IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
The roles of process parameters on structures and mechanical properties of po...Bambang Afrinaldi
Process parameters are crucial to produce targeted qualities in polypropylene (PP)/clay nanocomposites, due to their roles on the generation of shear and diffusion. Thus, this research aims to observe their effects on structures and properties of PP/clay nanocomposites. Samples were produced by mixing PP, PP grafting maleic anhydride (PP-gMA), and Cloisite 20A at fixed compositions, 88/9/3 wt%, respectively, in an internal mixer with variations on temperatures (210, 220, 230 °C) and speeds (60, 80, 100 rpm). Effect of mixing parameters on nanocomposite structures and properties were investigated from XRD, SEM and flexural properties. The results showed that all samples had intercalated as well as agglomerated structures. Further analysis on XRD and SEM showed that samples produced at
high conditions (230C or 100 rpm) had similar structures. In contrast, low setting sample (210C and 60 rpm), despite its similarity on dispersion level, had longer agglomerates than that of mixed at high settings. Correlated both increase of d-spacing and agglomerates length to flexural properties suggested that modulus was more influenced by dispersion level, while strength
was affected by agglomerates. However, it was worth to note that improvement on dspacing, with availability of long agglomerates might not guarantee modulus and strength improvement due to low interfacial bonding.
Dry Sliding Wear Behavior of Glass and Jute Fiber Hybrid Reinforced Epoxy Com...IJERD Editor
Glass Fiber reinforced composites are emerging as a potential material for a wide variety of
industrial applications owing to their good combination of physical and mechanical properties. In recent
decades, glass fiber composites parts are widely used as sliding components in different engineering
applications. Due to the legitimate theoretical and practical importance, the study of tribological performance of
these emerging materials becomes highly decisive. In the present research initiative, two type of reinforcements
are selected there are Glass and jute fibers with matrix of epoxy 551 was used for composite specimen
preparation. The frictional and wear characteristics of the developed composites have been studied under
different sliding conditions. From the results it is conclude that jute is more efficient in improving the
tribological Performance of glass-epoxy composites than the raw glass fiber reinforced epoxy composites.
The roles of process parameters on structures and mechanical properties of po...Bambang Afrinaldi
Process parameters are crucial to produce targeted qualities in polypropylene (PP)/clay nanocomposites, due to their roles on the generation of shear and diffusion. Thus, this research aims to observe their effects on structures and properties of PP/clay nanocomposites. Samples were produced by mixing PP, PP grafting maleic anhydride (PP-gMA), and Cloisite 20A at fixed compositions, 88/9/3 wt%, respectively, in an internal mixer with variations on temperatures (210, 220, 230 °C) and speeds (60, 80, 100 rpm). Effect of mixing parameters on nanocomposite structures and properties were investigated from XRD, SEM and flexural properties. The results showed that all samples had intercalated as well as agglomerated structures. Further analysis on XRD and SEM showed that samples produced at
high conditions (230C or 100 rpm) had similar structures. In contrast, low setting sample (210C and 60 rpm), despite its similarity on dispersion level, had longer agglomerates than that of mixed at high settings. Correlated both increase of d-spacing and agglomerates length to flexural properties suggested that modulus was more influenced by dispersion level, while strength
was affected by agglomerates. However, it was worth to note that improvement on dspacing, with availability of long agglomerates might not guarantee modulus and strength improvement due to low interfacial bonding.
Dry Sliding Wear Behavior of Glass and Jute Fiber Hybrid Reinforced Epoxy Com...IJERD Editor
Glass Fiber reinforced composites are emerging as a potential material for a wide variety of
industrial applications owing to their good combination of physical and mechanical properties. In recent
decades, glass fiber composites parts are widely used as sliding components in different engineering
applications. Due to the legitimate theoretical and practical importance, the study of tribological performance of
these emerging materials becomes highly decisive. In the present research initiative, two type of reinforcements
are selected there are Glass and jute fibers with matrix of epoxy 551 was used for composite specimen
preparation. The frictional and wear characteristics of the developed composites have been studied under
different sliding conditions. From the results it is conclude that jute is more efficient in improving the
tribological Performance of glass-epoxy composites than the raw glass fiber reinforced epoxy composites.
Study of mechanical and morphological properties of glass fiber reinforced mo...eSAT Journals
Abstract Polymethylmethacrylate and Poly (acrylonitrile-co-butadiene) rubber were used to modify Diglycidyl ether of bisphenol A (DGEBA) type epoxy resin and cured with stoichiometric quantities of the hardener 4,4’ diamino dipheny methane. This modified epoxy resin was used as the matrix for the preparation of glass fiber reinforced composites. E- Glass fiber was used as fiber reinforcement. The morphology and mechanical properties of the composite analysed. Morphological analysis of the fractured surface of the composites indicated good adhesion between the matrix polymer and the glass fibers. Hence an enhancement in mechanical properties of the composite such as tensile, flexural, impact and fracture toughness has been observed as there has been an effective transfer of the load from the matrix to the fiber. Hence these composites which exhibit high toughness, strength and dimensional stability can be envisaged to provide valuable contribution to high performance structural applications. Keywords: Glass composites, mechanical properties, modified epoxy matrix, morphology and ternary blend
Experimental Behaviour of Steel Fiber Reinforced Concrete with partial Replac...ijtsrd
Concrete is generally used due to the abundance of uncooked material, low manufacturing and protection cost, excellence in compression, corrosion aspects, and versatility in forming more than a few shapes and its limitless structural purposes in aggregate with metal reinforcement. All these elements have contributed pressures to decrease cement consumption and to intensify lookup in exploring the probabilities of improving strength, sturdiness and corrosion discount via the use of pozzolonas as supplementary cementing materials. Fibre bolstered concrete FRC is a fibre reinforcing cementitious concrete composite, and by way of including discrete brief fibres randomly in concrete it famous many appreciably multiplied engineering residences It is manufactured from kaolin which makes the concrete extra long lasting and ecofriendly. In the current investigation mechanical residences of concrete containing each Fly ash and Metakaolin at a number of combos are studied. For the a range of mixtures of Fly ash and Metakaolin, cubes cylindrical and prism specimens are casted with 1 of fibres and the compression strength, break up tensile energy and flexural energy take a look at consequences are got and in contrast with the traditional combine having 1 fibres. It is thereby counseled that utilization of these cementitious substances in concrete will decrease the requirement for cement thereby marching in the direction of green construction. M. Sankaran | Dr. M. Gunasekaran | M. Loganathan "Experimental Behaviour of Steel Fiber Reinforced Concrete with partial Replacement of Fly Ash & Metakaolin" Published in International Journal of Trend in Scientific Research and Development (ijtsrd), ISSN: 2456-6470, Volume-4 | Issue-5 , August 2020, URL: https://www.ijtsrd.com/papers/ijtsrd33163.pdf Paper Url :https://www.ijtsrd.com/engineering/civil-engineering/33163/experimental-behaviour-of-steel-fiber-reinforced-concrete-with-partial-replacement-of-fly-ash-and-metakaolin/m-sankaran
Mechanical Characterization of Bio-Char Made Hybrid CompositeIJERA Editor
Material discoveries and development have always been the cause of the growth and development of a nation
and the need of naturally made materials is the need of hours. Thus this paper takes you to the development of a
hybrid composite made of sisal fiber with epoxy as the matrix intertwined with softwood bio-char. Softwood
chip bio-char, produced by slow pyrolysis, has a porous structure improving its nutrient absorbing capacity,
surface area and thus a potential substituent. Bio-char has an appreciable carbon sequestration value i.e. a carbon
absorbing product. The orientation of sisal fiber are changed and studied in longitudinal and orthogonal
direction indicating superiority of longitudinal fiber orientation .It also addresses the variation in mechanical
characteristic (tensile flexural and impact) with different constituent of the new composite and its position in
material selection charts with a direction for further work.
