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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2411
Utilizing Porous Light Weight Aggregates for Self-Curing Concrete:
Mechanism & Practical Considerations in Ready-Mixed Concrete Plant
Dada S. Patil1, Dr. S. B. Anadinni2
1Assistant Professor, Civil Engineering Department, Anjuman-I-Islam’s Kalsekar Technical Campus, School of
Engineering & Technology, Panvel, Navi Mumbai, Maharashtra, India
2Professor & Head, Civil Engineering Department, Presidency University, Bengaluru, Karnataka, India
----------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - Concrete needs adequate curing in order to
exhibit desired strength & durabilityproperties. Iftheconcrete
receives insufficient curing, thecementwill nothydratefully. It
is well known fact that higher fraction of cement getting
hydrated produces the desirable compounds in the concrete.
Moreover, it leads to an enhanced field performance of the
concrete. Development of concrete with self curing (internal
curing) ability can be the solution. Internal curing (IC) is
curing the concrete from inside. The additives like Super-
absorbent Polymer (SAP), Shrinkage Reducing Admixture
(SRA) viz., Polyethylene glycol, propylene glycol, polyvinyl
alcohol, paraffin wax, acrylic acid & pre-wetted light weight
aggregates can be used as self curing agents. These materials
facilitate extended hydration of the cement & cause lesser
shrinkage. The research in the field of Self-Curing Concrete
indicates the encouraging effects of these additives on degree
of hydration, interface transition zone(ITZ), microstructure&
other properties of concrete. The studies in the field show that
Internal Curing has advantagessuchasreductioninshrinkage
cracking, plastic shrinkagecrackformation, waterabsorption,
etc. The effectiveness of self curing has been proved in the
laboratory, but the implementation on the field is yet not so
common & encouraging. In this paper, an attempt has been
made to discuss the mechanism & advantages of internal
curing by incorporating Light Weight Aggregates. The paper
also throws some light on how the internal curing can be
practiced in the construction field. The practical
considerations at the RMC plant are discussed.
Key words: Concrete, plastic shrinkage, w/c ratio,
autogenous shrinkage, internal curing, ITZ, chemical
shrinkage, RMC plant.
1. INTRODUCTION
Chemical shrinkage is an important mechanism to be
considered in order to deal with the internal curing.
Products of a reaction occupy smaller volume than the
reactants in the process of chemical shrinkage [1, 2]. During
hydration, chemical reaction takes place which leads to the
reduction of volume. Before the concrete sets,theprocessof
volume change will not pose any problem. As chemical
shrinkage takes place, the concrete is still in fresh sate,
sufficiently fluid & the particles have ability to re-arrange
themselves. They can fill in the space which gets created by
the chemical shrinkage. But, once the concrete sets, it
becomes a rigid mass. The particles will not be able to re-
arrange themselves. This eventually leads to the creation of
vapor-filled voids in the body of the concrete [3].
The voids generated by the chemical shrinkage can be filled
by supplying the water from the prewetted porous Light
Weight Aggregates (LWAs). These LWAs act as self curing
agents & bring about the internal curing process[4,5].Inthe
laboratory, internal curing is shown to be beneficial for
reducing self-desiccation & autogenous shrinkage[6,7].The
research work across the world has shown that internal
curing can also decrease plastic shrinkage cracking [8],
shrinkage cracking [9] & water absorption [10]. The current
paper discusses about the use of Light Weight Aggregate as
potential internal curing material. It alsofocuses ontheneed
of implementing internal curing on the field.
1.1 Importance of Curing
Curing is the process of controlling the moisture movement
from the concrete mass during the process of hydration of
cement. For the concrete to be strong & durable enough, it
must be cured properly. The hydration of cement must be
adequate to ensure that the concrete porosity is reduced to
such an extent that the required strength & durability are
obtained; moreover, the volume changes in the concrete
because of shrinkage are also reduced [11]. Early age drying
shrinkage is due to rapid drying of concrete. It leads to the
formation of powdery surfaces which have low resistance
against abrasion. The insufficientcuringleadstotheincrease
in absorptivity & permeability. Inotherwords,thedurability
of concrete gets hampered badly. These two important
parameters are a function of concrete porosity. The
durability is dependent upon whetherthepores&capillaries
are interconnected or discrete. The size & the quantityofthe
capillaries & pores present in the cement paste are a
function of water curing & water-cement ratio. The
capillaries & pores are partially or completely filled by the
hydration products. Therefore, proper curing becomes vital
for the concrete to have required properties [11, 12, 13].
