils, purification of organic solvents and drugs, and refining of petroleum products. Various distillation assembly equipment and concepts such as the still, condenser, receiver, and Raoult's law are also described. Finally, different classifications of distillation methods like simple distillation, fractional distillation, and steam distillation are briefly outlined.
Distillation is a method of separating mixtures based on differences in volatility. It involves heating a mixture to vaporize components with lower boiling points and then condensing the vapors. There are several types of distillation including simple distillation, fractional distillation, steam distillation, and destructive distillation. Fractional distillation uses a fractionating column with multiple theoretical plates to achieve high purity separations, while steam distillation uses steam to lower boiling points of heat-sensitive materials. Distillation is an important separation technique used in pharmacy, chemistry, and other fields.
Introduction to multicomponent distillationSujeet TAMBE
This document provides an introduction and overview of multicomponent distillation processes. It discusses key concepts like key components, distributed vs. undistributed components, and challenges in designing multicomponent distillation columns compared to binary systems. The document then outlines the steps of the Fenske-Underwood-Gilliland short cut design method for solving multicomponent distillation problems, including calculating the minimum number of stages, minimum reflux ratio, actual number of stages, and feed stage location.
Extraction theory involves removing soluble materials from insolids using liquid solvents. Liquid-liquid extraction is a useful method to separate components of a mixture based on differences in solubility between solvents. For example, sugar can be extracted from vegetable oil by shaking the mixture with water, as sugar is more soluble in water than oil. The partition coefficient K quantifies differences in solubility, with some compounds made more water-soluble by conversion to ionic salt forms using acid or base treatment. This allows separation of organic acid/base mixtures based on differing solubility properties.
Slides for the eLearning course Separation and purification processes in biorefineries (https://open-learn.xamk.fi) in IMPRESS project (https://www.spire2030.eu/impress).
Section: Mass transfer
Subject: 3.2 Equipment
This document provides information about different types of evaporators used to concentrate solutions. It discusses natural circulation, forced circulation, falling film, rising film, and plate evaporators. It covers key aspects like heat transfer, material and energy balances, capacity, economy, fouling, and multiple effect evaporation. The main types discussed are horizontal tube, short tube vertical, basket, long tube vertical, forced circulation, falling film, rising film, agitated thin film, and plate evaporators.
This document describes fractional distillation and cracking processes used to separate crude oil into its components. Fractional distillation uses differences in boiling points to separate a mixture by heating it into a distillation tower, where vapors condense into fractions of similar hydrocarbon chain lengths. Cracking processes like thermal cracking and catalytic cracking are then used to break larger hydrocarbon chains into more valuable shorter chains and alkenes.
Crude oil contains a mixture of hydrocarbons that can be separated using fractional distillation. This process involves heating the crude oil to vaporize the components and sending the vapor up a distillation column containing plates where the different components condense out at different temperatures based on their varying boiling points. The end result is separated fractions of useful products like gasoline, kerosene, and diesel fuel that are extracted from the crude oil.
Fractional distillation is a method to separate mixtures with different boiling points. It has been used since ancient times by Greek alchemists and in China during the Han dynasty. The process works by heating a mixture so it forms vapors, which rise up a fractional distillation column and condense based on their boiling points. Common uses are separating crude oil into hydrocarbon products like gasoline and separating chemicals in a lab. Current research is improving efficiency and applications in areas like oil refining.
Distillation is the most common separation technique that involves evaporating and condensing components of a liquid mixture to separate them based on differences in their boiling points. It consumes large amounts of energy for heating and cooling. Fractional distillation uses a fractionating column and refluxing to improve separation efficiency compared to simple distillation. Various parameters like reflux ratio, pressure, temperature controls are optimized to achieve desired purities and specifications of fractions in a distillation column. Stripping steam is also used to help separate lighter components from heavier fractions.
Fractional distillation is a process that separates mixtures into their individual parts or fractions by heating them to the boiling point of each component and condensing the vapors, allowing different chemical compounds to be isolated based on their differing volatility and boiling points. It involves heating a substance to the point where its components vaporize and then cooling the vapors to condense them back into liquid form, with the heavier fractions requiring higher temperatures to vaporize collecting lower in the distillation apparatus.
