Fly ash from a coal power plant and waste glass were used to produce glass-ceramic composites. The addition of 50% flask glass to fly ash increased bending strength from 9 MPa to 77 MPa and elastic modulus from 6 GPa to 29 GPa. Porous composites made with polyurethane foam had 70% porosity, 3.5 GPa elastic modulus and 6 MPa bending strength. The composites showed good durability in acid with less than 0.05% mass loss, making them suitable for applications like filters or insulation.
Physical Properties and Compressive Strength of Zinc Oxide Nanopowder as a Po...IJAAS Team
In this study, the application of nanotechnology was applied in the dentistry field, especially in the innovation of dental amalgam material. To date, mercury (Hg) has been used widely as dental amalgam material with consideration of the cheap price, ease of use, and good mechanical strength. However, last few years, many problems have been faced in the dentistry field due to the use of mercury. Hence, new material is needed as an innovation to eliminate the mercury from dental amalgam composition. This research was conducted to analyze the physical properties and compressive strength of zinc oxide (ZnO) nanopowder as a potential dental amalgam material. The physical properties such as morphology and dimensions were analyzed by SEM and XRD. Further, the compression test was conducted by using hydraulic press machine. The results showed that the ZnO nanopowder analyzed has the particle size of 14.34 nm with the morphology classified as nanorods type. On the compression load of 500 kg, the average of ZnO green density is 3.170 g/cm3. This value experienced the increase of 4.763% when the load was set to 1000 kg, and 7.539% at 2000 kg. The dwelling time also took the same effect. At 30 seconds, the average of ZnO green density is 3.260 g/cm3. This value experienced the increase of 0.583% at 60 seconds and 3.098% at 90 seconds.
Surfactant-assisted Hydrothermal Synthesis of Ceria-Zirconia Nanostructured M...IOSR Journals
CeO2–ZrO2 oxides were prepared by the surfactant-templated method using cetyl trimethyl ammonium bromide (CTAB) as template and modified with chromium nitrate. These were characterized by XRD, FT-IR, TEM, SEM, BET and TPD-CO2. The XRD data showed that as prepared CeO2-ZrO2 powder particles have single phase cubic fluorite structure. HRTEM shows mesoscopic ordering. Average particle size is 12-13 nm as calculated from particle histogram. The nitrogen adsorption/desorption isotherm were classified to be type IV isotherm, typical of mesoporous material. The presence of uni-modal mesopores are confirmed by the pore size distribution which shows pore distribution at around 60 A°. Catalytic activity was studied towards liquid-phase oxidation of benzene.
SIMONA CAVALU_Surface Modification of Alumina/ Zirconia Ceramics Upon Differe...Simona Cavalu
The aim of this study was to prepare and to characterize the structure of Al2O3–3YSZ composites with 5% TiO2 addition
as well as the surface modification upon treatments with SnF2 and NaBF4, respectively. SEM micrographs showed the
controlled densification of the composites as an effect of 3YSZ and TiO2 addition to alumina matrix. By FTIR and XRD,
the characteristics of Al-O and Zr-O vibrations, respectively, the diffractions lines related to a-corundum and zirconia in
tetragonal phase were discussed. Qualitative and quantitative results obtained by XPS and ATR FTIR demonstrated that the
proposed materials are more sensitive to SnF2 than to NaBF4 treatment.
Physical Properties and Compressive Strength of Zinc Oxide Nanopowder as a Po...IJAAS Team
In this study, the application of nanotechnology was applied in the dentistry field, especially in the innovation of dental amalgam material. To date, mercury (Hg) has been used widely as dental amalgam material with consideration of the cheap price, ease of use, and good mechanical strength. However, last few years, many problems have been faced in the dentistry field due to the use of mercury. Hence, new material is needed as an innovation to eliminate the mercury from dental amalgam composition. This research was conducted to analyze the physical properties and compressive strength of zinc oxide (ZnO) nanopowder as a potential dental amalgam material. The physical properties such as morphology and dimensions were analyzed by SEM and XRD. Further, the compression test was conducted by using hydraulic press machine. The results showed that the ZnO nanopowder analyzed has the particle size of 14.34 nm with the morphology classified as nanorods type. On the compression load of 500 kg, the average of ZnO green density is 3.170 g/cm3. This value experienced the increase of 4.763% when the load was set to 1000 kg, and 7.539% at 2000 kg. The dwelling time also took the same effect. At 30 seconds, the average of ZnO green density is 3.260 g/cm3. This value experienced the increase of 0.583% at 60 seconds and 3.098% at 90 seconds.
Surfactant-assisted Hydrothermal Synthesis of Ceria-Zirconia Nanostructured M...IOSR Journals
CeO2–ZrO2 oxides were prepared by the surfactant-templated method using cetyl trimethyl ammonium bromide (CTAB) as template and modified with chromium nitrate. These were characterized by XRD, FT-IR, TEM, SEM, BET and TPD-CO2. The XRD data showed that as prepared CeO2-ZrO2 powder particles have single phase cubic fluorite structure. HRTEM shows mesoscopic ordering. Average particle size is 12-13 nm as calculated from particle histogram. The nitrogen adsorption/desorption isotherm were classified to be type IV isotherm, typical of mesoporous material. The presence of uni-modal mesopores are confirmed by the pore size distribution which shows pore distribution at around 60 A°. Catalytic activity was studied towards liquid-phase oxidation of benzene.
SIMONA CAVALU_Surface Modification of Alumina/ Zirconia Ceramics Upon Differe...Simona Cavalu
The aim of this study was to prepare and to characterize the structure of Al2O3–3YSZ composites with 5% TiO2 addition
as well as the surface modification upon treatments with SnF2 and NaBF4, respectively. SEM micrographs showed the
controlled densification of the composites as an effect of 3YSZ and TiO2 addition to alumina matrix. By FTIR and XRD,
the characteristics of Al-O and Zr-O vibrations, respectively, the diffractions lines related to a-corundum and zirconia in
tetragonal phase were discussed. Qualitative and quantitative results obtained by XPS and ATR FTIR demonstrated that the
proposed materials are more sensitive to SnF2 than to NaBF4 treatment.