Developments of nano clay particle reinforced plastics are of growing interest towards the
emergence of new materials which enhance optimal utilization of natural resources and particularly of
renewable resources. The effects of nano clay as filler in Basalt–epoxy composite systems on the
tribological properties have been discussed in this article. Basalt fiber reinforced epoxy (BE) composite
finds widespread application in erosive environment due to its several advantages like high wear
resistance, high strength-to-weight ratio and low cost. Experiments were carried out to study the effects
of impingement angle, particle velocity and filler material on the solid particle erosive wear behavior of
BE composite. The erosive wear is evaluated at different impingement angles from 30° to 90° at three
different velocities of 23, 42, & 60 m/s. The erodent used is silica sand with the size range (150 – 280 µm)
of irregular shape. The result shows semi-ductile behavior with maximum erosion rate at 60°
impingement angle. It is observed that wear rate increases with increasing particle velocity and
decreases with increases of filler percentage. The morphology of the eroded surfaces was examined by
using Scanning electron microscopy (SEM).
Study of mechanical and morphological properties of glass fiber reinforced mo...eSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
Physical Properties and Compressive Strength of Zinc Oxide Nanopowder as a Po...IJAAS Team
In this study, the application of nanotechnology was applied in the dentistry field, especially in the innovation of dental amalgam material. To date, mercury (Hg) has been used widely as dental amalgam material with consideration of the cheap price, ease of use, and good mechanical strength. However, last few years, many problems have been faced in the dentistry field due to the use of mercury. Hence, new material is needed as an innovation to eliminate the mercury from dental amalgam composition. This research was conducted to analyze the physical properties and compressive strength of zinc oxide (ZnO) nanopowder as a potential dental amalgam material. The physical properties such as morphology and dimensions were analyzed by SEM and XRD. Further, the compression test was conducted by using hydraulic press machine. The results showed that the ZnO nanopowder analyzed has the particle size of 14.34 nm with the morphology classified as nanorods type. On the compression load of 500 kg, the average of ZnO green density is 3.170 g/cm3. This value experienced the increase of 4.763% when the load was set to 1000 kg, and 7.539% at 2000 kg. The dwelling time also took the same effect. At 30 seconds, the average of ZnO green density is 3.260 g/cm3. This value experienced the increase of 0.583% at 60 seconds and 3.098% at 90 seconds.
International Journal of Engineering Research and Applications (IJERA) is an open access online peer reviewed international journal that publishes research and review articles in the fields of Computer Science, Neural Networks, Electrical Engineering, Software Engineering, Information Technology, Mechanical Engineering, Chemical Engineering, Plastic Engineering, Food Technology, Textile Engineering, Nano Technology & science, Power Electronics, Electronics & Communication Engineering, Computational mathematics, Image processing, Civil Engineering, Structural Engineering, Environmental Engineering, VLSI Testing & Low Power VLSI Design etc.
Mechanical and Chemical Properties of Bamboo/Glass Fibers Reinforced Polyeste...IJERA Editor
The chemical resistance of Bamboo/Glass reinforced Polyester hybrid composites to acetic acid, Nitric acid, Hydrochloric acid, Sodium hydroxide, Sodium carbonate, Benzene, Toluene, Carbon tetrachloride and Water was studied. The tensile and impact properties of these composites were also studied. The effect of alkali treatment of bamboo fibers on these properties was studied. It was observed that the tensile and impact properties of the hybrid composites increase with glass fiber content. The author investigated the interfacial bonding between Glsss/Bamboo fiber composites by SEM. These properties found to be higher when alkali treated bamboo fibers were used in hybrid composites. The hybrid fiber composites showed better resistance to the chemicals mentioned above. The elimination of amorphous hemi-cellulose with alkali treatment leading to higher crystallinity of the bamboo fibers with alkali treatment may be responsible for these observations.
Study on Vibration Analysis of Hybrid Laminated CompositesPremier Publishers
This paper represents the review on vibration analysis of hybrid composites. As we know that vibration and composite materials are two main growing research topics now-a-days. Almost all the structural components subjected to dynamic loading in their working life and vibration affects working life of the structure so it is very important in designing a component to reduce the structural vibration and its amplitude. Composite material applications are wide in the aerospace, civil, marine, and automotive industries due to their high specific stiffness and strength, excellent fatigue resistance, long durability and many other superior properties compared to ordinary composites. Carbon fiber reinforced polymers have high strength and light weight properties. But CFRP suffer from high frequency vibrations at low operating conditions. In this paper studying the hybridization of high stiffened CFRP with basalt fiber to reduce vibrations under cantilever boundary condition.
