Differential thermal analysis (DTA) measures the temperature difference between a sample and a reference material as both are heated. The apparatus consists of a sample holder with thermocouples, a furnace, temperature programmer, and recording system. The sample and reference are placed in identical cavities in a heating block within an oven. Thermocouples contact each to measure any temperature difference. Changes appear as endothermic or exothermic curves on a graph. DTA allows accurate determination of transition temperatures and is highly sensitive even at very high temperatures.