1.2 Age old Curing Methods: Limitations &
Difficulties
The curing methods involving external application of water
or curing compounds are not sustainable solutions for the
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2412
problem. The water curing also leads to the wastage of large
quantity of water, owing to the considerable evaporation &
run-offs. The concrete quality affects the effectiveness &
penetration depth of externally applied curing water, to a
large extent. The external curing water is unable to supply
in-depth hydration to the cement in the first 2 to 3 days, as
the concrete permeability reduces. The hydration products
fill-in & disconnect the capillary pore network [14].
2. SELF - CURING OF CONCRETE
The phenomenon of increase in the cement hydration by
using the Light Weight Aggregates was brought to light by
Paul Klieger [15] in 1950s. He quoted, “LWAs absorb
considerable water during mixing which apparently can
transfer to the paste during hydration”.Thiswasaffirmedby
Campbell & Tobin [16] in 1967, the absorbed moisture
presence in LWAs produced a concrete which was less
sensitive to the poor field curing conditions. Research work
on deliberately incorporating LWAs for internal curing of
concrete started in 1990s. Robert Phileo [17] made a
statement, “Either the basic nature of Portland cement must
be changed so that self-desiccation is reduced or a way must
be found to get curing water in to the interior of high-
strength structural members. The latter is possible by
incorporating saturated LWAs in the concrete”. ACI-308
gives revised definition of IC as, “internal curing referstothe
process by which the hydration of cement occurs because of
the availability of additional internal water thatisnotpart of
the mixing water”. [18].
The basic difference between the conventional curing&ICis
depicted in fig. 1 [19]. In external curing, water is applied on
the surface. The water penetrationdepthisinfluenced bythe
number of factors such as quality of concrete, age. The
advantage of IC is that the water gets distributedthroughout
the concrete mix.
Fig. 1: Difference between External Curing & Internal
Curing.
Owing to the chemical shrinkage, empty pores get created in
the concrete mix during the process of hydration of cement
paste. This results in to the reduction of internal Relative
Humidity (RH) within the cement paste. The formation of
micro-cracks & capillary pores occurs because of the self-
desiccation & non-availability of moisture within the
hydrating cement paste [20-25]. The weak planeswithin the
matrix are these micro-cracks. Internal Curing helps to
provide extra water throughout the concrete mix. This
results in to maintaining the RH, avoiding the self-
desiccation & reducing the autogenous shrinkage. The
supplementary Cementitious Materials (SCMs) need extra
water for their reaction in later age. Internal curing is
appropriate for concrete with SCMs [19-28].
2.1 Light Weight Aggregates (LWAs) as Potential
Self Curing Agents
The ready mix concrete producer is concerned about the
amount of pre-wetted LWAs to be incorporated in to
concrete mix for internal curing from practical
considerations. An equation for mixture proportioning [29,
30] was given by working out a balance between the water
demand by the cement for hydration process & the water
supplied by the pre-wetted LWAs.
