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Laboratory of
Vacuum Technologies Plus, LLC
Our competence in
Technology
• magnetron sputtering for deposition of metals and dielectrics;
• ion beam cleaning, etching, sputtering, polishing;
• electron beam melting and evaporation;
• low pressure plasma nitriding;
• high rate magnetron evaporation (up to 40 µm/min);
• large area high rate ion and plasma chemical etching (Si and GaAs up to 40 µm/min, SiO2
– up to 6
µm/min, Cu – up to 0,4 µm/min)
• PECVD for semiconductor, optical and protection layers deposition
• vacuum arc and pulsed arc deposition; DLC coatings;
• thermal evaporation of pure metals, alloys and compositions.
Our competence in
Design and Assembly of devices/ components for sputter tools
20 years experience of component design and production for different sputter systems.
The range of devices includes:

magnetron sputtering sources

ion beam sources for cleaning, etching and sputtering,

plasma sources,

arc and pulsed arc evaporators,

electon beam guns,

resistive heating evaporation systems and powder feeders for them,

heaters.
Additional: customer tailored power supplies, vacuum gauges, control systems, etc.
Our competence in
Customized PVD systems
We offer for more than 10 years standard and customized PVD systems do to increased market demand
for complete technology solutions in Russia.
In house assembly, broad range of different applications (coaters, ion beam and plasma etching
systems, e-beam melting furnaces and systems for some special applications upon customer
requirements.
Our components for PVD tools:
Plasma sources
Two Plasma sources from our assembly line
RFPG-250 RFPG-128
For uniform treatment of large
surfaces or volumes
Housing diameter 245 mm
ion flux density up to 25 mA/cm2 with
high uniformity
Housing diameter 128 mm
ion flux density up to 50 mA/cm2
For high density plasma generation or
implementation into a small system
Plasma sources provide dense electrodeless plasma that can be used for different applications.
• Cleaning and activation
• Ion plasma and plasmachemical etching
• Assisted deposition
• Sputtering
• Surface modification (polishing, nitriding, oxydation)
• Two-step deposition of compositions
Plasma sources applications
Plasma properties
100 Pa 10 Pa
1 Pa
0.1 Pa
Ion current density
RFPG-250 vs. RFPG-128
An example of RFPG application
X82WMoCrV6 steel sample
• Ion beam source cleaning
• Nitriding at 450°C for 30 minutes in Nitrogen
RFPG plasma
• Deposition of (TiAlCrY)N/ZrN multilayer coating
from a magnetron with RFPG assistance
Resulting microhardness is 68 GPa
Scalable for different applications
Our components for PVD tools:
Linear and circular Ion Beam Sources
Anode layer type ion beam sources
(inverted magnetron)
A wide range of applications:
sputtering of materials both dielectric and conductive targets;
magnetron sputtering assistance;
ion cleaning, etching;
polishing;
plasma-enhanced chemical vapor deposition (PECVD);
surface modification.
Technical data
Parameter IBS-125 IBS-145 IBS-400 IBS-600 IBS-700 IBS-800
Supply voltage, kV 1.5-5
Mean ion energy Approx. of supply voltage½
Maximum beam current, A* 0.3 0.4 1.0 1.5 1.75 2.0
Gas efficiency, mA/sccm* 10
Electrode lifetime (Ar at maximal
current), hours** 200
Beam shape Hollow rectangular
Beam size, WхT, mm 100х42 120x42 375х42 575х42 675x42 775x42
Beam divergence angle 2°
Maximum operating pressure, Pa 10
Work gas Ar, H2
, He, Xe, O2
, N2
, Ne, Cx
Hy
, CO2
, Cx
Fy
* Parameters measured in the following conditions:
Argon, voltage 3 kV, chamber pressure 0.1 Pa
** Electrodes are sputtered in inert gases except He only .
IBS-125
Current vs Voltage graph Current vs gas flow rate graph
(IBS-145)
Gas – N2, flow rates (sccm) are shown in the legend Supply voltage 3000 Volts
500 1000 1500 2000 2500 3000 3500
0
50
100
150
200
250
300
350
400
450
0,67
0,64
0,58
0,53
0,47
0,42
0,36
0,31
Supply voltage, V
Beamcurrent,mA
0,00 5,00 10,0015,0020,0025,0030,0035,0040,0045,00
0
50
100
150
200
250
300
350
400
450
f(x) = 8,9 x
f(x) = 10,0 x
Gas flow, sccm
Beamcurrent,mA
Ar
N2
IBS-600..800
Device A
IBS-400 398
IBS-600 598
IBS-700 698
IBS-800 798
IBS-52
Narrow cylindrical ion beam that is ideal for sputtering of small
targets, polishing and other applications that require high sputtering
rate on a small spot.
Ion current up to 160 mA with mean ion energy up to 2500 eV is
concentrated on a 25 mm spot. E.g. 20 μm Iron foil is etched through
in 25 minutes.
Low deflection of the beam allows to place the source away from a
target to prevent its contamination with the sputtered material.
IBS-52 technical data
Parameter Value
Voltage, kV 2.5..5
Beam shape Circular, tubular
Beam diameter, mm 20
Housing diameter, mm 52
Housing length, mm 80
Maximum beam current, mA* 160
Gas efficiency, mA/sccm* 6
Beam angle, maximum, º 2
Operating pressure range in the
chamber, Pa
0.001..10
Weight (kg) 0.3
*plasma-forming gas at 5 kV supply voltage: Ar
* Parameters measured in the following conditions:
Argon, voltage 3 kV, chamber pressure 0.1 Pa .
Special Customer application:
High rate magnetron evaporation
This technology has a combination of benefits of
thermal evaporation and magnetron sputtering

