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AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110
www.ijera.com 107|P a g e
Testing theOdour Quality of Non-Metallic Materials
AVIJIT SINGH GANGWAR
B.E. Automobile Engineer, Manipal Institute Of Technology
Abstract-
This report has been compiled on the completion of 3 week summer training at ICAT. It discusses about a very
necessary and least popular part of the Automotive Industry i.e. Testing and Certification. It discusses about one
of the government notified Testing body ICAT which is one of just 6 such organisations in India.This report
deals with the odour quality testing of non-metallic materials that are used for automobile compartment and
parts associated with the compartment.
Keywords –Odour Quality, Testing.
I. INTRODUCTION(Heading1)
The Project aims at creating core global
competencies in Automotive sector in India and
facilitate seamless integration of Indian Automotive
industry with the world as also to position the country
prominently on the global automotive map.
II. CMEL- Component & Material
Evaluation Lab
As it is clear from the name CMEL is a state of
art laboratory established by iCAT equipped with
many national, international and self development test
equipments for the testing and evolution purpose.
These equipments are also used for certification of
specimen as per various norms both national and
international.
III. EVALUATION
Evaluation is a systematic determination of a
subject's merit, worth and significance, using criteria
governed by a set of standards. It can assist an
organization to assess any aim, realisable
concept/proposal, or any alternative, to help in
decision-making; or to ascertain the degree of
achievement or value in regard to the aim and
objectives and results of any such action that has been
completed. The primary purpose of evaluation, in
addition to gaining insight into prior or existing
initiatives, is to enable reflection and assist in the
identification of future change.
Evaluation is often used to characterize and apprise
subjects of interest in a wide range of human
enterprises, including the arts, criminal justice,
foundations, non-profit organizations, government,
health care, and other human services.
A systematic, rigorous, and meticulous application of
scientific methods to assess the design,
implementation, improvement, or outcomes of a
program. It is a resource-intensive process, frequently
requiring resources, such as, evaluator expertise,
labour, time, and a sizeable budget
IV. ODOUR TEST
When we purchase items, odor is one of the
criteria we use to judge products. A delightful odor
causes an attraction to an item while a noxious odor
may cause one to walk away from an item. In the
automotive industry, the same principle holds true.
While with a single item, an apple, or piece of
clothing, the control over odor is minimal because the
article is relatively simple. The automobile has
greater challenges since it is a complex article with a
variety of materials each that potentially may emit
odors that could adversely affect a sale or customer
satisfaction. Therefore it is critical to be able to test
each component that is used in the construction of a
vehicle.
Automotive interior pollution has become a
concerned topic of the general consumers. World's
leading automotive companies have all developed
standards to monitor their own business-related
substances which may create a scent in a car.
Control vehicle air pollution, improve air inside air
quality, is today’s development of domestic and
foreign automobile technology issue. It is reported
that the forthcoming national air pollution limits for
standard car, car interior pollution has become a hot
concern for the public. Sometimes there is unknown
odor in a car, even some instrument can not identify,
therefore there is a industrial testing service for
automotive manufacturing industry, odor test.
Odor refers to automotive interiors smell directly
or indirectly from any part of an automotive interior,
based on human olfactory senses and a comfort
evaluation of vehicle quality. It should be noted that
some of the odor may be harmful, and some good
small may also be harmful. The smell in a vehicle is a
RESEARCH ARTICLE OPEN ACCESS
AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110
www.ijera.com 108|P a g e
key concern when purchasing a vehicle, so car
manufacturers are requiring their suppliers to carry
out odor testing to prove their products are free of
odor, to ensure that the car smell is not cause
consumer dissatisfaction.
Odor testing requires the intimate involvement of
people to do testing and rating of various materials.
With the increased emphasis of corporations to
improve Environment, Health and Safety, there is a
desire to minimize the human interaction with odor
testing. At the same time and in conjunction with an
increased emphasis on reducing volatile organic
compounds in vehicles, rigorous testing is required to
produce vehicles with acceptable odor performance.
Through component level odor testing, hopefully the
full vehicle odor test will be acceptable
V. TESTING(Heading 2)
i. SCOPE OF THE PROJECT: The odour
quality of non-metallic materials that are used
for automobile compartment and parts
associated with the compartment.
ii. TEST OUTLINE :
1. Preparation for water extraction
a. Prepare test equipment and samples
2. Water extraction
a. Heat the sample, sample component that
emits smell.