The following equation, by considering Ordinary Portland
Cement (OPC) was given
MLWA = (Cf X CS X αmax) / (S X ΦLWA) ------------ (i)
Where, MLWA = mass of (dry) LWAs requiredperunitvolume
of concrete (kg/m3)
Cf = cement factor or binder content (kg/m3)
CS = chemical shrinkage of concrete (g of water / g of
cement)
αmax = maximum expected degree of cement hydration
S = degree of saturation of LWAs (0 to 1)
ΦLWA = absorption (desorption)capacityofLWAs(kgwater/
kg dry LWAs)
Correct approach to get ΦLWA is to use the measured
desorption capacity of the LWAs at Relative Humidity of
92%. Practically, LWAs are saturated initially. Afterwards,
they undergo desorption duringtheinternal curing(Bentzet
al. 2005) [30]. Typical coefficients forchemical shrinkagefor
an OPC concrete are between 0.06 & 0.08 at room
temperature. The maximum expected degreeofhydrationof
cement under saturated condition (αmax) can be considered
as [(w/c)/0.36], for w/c ratio below 0.36. However, the
maximum expected degree of hydration can be estimated as
1 for (w/c) ratio > 0.36. It is necessary that the LWAs should
be distributed throughouttheconcretemass.Therefore,Fine
Light Weight Aggregates (FLWAs) are preferred to Coarse
Light Weight Aggregates (CLWAs). The advantage of FLWAs
is the lesser distance between the aggregates. It will provide
beneficial effects of IC to a large paste volume.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2413
2.2 Role of Water-Filled LWAs
Plastic shrinkage cracking is reduced due to IC because
water from the LWAs replenishes thewaterwhichislostdue
to evaporation (fig. 2). Immediately after the concrete gets
placed, the system is in a fluid state. Cement grains &
aggregates try to settle because of gravity. The pore fluid
(water) is forced to the surface. During theinitial period,this
bleed water forms a thin layer over the concrete surface.
Water evaporates from the concrete surface at a fairly
constant rate (provided the environmental exposure
conditions are constant). This is known as constant rate
period of drying [31]. During this period, the concrete
continues to consolidateinthevertical direction.Thisresults
in to the settlement of surface. However,aftercertainperiod,
the rate of settlement drastically reduces because the
particles begin to come in each other’s contact. Assuming
that the evaporation rate is relatively high, the bleed water
layer will be lost from the concrete surface.
Fig. 2: A conceptual illustration of the role of water-
filled lightweight aggregate at the surface of a
concrete exposed to drying immediately after
placement (Henkensiefken, Briatka, Bentz, Nantung, &
Weiss, 2010).
A slower rate of evaporation is seen when the water
available to evaporate reduces. This is referred to as the
falling rate period [31]. During this period, water between
the particles is drawn because of evaporation.Thisresultsin
to capillary stress development. This leads to further
consolidation & it may subsequently cause concrete
cracking. In the case of conventional concrete, the stresses
will increase drastically during this period; however, in the
system with IC, water is supplied by the pre-wettedLWAs to
compensate for the evaporating water from the concrete
surface. Due to this, capillary stresses are low during the
falling rate period. Low consolidation & lower potential for
plastic shrinkage cracking are the results. National Institute
of Standards & Technology (NIST) [8] verified the water
removal from LWAs while the surrounding cement paste
remains saturated, using 3-dimentional x-ray absorption
microtomography measurements. On the other hand, it is
seen that in a sealed system which was not exposed to
drying, the water remained in the LWAs until it was drawn
out to the surrounding cement paste due to capillary forces
generated during hydration [32].
Though pre-wetted LWAs are useful in decreasing the
potential for cracking dueto plasticshrinkage& reducing the
crack width, any water consumed in this phase will not be
available later to decrease the autogenous &/or drying
shrinkage. Water lost at a high RH (RH > 96%) corresponds
to the pores in the LWAs as large as > 25 nm. Water lost at
high RH is preferred for self-curing. The water leaves the
pores of the LWAs provided that enough suction pressure
exists. However, this favorable desorption behaviour is not
characteristic of all the LWAs (Lura 2004) [33].Thedistance
of water travelled from the surfaces of internal reservoirs
was estimated by Bentz et. al. [34] in terms of hydration age.
Early age (< 1 day): 20 mm, middle age (1day to 3 days): 5
mm, late (3 to 7 days): 1mm, worst case (> 28 days): 0.25
mm.
