Coating Process Development
John Glenning
January 15, 2010
Coating Process Development
Coating is a complex operation
• Integration of materials, equipment and
processes
• Coating Formulation
• Coating Equipment and Process
• Surface of the film to be coated
• Transportation of the film through the
process
• Drying/Curing of the coating
Coating Process Development
Coating Formulation
• Uniform coating formulation within a batch, batch-to-batch & over time
Coating Process Development
Coating Formulation
• Uniform coating formulation within a batch, batch-to-batch & over time
• Understand the nature of the coating
Coating Process Development
Coating Formulation
• Uniform coating formulation within a batch, batch-to-batch & over time
• Understand the nature of the coating
• Newtonian Fluid: The viscosity of the fluid is independent on the
forces acting on the fluid (water)
Coating Process Development
Coating Formulation
• Uniform coating formulation within a batch, batch-to-batch & over time
• Understand the nature of the coating
• Newtonian Fluid: The viscosity of the fluid is independent on the
forces acting on the fluid (water)
• Non-Newtonian Fluid: The viscosity of the fluid is dependent on the
forces acting on the fluid (polymers)
Coating Process Development
Coating Formulation
• Uniform coating formulation within a batch, batch-to-batch & over time
• Understand the nature of the coating
• Newtonian Fluid: The viscosity of the fluid is independent on the
forces acting on the fluid (water)
• Non-Newtonian Fluid: The viscosity of the fluid is dependent on the
forces acting on the fluid (polymers)
• Thixotropic: Viscosity decreases with increasing rate of shear
over time (ketchup)
• Pseudoplastic: Viscosity decreases with increasing rate of
shear independent of time (paint)
• Rheopectic: Viscosity increases with increasing rate of shear
over time (pastes)
• Dilatant: Viscosity increases with increasing rate of shear
independent of time (corn starch and water)
Coating Process Development
Coating Formulation
• Uniform coating formulation within a batch, batch-to-batch & over time
• Understand the nature of the coating
• Newtonian Fluid: The viscosity of the fluid is independent on the
forces acting on the fluid (water)
• Non-Newtonian Fluid: The viscosity of the fluid is dependent on the
forces acting on the fluid (polymers)
• Thixotropic: Viscosity decreases with increasing rate of shear
over time (ketchup)
• Pseudoplastic: Viscosity decreases with increasing rate of
shear independent of time (paint)
• Rheopectic: Viscosity increases with increasing rate of shear
over time (pastes)
• Dilatant: Viscosity increases with increasing rate of shear
independent of time (corn starch and water)
• Impact process equipment that manufactures a wide range of products
Coating Process Development
Coating Equipment & Process
• Extrusion coating process shears the polymer coating
Coating Process Development
Coating Equipment & Process
• Extrusion coating process shears the polymer coating
• Shearing applies stresses to the coating material
• Coating performance depends on the type of coating
Coating Process Development
Coating Equipment & Process
• Extrusion coating process shears the polymer coating
• Shearing applies stresses to the coating material
• Coating performance depends on the type of coating
• Control the coating process and equipment
• Uniform & proper gap in space and time
• Uniform & proper vacuum in space and time
• Uniform & proper flow rate in space and time
• Uniform & proper coating temperature in space and time
• Uniform & proper solids concentration in space and time
Coating Process Development
Coating Equipment & Process
• Extrusion coating process shears the polymer coating
• Shearing applies stresses to the coating material
• Coating performance depends on the type of coating
• Control the coating process and equipment
• Uniform & proper gap in space and time
• Uniform & proper vacuum in space and time
• Uniform & proper flow rate in space and time
• Uniform & proper coating temperature in space and time
• Uniform & proper solids concentration in space and time
• Season change impacts coating processes
Coating Process Development
Material To Be Coated
• Surface conditions are critical
• Low and uniform surface tension
• Surface tension too high: Delamination
• Uniform surface tension: Uniform coating thicknesses
Coating Process Development
Material To Be Coated
• Surface conditions are critical
• Low and uniform surface tension
• Surface tension too high: Delamination
• Uniform surface tension: Uniform coating thicknesses
• Prepare the surface: Cannot “over clean” or “over dry”
• Remove oils
• Remove debris
• Remove oxides
• Dry the surface
• How fast do oxides reform
Coating Process Development
Material To Be Coated
• Surface conditions are critical
• Low and uniform surface tension
• Surface tension too high: Delamination
• Uniform surface tension: Uniform coating thicknesses
• Prepare the surface: Cannot “over clean” or “over dry”
• Remove oils
• Remove debris
• Remove oxides
• Dry the surface
• How fast do oxides reform
• Coat immediately after the surface is dried
Coating Process Development
Material To Be Coated
• Surface conditions are critical
• Low and uniform surface tension
• Surface tension too high: Delamination