Fabrication and Mechanical Charecterization of Cnt NanocompositesIOSR Journals
The effects of Amine, Epoxide functionalization of multi-wall carbon nanotubes on properties of CNT/epoxy nanocomposites are investigated in this work. Adding CNTs to the matrix is expected to improve the stiffness, toughness, interlaminar shear strength of and many other properties of composites. Functionalization with different amino and epoxide groups of multi-walled carbon nanotubes was achieved and nanotube-reinforced epoxy nanocomposites were prepared by mixing amino, epoxide-functionalized multi-walled carbon nanotubes with epoxy resin. The reinforcement mechanism of amino-functionalized multi-walled carbon nanotubes in epoxy resin was discussed. Interlaminar shear strength (ILSS), Three point bending test and Re-bound hardness tests were used to investigate the mechanical properties of the nanocomposites and functionalization groupings are investigated by Fourier transform spectroscopy (FTIR). Then the results of amine, epoxide group are compared with No-CNT nanocomposite. The results showed that different percentage of amino, epoxide -functionalized multi-walled carbon nanotubes would have different effects on the mechanical properties of the nanocomposites. The amine functionalizes CNT composites are giving good results compare to another samples
Power saving mechanism for hybrid routing protocol using scheduling techniqueeSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
Study of mechanical and morphological properties of glass fiber reinforced mo...eSAT Journals
Abstract Polymethylmethacrylate and Poly (acrylonitrile-co-butadiene) rubber were used to modify Diglycidyl ether of bisphenol A (DGEBA) type epoxy resin and cured with stoichiometric quantities of the hardener 4,4’ diamino dipheny methane. This modified epoxy resin was used as the matrix for the preparation of glass fiber reinforced composites. E- Glass fiber was used as fiber reinforcement. The morphology and mechanical properties of the composite analysed. Morphological analysis of the fractured surface of the composites indicated good adhesion between the matrix polymer and the glass fibers. Hence an enhancement in mechanical properties of the composite such as tensile, flexural, impact and fracture toughness has been observed as there has been an effective transfer of the load from the matrix to the fiber. Hence these composites which exhibit high toughness, strength and dimensional stability can be envisaged to provide valuable contribution to high performance structural applications. Keywords: Glass composites, mechanical properties, modified epoxy matrix, morphology and ternary blend
Experimental Behaviour of Steel Fiber Reinforced Concrete with partial Replac...ijtsrd
Concrete is generally used due to the abundance of uncooked material, low manufacturing and protection cost, excellence in compression, corrosion aspects, and versatility in forming more than a few shapes and its limitless structural purposes in aggregate with metal reinforcement. All these elements have contributed pressures to decrease cement consumption and to intensify lookup in exploring the probabilities of improving strength, sturdiness and corrosion discount via the use of pozzolonas as supplementary cementing materials. Fibre bolstered concrete FRC is a fibre reinforcing cementitious concrete composite, and by way of including discrete brief fibres randomly in concrete it famous many appreciably multiplied engineering residences It is manufactured from kaolin which makes the concrete extra long lasting and ecofriendly. In the current investigation mechanical residences of concrete containing each Fly ash and Metakaolin at a number of combos are studied. For the a range of mixtures of Fly ash and Metakaolin, cubes cylindrical and prism specimens are casted with 1 of fibres and the compression strength, break up tensile energy and flexural energy take a look at consequences are got and in contrast with the traditional combine having 1 fibres. It is thereby counseled that utilization of these cementitious substances in concrete will decrease the requirement for cement thereby marching in the direction of green construction. M. Sankaran | Dr. M. Gunasekaran | M. Loganathan "Experimental Behaviour of Steel Fiber Reinforced Concrete with partial Replacement of Fly Ash & Metakaolin" Published in International Journal of Trend in Scientific Research and Development (ijtsrd), ISSN: 2456-6470, Volume-4 | Issue-5 , August 2020, URL: https://www.ijtsrd.com/papers/ijtsrd33163.pdf Paper Url :https://www.ijtsrd.com/engineering/civil-engineering/33163/experimental-behaviour-of-steel-fiber-reinforced-concrete-with-partial-replacement-of-fly-ash-and-metakaolin/m-sankaran
Mechanical Characterization of Bio-Char Made Hybrid CompositeIJERA Editor
Material discoveries and development have always been the cause of the growth and development of a nation
and the need of naturally made materials is the need of hours. Thus this paper takes you to the development of a
hybrid composite made of sisal fiber with epoxy as the matrix intertwined with softwood bio-char. Softwood
chip bio-char, produced by slow pyrolysis, has a porous structure improving its nutrient absorbing capacity,
surface area and thus a potential substituent. Bio-char has an appreciable carbon sequestration value i.e. a carbon
absorbing product. The orientation of sisal fiber are changed and studied in longitudinal and orthogonal
direction indicating superiority of longitudinal fiber orientation .It also addresses the variation in mechanical
characteristic (tensile flexural and impact) with different constituent of the new composite and its position in
material selection charts with a direction for further work.
Developments of nano clay particle reinforced plastics are of growing interest towards the
emergence of new materials which enhance optimal utilization of natural resources and particularly of
renewable resources. The effects of nano clay as filler in Basalt–epoxy composite systems on the
tribological properties have been discussed in this article. Basalt fiber reinforced epoxy (BE) composite
finds widespread application in erosive environment due to its several advantages like high wear
resistance, high strength-to-weight ratio and low cost. Experiments were carried out to study the effects
of impingement angle, particle velocity and filler material on the solid particle erosive wear behavior of
BE composite. The erosive wear is evaluated at different impingement angles from 30° to 90° at three
different velocities of 23, 42, & 60 m/s. The erodent used is silica sand with the size range (150 – 280 µm)
of irregular shape. The result shows semi-ductile behavior with maximum erosion rate at 60°
impingement angle. It is observed that wear rate increases with increasing particle velocity and
decreases with increases of filler percentage. The morphology of the eroded surfaces was examined by
using Scanning electron microscopy (SEM).