Distillation is a technique used to separate compounds based on differences in their boiling points. It involves heating a liquid mixture until it evaporates, then cooling the vapors to condense them back into separate liquids. Simple distillation is used when the boiling points are more than 40°C apart, while fractional distillation is needed for closer boiling points and allows for a more efficient separation. The key aspects of distillation setups are a round bottom flask for heating the mixture, a condenser to cool the vapors, and sometimes a fractionating column to promote multiple vaporizations during fractional distillation.
1) Distillation is a method used to separate components of a liquid solution based on differences in how the components distribute between the vapor and liquid phases when heated to their boiling points.
2) Raoult's law describes vapor-liquid equilibrium for ideal solutions, relating the partial pressure of a component in vapor phase to its mole fraction in the liquid phase. Boiling point diagrams can be constructed using vapor pressure data.
3) Equilibrium or flash distillation involves heating a liquid mixture to partially vaporize it in a single stage, separating the vapor and liquid which approach equilibrium compositions.
Distillation is a process that separates mixtures into their component parts based on differences in volatility. It works by heating the mixture to vaporize the more volatile components, which are then condensed and captured separately from the less volatile components. There are several types including batch, continuous, fractional, vacuum, and zone distillation. The efficiency of distillation can be measured by assessing the purity of separated components over time. Distillation has many industrial and commercial applications such as in oil refining, producing purified gases and solvents, separating fermentation products, and more.
Gea evaporation technology-brochure_en_tcm11-16319hung do
The document discusses GEA Wiegand's research and development center for evaporation technology. The R&D center contains numerous laboratory and pilot plants used to test over 3,000 product categories in different evaporator types. Certain pilot plants can be installed at customer sites. Data is collected and plant behavior is modeled using computer programs.
Distillation is a method to separate mixtures based on differences in volatility. It involves boiling the mixture and condensing the vapor produced. Simple distillation produces an impure distillate while fractional distillation uses a fractionating column for multiple vaporization-condensation cycles, allowing better separation. Vacuum distillation uses reduced pressure for distillation at lower temperatures to prevent degradation. Batch distillation processes mixtures in batches while continuous distillation constantly feeds and removes fractions.
- Distillation is a process that separates mixtures based on differences in boiling points. It involves heating a liquid mixture to form vapors, condensing the vapors back to liquid, and collecting the purified liquid fractions.
- There are several types of distillation including simple, steam, fractional, and vacuum distillation which vary based on conditions and mixtures separated.
- A laboratory experiment demonstrates simple distillation to separate ethanol and water using common distillation equipment like a round bottom flask, condenser, and receiver flask. The mixture is heated to form vapors that condense and drip into the collection flask.
Pharma Mfg BASICS for new learners useful informationraviralagiri02
Unit processes involve chemical changes through chemical reactions, while unit operations involve physical changes without chemical reactions. Common unit operations include separation, size reduction, heating and cooling. A batch process involves intermittent operation where materials are added and removed at different stages, while a continuous process operates continuously with constant feeding and removal of materials. Safety measures for working with reactors include proper earthing, not overfilling reactors, not exceeding agitator speed limits, and preventing sparks.
Paper 5 iven li Energy Efficiency Improvement and Cost-Saving for Oilseeds p...pakistanoilseeds
This document discusses various methods to improve energy efficiency and reduce costs in oilseed processing. It proposes 10 technical solutions to reduce steam consumption, including a force-draining extractor design to reduce solvent carryover in spent meal by 20%, and a DT vapor heat exchanger to pre-heat fresh solvent. Overall implementation could save over 20 kg of steam per ton of seeds processed through reduced drying needs and equipment downsizing. The document also analyzes solvent consumption and outlines measures like improved vent air control to minimize losses.
Distillation is one of unit operation which is uses for separation of two or more liquids which have difference in boiling points. Basic theory and calculation of Distillation which will help to understand Distillation and stage calculation. it will be helpful for students who are studying chemical engineering and fresh engineers in chemical process industries.