high deposition rate (10 grams/min)

a substantial material volume

high quality of the deposited films and perfect
adhesion due to high vapor ionization
Special Customer application:
Cr deposition upon an Al alloy substrate
Back side 1 µm
Front side 7 µm
Element concentration across the film boundary
Summary
Laboratory of Vacuum Technologies (Beams&Plasmas®) develops and produces vacuum components,
standard and customized tools for coating deposition.
State-of-the-art technical concepts, high reliability and capacity, as well as reasonable prices and
compact sizes are distinguishing features of our machines.
We offer:

Vacuum components for process equipment (magnetrons, ion beam sources, plasma generators,
vacuum system matching units, sensors and accessories)

Engineering and technology consultancy

Maintenance and repair of vacuum equipment

Refit of the existing vacuum process equipment
Laboratory of Vacuum Technologies Plus, LLC
Deputy Director for Research and Development
Grigoriev Vassily
Zelenograd, Russia
E-mail: vgrig@e-beam.ru
Phone +7 (499) 346 0667
http://e-beam.ru
BeamTec GmbH
Managin Director
Ralph Kempter
Ulm, Germany
E-mail: rkempter@beamtec.de
Phone +49 731 146620-0
Fax +49 731 146620-99
http://beamtec.de

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Ion beam and plasma sources

  • 2. Our competence in Technology • magnetron sputtering for deposition of metals and dielectrics; • ion beam cleaning, etching, sputtering, polishing; • electron beam melting and evaporation; • low pressure plasma nitriding; • high rate magnetron evaporation (up to 40 µm/min); • large area high rate ion and plasma chemical etching (Si and GaAs up to 40 µm/min, SiO2 – up to 6 µm/min, Cu – up to 0,4 µm/min) • PECVD for semiconductor, optical and protection layers deposition • vacuum arc and pulsed arc deposition; DLC coatings; • thermal evaporation of pure metals, alloys and compositions.
  • 3. Our competence in Design and Assembly of devices/ components for sputter tools 20 years experience of component design and production for different sputter systems. The range of devices includes:  magnetron sputtering sources  ion beam sources for cleaning, etching and sputtering,  plasma sources,  arc and pulsed arc evaporators,  electon beam guns,  resistive heating evaporation systems and powder feeders for them,  heaters. Additional: customer tailored power supplies, vacuum gauges, control systems, etc.
  • 4. Our competence in Customized PVD systems We offer for more than 10 years standard and customized PVD systems do to increased market demand for complete technology solutions in Russia. In house assembly, broad range of different applications (coaters, ion beam and plasma etching systems, e-beam melting furnaces and systems for some special applications upon customer requirements.
  • 5. Our components for PVD tools: Plasma sources
  • 6. Two Plasma sources from our assembly line RFPG-250 RFPG-128 For uniform treatment of large surfaces or volumes Housing diameter 245 mm ion flux density up to 25 mA/cm2 with high uniformity Housing diameter 128 mm ion flux density up to 50 mA/cm2 For high density plasma generation or implementation into a small system
  • 7. Plasma sources provide dense electrodeless plasma that can be used for different applications. • Cleaning and activation • Ion plasma and plasmachemical etching • Assisted deposition • Sputtering • Surface modification (polishing, nitriding, oxydation) • Two-step deposition of compositions Plasma sources applications
  • 8. Plasma properties 100 Pa 10 Pa 1 Pa 0.1 Pa
  • 10. An example of RFPG application X82WMoCrV6 steel sample • Ion beam source cleaning • Nitriding at 450°C for 30 minutes in Nitrogen RFPG plasma • Deposition of (TiAlCrY)N/ZrN multilayer coating from a magnetron with RFPG assistance Resulting microhardness is 68 GPa