Study of mechanical and morphological properties of glass fiber reinforced mo...eSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
Physical Properties and Compressive Strength of Zinc Oxide Nanopowder as a Po...IJAAS Team
In this study, the application of nanotechnology was applied in the dentistry field, especially in the innovation of dental amalgam material. To date, mercury (Hg) has been used widely as dental amalgam material with consideration of the cheap price, ease of use, and good mechanical strength. However, last few years, many problems have been faced in the dentistry field due to the use of mercury. Hence, new material is needed as an innovation to eliminate the mercury from dental amalgam composition. This research was conducted to analyze the physical properties and compressive strength of zinc oxide (ZnO) nanopowder as a potential dental amalgam material. The physical properties such as morphology and dimensions were analyzed by SEM and XRD. Further, the compression test was conducted by using hydraulic press machine. The results showed that the ZnO nanopowder analyzed has the particle size of 14.34 nm with the morphology classified as nanorods type. On the compression load of 500 kg, the average of ZnO green density is 3.170 g/cm3. This value experienced the increase of 4.763% when the load was set to 1000 kg, and 7.539% at 2000 kg. The dwelling time also took the same effect. At 30 seconds, the average of ZnO green density is 3.260 g/cm3. This value experienced the increase of 0.583% at 60 seconds and 3.098% at 90 seconds.
International Journal of Engineering Research and Applications (IJERA) is an open access online peer reviewed international journal that publishes research and review articles in the fields of Computer Science, Neural Networks, Electrical Engineering, Software Engineering, Information Technology, Mechanical Engineering, Chemical Engineering, Plastic Engineering, Food Technology, Textile Engineering, Nano Technology & science, Power Electronics, Electronics & Communication Engineering, Computational mathematics, Image processing, Civil Engineering, Structural Engineering, Environmental Engineering, VLSI Testing & Low Power VLSI Design etc.
Mechanical and Chemical Properties of Bamboo/Glass Fibers Reinforced Polyeste...IJERA Editor
The chemical resistance of Bamboo/Glass reinforced Polyester hybrid composites to acetic acid, Nitric acid, Hydrochloric acid, Sodium hydroxide, Sodium carbonate, Benzene, Toluene, Carbon tetrachloride and Water was studied. The tensile and impact properties of these composites were also studied. The effect of alkali treatment of bamboo fibers on these properties was studied. It was observed that the tensile and impact properties of the hybrid composites increase with glass fiber content. The author investigated the interfacial bonding between Glsss/Bamboo fiber composites by SEM. These properties found to be higher when alkali treated bamboo fibers were used in hybrid composites. The hybrid fiber composites showed better resistance to the chemicals mentioned above. The elimination of amorphous hemi-cellulose with alkali treatment leading to higher crystallinity of the bamboo fibers with alkali treatment may be responsible for these observations.
Study on Vibration Analysis of Hybrid Laminated CompositesPremier Publishers
This paper represents the review on vibration analysis of hybrid composites. As we know that vibration and composite materials are two main growing research topics now-a-days. Almost all the structural components subjected to dynamic loading in their working life and vibration affects working life of the structure so it is very important in designing a component to reduce the structural vibration and its amplitude. Composite material applications are wide in the aerospace, civil, marine, and automotive industries due to their high specific stiffness and strength, excellent fatigue resistance, long durability and many other superior properties compared to ordinary composites. Carbon fiber reinforced polymers have high strength and light weight properties. But CFRP suffer from high frequency vibrations at low operating conditions. In this paper studying the hybridization of high stiffened CFRP with basalt fiber to reduce vibrations under cantilever boundary condition.
Fabrication and Mechanical Charecterization of Cnt NanocompositesIOSR Journals
The effects of Amine, Epoxide functionalization of multi-wall carbon nanotubes on properties of CNT/epoxy nanocomposites are investigated in this work. Adding CNTs to the matrix is expected to improve the stiffness, toughness, interlaminar shear strength of and many other properties of composites. Functionalization with different amino and epoxide groups of multi-walled carbon nanotubes was achieved and nanotube-reinforced epoxy nanocomposites were prepared by mixing amino, epoxide-functionalized multi-walled carbon nanotubes with epoxy resin. The reinforcement mechanism of amino-functionalized multi-walled carbon nanotubes in epoxy resin was discussed. Interlaminar shear strength (ILSS), Three point bending test and Re-bound hardness tests were used to investigate the mechanical properties of the nanocomposites and functionalization groupings are investigated by Fourier transform spectroscopy (FTIR). Then the results of amine, epoxide group are compared with No-CNT nanocomposite. The results showed that different percentage of amino, epoxide -functionalized multi-walled carbon nanotubes would have different effects on the mechanical properties of the nanocomposites. The amine functionalizes CNT composites are giving good results compare to another samples
Power saving mechanism for hybrid routing protocol using scheduling techniqueeSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
Noise reduction in speech processing using improved active noise control (anc...eSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
Mining elevated service itemsets on transactional recordsets using slicingeSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
Performance evaluation of path loss parameters for broadcasting applicationseSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
Experimental investigation on halloysite nano tubes & clay an infilled compos...eSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
Production of lactic acid from sweet meat industry waste by lactobacillus del...eSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
A novel association rule mining and clustering based hybrid method for music ...eSAT Publishing House
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology.
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
IJRET : International Journal of Research in Engineering and Technology is an international peer reviewed, online journal published by eSAT Publishing House for the enhancement of research in various disciplines of Engineering and Technology. The aim and scope of the journal is to provide an academic medium and an important reference for the advancement and dissemination of research results that support high-level learning, teaching and research in the fields of Engineering and Technology. We bring together Scientists, Academician, Field Engineers, Scholars and Students of related fields of Engineering and Technology
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin CompositesIJMER
In the present work fabrication of composite material(E-Glass Fiber Epoxy Resin +
NANO CaCO3) was carried out and their tensile properties viz tensile strength, tensile
strain(%),young's modulus, energy at maximum load and brihnall hardness number were found.