This document discusses different types of distillation processes used to separate liquid mixtures based on volatility. It focuses on the design and components of distillation columns. Distillation processes separate mixtures through evaporation and condensation, and include simple, fractional, vacuum, and steam distillation. A distillation column consists of a vertical shell containing internal trays or packings to facilitate separation, and components like a condenser, reboiler, and reflux drum. The condenser converts vapors into liquid, the reboiler generates vapors from the column bottom, and the reflux drum holds condensed vapors to recirculate liquid back up the column.
Steam distillation and azeotropic distillation are separation processes.
Steam distillation uses steam to distill temperature sensitive compounds like essential oils at lower temperatures to prevent decomposition. It produces a mixture of water and organic distillate that can be separated.
Azeotropic distillation uses an entrainer added to the original mixture to form a new azeotrope that distills off, allowing separation of the original components which could not be separated otherwise due to forming an azeotrope. Both processes exploit differences in volatility between mixture components to achieve separation.
The equipment used to remove water from the food product is called evaporator.
A food dehydrator refers to a device that removes moisture from food to aid in its preservation. A food dehydrator uses a heat source and air flow to reduce the water content of foods.
Distillation is a method of separating mixtures based on differences in their volatilities through boiling and condensation. Key points:
- It involves heating a mixture to vaporize more volatile components, cooling to condense the vapor into separate products.
- Common uses include separating crude oil, purifying water and air, producing alcoholic beverages.
- Types include simple, fractional, flash, and vacuum distillation. Flash distillation partially vaporizes a liquid through pressure reduction.
- Distillation columns contain internals like trays or packings to facilitate vapor-liquid contact during separation. Fractional distillation uses multiple equilibrium stages for high purity products.
The document discusses evaporation as a unit operation used to concentrate solutions by removing water or other volatile solvent. It describes different types of evaporators used for this purpose, including batch pans, rising film evaporators, falling film evaporators, and multiple effect evaporators. The key components and working principles of evaporators are explained. Specific examples of evaporation applications are also provided.
The document discusses retort packaging and processing. It defines sterilization and describes the key components of retort packaging including retorts, retort pouches, and retort operations. It discusses the different types of retorts and retort pouches as well as the materials used to construct retort pouches. The document also summarizes the advantages of retort packaging and some common products packaged using this method.
UNIT OPERATIONS (unit 2) pharmaceutical process chemistrySaketChoudhary13
its a presentation on the 2nd unit of pharmaceutical process chemistry which include extraction ,filtration and steam distillation and azeotropic distillation
Unit operations involve physical changes or chemical transformations such as separation, crystallization, evaporation, and filtration. Extraction is defined as treating plant or animal tissues with a solvent to dissolve active constituents. Common extraction methods include maceration, percolation, decoction, digestion, and infusion. Filtration separates solids from fluids using a porous medium, with pressure filtration employing increased pressure. Distillation techniques like azeotropic distillation and steam distillation allow separation of compounds that form azeotropes or are heat sensitive.
RETORT PROCESSING BY Dr.P.RAJKUMAR-HOD (F&PE)kurinchisiva
The document discusses retort packaging and processing. It defines retort as a closed chamber that can withstand high temperatures and pressures used for sterilization. It describes the various types of retorts including batch, continuous, steam, water spray, and agitating retorts. It also discusses retort pouches, their construction and materials, products packaged in pouches, and the advantages of retort packaging over other methods.
This document discusses methods for freezing and preserving food, including chilling, refrigeration, and different types of freezing. It explains that freezing food involves removing heat to slow microbial growth. Various freezing techniques are covered, such as air blast freezing, tunnel freezing, belt freezing, fluidized bed freezing, contact freezing using plates or immersion, and cryogenic freezing using liquid nitrogen or carbon dioxide. Factors like ingredients, food preparation, packaging, and freezing time are also addressed in the document.
This slide consists of the definition, parts, and functions, and the principle of the rotary evaporator. Besides this, I also added why we using a rotary evaporator and the comparison between a rotary evaporator and a lyophilizer.