• Uniform surface tension: Uniform coating thicknesses
• Prepare the surface: Cannot “over clean” or “over dry”
• Remove oils
• Remove debris
• Remove oxides
• Dry the surface
• How fast do oxides reform
• Coat immediately after the surface is dried
• Does the material being coated out-gasses: Delamination
Coating Process Development
Material To Be Coated
• Surface conditions are critical
• Low and uniform surface tension
• Surface tension too high: Delamination
• Uniform surface tension: Uniform coating thicknesses
• Prepare the surface: Cannot “over clean” or “over dry”
• Remove oils
• Remove debris
• Remove oxides
• Dry the surface
• How fast do oxides reform
• Coat immediately after the surface is dried
• Does the material being coated out-gasses: Delamination
• Microetch the surface-Increasing the surface area
Coating Process Development
Material Handling
• Material handling is a critical component of coating
Coating Process Development
Material Handling
• Material handling is a critical component of coating
• Uniform and proper tension
• Coating Uniformity
• Coating Adhesion
Coating Process Development
Material Handling
• Material handling is a critical component of coating
• Uniform and proper tension
• Coating Uniformity
• Coating Adhesion
• Uniform and proper line speed
• Coating Thickness
• Coating Uniformity
Coating Process Development
Material Handling
• Material handling is a critical component of coating
• Uniform and proper tension
• Coating Uniformity
• Coating Adhesion
• Uniform and proper line speed
• Coating Thickness
• Coating Uniformity
• Uniform and proper tracking
• Coating Thickness
• Coating Uniformity
• Coating Adhesion
Coating Process Development
Drying/Curing Oven
• More of an art form than a science
Coating Process Development
Drying/Curing Oven
• More of an art form than a science
• Surface “skinning”
• Trap solvents
• Slow down drying
• Surface damage due to “blistering”
• Heat from the bottom up
Coating Process Development
Drying/Curing Oven
• More of an art form than a science
• Surface “skinning”
• Trap solvents
• Slow down drying
• Surface damage due to “blistering”
• Heat from the bottom up
• Air Flow
• Coating damage due to air flow: Turbulent Flow
• Break-up the boundary layer: Laminar flow
• Rapid air exchange in the oven
• No eddy currents in the oven
• Counter-current air flow
Coating Process Development
End of Presentation

Coating processes

  • 1.
    Coating Process Development JohnGlenning January 15, 2010
  • 2.
    Coating Process Development Coatingis a complex operation • Integration of materials, equipment and processes • Coating Formulation • Coating Equipment and Process • Surface of the film to be coated • Transportation of the film through the process • Drying/Curing of the coating
  • 3.
    Coating Process Development CoatingFormulation • Uniform coating formulation within a batch, batch-to-batch & over time
  • 4.
    Coating Process Development CoatingFormulation • Uniform coating formulation within a batch, batch-to-batch & over time • Understand the nature of the coating
  • 5.
    Coating Process Development CoatingFormulation • Uniform coating formulation within a batch, batch-to-batch & over time • Understand the nature of the coating • Newtonian Fluid: The viscosity of the fluid is independent on the forces acting on the fluid (water)
  • 6.
    Coating Process Development CoatingFormulation • Uniform coating formulation within a batch, batch-to-batch & over time • Understand the nature of the coating • Newtonian Fluid: The viscosity of the fluid is independent on the forces acting on the fluid (water) • Non-Newtonian Fluid: The viscosity of the fluid is dependent on the forces acting on the fluid (polymers)
  • 7.
    Coating Process Development CoatingFormulation • Uniform coating formulation within a batch, batch-to-batch & over time • Understand the nature of the coating • Newtonian Fluid: The viscosity of the fluid is independent on the forces acting on the fluid (water) • Non-Newtonian Fluid: The viscosity of the fluid is dependent on the forces acting on the fluid (polymers) • Thixotropic: Viscosity decreases with increasing rate of shear over time (ketchup) • Pseudoplastic: Viscosity decreases with increasing rate of shear independent of time (paint) • Rheopectic: Viscosity increases with increasing rate of shear over time (pastes) • Dilatant: Viscosity increases with increasing rate of shear independent of time (corn starch and water)
  • 8.
    Coating Process Development CoatingFormulation • Uniform coating formulation within a batch, batch-to-batch & over time • Understand the nature of the coating • Newtonian Fluid: The viscosity of the fluid is independent on the forces acting on the fluid (water) • Non-Newtonian Fluid: The viscosity of the fluid is dependent on the forces acting on the fluid (polymers) • Thixotropic: Viscosity decreases with increasing rate of shear over time (ketchup) • Pseudoplastic: Viscosity decreases with increasing rate of shear independent of time (paint) • Rheopectic: Viscosity increases with increasing rate of shear over time (pastes) • Dilatant: Viscosity increases with increasing rate of shear independent of time (corn starch and water) • Impact process equipment that manufactures a wide range of products
  • 9.