3. Odour test
a. Prepare bag,make standard odour, pour
sample, smell, summarize results.
iii. Preparation of water extraction
1. Preparation of test equipment
a. Table 1 lists the tools and devices
necessary for the test. Test equipment,
tools and devices must be free from
smell, except for reagents.
b.
AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110
www.ijera.com 109|P a g e
Table 1 - Test equipment
iv. PREPARATION OF SAMPLE :
Prepare 15 test pieces when using a 4-L
container.
v. WATER EXTRACTION :
 HEATING OF SAMPLE :
1. Place the sample in the stainless can.
2. Heat using the dryer. Heating temperature
should be 80°C. The heating duration should
be 4 hours after the temperature in the dryer
reached the specified temperature.
 Sampling of component that emits smell
1. Pour 8ml of non-smell distilled water in the
bubbler shown in figure and place the
bubbler in the container with ice in it.
2. One hour after the
temperature in the dryer
reached the specified
temperature, operate the
pump at a rate of 1 L/min
and sample the component
that emits smell in the
distilled water. Sampling
duration shall be 3 hours.
3. Three hours after
sampling, stop pump,
remove the bubbler from
the test equipment, seal
the opening with a sealing
tape , etc. , and store until
the odour test. The
maximum storage period
shall be 24hours after
sampling.
vi. ODOUR TEST :
 Preparation of standard smell
Dilute the acetic acid reagent with
distilled water up to the following
concentration and use the solution
as standard smell.
When the acetic acid concentration
is 0.05 mass % , smell intensity- 3,
pleasantness / unpleasantness - −1.5
When the acetic acid concentration
is 0.005 mass%, smell intensity 2,
pleasantness / unpleasantness −1.
 Pouring of sample
Use a syringe and drop 2ml water in
the bubbler where the component
that emits smell is sampled into the
bag. Fill 2.2L of N2 gases and
block the sleeve using a silicon
rubber cap etc. And leave under
room temperature for 6hours. Do
the same way for the standard smell
too.
 Smelling should be done by 5 different
panellists against the standard smells.
 Summarize the results.
VI. CONCLUSION
Sample and the other odor samples from the
sample set were tested by the odor panel to determine
concentration, intensity, persistency, character and
Hedonic tone. The results of testing Sample are
summarized below:
PRODUCT MATERIAL DIMENSIONS QUANTITY
CHAMBER STAINLESS STEEL 150*150*150mm 1
VOLUME - 3.1L
AIR BUBBLER GLASS CAP DIAMETER - 20mm 1
VOLUME - 22ml
LENGTH - 143mm
COMPRESSED AIR PUMP FLOW RATE - 1 L/min 1
SILICON TUBES SILICON INSIDE DIAMETER - 5mm 2m tube
OUTSIDE DIAMETER - 9mm
TEFLON TUBES TEFLON INSIDE DIAMETER - 5mm 5-10 m tube
OUTSIDE DIAMETER - 8mm
GLACIAL ACETIC ACID MIN. CONC. - 99.7% 500ml
NITROGEN GAS MIN. CONC. - 99.999% 1 CYLINDER
MILER BAG PET OUTSIDE DIAMETER - 7mm 1
VOLUME - 3 L
JOINT FLUOROCARBON RESINS OUTSIDE DIAMETER - 8mm
CAP SILICON RUBBER
AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110
www.ijera.com 110|P a g e
TABLE 2 - RESULTS
Detection Threshold
430
Recognition threshold
180
Intensity as ppm n-butanol
37
Character descriptors
Sewer
Ammonia
Amine
Hedonic tone
−4
REFERENCES
[1.] Government Policy,
http://www.dhi.nic.in/autopolicy.html
[2.] Automobile policy,
http://www.siamindia.com/scripts/auto-
policy.aspx
[3.] Policy Report,
http://autocarpro.in/contents/specialReportD
etails.aspx?SpecialReportID=90
[4.] http://www.natrip.in/
[5.] http://www.icat.in/
[6.] Automotive Safety,
http://en.wikipedia.org/wiki/Automobile_saf
ety#Active_and_passive_safety
[7.] ICAT,
http://en.wikipedia.org/wiki/International_C
entre_for_Automotive_Technology
[8.] NATRiP
http://en.wikipedia.org/wiki/NATRiP
[9.] NATRiP ,
http://www.natrip.in/DisplayContents.aspx?
