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Internal quality control
Soil-Agrochemistry laboratory of
Plant and Agriculture Science
Institute
Mongolia
Do you have and use an internal quality control
system
i.e. do you have a set of rules to detect analytical errors
within your laboratory?
YES
If yes, are these rules written?
YES(lab manual but old one, so we need change it)
If yes, how often to you use your internal
quality control system?
Every new analitical bach
What are the characteristics of the material
used for quality control (QC)?
What kind of material is used to perform the quality control?
Чанарын хяналтыг гүйцэтгэхэд ямар төрлийн материал
ашигладаг вэ?
- natural soils? YES
- synthetic material? NO
- chemicals? NO
Is the material used for QC:
- prepared by yourself ? YES (Internal Control)
- prepared out of the laboratory ? YES (External Control)
- bought to a company as a certified reference material ?
NO
Analysis of the control material
Are you using the control material for all your analytical parameters? NO
If 'NO' are you using it for:
- pH YES
- P2O5 YES
- K2O YES
- NO3 YES
- Carbon/ Humus YES
- Ca/ Mg YES
- etc. (please make the list of the top ten analysis according to on line
survey) YES/NO
How often do you analyze your control material?
- in every analytical batch YES
- once a month YES
Comparison of control material results to
specific statistical limits
Do you have a data base where the control material results are collected?
NO (but we have all results written in the lab journals)
Are you using quality charts to plot your results (like in the figure
attached this email)?
YES
Can you show an example of quality control chart obtained in your
laboratory?
YES
How do you determine the specific statistical limits for
acceptable/rejection limits? Please describe it shortly or provide the statistical
test
Action after a negative results
for quality control
• If the quality control procedure indicates a failure (results out the statistical limits),
what do you do? Please explain shortly the procedure
• Standard soil prepared by laboratory staff we are used as an
internal reference. We took sample many years ago before
cultivating soil (ploughing) and use in the laboratory and to
compare how soil nutrient content have to changing.
• We also including duplicates (more than 2) of each set of
samples and checks between sets of samples
• If the quality control procedure indicates a failure, we
repeated the analysis .
Staff qualification
Is there a quality control officer to look into the quality of the results?
Officialy NO but lab in charge Mrs Bayasgalan (Agronomy)
If YES, did she/he get some special training to do this control?
NO (only head of departments participated special training two time )
If YES, please provide some short information on the type of training she/he received
Does she/he continue to be trained on a regular basis?
YES ( Mrs Bayasgalan was regularly practices in the lab and she trains to other
lab staffs. Now she is waiting to participate the special training)
If YES, please provide information on the frequency and duration of the training
Training organizing a 4 time for year in Mongolia
Standart solution
¹
Number 1 2 3 4 5 6 7
1
Standart solution,ìë 0 2.0 4.0 6.0 8.0 10.0 20.0
2
P 2O5 , mg 0 0.02 0.04 0.06 0.08 0.10 0.20
Establishing a calibration curve
0.1917ã (KH2 PO4)+ 1 l DW and diluted 10 times
Examples coming from our lab
Examples coming from our lab
Thanks for your
attention

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Countries’ presentation on internal quality control: Mongolia

  • 1. Internal quality control Soil-Agrochemistry laboratory of Plant and Agriculture Science Institute Mongolia
  • 2. Do you have and use an internal quality control system i.e. do you have a set of rules to detect analytical errors within your laboratory? YES If yes, are these rules written? YES(lab manual but old one, so we need change it) If yes, how often to you use your internal quality control system? Every new analitical bach
  • 3. What are the characteristics of the material used for quality control (QC)? What kind of material is used to perform the quality control? Чанарын хяналтыг гүйцэтгэхэд ямар төрлийн материал ашигладаг вэ? - natural soils? YES - synthetic material? NO - chemicals? NO Is the material used for QC: - prepared by yourself ? YES (Internal Control) - prepared out of the laboratory ? YES (External Control) - bought to a company as a certified reference material ? NO
  • 4. Analysis of the control material Are you using the control material for all your analytical parameters? NO If 'NO' are you using it for: - pH YES - P2O5 YES - K2O YES - NO3 YES - Carbon/ Humus YES - Ca/ Mg YES - etc. (please make the list of the top ten analysis according to on line survey) YES/NO How often do you analyze your control material? - in every analytical batch YES - once a month YES
  • 5. Comparison of control material results to specific statistical limits Do you have a data base where the control material results are collected? NO (but we have all results written in the lab journals) Are you using quality charts to plot your results (like in the figure attached this email)? YES Can you show an example of quality control chart obtained in your laboratory? YES How do you determine the specific statistical limits for acceptable/rejection limits? Please describe it shortly or provide the statistical test
  • 6. Action after a negative results for quality control • If the quality control procedure indicates a failure (results out the statistical limits), what do you do? Please explain shortly the procedure • Standard soil prepared by laboratory staff we are used as an internal reference. We took sample many years ago before cultivating soil (ploughing) and use in the laboratory and to compare how soil nutrient content have to changing. • We also including duplicates (more than 2) of each set of samples and checks between sets of samples • If the quality control procedure indicates a failure, we repeated the analysis .
  • 7. Staff qualification Is there a quality control officer to look into the quality of the results? Officialy NO but lab in charge Mrs Bayasgalan (Agronomy) If YES, did she/he get some special training to do this control? NO (only head of departments participated special training two time ) If YES, please provide some short information on the type of training she/he received Does she/he continue to be trained on a regular basis? YES ( Mrs Bayasgalan was regularly practices in the lab and she trains to other lab staffs. Now she is waiting to participate the special training) If YES, please provide information on the frequency and duration of the training Training organizing a 4 time for year in Mongolia
  • 8. Standart solution ¹ Number 1 2 3 4 5 6 7 1 Standart solution,ìë 0 2.0 4.0 6.0 8.0 10.0 20.0 2 P 2O5 , mg 0 0.02 0.04 0.06 0.08 0.10 0.20 Establishing a calibration curve 0.1917ã (KH2 PO4)+ 1 l DW and diluted 10 times