Size Reduction and the
Importance of Low Particle Size
Who Am I?
Rich Robatzek – Product Manager, Sturtevant Inc.
 Business development manager for the Micronizer® jet
mill product line.
 Extensive background as a Sales Manager contributing to
the growth and profitability of manufacturing companies
 More than 20 years of industrial sales experience,
growing sales territories, leading sales teams and
developing new business.
 Experience in food, pharmaceutical, and consumer good
industries
Sturtevant - Perfecting Particle Size
Perfecting Service
Over 60% of our sales are repeat customers
• All operations are under one roof which results in fast, reliable problem solving
• open, full service testing facility to test each customer’s specific material and understand the
grinding characteristics
• An experienced field team is available for startup and field service.
Perfecting Experience
Thousands of installations, 60 years of micronizing
• The original Micronizer® company
• Sturtevant employees average over 20 years of service
• Customer driven innovations including more sizes, varieties and accessories than any other jet
mill manufacturer
Perfecting Reliability
130 years of family operated, US manufacturing
• Sturtevant President W. Sturtevant English, Jr. is the fifth generation of family management
• Made in the USA means Sturtevant’s Center of Excellence and all product knowledge is
domestic and easy to access
• Installations in over 50 countries with every major manufacturer requiring fine grinding
Crushing / Grinding Methods
• Impact
• Compression
• Shear
• Attrition
What is Micronization?
Micronization is the process of reducing a
solid materials average particle size to low
micron and sub micron particle sizes.
Why is Micronization Important
in Industry?
• Control of rate of dissolution and absorption
• Control of chemical reactions.
• Control of physical characteristics
Why is Micronization Important
in Industry?
• Control optical properties.
• Product Preparations.
• Efficiency – Your competitive advantage.
Benefits of Micronized Particles
• Higher Surface Area
• Tight Particle Size Distribution
• Uniform Size, Spherical Shape
• Better Control Properties of Powders,
• (suspension, dispersion & absorption)
• More Predictable Performance of Powders
Total Surface Area vs Particle Diameter
for Spherical Objects
0
10000
20000
30000
40000
50000
60000
70000
0 10 20 30 40 50 60 70 80 90
TotalSurfaceArea(in2)
Diameter (µm)
0.5 µm = 500 Nm
1 µm = 1,000 Nm
2 µm = 2,000 Nm
5 µm = 5,000 Nm
10 µm = 10,000 Nm
Tight Particle Size Distribution
d50 d90d10
Ultra Fines Grit
Micronized PSD
Similar d50
Median
But Lower Mean
(Average)
Less Grit/Less
Ultrafines
Uniform Spherical Particles
Wide PSD – Irregular Particles Tight PSD – Uniform Spherical Particles
Before Micronizing (-50 microns) After Micronizing (-10 microns)
Principals of Operation
Factors of Grindability
• Brittle vs. Resilient
• Crystalline
• Fibrous or Polymeric
• Feed Particle Size
• Typically 75-150 Microns
• Max 800 Microns
• Multi-Element Formulation
• Moisture or Cohesive
How Feed Rate Affects Particle
Size Distribution
Cosmetic Powders
Feed: d100 = 416 µm, d90 = 29 µm, d50 = 6.0 µm, d10 = 1.3 µm
Test No. 11: d100 = 15 µm, d90 = 6.0 µm, d50 = 2.7 µm, d10 = 1.0 µm
Test No. 12: d100 = 20 µm, d90 = 7.5 µm, d50 = 3.2 µm, d10 = 1.1 µm
Pharmaceuticals
Advantageous for Ease of Cleaning,
No Contamination & Small Batches
• Orals, Injectables, Inhalers, Topicals, etc.