Specimens of E-Glass Fiber Epoxy Resin) hybrid composites are prepared with four different
compositions of nano-calcium carbonate (CaCO3), viz., 0,3,5 and 7%.Each specimen consisting of
40%GF. The specimens are prepared by hand lay up method.. Tests are conducted on these specimens
to determine the tensile strength, tensile strain, young's modulus energy at maximum load and
hardness number at room temperature using universal testing machine and Brihnell hardness testing
machine. The influence of the nano-CaCO3 content on the mechanical properties tensile of hybrid
composites was studied. It is found that the reinforcing and toughening effects of the E-Glass epoxy
hybrid composites are increased by adding nano-CaCO3.The tensile strength, tensile strain, young’s
modulus and energy at max load of these composites increased nonlinearly with the addition of the
nano-CaCO3
FLEXURAL PROPERTIES OF HYBRID FIBRE REINFORCED CONCRETE - A COMPARATIVE EXPER...Journal For Research
Fiber-reinforced concrete (FRC) is concrete containing fibrous material which increases its structural integrity. It contains short discrete fibers that are uniformly distributed and randomly oriented. The most important advantages are hindrance of macro-cracks’ development, delay in micro-cracks’ propagation to macroscopic level. In this project the flexural properties were studied for concrete prepared using different hybrid fibre combinations of glass fibres and polypropylene fibres. The volume fraction of the glass fibres and polypropylene fibres used in this study are 0.4% and 0.5% of total volume of concrete. The flexural properties were studied using centre point loading method on beam specimens. The objective of this study is to evaluate flexural strength of fibre reinforced concrete with respect to different combination of glass fibres and polypropylene fibres. It is observed that quantity of fibres both glass fibres and polypropylene fibres play significant role in increment flexural properties of concrete.
Effect of stacking sequence and hybridization on the tensile and flexural properties of composite
laminates between basalt, jute and flax with E-glass reinforced epoxy have been investigated experimentally. It
was found that stacking sequence is not highly significant on tensile properties, contrasting with flexural strength
and modulus which were strongly dependent on the hybrid configuration between sandwich-like (SL) and
intercalation (IC) sequences. Specific modulus based on the variation densities of the hybrid laminates was used
to discover the best combination either basalt, jute or flax with E-glass exhibits superior properties concerning
on the strength to weight- ratio. Hence, stacking sequences and material selection are among predominant factors
that influence on mechanical properties and very crucial in designing composite hybrid system to meet the desired
requirements.
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer CompositeIJMER
Amids the growing concern on environmental issues, science is seeking various alternatives to replace the synthetic and non degradable fibers composites with environment friendly biocomposites of comparable characteristics and performance. Visualizing the importance of polymer composites and owing to issue of ecological concerns, this experiment is an attempt to further investigate possibility of bio composites (Particularly maize husk) as an alternative of available synthetic polymer composites. Taking one leap forward the experiment also approximate qualities the effect of individual parameters on erosion by the application of Taguchi Technique. Experimental system were devised and designed to study the erosion rate of maize husk fiber Reinforced Polymer composites at various impingement angles, with profound variables such as particle velocity, fiber content, and particle size (erodent size) To cast the composite epoxy Resin LY 556 with corresponding hardener HY 551 was used. The erodent size was in range of it irregular shape. The tribological performance of sheets was investigated in respect to set of various variable parameters as suggested by L16 series of Taguchi Techniques. The morphological feature before and after the experiments were studies using SEM.
Influence of Carbon & Glass Fiber Reinforcements on Flexural Strength of Epox...IJERA Editor
Hybrid composite materials are more attracted by the engineers because of their properties like stiffness and high specific strength which leads to the potential application in the area of aerospace, marine and automobile sectors. In the present investigation, the flexural strength and flexural modulus of carbon and glass fibers reinforced epoxy hybrid composites were studied. The vacuum bagging technique was adopted for the fabrication of polymer hybrid composite materials. The hardness, flexural strength and flexural modulus of the hybrid composites were determined as per ASTM standards. The hardness, flexural strength and flexural modulus were improved as the fiber reinforcement contents increased in the epoxy matrix material.
Saudi Arabia stands as a titan in the global energy landscape, renowned for its abundant oil and gas resources. It's the largest exporter of petroleum and holds some of the world's most significant reserves. Let's delve into the top 10 oil and gas projects shaping Saudi Arabia's energy future in 2024.
Cosmetic shop management system project report.pdfKamal Acharya
Buying new cosmetic products is difficult. It can even be scary for those who have sensitive skin and are prone to skin trouble. The information needed to alleviate this problem is on the back of each product, but it's thought to interpret those ingredient lists unless you have a background in chemistry.
Instead of buying and hoping for the best, we can use data science to help us predict which products may be good fits for us. It includes various function programs to do the above mentioned tasks.
Data file handling has been effectively used in the program.
The automated cosmetic shop management system should deal with the automation of general workflow and administration process of the shop. The main processes of the system focus on customer's request where the system is able to search the most appropriate products and deliver it to the customers. It should help the employees to quickly identify the list of cosmetic product that have reached the minimum quantity and also keep a track of expired date for each cosmetic product. It should help the employees to find the rack number in which the product is placed.It is also Faster and more efficient way.
Overview of the fundamental roles in Hydropower generation and the components involved in wider Electrical Engineering.
This paper presents the design and construction of hydroelectric dams from the hydrologist’s survey of the valley before construction, all aspects and involved disciplines, fluid dynamics, structural engineering, generation and mains frequency regulation to the very transmission of power through the network in the United Kingdom.
Author: Robbie Edward Sayers
Collaborators and co editors: Charlie Sims and Connor Healey.
(C) 2024 Robbie E. Sayers
Welcome to WIPAC Monthly the magazine brought to you by the LinkedIn Group Water Industry Process Automation & Control.
In this month's edition, along with this month's industry news to celebrate the 13 years since the group was created we have articles including
A case study of the used of Advanced Process Control at the Wastewater Treatment works at Lleida in Spain
A look back on an article on smart wastewater networks in order to see how the industry has measured up in the interim around the adoption of Digital Transformation in the Water Industry.
Quality defects in TMT Bars, Possible causes and Potential Solutions.PrashantGoswami42
Maintaining high-quality standards in the production of TMT bars is crucial for ensuring structural integrity in construction. Addressing common defects through careful monitoring, standardized processes, and advanced technology can significantly improve the quality of TMT bars. Continuous training and adherence to quality control measures will also play a pivotal role in minimizing these defects.
Democratizing Fuzzing at Scale by Abhishek Aryaabh.arya
Presented at NUS: Fuzzing and Software Security Summer School 2024
This keynote talks about the democratization of fuzzing at scale, highlighting the collaboration between open source communities, academia, and industry to advance the field of fuzzing. It delves into the history of fuzzing, the development of scalable fuzzing platforms, and the empowerment of community-driven research. The talk will further discuss recent advancements leveraging AI/ML and offer insights into the future evolution of the fuzzing landscape.