Influence of reaction medium on morphology and crystallite size of zinc oxidejournal ijrtem
ABSTRACT : Zinc oxide nanoparticles were prepared by reacting zinc chloride and sodium hydroxide in different mediums such as chitosan, poly vinyl alcohol, ethanol and starch. The materials were characterized by scanning electron microscopy (SEM), x-ray diffraction (XRD) studies, transmission electron microscopy (TEM) and thermogravimetric analysis (TGA). Elemental analysis was done by energy dispersive X-ray Analysis (EDAX).
KEY WORDS : Nano zinc oxide, morphology, crystallite size
The International Journal of Engineering & Science is aimed at providing a platform for researchers, engineers, scientists, or educators to publish their original research results, to exchange new ideas, to disseminate information in innovative designs, engineering experiences and technological skills. It is also the Journal's objective to promote engineering and technology education. All papers submitted to the Journal will be blind peer-reviewed. Only original articles will be published.
The papers for publication in The International Journal of Engineering& Science are selected through rigorous peer reviews to ensure originality, timeliness, relevance, and readability.
Theoretical work submitted to the Journal should be original in its motivation or modeling structure. Empirical analysis should be based on a theoretical framework and should be capable of replication. It is expected that all materials required for replication (including computer programs and data sets) should be available upon request to the authors.
Deposition of Antimony Trioxide on the Composite Surface to Increase Its Fla...Ali I. Al-Mosawi
In the present work, the preparation method of antimony trioxide and its thermal properties
were extracted, as well as identified the manufacturing method to form an insulation layer
from this oxide as a thickness of the covering layer (2 mm), deposited on the composite material consisting of unsaturated polyester resin and glass fiber which acts as a paste and take for the material to the insulation and flame retardant oxide. Thermal erosion test was performed to assess the functioning of the antimony oxide efficiency to flame retardants. The
result obtained from erosion test done at (2000 °C) is an evidence that the antimony trioxide has an efficiency of as a flame retardant material at elevated temperatures.
Crystallization of synthetic wollastonite prepared from local raw materialsMohammed Obeid
Wollastonite (CaSiO3) has been synthesized by the solid state reaction method at a temperature range of 1050-1250℃ from local raw materials, e.g. silica sand and limestone as well as pure chemicals in the form of carbonate and quartz with and without B2O3 adding as a mineralized. The resulting products are investigated employing XRD and SEM techniques. β-wollastonite was obtained at 1050℃ and transformed to pseudowollastonite (α- CaSiO3) at 1150℃ due to the presence of B2O3. While the pure chemicals failed to give wollastonite at this range of temperature 1050-1150℃. As the temperature increased up to 1400℃, both experimental and standard samples have been melted.
Barium titanate (BaTiO3) doped with rare-earth elements (REE) is used as dielectric in the manufacture of multilayer ceramic capacitors (MLCCs). The most common REE oxide employed as dopant for this application is Y2O3. The behavior of the Y3+ in the BaTiO3 structure depends on its concentration and the sintering conditions, among other factors, which can induce the formation of secondary phases that are a potential cause a detriment to the electrical properties of BaTiO3. The purpose of this work is to perform a phase characterization of BaTiO3 doped with different concentrations of Y2O3, validating its possible contribution to the formation of secondary phases. The role of Y2O3 was evaluated on two kinds of raw materials. The first one is pure BaTiO3 (< 100 ppm Y) and the second kind is a commercial formulation designed for MLCCs known as X7R (-55°C and 125°C, 15% tolerance), which among other elements, already contained 1 wt% of Y2O3. High concentrations of Y2O3 (1% up to 20 wt%) were used aiming to promote structural changes, and even the formation of secondary phases in amounts suitable to be detected by X-ray diffraction. Heat treatment of powder and sintering of ceramics (powder compacted at 2 MPa) were conducted in air (1310°C in air for 3 h, two steps: 1350°C then 1150°C 15 h). A phase transition from tetragonal to a mixture of tetragonal and cubic was observed as Y2O3 concentration increases in the thermally treated powder and in the corresponding ceramics. Commercially formulated powder showed higher densification than pure BaTiO3, and produced cubic structure at higher Y2O3concentrations. The phase Ba6Ti17O40is detected in the 20 wt% Y2O3-doped sample.
Flame Retarding-Stabilizing Behavior of Plasticized Poly(vinyl chloride) Cont...Ali I. Al-Mosawi
PhD dissertation:
https://doi.org/10.14750/ME.2021.039
Abstract: There is no universal super-material in the universe, but there are compounds that can have more than one characteristic that make it unconventional, and one of these is discovered in this study, which is Oxydtron (nano cement). Oxydtron has proven excellent efficiency as a flame retardant and surprisingly also showed excellent heat stabilizing effect. Tests carried out were limiting oxygen index, static heat stability, congo-red, differential scanning calorimetry, dehydrochlorination, capillary rheometry analysis, dynamic mechanical analysis, and color change measurement.
These thermal tests proved the ability of Oxydtron to improve the properties of poly(vinyl chloride) at high temperatures reducing the risks associated with the combustion of plasticized poly(vinyl chloride) by increasing its thermal stability, flame retardation, and rate of degradation was effectively decreased. These tests has been shown that Oxydtron is not only a material used to improve the properties of concrete; but also a material that has shown a significant indication in the stabilization process of plasticized poly(vinyl chloride).
As well, the structural changes in the poly(vinyl chloride) layer located directly under the flame zone (heat affected zone-HAZ), which is exposed to high temperatures without burning, have been checked by scanning electron microscopy (SEM) and FLIR analysis. Images obtained from SEM and FLIR analysis for the heat affected zone of limiting oxygen index samples showed a significant decrease in the chlorine content in the poly(vinyl chloride) structure accompanied by considerable stability of the carbon content when compared to the untested samples images. But after adding Oxydtron, the chlorine percentage was maintained at acceptable levels. Also, the effect of the processing method on poly(vinyl chloride)'s properties has been studied. The results obtained from the L.O.I test showed that the extrusion method was better than the rolling method for L.O.I. This behavior because the heat will be distributed uniformly in the screw-extrusion process, which reduces thermal stresses in the final product.
