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Explora FDG-4 Troubleshooting Chuck Rector August 01, 2011
Troubleshooting the two most common faults with the Explora FDG-4 Chemistry Module ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
 
 
Plumbing Schematic
Reaction Vessel PIT P ressure  I ntegrity  T est of the Reaction Vessel -- Pressure the Reaction Vessel and associated tubing with pressurized nitrogen -- Close nitrogen supply and “isolation valves” and the system must hold pressure (minimum of 30 seconds & >200kPa)
Simplified Plumbing Diagram Reaction Vessel PIT V8 V14 V3 V6 V15 V16 V7 MVP2 MVP1 N 2  In N 2  cross-connect (4-way) N 2  manifold (5-way) Pressure Transducer Vent Trap Reaction Vessel Dip Tube CLOSED OPEN OPEN CLOSED CLOSED CLOSED CLOSED
V8 V14 V3 V6 V15 V16 V7 MVP2 MVP1 N 2  In N 2  cross-connect (4-way) N 2  manifold (5-way) Pressure Transducer Vent Trap Reaction Vessel Dip Tube CLOSED OPEN OPEN CLOSED CLOSED CLOSED CLOSED
[object Object],[object Object],[object Object],[object Object],[object Object],V14 V15 V16 Pressure Transducer Vent Trap Reaction Vessel Dip Tube CLOSED OPEN CLOSED
Pump Addition -- Micro Pump (Lee Pump) is used to add Kryptofix solution to the Reaction Vessel -- While the pump itself is only used to add K-222, the other aqueous reagents (H 2 O and HCl) are added thru the pump (using vacuum system) -- For this reason, we can check the operation of the Lee Pump using water -- Additions are checked by taring an empty vessel, performing an add, and weighing the vessel
 
H2O MVP1 Lee Pump Reaction Vessel MVP5 MVP4 MVP6 MVP7 V14
Low Pump Addition Troubleshooting --
 
 
 

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Explora power point d

  • 1. Explora FDG-4 Troubleshooting Chuck Rector August 01, 2011
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  • 6. Reaction Vessel PIT P ressure I ntegrity T est of the Reaction Vessel -- Pressure the Reaction Vessel and associated tubing with pressurized nitrogen -- Close nitrogen supply and “isolation valves” and the system must hold pressure (minimum of 30 seconds & >200kPa)
  • 7. Simplified Plumbing Diagram Reaction Vessel PIT V8 V14 V3 V6 V15 V16 V7 MVP2 MVP1 N 2 In N 2 cross-connect (4-way) N 2 manifold (5-way) Pressure Transducer Vent Trap Reaction Vessel Dip Tube CLOSED OPEN OPEN CLOSED CLOSED CLOSED CLOSED
  • 8. V8 V14 V3 V6 V15 V16 V7 MVP2 MVP1 N 2 In N 2 cross-connect (4-way) N 2 manifold (5-way) Pressure Transducer Vent Trap Reaction Vessel Dip Tube CLOSED OPEN OPEN CLOSED CLOSED CLOSED CLOSED
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  • 10. Pump Addition -- Micro Pump (Lee Pump) is used to add Kryptofix solution to the Reaction Vessel -- While the pump itself is only used to add K-222, the other aqueous reagents (H 2 O and HCl) are added thru the pump (using vacuum system) -- For this reason, we can check the operation of the Lee Pump using water -- Additions are checked by taring an empty vessel, performing an add, and weighing the vessel
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  • 12. H2O MVP1 Lee Pump Reaction Vessel MVP5 MVP4 MVP6 MVP7 V14
  • 13. Low Pump Addition Troubleshooting --
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