Immunizing Image Classifiers Against Localized Adversary Attacksgerogepatton
This paper addresses the vulnerability of deep learning models, particularly convolutional neural networks
(CNN)s, to adversarial attacks and presents a proactive training technique designed to counter them. We
introduce a novel volumization algorithm, which transforms 2D images into 3D volumetric representations.
When combined with 3D convolution and deep curriculum learning optimization (CLO), itsignificantly improves
the immunity of models against localized universal attacks by up to 40%. We evaluate our proposed approach
using contemporary CNN architectures and the modified Canadian Institute for Advanced Research (CIFAR-10
and CIFAR-100) and ImageNet Large Scale Visual Recognition Challenge (ILSVRC12) datasets, showcasing
accuracy improvements over previous techniques. The results indicate that the combination of the volumetric
input and curriculum learning holds significant promise for mitigating adversarial attacks without necessitating
adversary training.
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CFD Simulation of By-pass Flow in a HRSG module by R&R Consult.pptxR&R Consult
CFD analysis is incredibly effective at solving mysteries and improving the performance of complex systems!
Here's a great example: At a large natural gas-fired power plant, where they use waste heat to generate steam and energy, they were puzzled that their boiler wasn't producing as much steam as expected.
R&R and Tetra Engineering Group Inc. were asked to solve the issue with reduced steam production.
An inspection had shown that a significant amount of hot flue gas was bypassing the boiler tubes, where the heat was supposed to be transferred.
R&R Consult conducted a CFD analysis, which revealed that 6.3% of the flue gas was bypassing the boiler tubes without transferring heat. The analysis also showed that the flue gas was instead being directed along the sides of the boiler and between the modules that were supposed to capture the heat. This was the cause of the reduced performance.
Based on our results, Tetra Engineering installed covering plates to reduce the bypass flow. This improved the boiler's performance and increased electricity production.
It is always satisfying when we can help solve complex challenges like this. Do your systems also need a check-up or optimization? Give us a call!
Work done in cooperation with James Malloy and David Moelling from Tetra Engineering.
More examples of our work https://www.r-r-consult.dk/en/cases-en/
Industrial Training at Shahjalal Fertilizer Company Limited (SFCL)MdTanvirMahtab2
This presentation is about the working procedure of Shahjalal Fertilizer Company Limited (SFCL). A Govt. owned Company of Bangladesh Chemical Industries Corporation under Ministry of Industries.
Hybrid optimization of pumped hydro system and solar- Engr. Abdul-Azeez.pdffxintegritypublishin
Advancements in technology unveil a myriad of electrical and electronic breakthroughs geared towards efficiently harnessing limited resources to meet human energy demands. The optimization of hybrid solar PV panels and pumped hydro energy supply systems plays a pivotal role in utilizing natural resources effectively. This initiative not only benefits humanity but also fosters environmental sustainability. The study investigated the design optimization of these hybrid systems, focusing on understanding solar radiation patterns, identifying geographical influences on solar radiation, formulating a mathematical model for system optimization, and determining the optimal configuration of PV panels and pumped hydro storage. Through a comparative analysis approach and eight weeks of data collection, the study addressed key research questions related to solar radiation patterns and optimal system design. The findings highlighted regions with heightened solar radiation levels, showcasing substantial potential for power generation and emphasizing the system's efficiency. Optimizing system design significantly boosted power generation, promoted renewable energy utilization, and enhanced energy storage capacity. The study underscored the benefits of optimizing hybrid solar PV panels and pumped hydro energy supply systems for sustainable energy usage. Optimizing the design of solar PV panels and pumped hydro energy supply systems as examined across diverse climatic conditions in a developing country, not only enhances power generation but also improves the integration of renewable energy sources and boosts energy storage capacities, particularly beneficial for less economically prosperous regions. Additionally, the study provides valuable insights for advancing energy research in economically viable areas. Recommendations included conducting site-specific assessments, utilizing advanced modeling tools, implementing regular maintenance protocols, and enhancing communication among system components.
Sachpazis:Terzaghi Bearing Capacity Estimation in simple terms with Calculati...Dr.Costas Sachpazis
Terzaghi's soil bearing capacity theory, developed by Karl Terzaghi, is a fundamental principle in geotechnical engineering used to determine the bearing capacity of shallow foundations. This theory provides a method to calculate the ultimate bearing capacity of soil, which is the maximum load per unit area that the soil can support without undergoing shear failure. The Calculation HTML Code included.
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A study on glass fiber reinforced polymer clay nanocomposites with sandwich structure
1. IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308
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Volume: 03 Issue: 07 | Jul-2014, Available @ http://www.ijret.org 194
A STUDY ON GLASS FIBER REINFORCED POLYMER-CLAY
NANOCOMPOSITES WITH SANDWICH STRUCTURE
Shivraj Puggal1
, Sumit Mahajan2
, Novepreet Dhall3
1
Department of Mechanical Engineering, Lovely Professional University, Punjab, India
2
Department of Mechanical Engineering, Lovely Professional University, Punjab, India
3
Department of Mechanical Engineering, Lovely Professional University, Punjab, India
Abstract
Glass fiber reinforced polymer (GFRP) has been found attractive due to high strength-to-weight ratio, high stiffness-to-weight
ratio, and corrosion and fatigue resistance. The properties of GFRP are further enhanced by adding very small amount of
nanometer size particles. The use of sandwich composites with GFRP face sheets is becoming popular in structural design
because of their ability to substantially decrease weight while maintaining mechanical performance. In this study face sheets of
sandwich composites are modified using nanoclay particles. The sandwich structure composed of bidirectional E-glass fiber,
Closite 30B nanoclay, epoxy resin and high density thermocol. Hand layup method was used for fabrication of sheets also the
nanoclay percentage was varied subjected to various test. The use of nano composite increases the bending strength up to 41% as
compared to virgin epoxy. The natural degradation of bending specimen with neat epoxy showed the maximum degradation up to
10% and it was 5% in case of specimens with nano composite sheets. The water resistance property of epoxy was improved by the
addition of both glass fibre and nanoclay. The tensile strength is raised by 33% by using 3% of clay in the epoxy. The SEM and
XRD were performed for characterization of the nano composites.
Keywords: Nanocomposites, Sandwich structure, Bending strength, and Natural degradation.