Influence of reaction medium on morphology and crystallite size of zinc oxidejournal ijrtem
ABSTRACT : Zinc oxide nanoparticles were prepared by reacting zinc chloride and sodium hydroxide in different mediums such as chitosan, poly vinyl alcohol, ethanol and starch. The materials were characterized by scanning electron microscopy (SEM), x-ray diffraction (XRD) studies, transmission electron microscopy (TEM) and thermogravimetric analysis (TGA). Elemental analysis was done by energy dispersive X-ray Analysis (EDAX).
KEY WORDS : Nano zinc oxide, morphology, crystallite size
The International Journal of Engineering & Science is aimed at providing a platform for researchers, engineers, scientists, or educators to publish their original research results, to exchange new ideas, to disseminate information in innovative designs, engineering experiences and technological skills. It is also the Journal's objective to promote engineering and technology education. All papers submitted to the Journal will be blind peer-reviewed. Only original articles will be published.
The papers for publication in The International Journal of Engineering& Science are selected through rigorous peer reviews to ensure originality, timeliness, relevance, and readability.
Theoretical work submitted to the Journal should be original in its motivation or modeling structure. Empirical analysis should be based on a theoretical framework and should be capable of replication. It is expected that all materials required for replication (including computer programs and data sets) should be available upon request to the authors.
Deposition of Antimony Trioxide on the Composite Surface to Increase Its Fla...Ali I. Al-Mosawi
In the present work, the preparation method of antimony trioxide and its thermal properties
were extracted, as well as identified the manufacturing method to form an insulation layer
from this oxide as a thickness of the covering layer (2 mm), deposited on the composite material consisting of unsaturated polyester resin and glass fiber which acts as a paste and take for the material to the insulation and flame retardant oxide. Thermal erosion test was performed to assess the functioning of the antimony oxide efficiency to flame retardants. The
result obtained from erosion test done at (2000 °C) is an evidence that the antimony trioxide has an efficiency of as a flame retardant material at elevated temperatures.
Crystallization of synthetic wollastonite prepared from local raw materialsMohammed Obeid
Wollastonite (CaSiO3) has been synthesized by the solid state reaction method at a temperature range of 1050-1250℃ from local raw materials, e.g. silica sand and limestone as well as pure chemicals in the form of carbonate and quartz with and without B2O3 adding as a mineralized. The resulting products are investigated employing XRD and SEM techniques. β-wollastonite was obtained at 1050℃ and transformed to pseudowollastonite (α- CaSiO3) at 1150℃ due to the presence of B2O3. While the pure chemicals failed to give wollastonite at this range of temperature 1050-1150℃. As the temperature increased up to 1400℃, both experimental and standard samples have been melted.
Barium titanate (BaTiO3) doped with rare-earth elements (REE) is used as dielectric in the manufacture of multilayer ceramic capacitors (MLCCs). The most common REE oxide employed as dopant for this application is Y2O3. The behavior of the Y3+ in the BaTiO3 structure depends on its concentration and the sintering conditions, among other factors, which can induce the formation of secondary phases that are a potential cause a detriment to the electrical properties of BaTiO3. The purpose of this work is to perform a phase characterization of BaTiO3 doped with different concentrations of Y2O3, validating its possible contribution to the formation of secondary phases. The role of Y2O3 was evaluated on two kinds of raw materials. The first one is pure BaTiO3 (< 100 ppm Y) and the second kind is a commercial formulation designed for MLCCs known as X7R (-55°C and 125°C, 15% tolerance), which among other elements, already contained 1 wt% of Y2O3. High concentrations of Y2O3 (1% up to 20 wt%) were used aiming to promote structural changes, and even the formation of secondary phases in amounts suitable to be detected by X-ray diffraction. Heat treatment of powder and sintering of ceramics (powder compacted at 2 MPa) were conducted in air (1310°C in air for 3 h, two steps: 1350°C then 1150°C 15 h). A phase transition from tetragonal to a mixture of tetragonal and cubic was observed as Y2O3 concentration increases in the thermally treated powder and in the corresponding ceramics. Commercially formulated powder showed higher densification than pure BaTiO3, and produced cubic structure at higher Y2O3concentrations. The phase Ba6Ti17O40is detected in the 20 wt% Y2O3-doped sample.
Flame Retarding-Stabilizing Behavior of Plasticized Poly(vinyl chloride) Cont...Ali I. Al-Mosawi
PhD dissertation:
https://doi.org/10.14750/ME.2021.039
Abstract: There is no universal super-material in the universe, but there are compounds that can have more than one characteristic that make it unconventional, and one of these is discovered in this study, which is Oxydtron (nano cement). Oxydtron has proven excellent efficiency as a flame retardant and surprisingly also showed excellent heat stabilizing effect. Tests carried out were limiting oxygen index, static heat stability, congo-red, differential scanning calorimetry, dehydrochlorination, capillary rheometry analysis, dynamic mechanical analysis, and color change measurement.
These thermal tests proved the ability of Oxydtron to improve the properties of poly(vinyl chloride) at high temperatures reducing the risks associated with the combustion of plasticized poly(vinyl chloride) by increasing its thermal stability, flame retardation, and rate of degradation was effectively decreased. These tests has been shown that Oxydtron is not only a material used to improve the properties of concrete; but also a material that has shown a significant indication in the stabilization process of plasticized poly(vinyl chloride).
As well, the structural changes in the poly(vinyl chloride) layer located directly under the flame zone (heat affected zone-HAZ), which is exposed to high temperatures without burning, have been checked by scanning electron microscopy (SEM) and FLIR analysis. Images obtained from SEM and FLIR analysis for the heat affected zone of limiting oxygen index samples showed a significant decrease in the chlorine content in the poly(vinyl chloride) structure accompanied by considerable stability of the carbon content when compared to the untested samples images. But after adding Oxydtron, the chlorine percentage was maintained at acceptable levels. Also, the effect of the processing method on poly(vinyl chloride)'s properties has been studied. The results obtained from the L.O.I test showed that the extrusion method was better than the rolling method for L.O.I. This behavior because the heat will be distributed uniformly in the screw-extrusion process, which reduces thermal stresses in the final product.
Elastic studies of Glass Materials Studied by Ultrasonic TechniqueSidek Aziz
Brief review about glass and its physical, elastic and other properties. It also covers the glass preparation techniques, characterization as well as elasticity.