• Antibiotics
• Amino Acids
• Steroids
• Vitamins
Pharmaceuticals
Dolasetron
Mesylate
for Nausea
Ibuprophen
Feed d50=25 µm
Test 1 d50=1.5 µm
Test 2 d50=2.1 µm
Advantageous for High Surface Area
• Greater Coverage, Consistent Color in Paints
• TiO2, Carbon Black, Iron Oxide
• Finer than hammer mill
• No oversize grit
• Very smooth products
Pigment
Iron Oxide Pigment
Cosmetics
Advantageous for Silky Texture, No Heat
• Eye Shadow, Blush, Lipstick, Eye Liners
• Finer than hammer mill
• No oversize grit
• Very smooth products
Cosmetic Powder
Feed: d90 = 17.2 µm, d50 = 5.84 µm, d10 = 1.56 µm
Test 1: d90 = 7.17 µm, d50 = 3.41 µm, d10 = 1.17 µm
Agricultural Chemicals
Advantageous for Heat Sensitive Powders
• Herbicides, Pesticides, Insecticides, Fungicides
• No temperature rise
• Powder dissolves easily
• No spray nozzle clog
Agricultural Chemicals
Herbicide used in the Agricultural Industry
Feed: d100 = 665 µm, d90 = 81.6 µm, d50 = 8.51 µm, d10 = 1.43 µm
Test 1: d100 = 21.1 µm,d90 = 8.59 µm, d50 = 2.90 µm, d10 = 0.56 µm
Ceramics
Advantageous for Abrasive Powders
• No contamination in electronics & dental implants
• Aluminum Oxide, Zirconium Oxide, Glass
• No moving parts
• Ceramic wear liners
• No lubrication
• No oversize grit
Foods & Additives
Advantageous for Ease of Cleaning, No
Contamination & No Heat
• Sugar/Sweeteners/Salts (instant soups, sodas)
• Proteins (baby formulas)
• Gelatin/Sodium Cellulose (thickeners)
11 Micronizer Sizes
Fineness Vs Energy
Equipment Product HP lb/hr lb/hr per HP
Jaw Crusher 1/2”- 2” 10 6K – 20K 600-2000
Pin Mill 45-75 µm 20 2K – 4K 100-200
ACM 20-45 µm 35 200 – 2K 6-60
Jet Mill 0-20 µm 40 10 – 100 0.25-2.5
Production System
1
2
3
1) Feeder
2) Micronizer®
3) Bag House
4) Product Collector
4
Up to 42” diameter
6,000 lbs/hr
Q&A
Rich Robatzek
Micronizer® Product Manager
Office: 978-829-1418
Cell: 617-615-7176
rrobatzek@sturtevantinc.com
Micronizer® is a registered trademark of Sturtevant Inc.
Perfecting Particle Size since 1883

Size reduction and the importance of particle size

  • 1.
    Size Reduction andthe Importance of Low Particle Size
  • 2.
    Who Am I? RichRobatzek – Product Manager, Sturtevant Inc.  Business development manager for the Micronizer® jet mill product line.  Extensive background as a Sales Manager contributing to the growth and profitability of manufacturing companies  More than 20 years of industrial sales experience, growing sales territories, leading sales teams and developing new business.  Experience in food, pharmaceutical, and consumer good industries
  • 3.
    Sturtevant - PerfectingParticle Size Perfecting Service Over 60% of our sales are repeat customers • All operations are under one roof which results in fast, reliable problem solving • open, full service testing facility to test each customer’s specific material and understand the grinding characteristics • An experienced field team is available for startup and field service. Perfecting Experience Thousands of installations, 60 years of micronizing • The original Micronizer® company • Sturtevant employees average over 20 years of service • Customer driven innovations including more sizes, varieties and accessories than any other jet mill manufacturer Perfecting Reliability 130 years of family operated, US manufacturing • Sturtevant President W. Sturtevant English, Jr. is the fifth generation of family management • Made in the USA means Sturtevant’s Center of Excellence and all product knowledge is domestic and easy to access • Installations in over 50 countries with every major manufacturer requiring fine grinding
  • 4.
    Crushing / GrindingMethods • Impact • Compression • Shear • Attrition
  • 5.
    What is Micronization? Micronizationis the process of reducing a solid materials average particle size to low micron and sub micron particle sizes.
  • 6.
    Why is MicronizationImportant in Industry? • Control of rate of dissolution and absorption • Control of chemical reactions. • Control of physical characteristics
  • 7.
    Why is MicronizationImportant in Industry? • Control optical properties. • Product Preparations. • Efficiency – Your competitive advantage.
  • 8.
    Benefits of MicronizedParticles • Higher Surface Area • Tight Particle Size Distribution • Uniform Size, Spherical Shape • Better Control Properties of Powders, • (suspension, dispersion & absorption) • More Predictable Performance of Powders
  • 9.