This document discusses distillation systems and processes. It begins by defining distillation as a process that separates liquid or vapor mixtures into purified components by applying and removing heat. It then describes the basic concepts of vapor pressure and how boiling occurs when vapor pressure equals atmospheric pressure. Various types of distillation systems and processes are outlined, including simple, fractional, steam, vacuum, extractive, and azeotropic distillation. Key aspects like batch vs continuous operation and different column internals are also summarized.
Event Report - SAP Sapphire 2024 Orlando - lots of innovation and old challengesHolger Mueller
Holger Mueller of Constellation Research shares his key takeaways from SAP's Sapphire confernece, held in Orlando, June 3rd till 5th 2024, in the Orange Convention Center.
Part 2 Deep Dive: Navigating the 2024 Slowdownjeffkluth1
Introduction
The global retail industry has weathered numerous storms, with the financial crisis of 2008 serving as a poignant reminder of the sector's resilience and adaptability. However, as we navigate the complex landscape of 2024, retailers face a unique set of challenges that demand innovative strategies and a fundamental shift in mindset. This white paper contrasts the impact of the 2008 recession on the retail sector with the current headwinds retailers are grappling with, while offering a comprehensive roadmap for success in this new paradigm.
Building Your Employer Brand with Social MediaLuanWise
Presented at The Global HR Summit, 6th June 2024
In this keynote, Luan Wise will provide invaluable insights to elevate your employer brand on social media platforms including LinkedIn, Facebook, Instagram, X (formerly Twitter) and TikTok. You'll learn how compelling content can authentically showcase your company culture, values, and employee experiences to support your talent acquisition and retention objectives. Additionally, you'll understand the power of employee advocacy to amplify reach and engagement – helping to position your organization as an employer of choice in today's competitive talent landscape.
Understanding User Needs and Satisfying ThemAggregage
https://www.productmanagementtoday.com/frs/26903918/understanding-user-needs-and-satisfying-them
We know we want to create products which our customers find to be valuable. Whether we label it as customer-centric or product-led depends on how long we've been doing product management. There are three challenges we face when doing this. The obvious challenge is figuring out what our users need; the non-obvious challenges are in creating a shared understanding of those needs and in sensing if what we're doing is meeting those needs.
In this webinar, we won't focus on the research methods for discovering user-needs. We will focus on synthesis of the needs we discover, communication and alignment tools, and how we operationalize addressing those needs.
Industry expert Scott Sehlhorst will:
• Introduce a taxonomy for user goals with real world examples
• Present the Onion Diagram, a tool for contextualizing task-level goals
• Illustrate how customer journey maps capture activity-level and task-level goals
• Demonstrate the best approach to selection and prioritization of user-goals to address
• Highlight the crucial benchmarks, observable changes, in ensuring fulfillment of customer needs
The Evolution and Impact of OTT Platforms: A Deep Dive into the Future of Ent...ABHILASH DUTTA
This presentation provides a thorough examination of Over-the-Top (OTT) platforms, focusing on their development and substantial influence on the entertainment industry, with a particular emphasis on the Indian market.We begin with an introduction to OTT platforms, defining them as streaming services that deliver content directly over the internet, bypassing traditional broadcast channels. These platforms offer a variety of content, including movies, TV shows, and original productions, allowing users to access content on-demand across multiple devices.The historical context covers the early days of streaming, starting with Netflix's inception in 1997 as a DVD rental service and its transition to streaming in 2007. The presentation also highlights India's television journey, from the launch of Doordarshan in 1959 to the introduction of Direct-to-Home (DTH) satellite television in 2000, which expanded viewing choices and set the stage for the rise of OTT platforms like Big Flix, Ditto TV, Sony LIV, Hotstar, and Netflix. The business models of OTT platforms are explored in detail. Subscription Video on Demand (SVOD) models, exemplified by Netflix and Amazon Prime Video, offer unlimited content access for a monthly fee. Transactional Video on Demand (TVOD) models, like iTunes and Sky Box Office, allow users to pay for individual pieces of content. Advertising-Based Video on Demand (AVOD) models, such as YouTube and Facebook Watch, provide free content supported by advertisements. Hybrid models combine elements of SVOD and AVOD, offering flexibility to cater to diverse audience preferences.