Sinthesis and Properties of Marble-Like Glass-Ceramics Using of Ash from Ther...Scientific Review SR
Color marble-like glass-ceramic materials were obtained through thermal treatment of glasses of the system CaO-Al2O3-SiO2 by using natural materials with the introduction of waste materials - ash from thermal power plants (TPP). The melting of the glass batch was in corundum crucibles at 1450oC with an isothermal hold of 60 min. The glasses obtained was fritted in distilled water and dried for 6 hours at 100oC, then completely crushed and divided into fractions with grain size of 0.8 mm, 1.0 mm, 2 mm, 2.5 mm and over 2.5 mm. It was found that the use of ash from TPP lead to higher values of degree of transformation (crystallization) than using base composition. Values of Avramy parameter’s in the range n=1,0 ÷ 1,6 are showed that crystallization of the glass frit is largely heterogeneous and crystal growing starts from the surface. The introduction of ash from TPP to native glasses carry out to significant reduction of energy of crystallization by Ес=289 kJ/mol to Ec=221 kJ/mol. The glass-ceramic materials were obtained through a one stage crystallization - 1050÷1070оС and an isothermal hold of 60 min., colored white, yellow brown to dark brown. The main crystalline phase in glass-ceramics is β-vollastonite with needle habit, size of crystals - ĺ = 40 ÷ 120 μm and d <5 μm in quantities 37 ÷ 42%. As secondary phases depending on the amount of ash have been identified - the anorthite, gehlenite and α-quartz with prismatic habit were appeared. The obtained glass-ceramic materials have a marble-like effect and technical parameters compared with natural granite and marble and have higher values of density, micro hardness, speed grinding, bending strength and chemical resistance. That’s why they can be used in construction such as lining materials.
Detecting of NH3, CO2 polluted gases by using ZnO- In2O3 thin filmsijceronline
International Journal of Computational Engineering Research (IJCER) is dedicated to protecting personal information and will make every reasonable effort to handle collected information appropriately. All information collected, as well as related requests, will be handled as carefully and efficiently as possible in accordance with IJCER standards for integrity and objectivity.
Detecting of NH3, CO2 polluted gases by using ZnO- In2O3 thin filmsijceronline
International Journal of Computational Engineering Research (IJCER) is dedicated to protecting personal information and will make every reasonable effort to handle collected information appropriately. All information collected, as well as related requests, will be handled as carefully and efficiently as possible in accordance with IJCER standards for integrity and objectivity.
Determination of volatile organic compounds emissions from wood processingMichal Jablonsky
Volatile organic compounds (VOCs) have received a great deal of attention due to their high abundance during the drying process of wood particles. This is a potential environmental issue due to being low level ozone precursors. This work aimed to study the emissions of VOCs during drying in the particleboard manufacturing process. In this study, wood particles were dry and VOCs were collected using a sorption tube. The VOCs were analyzed with gas chromatography-mass spectrometry to explore the effect of temperature on the composition of main components. The results indicated that α-pinene and D-limonene were the dominant components. The results also indicated that using natural gas or wood dust as a heat source did not have a major impact on the emission characteristics of VOCs.
Non‒Conventional Light‒Weight Clay Bricks from Homra and Kraft Pulp Wastes
Original Research Article
Journal of Chemistry and Materials Research Vol. 1 (4), 2014, 123–129
H. H. M. Darweesh,* and M. G. El-Meligy
Transparent and Conducting TiO2 : Nb Thin Films Prepared by Spray Pyrolysis T...arj_online
To date, only sputtering and pulsed laser deposition (PLD) techniques have been employed
successfully to fabricate highly conducting and transparent TiO2:Nb (TNO) films. In this article, we demonstrate
that transparent and conducting
TiO2
: Nb
films can be made by the spray pyrolysis technique. The films were
deposited on Corning 7059 glass substrates at 500
15˚C using an alcoholic precursor solution consisting of
titanium (iv) isopropoxide and
NbCl5
. The influence of increasing
Nb
concentration on the electrical, optical
and structural properties was investigated. The minimum resistivity, 3.36
-3 10
Ω cm, for
Ti1-xNbxO2
film (x
= 0.15) was obtained after 1 hour post deposition annealing in hydrogen atmosphere at 500˚C. The x-ray
diffraction of hydrogen annealed films showed a polycrystalline anatase (004)-oriented phase without any second
phases. The optical band gap for undoped and doped films lay in the range 3.38 – 3.47 eV. Using dispersion
analysis, optical constants were determined from spectro-photometric measurements for films on glass.
Fabrication of microfluidic channels in glass and siliconYichen Sun
Microfluidic channels in glass and silicon chips are fabricated in the cleanroom. Their acoustic focusing properties are then tested and reported in this project report (MEMS 5801).
Spectroscopic properties of lithium borate glass containing Sm3+ and Nd3+ ionsIJAAS Team
Lithium borate glass samples mixed with a different concentration of Sm3+ and Nd3+ ions organized by quenching technique. Structural, vibration groups and spectral properties of glass samples investigated using X-ray diffraction, FTIR, UV/Vis/NIR and photoluminescence spectroscopy. The X-ray confirmed the lithium borate glass samples containing Sm3+ and Nd3+ ions in the amorphous state. Luminescence spectra of glass samples excited at 400 nm recorded, here three luminescence bands observed in Visible region, which due to spectra materials (Sm3+, Nd3+). These indicate that these glass samples responsible orange emission and used in the improvement of materials for LED, and optical devices. The functional vibration groups of the glass matrix studied using FTIR spectroscopy.