Self-curing results in to producing a denser microstructure
with fewer & smaller unhydratedcementparticles&fewer&
smaller capillary pores. The microstructureoftheInterfacial
Transition Zones (ITZ) around LWAs & normal weight
aggregates (NWAs) are different (Fig. 3). In the case of
NWAs, a wall effect exists because of inherent size
differences between cement particles & aggregates. Thereis
a deficiency of cement particles & a surplus of water
(porosity) near the aggregate surface; so, a higher (w/c)
within the ITZ.
Sel-curing is useful for mitigating autogenous shrinkage
(chemical shrinkage), which decreases the internal RH in
the hydrating concrete. This increasesshrinkage& earlyage
cracking (Bentz et.al., 2005) [34].
Fig. 3: Diffrence in the moisture movement between
Porous Light Weight Aggrgates (LWAs) & Normal
Weight Aggregates (NWAs).
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2414
Due to this, strength & durability get hampered badly. To
combat the shrinkage thatresultsfromself-desiccation& the
associated drop in internal RH, the minimum amount of
water needed to supply IC is equal to the volume of water
that is needed to fill the empty pore space that results from
autogenous shrinkage associated with cement hydration.
Internal RH is a measure of the amountofinternal waterthat
is available for cement hydration in the cement paste.
Concretes containingLWAs haveincreasedinternal RH.They
reduce autogenous shrinkage & therefore reduce total
shrinkage. Due to this, there is a decresaed potential for
cracking. IC are suited for the concrete mixes with relatively
low w/cm ratios (ratios < 0.36) (Villarreal and Crocker,
2007). [35].
2.3 Ready Mixed Concrete (RMC) Plant: Practical
Feasibility of LWA Concrete for Internal Curing
The Ready-Mixed Concrete producers find it difficult to use
LWAs . The practical challenege for them is to maintain a
proper saturation to ensure that lightweight concrete will
pump. However, this diffuclty can be overcome by using a
sprinkler system, a saturation pit, a pug mill or by vacuum
saturating the aggregate. Fine Light Weight Aggreagtes
(FLWAs) are preferred over Coarse Light Weight Aggreates
(CLWAs). But, FLWAs exhibit cohesivepropertieswhenthey
are wet. This may lead to a difficulty of handling them in a
batching plant owing to the fact that they may stick or make
a bridge over the gate. However, an auger-screw gate on the
hopper instead of the typical clam-gate can be used.
Alternatively, batching the material as received &
determining water absorption before concrete sets, can be
carried out. But, this raises many questions. If the assumed
amount of water absorption by LWAs is wrong, the (w/c)
ratio of the concrete mix would be wrong. This would lead
to the concrete with much different properties than
expected. There is another issue of pumping the concrete.
The water quantity to be forced into the LWAs during
pumping needs to be determined at first. As the LWAs
absorb water until set, the slump test may not indicate the
normal slump. Since extra water would be placed in the
mixture for absorption, this water would increase the
concrete slump & appear wetter than it would be if the
LWAs were pre-soaked. This may necessitate a proper
correction to be applied to the observed slump value.
3. CONCLUSIONS
The benefits of Internal Curing using LWAs are as below:
 The use of LWAs decraseses the water absorption.
This leads to a good quality concrete.
 Shrinkage cracking can be delayed or prevented ifa
sufficient volume of LWAs is incorporated in to the
concrete.
 Plastic shrinkage cracking can be reduced or
eliminated by adding the required amountofLWAs.
In order to effectively utilize theadvantagesofIC&makingit
practically feasible for producing such a concrete on large
scale in RMC plant, certain aspects need attentionforfurther
development.
 IC is normally used for High Performance Concrete
(HPC) with low (w/c) ratio, to mitigate autogenous
shrinkage. For high (w/c) ratio concretes,problems
other than autogenous shrinkage such as plastic
shrinkage cracking & water absorption exist. More
research is required to extend IC to high (w/c)ratio
mixes.
 Mixture proportioningmethodshavefocusedonthe
autogenous shrinkage caused by the chemical
shrinkage of cement. This consideration is vital in
internal curing applications. But this should not be
the only consideration.
 Aggregate desorption needs more attention rather
than aggregate absorption.