--------------------------------------------------------------------***----------------------------------------------------------------------
1. INTRODUCTION
Sandwich composites are a specialized form of laminated
composites in which a thick, soft and light weight core is
sandwiched between two thin and stiff fiber reinforced
plastic skins (1). The use of light core reduces the weight so
this weight reduction results in a number of benefits,
including increased range, higher payloads and decreased
fuel consumption. All have a positive impact on cost as well
as a decreased impact on the environment. Desired
properties can be produced by modifying face sheets or core
material. The sandwich structure composed of GFRP face
sheets and thermocol core showed that higher thickness core
withstands a higher bending load showing less flexural
stress and flexure modulus(2). Aluminum composite made
by using Aluminum skin, polyethylene core and epoxy resin
is light and strong as compared to aluminum panel. Weight
reduction and lesser heat infiltration were observed by using
aluminum composite (3). The face sheets can be amended
using the nanocompoites as it produces various property
enhancements. Rajmohan concluded that the increase in wt
% of nano Copper oxide improves the mechanical properties
mainly due to the very large surface area of interaction
between polymer matrix and nano filler (4). The proper
dispersion montmorillonite clay in the epoxy resin produces
higher compressive stiffness compared to neat polymer. The
presence of agglomerates in epoxy reduces the compressive
strength so clay should be properly dispersed (5). B.
Sharma used hand lay-up method for preparing fiber
reinforced nanocomposites and agglomerates were visible
when 5% clay was added. Tensile strength and micro-
hardness increases with addition of nanoclay up to 3 wt%
(6).
2. MATERIALS AND MANUFACTURING
The materials used in this study were Bidirectional E-glass
fibers, Lapox a two part epoxy resin purchased from Atul
Polymers (India) Private, High density thermocol of
thickness 16mm and organically modified nanoclay Closite
30B purchased from Nano shell India.
2.1 Dispersion of Nanoclay into Base Epoxy
First the base epoxy and required amount of nanoclay is
measured with help of digital weighing machine. Epoxy
base L-12 is a transparent thick fluid. It is quite difficult to
mix nanoclay into it manually. As powder nanoparticles
adhere to each other due to interactive forces between the
particles, resulting in nanoparticle agglomerates with
dimensions of several micrometers. So we used a
homogeniser having RPM 2000 and a magnetic hot plate for
proper mixing of nanoclay. Hot plate was used to heat up
the base epoxy to desired temperature (60o
), so the viscosity
of epoxy is reduced as shown in Figure 1. Proper
mechanical stirring of epoxy at this stage resulted better
scattering of clay. The process of heating as well as stirring
was performed, concomitantly for 2 hours to ensure the
better dispersion to avoid agglomerates formation in the
base epoxy. The amount of nanoclay dispersed into the
epoxy system, in weight, is 1%, 3% and 5% respectively.
2. IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308
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Volume: 03 Issue: 07 | Jul-2014, Available @ http://www.ijret.org 195
Fig-1: Set up for mixing clay in epoxy
2.2 Preparation of Epoxy Resin for GFRP
Composites Fabrication
After mechanical stirring of the epoxy solution container
was placed into the ultra sonication bath for up to 2 hours.
During sonication sound energy is used to whisk particles
for evenly dispersing nanoparticles in liquids. After ultra
sonication, the solution is mixed with the hardener in the
ratio 10:1 by volume. After mixing, manual stirring up to 5
to 10 minutes was done such that the hardener mixes
properly in modified epoxy. The pot life of mixture is 15-20
minutes at ambient temperature.
2.3 Coating of Nanoclay Mixed Epoxy to Glass
Fiber Sheets
The mixture was then poured on to the glass fibre mat and
applied uniformly using the hand layup method. For this,
steel scraper was used to maintain consistency of the
solution. The full curing of sheet was done by leaving it
under ambient temperature for one day before processing
further.
2.4 Sizing of Sheet for Specimen
The specimen had been cut and prepared as per the ASTM
standard C-393 for bending and D3037/3039 for tensile. The
samples had to be tabbed on either side on two ends for
tensile testing. For the three point bending test the use of
high density thermocol was used and placed between two
face sheets of nano composites.
3. EXPERIMENTAL PROCEDURES
3.1 Characterization Techniques
X-ray diffraction was used to scrutinize the changes that
occur to the clay due to the intercalation and/or exfoliation
of the epoxy into the clay galleries. The measurements were
carried out in a X-ray diffractometer with Cu Kα radiation at
λ= 1.54 Å with a scanning speed of 1°/min and operating at
45 kV and 40. A scanning electron microscope (SEM) is a
type of electron microscope that produces images of a
sample by scanning it with a focused beam of electrons. The
polishing of specimen was done by using Gold coating
equipment. The polished specimen was used to contemplate
clay dispersion at different magnification.
3.2 Flexural Testing Analysis
The Three Point Bending flexural test provides values for
the flexural stress σf, flexural strain εf and the flexural stress-
strain response of the material. The main advantage of a
three point flexural test is the ease of the specimen
preparation and testing. Three point bending tests of
specimen were carried out in using Zwick / Roell. Flexural
stress for rectangular cross sections given by
σf=
𝟑𝑷𝑳
𝟐𝒃𝒅 𝟐
3.3 Tensile Testing Analysis
The test specimen for tensile testing had been prepared
according to ASTM-D-3039 standard. The specimens were
tested on universal testing machine until they break
stipulating the peak load and ultimate stress value they can
bear at required time period.
3.3 Weight Gain Analysis
The specimens of various clay loadings were dunked in
water at environmental temperature. The percentage weight
gain at any time (Wt) as a result of moisture absorption was
determined by eq. (1)
Wt= (Ww- Wd)/Wd × 100 (1)
Where Wd and Ww denote the weight of dry material prior to
exposure and weight of materials after exposure to natural
degradation.
4. RESULTS AND DISCUSSION
The X-ray diffraction (XRD) was used to discern the d-
spacing and corresponding intensity of the samples having
different nanoclay loading. The diffraction peak of Closite
30B nanoclay is visible at 2θ = 4.81° having interlayer
spacing 18.42 Å. The results of various specimens of
different loading showed that d-spacing of layers increased
from 18.42 Å to 32.32 Å Table 1 showing comparison for
various clay loadings and thus confirmed intercalation of
clay particles. This is due to the penetration of polymer
chains in between layered silicates which increases there
spacing.
