SALT PREPARATION
REVIEW
METHODS IN MAKING SALT
1. Reacting a metal with an acid
2. Reacting an insoluble base with an
   acid
3. Neutralising an alkali with an acid by
   titration
4. Precipitation
1. Reacting a metal with an acid




         Copyright © 2006-2011 Marshall Cavendish
             International (Singapore) Pte. Ltd.
Reacting a metal with an acid (cont.)




           Copyright © 2006-2011 Marshall Cavendish
               International (Singapore) Pte. Ltd.
2. Reacting an insoluble base
         with an acid
3. Neutralising an alkali
with an acid by titration
4. Precipitation




  Copyright © 2006-2011 Marshall Cavendish
      International (Singapore) Pte. Ltd.
Soluble or Insoluble?
Soluble Compounds                     Insoluble Compounds
All salts of Group I elements
All nitrates
All ammonium salts
Most chlorides, bromides and iodides Chlorides, bromides and iodides of
                                      silver and lead
Most sulfates                         Sulfates of calcium, barium and
                                      lead
Group I hydroxides and carbonates     Most hydroxides and carbonates
are soluble (calcium hydroxide is
slightly soluble)
Group I and II oxides react with water Most metal oxides
Soluble or Insoluble?
•   Potassium bromide
•   Silver bromide
•   Sodium hydroxide
•   Calcium sulfate
•   Lead iodide
How will you prepare ZnSO4?
    Since ZnSO4 is a soluble salt (Note: Most
sulphates are soluble), I can use reaction with
acid, base or carbonate or titration. If I have
available acid and metal then I can do that
instead of titration. I will then mix zinc powder
with sulphuric acid until no effervescence is
present. I will then filter it, collect the filtrate
and crystallise it. Once I reach a saturated
solution, I will let it cool. I will then wash it with
distilled water to remove impurities and then
dry it on filter paper.
How will you prepare these salts?

 • CuSO4 (Jorge & Holly)
 • CaCl (Satu & Alicia)
 • K2SO4 (Rizal & Vanessa)
 • PbCl2 (Zaynab & Reem)
TO PREPARE SALT

Reacting a
metal with                 Reacting an
an acid
                           insoluble base
                           with an acid
 Neutralising an
 alkali with an      Precipitation
 acid by titration

Salt preparation

  • 1.
  • 2.
    METHODS IN MAKINGSALT 1. Reacting a metal with an acid 2. Reacting an insoluble base with an acid 3. Neutralising an alkali with an acid by titration 4. Precipitation
  • 3.
    1. Reacting ametal with an acid Copyright © 2006-2011 Marshall Cavendish International (Singapore) Pte. Ltd.
  • 4.
    Reacting a metalwith an acid (cont.) Copyright © 2006-2011 Marshall Cavendish International (Singapore) Pte. Ltd.
  • 5.
    2. Reacting aninsoluble base with an acid
  • 6.
    3. Neutralising analkali with an acid by titration
  • 7.
    4. Precipitation Copyright © 2006-2011 Marshall Cavendish International (Singapore) Pte. Ltd.
  • 8.
    Soluble or Insoluble? SolubleCompounds Insoluble Compounds All salts of Group I elements All nitrates All ammonium salts Most chlorides, bromides and iodides Chlorides, bromides and iodides of silver and lead Most sulfates Sulfates of calcium, barium and lead Group I hydroxides and carbonates Most hydroxides and carbonates are soluble (calcium hydroxide is slightly soluble) Group I and II oxides react with water Most metal oxides
  • 9.
    Soluble or Insoluble? • Potassium bromide • Silver bromide • Sodium hydroxide • Calcium sulfate • Lead iodide
  • 10.
    How will youprepare ZnSO4? Since ZnSO4 is a soluble salt (Note: Most sulphates are soluble), I can use reaction with acid, base or carbonate or titration. If I have available acid and metal then I can do that instead of titration. I will then mix zinc powder with sulphuric acid until no effervescence is present. I will then filter it, collect the filtrate and crystallise it. Once I reach a saturated solution, I will let it cool. I will then wash it with distilled water to remove impurities and then dry it on filter paper.
  • 11.
    How will youprepare these salts? • CuSO4 (Jorge & Holly) • CaCl (Satu & Alicia) • K2SO4 (Rizal & Vanessa) • PbCl2 (Zaynab & Reem)
  • 12.
    TO PREPARE SALT Reactinga metal with Reacting an an acid insoluble base with an acid Neutralising an alkali with an Precipitation acid by titration