  • 11. Scalable for different applications Our components for PVD tools: Linear and circular Ion Beam Sources
  • 12. Anode layer type ion beam sources (inverted magnetron) A wide range of applications: sputtering of materials both dielectric and conductive targets; magnetron sputtering assistance; ion cleaning, etching; polishing; plasma-enhanced chemical vapor deposition (PECVD); surface modification.
  • 13. Technical data Parameter IBS-125 IBS-145 IBS-400 IBS-600 IBS-700 IBS-800 Supply voltage, kV 1.5-5 Mean ion energy Approx. of supply voltage½ Maximum beam current, A* 0.3 0.4 1.0 1.5 1.75 2.0 Gas efficiency, mA/sccm* 10 Electrode lifetime (Ar at maximal current), hours** 200 Beam shape Hollow rectangular Beam size, WхT, mm 100х42 120x42 375х42 575х42 675x42 775x42 Beam divergence angle 2° Maximum operating pressure, Pa 10 Work gas Ar, H2 , He, Xe, O2 , N2 , Ne, Cx Hy , CO2 , Cx Fy * Parameters measured in the following conditions: Argon, voltage 3 kV, chamber pressure 0.1 Pa ** Electrodes are sputtered in inert gases except He only .
  • 15. Current vs Voltage graph Current vs gas flow rate graph (IBS-145) Gas – N2, flow rates (sccm) are shown in the legend Supply voltage 3000 Volts 500 1000 1500 2000 2500 3000 3500 0 50 100 150 200 250 300 350 400 450 0,67 0,64 0,58 0,53 0,47 0,42 0,36 0,31 Supply voltage, V Beamcurrent,mA 0,00 5,00 10,0015,0020,0025,0030,0035,0040,0045,00 0 50 100 150 200 250 300 350 400 450 f(x) = 8,9 x f(x) = 10,0 x Gas flow, sccm Beamcurrent,mA Ar N2
  • 16. IBS-600..800 Device A IBS-400 398 IBS-600 598 IBS-700 698 IBS-800 798
  • 17. IBS-52 Narrow cylindrical ion beam that is ideal for sputtering of small targets, polishing and other applications that require high sputtering rate on a small spot. Ion current up to 160 mA with mean ion energy up to 2500 eV is concentrated on a 25 mm spot. E.g. 20 μm Iron foil is etched through in 25 minutes. Low deflection of the beam allows to place the source away from a target to prevent its contamination with the sputtered material.
  • 18. IBS-52 technical data Parameter Value Voltage, kV 2.5..5 Beam shape Circular, tubular Beam diameter, mm 20 Housing diameter, mm 52 Housing length, mm 80 Maximum beam current, mA* 160 Gas efficiency, mA/sccm* 6 Beam angle, maximum, º 2 Operating pressure range in the chamber, Pa 0.001..10 Weight (kg) 0.3 *plasma-forming gas at 5 kV supply voltage: Ar * Parameters measured in the following conditions: Argon, voltage 3 kV, chamber pressure 0.1 Pa .
  • 19. Special Customer application: High rate magnetron evaporation This technology has a combination of benefits of thermal evaporation and magnetron sputtering  high deposition rate (10 grams/min)  a substantial material volume  high quality of the deposited films and perfect adhesion due to high vapor ionization
  • 20. Special Customer application: Cr deposition upon an Al alloy substrate Back side 1 µm Front side 7 µm Element concentration across the film boundary
  • 21. Summary Laboratory of Vacuum Technologies (Beams&Plasmas®) develops and produces vacuum components, standard and customized tools for coating deposition. State-of-the-art technical concepts, high reliability and capacity, as well as reasonable prices and compact sizes are distinguishing features of our machines. We offer:  Vacuum components for process equipment (magnetrons, ion beam sources, plasma generators, vacuum system matching units, sensors and accessories)  Engineering and technology consultancy  Maintenance and repair of vacuum equipment  Refit of the existing vacuum process equipment Laboratory of Vacuum Technologies Plus, LLC Deputy Director for Research and Development Grigoriev Vassily Zelenograd, Russia E-mail: vgrig@e-beam.ru Phone +7 (499) 346 0667 http://e-beam.ru BeamTec GmbH Managin Director Ralph Kempter Ulm, Germany E-mail: rkempter@beamtec.de Phone +49 731 146620-0 Fax +49 731 146620-99 http://beamtec.de