    Coating Process Development CoatingEquipment & Process • Extrusion coating process shears the polymer coating
  • 10.
    Coating Process Development CoatingEquipment & Process • Extrusion coating process shears the polymer coating • Shearing applies stresses to the coating material • Coating performance depends on the type of coating
  • 11.
    Coating Process Development CoatingEquipment & Process • Extrusion coating process shears the polymer coating • Shearing applies stresses to the coating material • Coating performance depends on the type of coating • Control the coating process and equipment • Uniform & proper gap in space and time • Uniform & proper vacuum in space and time • Uniform & proper flow rate in space and time • Uniform & proper coating temperature in space and time • Uniform & proper solids concentration in space and time
  • 12.
    Coating Process Development CoatingEquipment & Process • Extrusion coating process shears the polymer coating • Shearing applies stresses to the coating material • Coating performance depends on the type of coating • Control the coating process and equipment • Uniform & proper gap in space and time • Uniform & proper vacuum in space and time • Uniform & proper flow rate in space and time • Uniform & proper coating temperature in space and time • Uniform & proper solids concentration in space and time • Season change impacts coating processes
  • 13.
    Coating Process Development MaterialTo Be Coated • Surface conditions are critical • Low and uniform surface tension • Surface tension too high: Delamination • Uniform surface tension: Uniform coating thicknesses
  • 14.
    Coating Process Development MaterialTo Be Coated • Surface conditions are critical • Low and uniform surface tension • Surface tension too high: Delamination • Uniform surface tension: Uniform coating thicknesses • Prepare the surface: Cannot “over clean” or “over dry” • Remove oils • Remove debris • Remove oxides • Dry the surface • How fast do oxides reform
  • 15.
    Coating Process Development MaterialTo Be Coated • Surface conditions are critical • Low and uniform surface tension • Surface tension too high: Delamination • Uniform surface tension: Uniform coating thicknesses • Prepare the surface: Cannot “over clean” or “over dry” • Remove oils • Remove debris • Remove oxides • Dry the surface • How fast do oxides reform • Coat immediately after the surface is dried
  • 16.
    Coating Process Development MaterialTo Be Coated • Surface conditions are critical • Low and uniform surface tension • Surface tension too high: Delamination • Uniform surface tension: Uniform coating thicknesses • Prepare the surface: Cannot “over clean” or “over dry” • Remove oils • Remove debris • Remove oxides • Dry the surface • How fast do oxides reform • Coat immediately after the surface is dried • Does the material being coated out-gasses: Delamination
  • 17.
    Coating Process Development MaterialTo Be Coated • Surface conditions are critical • Low and uniform surface tension • Surface tension too high: Delamination • Uniform surface tension: Uniform coating thicknesses • Prepare the surface: Cannot “over clean” or “over dry” • Remove oils • Remove debris • Remove oxides • Dry the surface • How fast do oxides reform • Coat immediately after the surface is dried • Does the material being coated out-gasses: Delamination • Microetch the surface-Increasing the surface area
  • 18.
    Coating Process Development MaterialHandling • Material handling is a critical component of coating
  • 19.
    Coating Process Development MaterialHandling • Material handling is a critical component of coating • Uniform and proper tension • Coating Uniformity • Coating Adhesion
  • 20.
    Coating Process Development MaterialHandling • Material handling is a critical component of coating • Uniform and proper tension • Coating Uniformity • Coating Adhesion • Uniform and proper line speed • Coating Thickness • Coating Uniformity
  • 21.
    Coating Process Development MaterialHandling • Material handling is a critical component of coating • Uniform and proper tension • Coating Uniformity • Coating Adhesion • Uniform and proper line speed • Coating Thickness • Coating Uniformity • Uniform and proper tracking • Coating Thickness • Coating Uniformity • Coating Adhesion
  • 22.
    Coating Process Development Drying/CuringOven • More of an art form than a science
  • 23.
    Coating Process Development Drying/CuringOven • More of an art form than a science • Surface “skinning” • Trap solvents • Slow down drying • Surface damage due to “blistering” • Heat from the bottom up
  • 24.
    Coating Process Development Drying/CuringOven • More of an art form than a science • Surface “skinning” • Trap solvents • Slow down drying • Surface damage due to “blistering” • Heat from the bottom up • Air Flow • Coating damage due to air flow: Turbulent Flow • Break-up the boundary layer: Laminar flow • Rapid air exchange in the oven • No eddy currents in the oven • Counter-current air flow
  • 25.