2018 khodan an-porous monoliths consisting of aluminum oxyhydroxide nanofibrilsAnatoleNKhodan
Abstract We present a study on the chemical and structural transformations in highly porous monolitic materials consisting of the nanofibrils of aluminum oxyhydroxides (NOA, Al2O3·nH2O) in the temperature range 20– 1700 °C. A remarkable property of the NOA material is the preservation of the monolithic state during annealing over the entire temperature range, although the density of the monolith increases from ~0.02 up to ~3 g/cm3, the total porosity decreases from 99.3 to 25% and remains open up to 4 h annealing at the temperature ~1300 °C. The physical parameters of NOA monoliths such as density, porosity, specific area were studied and a simple physical model describing these parameters as the function of the average size of NOA fibrils—the basic element of 3D structure—was proposed. The observed thermally induced changes in composition and structure of NOA were successfully described and two mechanisms of mass transport in NOA materials were revealed. (i) At moderate temperatures (T ≤ 800 °C), the mass transport occurs along a surface of amorphous single fibril, which results in a weak decrease of the length-to-diameter aspect ratio from the initial value ~24 till ~20; the corresponding NOA porosity change is also small: from initial ~99.5 to 98.5%. (ii) At high temperatures (T > 800 °C), the mass transport occurs in the volume of fibrils, that results in changes of fibrils shape to elliptical and strong decrease of the aspect ratio down to ≤ 2; the porosity of NOA decreases to 25%. These two regimes are characterized by activation energies of 28 and 61 kJ/mol respectively, and the transition temperature corresponds to the beginning of γ-phase crystallization at 870 °C.
Richard's aventures in two entangled wonderlandsRichard Gill
Since the loophole-free Bell experiments of 2020 and the Nobel prizes in physics of 2022, critics of Bell's work have retreated to the fortress of super-determinism. Now, super-determinism is a derogatory word - it just means "determinism". Palmer, Hance and Hossenfelder argue that quantum mechanics and determinism are not incompatible, using a sophisticated mathematical construction based on a subtle thinning of allowed states and measurements in quantum mechanics, such that what is left appears to make Bell's argument fail, without altering the empirical predictions of quantum mechanics. I think however that it is a smoke screen, and the slogan "lost in math" comes to my mind. I will discuss some other recent disproofs of Bell's theorem using the language of causality based on causal graphs. Causal thinking is also central to law and justice. I will mention surprising connections to my work on serial killer nurse cases, in particular the Dutch case of Lucia de Berk and the current UK case of Lucy Letby.
Nutraceutical market, scope and growth: Herbal drug technologyLokesh Patil
As consumer awareness of health and wellness rises, the nutraceutical market—which includes goods like functional meals, drinks, and dietary supplements that provide health advantages beyond basic nutrition—is growing significantly. As healthcare expenses rise, the population ages, and people want natural and preventative health solutions more and more, this industry is increasing quickly. Further driving market expansion are product formulation innovations and the use of cutting-edge technology for customized nutrition. With its worldwide reach, the nutraceutical industry is expected to keep growing and provide significant chances for research and investment in a number of categories, including vitamins, minerals, probiotics, and herbal supplements.
Seminar of U.V. Spectroscopy by SAMIR PANDASAMIR PANDA
Spectroscopy is a branch of science dealing the study of interaction of electromagnetic radiation with matter.
Ultraviolet-visible spectroscopy refers to absorption spectroscopy or reflect spectroscopy in the UV-VIS spectral region.
Ultraviolet-visible spectroscopy is an analytical method that can measure the amount of light received by the analyte.
This presentation explores a brief idea about the structural and functional attributes of nucleotides, the structure and function of genetic materials along with the impact of UV rays and pH upon them.
Remote Sensing and Computational, Evolutionary, Supercomputing, and Intellige...University of Maribor
Slides from talk:
Aleš Zamuda: Remote Sensing and Computational, Evolutionary, Supercomputing, and Intelligent Systems.
11th International Conference on Electrical, Electronics and Computer Engineering (IcETRAN), Niš, 3-6 June 2024
Inter-Society Networking Panel GRSS/MTT-S/CIS Panel Session: Promoting Connection and Cooperation
https://www.etran.rs/2024/en/home-english/
The ability to recreate computational results with minimal effort and actionable metrics provides a solid foundation for scientific research and software development. When people can replicate an analysis at the touch of a button using open-source software, open data, and methods to assess and compare proposals, it significantly eases verification of results, engagement with a diverse range of contributors, and progress. However, we have yet to fully achieve this; there are still many sociotechnical frictions.
Inspired by David Donoho's vision, this talk aims to revisit the three crucial pillars of frictionless reproducibility (data sharing, code sharing, and competitive challenges) with the perspective of deep software variability.
Our observation is that multiple layers — hardware, operating systems, third-party libraries, software versions, input data, compile-time options, and parameters — are subject to variability that exacerbates frictions but is also essential for achieving robust, generalizable results and fostering innovation. I will first review the literature, providing evidence of how the complex variability interactions across these layers affect qualitative and quantitative software properties, thereby complicating the reproduction and replication of scientific studies in various fields.
I will then present some software engineering and AI techniques that can support the strategic exploration of variability spaces. These include the use of abstractions and models (e.g., feature models), sampling strategies (e.g., uniform, random), cost-effective measurements (e.g., incremental build of software configurations), and dimensionality reduction methods (e.g., transfer learning, feature selection, software debloating).
I will finally argue that deep variability is both the problem and solution of frictionless reproducibility, calling the software science community to develop new methods and tools to manage variability and foster reproducibility in software systems.
Exposé invité Journées Nationales du GDR GPL 2024
Comparing Evolved Extractive Text Summary Scores of Bidirectional Encoder Rep...University of Maribor
Slides from:
11th International Conference on Electrical, Electronics and Computer Engineering (IcETRAN), Niš, 3-6 June 2024
Track: Artificial Intelligence
https://www.etran.rs/2024/en/home-english/
Professional air quality monitoring systems provide immediate, on-site data for analysis, compliance, and decision-making.
Monitor common gases, weather parameters, particulates.
Toxic effects of heavy metals : Lead and Arsenicsanjana502982
Heavy metals are naturally occuring metallic chemical elements that have relatively high density, and are toxic at even low concentrations. All toxic metals are termed as heavy metals irrespective of their atomic mass and density, eg. arsenic, lead, mercury, cadmium, thallium, chromium, etc.