 Volume of LWAs is an important factor. Along with
it, aggregate size & grading must also be given due
importance while proportioning the mix.
 Issues related to utilizing the pre-wetted LWAs in a
concrete batching plant must be given due
importance. The materials can be batched dry.
 In RMC plant, a method for finding the quantity of
water absorbed (& subsequently desorbed) needs
to be developed.
 During pumping, the water will be absorbed by the
LWAs. So, an extra amount of water has to be added
to the concrete mix.
 This addition of extra amount of water makes it
imperative to develop a new worakability test or
modify the slump test to cater to the practical
requirement.
REFERENCES
1. L'Hermite, R.G., Volume changes of concrete, in 4th
International Symposium on theChemistryofCement.1960:
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2. La Chatelier, H., Sur les changements de volume qui
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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2415
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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2416
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Utilizing Porous Light Weight Aggregates for Self-Curing Concrete

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2411 Utilizing Porous Light Weight Aggregates for Self-Curing Concrete: Mechanism & Practical Considerations in Ready-Mixed Concrete Plant Dada S. Patil1, Dr. S. B. Anadinni2 1Assistant Professor, Civil Engineering Department, Anjuman-I-Islam’s Kalsekar Technical Campus, School of Engineering & Technology, Panvel, Navi Mumbai, Maharashtra, India 2Professor & Head, Civil Engineering Department, Presidency University, Bengaluru, Karnataka, India ----------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - Concrete needs adequate curing in order to exhibit desired strength & durabilityproperties. Iftheconcrete receives insufficient curing, thecementwill nothydratefully. It is well known fact that higher fraction of cement getting hydrated produces the desirable compounds in the concrete. Moreover, it leads to an enhanced field performance of the concrete. Development of concrete with self curing (internal curing) ability can be the solution. Internal curing (IC) is curing the concrete from inside. The additives like Super- absorbent Polymer (SAP), Shrinkage Reducing Admixture (SRA) viz., Polyethylene glycol, propylene glycol, polyvinyl alcohol, paraffin wax, acrylic acid & pre-wetted light weight aggregates can be used as self curing agents. These materials facilitate extended hydration of the cement & cause lesser shrinkage. The research in the field of Self-Curing Concrete indicates the encouraging effects of these additives on degree of hydration, interface transition zone(ITZ), microstructure& other properties of concrete. The studies in the field show that Internal Curing has advantagessuchasreductioninshrinkage cracking, plastic shrinkagecrackformation, waterabsorption, etc. The effectiveness of self curing has been proved in the laboratory, but the implementation on the field is yet not so common & encouraging. In this paper, an attempt has been made to discuss the mechanism & advantages of internal curing by incorporating Light Weight Aggregates. The paper also throws some light on how the internal curing can be practiced in the construction field. The practical considerations at the RMC plant are discussed. Key words: Concrete, plastic shrinkage, w/c ratio, autogenous shrinkage, internal curing, ITZ, chemical shrinkage, RMC plant. 1. INTRODUCTION Chemical shrinkage is an important mechanism to be considered in order to deal with the internal curing. Products of a reaction occupy smaller volume than the reactants in the process of chemical shrinkage [1, 2]. During hydration, chemical reaction takes place which leads to the reduction of volume. Before the concrete sets,theprocessof volume change will not pose any problem. As chemical shrinkage takes place, the concrete is still in fresh sate, sufficiently fluid & the particles have ability to re-arrange themselves. They can fill in the space which gets created by the chemical shrinkage. But, once the concrete sets, it becomes a rigid mass. The particles will not be able to re- arrange themselves. This eventually leads to the creation of vapor-filled voids in the body of the concrete [3]. The voids generated by the chemical shrinkage can be filled by supplying the water from the prewetted porous Light Weight Aggregates (LWAs). These LWAs act as self curing agents & bring about the internal curing process[4,5].Inthe laboratory, internal curing is shown to be beneficial for reducing self-desiccation & autogenous shrinkage[6,7].The research work across the world has shown that internal curing can also decrease plastic shrinkage cracking [8], shrinkage cracking [9] & water absorption [10]. The current paper discusses about the use of Light Weight Aggregate as potential internal curing material. It alsofocuses ontheneed of implementing internal curing on the field. 