Content acquisition strategies are also discussed, highlighting the dual approach of purchasing broadcasting rights for existing films and TV shows and investing in original content production. This section underscores the importance of a robust content library in attracting and retaining subscribers.The presentation addresses the challenges faced by OTT platforms, including the unpredictability of content acquisition and audience preferences. It emphasizes the difficulty of balancing content investment with returns in a competitive market, the high costs associated with marketing, and the need for continuous innovation and adaptation to stay relevant.
The impact of OTT platforms on the Bollywood film industry is significant. The competition for viewers has led to a decrease in cinema ticket sales, affecting the revenue of Bollywood films that traditionally rely on theatrical releases. Additionally, OTT platforms now pay less for film rights due to the uncertain success of films in cinemas.
Looking ahead, the future of OTT in India appears promising. The market is expected to grow by 20% annually, reaching a value of ₹1200 billion by the end of the decade. The increasing availability of affordable smartphones and internet access will drive this growth, making OTT platforms a primary source of entertainment for many viewers.
Storytelling is an incredibly valuable tool to share data and information. To get the most impact from stories there are a number of key ingredients. These are based on science and human nature. Using these elements in a story you can deliver information impactfully, ensure action and drive change.
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Unveiling the Dynamic Personalities, Key Dates, and Horoscope Insights: Gemin...my Pandit
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Top mailing list providers in the USA.pptxJeremyPeirce1
Discover the top mailing list providers in the USA, offering targeted lists, segmentation, and analytics to optimize your marketing campaigns and drive engagement.
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Multiple new technologies have emerged, but Samsara and C3.ai are only two companies which have gone public so far.
Manufacturing startups constitute the largest pipeline share of unicorns and IPO candidates in the SF Bay Area, and software startups dominate in Germany.
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Discover timeless style with the 2022 Vintage Roman Numerals Men's Ring. Crafted from premium stainless steel, this 6mm wide ring embodies elegance and durability. Perfect as a gift, it seamlessly blends classic Roman numeral detailing with modern sophistication, making it an ideal accessory for any occasion.
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Taurus Zodiac Sign: Unveiling the Traits, Dates, and Horoscope Insights of th...my Pandit
Dive into the steadfast world of the Taurus Zodiac Sign. Discover the grounded, stable, and logical nature of Taurus individuals, and explore their key personality traits, important dates, and horoscope insights. Learn how the determination and patience of the Taurus sign make them the rock-steady achievers and anchors of the zodiac.
Navigating the world of forex trading can be challenging, especially for beginners. To help you make an informed decision, we have comprehensively compared the best forex brokers in India for 2024. This article, reviewed by Top Forex Brokers Review, will cover featured award winners, the best forex brokers, featured offers, the best copy trading platforms, the best forex brokers for beginners, the best MetaTrader brokers, and recently updated reviews. We will focus on FP Markets, Black Bull, EightCap, IC Markets, and Octa.
2. Fractional distillation is one of the widely used
distillation technique used in R & D sector because
of its efficiency and accuracy.
It is more efficient in separating ideal solutions
into their pure components than the traitional
method of distillation
3. Heat Source for e.g a hot plate with a bath
A distillation flask (preferably a round-bottom flask)
A collecting flask ( conical shaped or round-bottom flask)
Fractionating column ( elongated glass ware for solvent
cooling)
Distillation head
Thermometer (to measure the temperature of the solvent
placed)
Condenser
Vaccumed Adapter (to carry out distillations under reduced
pressure)
Boiling chips or Anti-bumping granules
Rubber bungs, unless laboratory glassware with ground
4. Purification of water and ethanol mixture is
usually carried in the research labs
The separation of ethanol and water is based upon
the different boiling point of the two solvent.
Ethanol require boiling point of 78.5 ° water boils
at a temperature of 100 degree Celsius
Boiling the mixture in fractional distillation
column separates the liquid into its respective
components
Usaully 96% of pure ethanol is extracted by
fractional distillation technique
5. Similarly various other Azeotropic mixture can be
extracted using fractional distillation technique
such as a mixture of cyclohexane and toluene, etc.
Fractional Distillation has gained a wider
application in scientific research laboratories and
in industrial application to extract the pure form of
solvent from its solvent mixture