3D Hybrid PIC simulation of the plasma expansion (ISSS-14)
Glass ceramic
1. Bulletin of the Chemists and Technologists of Macedonia, Vol. 23, No. 2, pp. 157–162 (2004)
GHTMDD – 448 ISSN 0350 – 0136
Received: May 11, 2004 UDC: 666.1 : 666.3/.7
Accepted: October 18, 2004
Original scientific paper
UTILISATION OF FLY ASH AND WASTE GLASS IN PRODUCTION
OF GLASS-CERAMICS COMPOSITES
Bianka Mangutova1
, Biljana Angjuševa1
, Darko Miloševski1
, Emilija Fidan~evska1
,
Jörg Bossert2
, Milosav Miloševski1
1
Faculty of Technology and Metallurgy, Ss Cyril and Methodius University,
P. O. Box 580, MK-1001 Skopje, Republic of Macedonia
2
Friedrich Schiller University, Institut of Materials Science and Technology,
Lobdergraben 32, Jena 07743, Germany
milo@unet.com.mk
Glass-ceramics composites were produced utilising fly ash from coal power stations and waste glass from TV
monitors, windows and flasks. The addition of 50% flask glass in the fly ash, increases the bending strength and E-
modulus from 9 ± 3 to 77 ± 3 MPa and 6 ± 2 to 29 ± 3 GPa, respectively. Using polyurethane foam as a creator of
porous structure, the obtained porous composites, consisted of fly ash–glass, had the porosity of 70 ± 5 %. E-
modulus and bending strength of the porous systems, obtained by polyurethane foam, were 3.5 ± 1.2 GPa and 6 ± 2
MPa, respectively. The porous materials had a durability (mass loss) of 0.03 – 0.05 % in 0.1 M HCl, which charac-
teristic is identical with the durability of the dense composites.
Key words: glass-ceramics; waste; fly ash; porosity; E-modulus, bending strength
1. INTRODUCTION
Every year about 500 000 tons of the coal
mining waste are produced at the thermal electric
power station “Oslomej” in the Republic of Mace-
donia. This waste is the result of burning of the
coal in the temperature range of 1100 to 1600 o
C.
Due to the burning procedure coal waste is avail-
able in the fine powder form. The waste is classi-
fied according to the size of particles. Waste with
the diameter not bigger than 0.1 mm is taken as fly
ash, and the others belong to slag-ashes and slags.
Their recycling is one of the tasks in the field of
the environment protection which should be solved
in near future. One kind of fly ash contains Fe2O3,
Al2O3, SiO2, MgO, Na2O as the main constituents
and a small amount of ecologically risky oxides as
MnO and PbO. Three kinds of waste glass were
taken from the dump. They are uniform in their
composition and may be considered in correspo-
dence with the original glass. The combination of
the fly ash with waste glass under controlled sinter-
ing procedure gave bulk or highly porous materials
with surface or/and bulk crystallization. The struc-
ture of glass-ceramics built in this way may pre-
vent the migration of ecologically risky elements
into environment due to corrosion or friction [1, 2].
The aim of the investigation is to produce
highly porous composites based on the interactions
between fly ash and waste glass from TV monitors,
windows and flasks. In this way the following ad-
vantages are present: the sintering process leads to
the reduction of energy consumption and ecologi-
cally risky components from the waste that are fixed
molecularly in the silicate phase and additionally
inserted in the ceramic matrix, which either have no
toxic inserted components or have them in eco-
compatible concentration. The porous glass-
ceramics obtained in this way which possesses a
foam like structure can be used as filters, thermal
insulation, lightweight structural laminates, dif-
fused aeration, dust collectors, acoustic absorbers
etc. The principle of this procedure was presented
2. 158 B. Mangutova, B. Angjuševa, D. Miloševski, E. Fidančevska, J. Bossert, M. Miloševski
Bull. Chem. Technol. Macedonia, 23, 2, 157–162 (2004)
as multibarrier-concept by Ondracek [3] and basi-
cally investigated for various waste combinations
[4, 5]. This work deals not only with the chemical
inertisation process and combination of waste ma-
terials but also with new application of these waste
materials as highly porous glass ceramics.
2. EXPERIMENTAL PROCEDURE
Chemical analysis of the waste materials was
carried out using an atomic absorption spectropho-
tometer (Rank Hilger, Atom Spek H-1580) and wet
chemical methods. X-ray diffraction (XRD) studies
on the samples were undertaken using a Philips X-
ray diffraction unit (Model PV 105-1) operating at
CuKα-radiation.
Glass from TV monitors (only from screen)
was treated with 12 %HF and NH4F to dissolve all
non glassy elements [6].
The homogenization of the mineral waste and
the glass waste was made in a planetar mill (Fritsch
pulverisette) for 60 min. The particle size distribu-
tion of the sample was determined by sieve analy-
sis. Thermal characteristics were determined by
heating the microscope (Leitz) in the temperature
interval RT-1500 o
C with a heating rate of 10
o
/min. Pressing the samples was performed by the
uniaxial press (Weber Pressen KIP 100). A pres-
sure of 50 MPa was employed to reach green den-
sities of 55 to 60 % of the theoretical density. Sin-
tering was realized in a chamber furnace in air at-
mosphere at the temperature region from 900 to
1150 o
C, using the heating rate of 10 o
/min and
isothermal treatment at the final temperature of 30
to 120 min. The bulk density of the sintered sam-
ples was determined by the water displacement
method according to EN-993. The value of the
theoretical density of the compacts were calculated
based on the composition of the initial mixture and
known densities of the fly ash and glasses.
Mechanical properties (E-modulus and bend-
ing strength) of the dense and porous specimens (8
pieces, 50×5×5 mm) were investigated at room
temperature. The samples were polished with dia-
mond paste of 15 µm and subjected to the 3-point
bending tester Netzsch 401/3 with 30 mm span and
0.5 mm/min crosshead speed. The thermal studies
of the waste and polyurethane foam were per-
formed by DTA/TG (Netzsch STA 409). Linear
thermal expansion of the dense materials was de-
termined by a dilatometer (Netzsch 402E) in the air
atmosphere and the temperature interval of RT-
650-RT. The measurements were performed with a
heating rate of 2 o
/min.
Open celled macrostructures were fabricated
by coating the struts of polyurethane foam with a
ceramic slurry and then firing the resultant struc-
ture to pyrolyse the substrate and sinter the ceramic
system [7, 8]. Commercial polyurethane foam with
density of 25 kg/m3
was used as a substrate. The
slurry contained 55 % solid (fly ash-glass), 27 %
water glass and 18 % Dolapix CE 64 (4 % water
solution). It coherently coated the polyurethane
substrate. The foam was squeezed and dipped into
slurry, looking in that case like a sponge. During
the expansion to the original shape and size, the
foam was impregnated by the mentioned slurry.