menuid=222

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Testing theOdour Quality of Non-Metallic Materials

  • 1. AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110 www.ijera.com 107|P a g e Testing theOdour Quality of Non-Metallic Materials AVIJIT SINGH GANGWAR B.E. Automobile Engineer, Manipal Institute Of Technology Abstract- This report has been compiled on the completion of 3 week summer training at ICAT. It discusses about a very necessary and least popular part of the Automotive Industry i.e. Testing and Certification. It discusses about one of the government notified Testing body ICAT which is one of just 6 such organisations in India.This report deals with the odour quality testing of non-metallic materials that are used for automobile compartment and parts associated with the compartment. Keywords –Odour Quality, Testing. I. INTRODUCTION(Heading1) The Project aims at creating core global competencies in Automotive sector in India and facilitate seamless integration of Indian Automotive industry with the world as also to position the country prominently on the global automotive map. II. CMEL- Component & Material Evaluation Lab As it is clear from the name CMEL is a state of art laboratory established by iCAT equipped with many national, international and self development test equipments for the testing and evolution purpose. These equipments are also used for certification of specimen as per various norms both national and international. III. EVALUATION Evaluation is a systematic determination of a subject's merit, worth and significance, using criteria governed by a set of standards. It can assist an organization to assess any aim, realisable concept/proposal, or any alternative, to help in decision-making; or to ascertain the degree of achievement or value in regard to the aim and objectives and results of any such action that has been completed. The primary purpose of evaluation, in addition to gaining insight into prior or existing initiatives, is to enable reflection and assist in the identification of future change. Evaluation is often used to characterize and apprise subjects of interest in a wide range of human enterprises, including the arts, criminal justice, foundations, non-profit organizations, government, health care, and other human services. A systematic, rigorous, and meticulous application of scientific methods to assess the design, implementation, improvement, or outcomes of a program. It is a resource-intensive process, frequently requiring resources, such as, evaluator expertise, labour, time, and a sizeable budget IV. ODOUR TEST When we purchase items, odor is one of the criteria we use to judge products. A delightful odor causes an attraction to an item while a noxious odor may cause one to walk away from an item. In the automotive industry, the same principle holds true. While with a single item, an apple, or piece of clothing, the control over odor is minimal because the article is relatively simple. The automobile has greater challenges since it is a complex article with a variety of materials each that potentially may emit odors that could adversely affect a sale or customer satisfaction. Therefore it is critical to be able to test each component that is used in the construction of a vehicle. Automotive interior pollution has become a concerned topic of the general consumers. World's leading automotive companies have all developed standards to monitor their own business-related substances which may create a scent in a car. Control vehicle air pollution, improve air inside air quality, is today’s development of domestic and foreign automobile technology issue. It is reported that the forthcoming national air pollution limits for standard car, car interior pollution has become a hot concern for the public. Sometimes there is unknown odor in a car, even some instrument can not identify, therefore there is a industrial testing service for automotive manufacturing industry, odor test. Odor refers to automotive interiors smell directly or indirectly from any part of an automotive interior, based on human olfactory senses and a comfort evaluation of vehicle quality. It should be noted that some of the odor may be harmful, and some good small may also be harmful. The smell in a vehicle is a RESEARCH ARTICLE OPEN ACCESS
  • 2. AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110 www.ijera.com 108|P a g e key concern when purchasing a vehicle, so car manufacturers are requiring their suppliers to carry out odor testing to prove their products are free of odor, to ensure that the car smell is not cause consumer dissatisfaction. Odor testing requires the intimate involvement of people to do testing and rating of various materials. With the increased emphasis of corporations to improve Environment, Health and Safety, there is a desire to minimize the human interaction with odor testing. At the same time and in conjunction with an increased emphasis on reducing volatile organic compounds in vehicles, rigorous testing is required to produce vehicles with acceptable odor performance. Through component level odor testing, hopefully the full vehicle odor test will be acceptable V. TESTING(Heading 2) i. SCOPE OF THE PROJECT: The odour quality of non-metallic materials that are used for automobile compartment and parts associated with the compartment. ii. TEST OUTLINE : 1. Preparation for water extraction a. Prepare test equipment and samples 2. Water extraction a. Heat the sample, sample component that emits smell. 3. Odour test a. Prepare bag,make standard odour, pour sample, smell, summarize results. iii. Preparation of water extraction 1. Preparation of test equipment a. Table 1 lists the tools and devices necessary for the test. Test equipment, tools and devices must be free from smell, except for reagents. b.