Table -1: XRD results for various clay loadings
S.No CLAY
LOADING
2θ d-spacing Å
1 1% 3.6513 24.1791
2 3% 2.8545 30.9262
3 5% 2.7308 32.3263
3. IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308
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Volume: 03 Issue: 07 | Jul-2014, Available @ http://www.ijret.org 196
The SEM images were used for the investigation of the
dispersion state of nanoclay particles in the epoxy and were
carried out at various magnifications. Some of the Scanning
electron micrographs are shown in Figures 1, 2 and 3. The
SEM micrographs have shown very good dispersion in case
of 1% and 3% however presence of agglomerates were
recognizable in 5% specimen.
Fig-2: SEM image of epoxy with 1% clay at 25KX
Fig-3: SEM image of epoxy with 3% clay at 25KX
Fig-4: SEM image of epoxy with 5% clay at 25KX
The tensile test was conducted for all the specimens and
specimen without nanoclay was used as bench mark. The
tensile strength increased 33% by the addition of nanoclay
particles in epoxy. The maximum tensile strength is
achieved by using 3% of clay and further addition reduced
the strength as shown in figure 5. The stress concentration is
the main reason for the reduction in tensile strength which is
due to agglomerates as visible in SEM images.
Fig-5: Tensile strength MPa of nanocomposite at different
clay loadings
In the specimens of various clay loading were tested under
three point bending test. The result of bending test showed
that the peak load of the specimen was increased as increase
in clay percentage from 1% to 5%. The use of nano
composites increases the bending strength up to 47% as
compared to virgin epoxy.
After the initial bending test effect of natural degradation
was calculated, specimens were dipped in a water bath for
15 days and were subjected to three point bending test.
Table -2: Natural degradation of specimens
Clay
loading
Initial
bending
strength
(MPa)
Bending
strength
after 15
days
(MPa)
%
Decrease in
bending
strength
0% 4.8048 4.1428 13.77
1% 5.5209 5.0358 8.787
3% 6.237 5.9136 5.185
5% 7.101 6.80 4.238
The results of the specimens before and after exposure are
equated it has been found that the degradation in the
samples without the clay is more as compared to the
specimens with modified epoxy with nanoclay. The face
sheets with nanoclay is offering barrier to the water. The
bending strength reduced from 4.8048 to 4.1428 there was
0
5
10
15
20
25
0 2 4 6
TensileStrengthinMpa
% Nanoclay content
4. IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308
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Volume: 03 Issue: 07 | Jul-2014, Available @ http://www.ijret.org 197
in total 13% reduction in the strength for composite with
neat epoxy. The modified epoxy specimens showed less
reduction in the strength after degradation and specimen
with 5% nanoclay particles showed the best result during the
natural degradation.
(a)
(b)
Fig-6: (a) Shiny Surface before Exposure; (b) Scale
formation after exposure
After 15 days there was some scale formation on the
specimen, with water immersed specimen. Surface
observation showed that due to scale formation the epoxy
had lost some shine on either side as shown in figure 6. But
still after bending (by hands) the epoxy showed considerable
strength and flexibility.
Fig-7: Delamination of sheets after Exposure
As per visual observation of specimen, it was observed that
core cracking and delamination occurred in thermocol sheet
during the flexural testing. Degradation in thermocol was
observed which is clearly visible in figure 7 shear cracks
and core crushing were observed. These defects affect the
strength and durability of sandwich composite structures.
Epoxy cracking was also observed in some portions.
Weight gains were indicated by periodic removal of the
specimens from the water bath and weighing on a digital
balance. The specimens of various clay loadings were
immersed in water at environmental temperature. Figure 8
shows the increase in weight percentage with respect to
number of days.
Fig-8: Percentage Weight gain versus No. of days
Table - 3: Percentage weight gain of specimens after
exposure
Clay
loading
Initial
weight
Weight
after 5
days
Weight
after 10
days
Weight
after 15
days
%
weight
gain
0% 64.746 65.10 66.013 66.801 3.174
0
0.5
1
1.5
2
2.5
0 5 10 15 20
%increaseinWtgain
No. of Days
0%
Clay
1%
Clay
3%
Clay
5%
Clay
Delamination
between skin
and core
5. IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308
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Volume: 03 Issue: 07 | Jul-2014, Available @ http://www.ijret.org 198
1% 66.201 66.507 67.127 67.612 2.131
3% 76.140 76.347 76.921 77.55 1.852
5% 75.355 75.601 76.027 76.59 1.641
It is very much clear from the table 3 and figure 8 that the
maximum weight gain percentage is shown by the sample of
without nanoclay loading. There is weight gain for other
specimens also but it is less comparative to neat epoxy
specimen showing less water intake.
5. CONCLUSIONS
The hand layup method was used for the manufacturing of
composites and characterization was performed using SEM
and XRD. The results show that the polymer intercalated in
the layered silicates increasing the D-spacing from 18 Å to
32.32 Å. The SEM micrographs showed that the proper
dispersion but agglomerates were visible in 5% clay loading.
The tensile strength increased 33% by the addition of
nanoclay particles in epoxy. The maximum tensile strength
is attained by using 3% of clay and further addition reduced
the strength. After natural degradation there was some
reduction in the peak loads and corresponding bending
strength. The specimen with neat epoxy showed the
maximum degradation up to 13% and it was less in case of
specimens with nanocomosite sheets. The water resistance
property of epoxy was improved by the addition of both
glass fibre and nanoclay, which is maybe attributed to the
increasing of the tortuosity path for water penetration. Three
point bending test performed after the exposure to water
showed shear cracks and delamination of sheets and core.
There was scale formation on the surface after natural
degradation. The percentage weight gain was highest in the
case of neat epoxy it was 4% but it was less when epoxy
was modified with nanoclay.
REFERENCES
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BIOGRAPHIES
Shivraj Puggal, a Lecturer at Lovely
Professional University with an experience
of 3 years, worked on Nanocomposites
Sumit Mahajan, a Assistant Professor at
Lovely Professional University with an
experience of 3 years, worked on
Nanocomposites
Novepreet Dhall, a Lecturer at Lovely
Professional University with an experience
of 3 years, worked on Nanocomposites