    Total Surface Areavs Particle Diameter for Spherical Objects 0 10000 20000 30000 40000 50000 60000 70000 0 10 20 30 40 50 60 70 80 90 TotalSurfaceArea(in2) Diameter (µm) 0.5 µm = 500 Nm 1 µm = 1,000 Nm 2 µm = 2,000 Nm 5 µm = 5,000 Nm 10 µm = 10,000 Nm
  • 10.
    Tight Particle SizeDistribution d50 d90d10 Ultra Fines Grit Micronized PSD Similar d50 Median But Lower Mean (Average) Less Grit/Less Ultrafines
  • 11.
    Uniform Spherical Particles WidePSD – Irregular Particles Tight PSD – Uniform Spherical Particles Before Micronizing (-50 microns) After Micronizing (-10 microns)
  • 12.
  • 13.
    Factors of Grindability •Brittle vs. Resilient • Crystalline • Fibrous or Polymeric • Feed Particle Size • Typically 75-150 Microns • Max 800 Microns • Multi-Element Formulation • Moisture or Cohesive
  • 14.
    How Feed RateAffects Particle Size Distribution Cosmetic Powders Feed: d100 = 416 µm, d90 = 29 µm, d50 = 6.0 µm, d10 = 1.3 µm Test No. 11: d100 = 15 µm, d90 = 6.0 µm, d50 = 2.7 µm, d10 = 1.0 µm Test No. 12: d100 = 20 µm, d90 = 7.5 µm, d50 = 3.2 µm, d10 = 1.1 µm
  • 15.
    Pharmaceuticals Advantageous for Easeof Cleaning, No Contamination & Small Batches • Orals, Injectables, Inhalers, Topicals, etc. • Antibiotics • Amino Acids • Steroids • Vitamins
  • 16.
  • 17.
    Advantageous for HighSurface Area • Greater Coverage, Consistent Color in Paints • TiO2, Carbon Black, Iron Oxide • Finer than hammer mill • No oversize grit • Very smooth products Pigment
  • 18.
  • 19.
    Cosmetics Advantageous for SilkyTexture, No Heat • Eye Shadow, Blush, Lipstick, Eye Liners • Finer than hammer mill • No oversize grit • Very smooth products
  • 20.
    Cosmetic Powder Feed: d90= 17.2 µm, d50 = 5.84 µm, d10 = 1.56 µm Test 1: d90 = 7.17 µm, d50 = 3.41 µm, d10 = 1.17 µm
  • 21.
    Agricultural Chemicals Advantageous forHeat Sensitive Powders • Herbicides, Pesticides, Insecticides, Fungicides • No temperature rise • Powder dissolves easily • No spray nozzle clog
  • 22.
    Agricultural Chemicals Herbicide usedin the Agricultural Industry Feed: d100 = 665 µm, d90 = 81.6 µm, d50 = 8.51 µm, d10 = 1.43 µm Test 1: d100 = 21.1 µm,d90 = 8.59 µm, d50 = 2.90 µm, d10 = 0.56 µm
  • 23.
    Ceramics Advantageous for AbrasivePowders • No contamination in electronics & dental implants • Aluminum Oxide, Zirconium Oxide, Glass • No moving parts • Ceramic wear liners • No lubrication • No oversize grit
  • 24.
    Foods & Additives Advantageousfor Ease of Cleaning, No Contamination & No Heat • Sugar/Sweeteners/Salts (instant soups, sodas) • Proteins (baby formulas) • Gelatin/Sodium Cellulose (thickeners)
  • 25.
  • 26.
    Fineness Vs Energy EquipmentProduct HP lb/hr lb/hr per HP Jaw Crusher 1/2”- 2” 10 6K – 20K 600-2000 Pin Mill 45-75 µm 20 2K – 4K 100-200 ACM 20-45 µm 35 200 – 2K 6-60 Jet Mill 0-20 µm 40 10 – 100 0.25-2.5
  • 27.
    Production System 1 2 3 1) Feeder 2)Micronizer® 3) Bag House 4) Product Collector 4 Up to 42” diameter 6,000 lbs/hr
  • 28.
    Q&A Rich Robatzek Micronizer® ProductManager Office: 978-829-1418 Cell: 617-615-7176 rrobatzek@sturtevantinc.com Micronizer® is a registered trademark of Sturtevant Inc.
  • 29.