  • 3. AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110 www.ijera.com 109|P a g e Table 1 - Test equipment iv. PREPARATION OF SAMPLE : Prepare 15 test pieces when using a 4-L container. v. WATER EXTRACTION :  HEATING OF SAMPLE : 1. Place the sample in the stainless can. 2. Heat using the dryer. Heating temperature should be 80°C. The heating duration should be 4 hours after the temperature in the dryer reached the specified temperature.  Sampling of component that emits smell 1. Pour 8ml of non-smell distilled water in the bubbler shown in figure and place the bubbler in the container with ice in it. 2. One hour after the temperature in the dryer reached the specified temperature, operate the pump at a rate of 1 L/min and sample the component that emits smell in the distilled water. Sampling duration shall be 3 hours. 3. Three hours after sampling, stop pump, remove the bubbler from the test equipment, seal the opening with a sealing tape , etc. , and store until the odour test. The maximum storage period shall be 24hours after sampling. vi. ODOUR TEST :  Preparation of standard smell Dilute the acetic acid reagent with distilled water up to the following concentration and use the solution as standard smell. When the acetic acid concentration is 0.05 mass % , smell intensity- 3, pleasantness / unpleasantness - −1.5 When the acetic acid concentration is 0.005 mass%, smell intensity 2, pleasantness / unpleasantness −1.  Pouring of sample Use a syringe and drop 2ml water in the bubbler where the component that emits smell is sampled into the bag. Fill 2.2L of N2 gases and block the sleeve using a silicon rubber cap etc. And leave under room temperature for 6hours. Do the same way for the standard smell too.  Smelling should be done by 5 different panellists against the standard smells.  Summarize the results. VI. CONCLUSION Sample and the other odor samples from the sample set were tested by the odor panel to determine concentration, intensity, persistency, character and Hedonic tone. The results of testing Sample are summarized below: PRODUCT MATERIAL DIMENSIONS QUANTITY CHAMBER STAINLESS STEEL 150*150*150mm 1 VOLUME - 3.1L AIR BUBBLER GLASS CAP DIAMETER - 20mm 1 VOLUME - 22ml LENGTH - 143mm COMPRESSED AIR PUMP FLOW RATE - 1 L/min 1 SILICON TUBES SILICON INSIDE DIAMETER - 5mm 2m tube OUTSIDE DIAMETER - 9mm TEFLON TUBES TEFLON INSIDE DIAMETER - 5mm 5-10 m tube OUTSIDE DIAMETER - 8mm GLACIAL ACETIC ACID MIN. CONC. - 99.7% 500ml NITROGEN GAS MIN. CONC. - 99.999% 1 CYLINDER MILER BAG PET OUTSIDE DIAMETER - 7mm 1 VOLUME - 3 L JOINT FLUOROCARBON RESINS OUTSIDE DIAMETER - 8mm CAP SILICON RUBBER
  • 4. AVIJIT SINGH GANGWAR Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 10( Part - 3), October 2014, pp.107-110 www.ijera.com 110|P a g e TABLE 2 - RESULTS Detection Threshold 430 Recognition threshold 180 Intensity as ppm n-butanol 37 Character descriptors Sewer Ammonia Amine Hedonic tone −4 REFERENCES [1.] Government Policy, http://www.dhi.nic.in/autopolicy.html [2.] Automobile policy, http://www.siamindia.com/scripts/auto- policy.aspx [3.] Policy Report, http://autocarpro.in/contents/specialReportD etails.aspx?SpecialReportID=90 [4.] http://www.natrip.in/ [5.] http://www.icat.in/ [6.] Automotive Safety, http://en.wikipedia.org/wiki/Automobile_saf ety#Active_and_passive_safety [7.] ICAT, http://en.wikipedia.org/wiki/International_C entre_for_Automotive_Technology [8.] NATRiP http://en.wikipedia.org/wiki/NATRiP [9.] NATRiP , http://www.natrip.in/DisplayContents.aspx? menuid=222