After drying, the coated substrates were heated up
to 950 o
C/1 h in a schedule which minimized dis-
ruption during pyrolysis and allowed the ceramic
to achieve high density. This heating schedule con-
sisted of a heating rate of 1 o
/min up to 500 o
C and
rapid heating of 10 o
/min from 500 o
C to 950 o
C,
1 h held at 950 o
C and then cooling in the furnace.
The relative density of the foam material was de-
termined from the ratio of mass and volume.
Durability of the glass-ceramics was tested
using standard methods both for glass and ceram-
ics. The durability was determined as a mass lost in
0.1 M HCl, 0.1 M Na2CO3 and distilled water. Af-
ter treatment of 24 h and 30 days, the risky ele-
ments like Zn2+
, and Pb2+
were removed from the
tested materials and analysed by atomic absorbtion
spectroscopy. The measurement of radioactivity of
the fly ashes was performed by gamaspectrometry.
3. RESULTS AND DISCUSSION
The chemical composition of the investigated
wastes is shown in Table 1.
The wastes contain Fe2O3, Al2O3, SiO2, and
CaO as the main constituents and a small amount
of ecologically risky oxides as MnO and PbO.
The values of the radioactivity which is very
important as a property of fly ash, are given in Table 2.
According to the book of regulations the
maximal levels of the radioactive contamination of
the human environment (Sl. list No
8/87), the in-
3. Utilisation of fly-ash and waste glass in production of glass-ceramics composites 159
Glas. hem. tehnol. Makedonija, 23, 2, 157‡162 (2004)
vestigated fly ash can be used as a material in a
civil engineering.
T a b l e 1
Chemical compostion of the fly ash Oslomej and
waste glasses
Oslomej TV glass Window glass Flask glassChemical
composition % wt % wt. % wt % wt
ZnO – 0.06 0.09 –
TiO2 0.77 0.09 0.07 –
SO3 0.67 0.11 0.37 0.41
K2O 1.90 6.40 0.19 2.31
Na2O 0.45 7.10 9.50 8.67
Fe2O3 10.02 0.31 0.31 –
CaO 3.36 1.65 8.96 0.21
MgO 1.21 2.42 4.22 7.34
Al2O3 24.13 3.75 3.38 4.76
SiO2 49.60 58.50 71.50 71.62
PbO 0.01 8.18 – –
CoO 0.01 0.08 0.12 –
CO2 5.90 6.30 1.29 –
BaO – 4.81 – –
B2O3 – – – 4.00
MnO 0.27 – – –
NiO 0.02 – – –
Lost of
ignition 2,69 – – –
T a b l e 2
Results of measurements of radioactivity
of fly ash Oslomej
Fly ash Oslomej
40
K 944.7±206.9
212
Bi 62.8±51.9
212
Pb 115.6±18.6
214
Bi 35.8±16.1
214
Pb 72.5±18.7
228
Ac 83.3±19.4
226
Ra –
137
Cs –
134
Cs –
Following to the XRD, the as-received fly ash
contains small amounts of crystalline phases such
as quartz, mullite, hematite and amorphous phase.
The density of the as-received fly ash was
ρf = 2.42 g/cm3
. The thermal characteristics of the
fly ash and glasses are shown in Table 3.
T a b l e 3
Thermal characteristics of the fly ash and waste
glasses (heating microscopy)
Material Significant
shrinkage
Softening
temperature
Melting
temperature
o
C o
C o
C
Fly ash 1140 1300 1340
TV-glass 600 700 800
Window glass 650 850 950
Flask glass 650 850 960
The sintering studies of the pressed compacts
of fly ash showed the highest relative density of 71
± 1% after sintering at 1050 o
C/2h. Sintering at
higher temperature of 1050 o
C exibits side effects
as bending and degassing.
E-modulus, bending strength and technical co-
efficient of thermal expansion of the fly ash sintered
at 1050 o
C/2h and glasses are shown in Table 4.
T a b l e 4
E-modulus, bending strength and thermal
coefficient of thermal expansion
of the fly ash and glasses
Material E-modulus Bending
strength
Tech. coeff. therm.
expan. 106
GPa MPa o
C
Fly ash 6± 2 9 ± 3 6.45
TV glass 72±8 136±10 10.61
Window glass 51±7 125±10 10.10
Flask glass 53±7 127±10 10.80
For the purpose of aiding the sintering proc-
ess and to encapsulate the particles of industrial
wastes into matrix, compatible with the environ-
ment, waste glasses in quantity of 10 to 60 wt%
have been used. By variation of the temperature
(900–1100o
C) and time (0.5–2h) of sintering, com-
pacts with different density were obtained. Optimal
composition of the waste composites, sintering
4. 160 B. Mangutova, B. Angjuševa, D. Miloševski, E. Fidančevska, J. Bossert, M. Miloševski
Bull. Chem. Technol. Macedonia, 23, 2, 157–162 (2004)
temperature, relative density, E-modulus and bend-
ing strength are shown in Table 5.
T a b l e 5
Optimal composition of the waste composites,
sintering temperature, relative density (ρrel.),
E-modulus, bending strength (σ)
Composite Sinter. temp. ρrel. E σ
Fly ash – %glass o
C/1h % GPa MPa
Fly ash – 50 % TV glass 1050 90 30 ± 1 76 ± 2
Fly ash – 50 % window glass 1050 92 29 ± 2 73 ± 3
Fly ash – 50 % flask glass 1050 94 29 ± 2 77 ± 3
From the Table 5 it is evident that the compo-
sition fly ash – 50% flask glass sintered at
1050o
C/1h showed the highest relative density.
The variation of E-modulus and the bending
strength of this system with porosity is shown in
Figs. 1 and 2.
Fig. 1. Variation of the bending strength with the porosity
of the system fly ash – 50% flask glass
Fig. 2. Variation of the E-modulus with the porosity
of the system fly ash – 50% flask glass
Approximation of the E-modulus and the
bending strength with porosity are given with
eqs.(1, 2):
E = 37.9 exp (–0.026 Θ) , (1)
σ = 100.1 exp(–0.037 Θ) , (2)
where: Θ – porosity / %; E / GPa; σ /MPa.
In the first approximation, for zero porosity,
E-modulus and the bending strength have values of
Eo = 37.9 GPa and σo = 100.1 MPa
Figures 1 and 2 show that increase of the po-
rosity from 6 to 26 % leads to a 51 % reduction for
σ, and 45 % for E-modulus.
Thermal expansion characteristics of these
investigated systems in the interval RT-600-RT
showed absence of hysteresis effect, that proves
that the systems are in thermal equilibrium [9]. The
temperature dependence of the thermal expansion
in the interval RT-600 o
C can be represented by a
II order polynomial form. Table 6 shows the tem-
perature variation of the physical and the technical
coefficient of thermal expansion.
T a b l e 6
Temperature variation of the physical and the technical coefficient of thermal expansion
Composite ∂(∆ L/Lo)/∂T = f(T) αtech 10–6
/ o
C
Oslomej – 50%TV glass 0.017 – 7.178·10–5
T + 1.097·10–9
T2
8.53
Oslomej – 50% window glass 0.031 – 1.069·10–6
T + 1.303·10–9
T2
8.28
Oslomej – 50% flask glass 0.019 – 7.736·10–5
T + 1.113·10–9
T2
8.62
Durability of the investigated dense materials
(mass lost after 30 days) was determined for ce-
ramics containing only fly ash (F) and the compos-
ites, fly ash – 50 % TV glass (TV50), fly ash –
50 % window glass (W50) and fly ash – 50 % flask
glass (FG50). The composite (TV50) possesses
durability of 0.12 %, (W50) of 0.06 %, (FG50) of
0.07 %, where as (F) possesses durability of 4.54 %
0
20
40
60
80
100
5 10 15 20 25 30
Θ / %
Bendingstrength
5
10
15
20
25
30
35
40
5 10 15 20 25 30
Θ / %
E-modulus
5. Utilisation of fly-ash and waste glass in production of glass-ceramics composites 161
Glas. hem. tehnol. Makedonija, 23, 2, 157‡162 (2004)
in 0.1M HCl. The change in mass in 0.1M Na2CO3
was –0.01 % for (TV50), –0.02 % for (W50),
–0.01 % for (FG50) and –0.07 % for (F). In all in-
vestigated specimens durability in water was
0.001 %. The durability allows the categorization
of these materials to definite classes according to
DIN EN 122. All investigated composites belong
to the class B (visible changes of colour). The
durabilities show that the ceramics meet the re-
quirements of dense unglazed, dust-pressed ce-
ramic tiles according to building ceramic norms
DIN EN 106.
By using a polyurethane foam as the creator
of a porous structure, samples of fly ash –50 %
flask glass with a porosity of 70 ± 5 % were fabri-
cated (Fig. 3).
The pores with diameters from 300 to 600 µm
are interconnected. The E-modulus of this system
was 3.5±1.2 GPa, bending strength was 6±2 MPa.
Fractures among the pore walls were not evident.
Durability of this porous system (mass lost) was
0.065% in 0.1M HCl and 0.01% in 0.1M Na2CO3.
The dense composites can be used in the building
industry [1], while the porous composites are a
potential material for producing diffusers which
could be used for water aeration [10].
Fig. 3. Macrostructure of cell foam fly ash – 50% flask glass
(bar 1200 µm)
CONCLUSIONS
Ecologically harmless materials (glass ce-
ramics) can be created from fly ash and waste
glasses.
The addition of 50% flask glass in the fly
ash, increases the bending strength and E-modulus
from 9±3 to 77±3 MPa and 6±2 to 29±2 GPa, re-
spectively.
Approximation of the E-modulus and bend-
ing strength with porosity are given with equations
E = 37.9exp(–0.026Θ) and σ = 100.1exp(–0.037Θ)
Polyurethane foam was used as a creator of
porous structure and the obtained porous compos-
ites consisted of fly ash – glass had the porosity of
70 ±5%.
E-modulus and bending strength of the
porous systems consisted of fly ash-glass were
3.5 ± 1.2 GPa and 6 ± 2 MPa, respectively.
The chemical and physical properties of the
dense material, makes them suitable for a wide
range of applications in the building industry.
AAcckknnoowwlleeddggeemmeenntt:: This work was supported by
the European Community, contract ICA2-CT-2002-
10003-REINTRO in the frame of the INCO COPER-
NICUS program.
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R e z i m e
PRIMENA NA LEBDE^KA PRA[INA I OTPADNO STAKLO VO PROIZVODSTVOTO
NA STAKLO-KERAMI^KI KOMPOZITI
Bianka Mangutova1
, Biljana An|u{eva1
, Darko Milo{evski1
, Emilija Fidan~evska1
,
Jörg Bossert2
, Milosav Milo{evski1
1
Tehnolo{ko-metalur{ki fakultet, Univerzitet "Sv. Kiril i Metodij",
p. fah 580, MK-1001 Skopje, Republika Makedonija
2
Friedrich Schiller University, Institut of Materials Science and Technology,
Lobdergraben 32, Jena 07743, Germany
milo@unet.com.mk
Klu~ni zborovi: staklo-keramika; otpad; lebde~ka pra{ina; porozitet; E-modul; rastvorlivost
Staklo-kerami~kite kompoziti bea dobieni so
primena na lebde~ka pra{ina od termocentralite i
na otpadno staklo od TV monitori, prozorsko i am-
bala`no. So dodavawe na 50% ambala`no staklo vo
lebde~kata pra{ina ja~inata na svitkuvawe i E-
modulot bea zgolemeni od 9 ± 3 na 77 ± 3 MRa i od 6 ± 2
na 29 ± 3 GPa, soodvetno. So upotreba na poliuretan-
ska pena, kako kreator na porozna struktura, bea do-
bieni porozni kompoziti od lebde~ka pra{ina i
staklo, so porozitet od 70 ± 5 %. E-modulot i ja~ina-
ta na svitkuvawe na poroznite sistemi bea 3,5 ±
1,2 GPa i 6 ± 2 MRa, soodvetno. Poroznite materijali
poseduvaat rastvorlivost (zaguba na masa) od 0,03 do
0,05 % vo 0,1 M HCl, identi~no so rastvorlivosta na
gustite kompoziti so ist sostav.