1.1 Importance of Curing Curing is the process of controlling the moisture movement from the concrete mass during the process of hydration of cement. For the concrete to be strong & durable enough, it must be cured properly. The hydration of cement must be adequate to ensure that the concrete porosity is reduced to such an extent that the required strength & durability are obtained; moreover, the volume changes in the concrete because of shrinkage are also reduced [11]. Early age drying shrinkage is due to rapid drying of concrete. It leads to the formation of powdery surfaces which have low resistance against abrasion. The insufficientcuringleadstotheincrease in absorptivity & permeability. Inotherwords,thedurability of concrete gets hampered badly. These two important parameters are a function of concrete porosity. The durability is dependent upon whetherthepores&capillaries are interconnected or discrete. The size & the quantityofthe capillaries & pores present in the cement paste are a function of water curing & water-cement ratio. The capillaries & pores are partially or completely filled by the hydration products. Therefore, proper curing becomes vital for the concrete to have required properties [11, 12, 13]. 1.2 Age old Curing Methods: Limitations & Difficulties The curing methods involving external application of water or curing compounds are not sustainable solutions for the
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2412 problem. The water curing also leads to the wastage of large quantity of water, owing to the considerable evaporation & run-offs. The concrete quality affects the effectiveness & penetration depth of externally applied curing water, to a large extent. The external curing water is unable to supply in-depth hydration to the cement in the first 2 to 3 days, as the concrete permeability reduces. The hydration products fill-in & disconnect the capillary pore network [14]. 2. SELF - CURING OF CONCRETE The phenomenon of increase in the cement hydration by using the Light Weight Aggregates was brought to light by Paul Klieger [15] in 1950s. He quoted, “LWAs absorb considerable water during mixing which apparently can transfer to the paste during hydration”.Thiswasaffirmedby Campbell & Tobin [16] in 1967, the absorbed moisture presence in LWAs produced a concrete which was less sensitive to the poor field curing conditions. Research work on deliberately incorporating LWAs for internal curing of concrete started in 1990s. Robert Phileo [17] made a statement, “Either the basic nature of Portland cement must be changed so that self-desiccation is reduced or a way must be found to get curing water in to the interior of high- strength structural members. The latter is possible by incorporating saturated LWAs in the concrete”. ACI-308 gives revised definition of IC as, “internal curing referstothe process by which the hydration of cement occurs because of the availability of additional internal water thatisnotpart of the mixing water”. [18]. The basic difference between the conventional curing&ICis depicted in fig. 1 [19]. In external curing, water is applied on the surface. The water penetrationdepthisinfluenced bythe number of factors such as quality of concrete, age. The advantage of IC is that the water gets distributedthroughout the concrete mix. Fig. 1: Difference between External Curing & Internal Curing. Owing to the chemical shrinkage, empty pores get created in the concrete mix during the process of hydration of cement paste. This results in to the reduction of internal Relative Humidity (RH) within the cement paste. The formation of micro-cracks & capillary pores occurs because of the self- desiccation & non-availability of moisture within the hydrating cement paste [20-25]. The weak planeswithin the matrix are these micro-cracks. Internal Curing helps to provide extra water throughout the concrete mix. This results in to maintaining the RH, avoiding the self- desiccation & reducing the autogenous shrinkage. The supplementary Cementitious Materials (SCMs) need extra water for their reaction in later age. Internal curing is appropriate for concrete with SCMs [19-28]. 2.1 Light Weight Aggregates (LWAs) as Potential Self Curing Agents The ready mix concrete producer is concerned about the amount of pre-wetted LWAs to be incorporated in to concrete mix for internal curing from practical considerations. An equation for mixture proportioning [29, 30] was given by working out a balance between the water demand by the cement for hydration process & the water supplied by the pre-wetted LWAs. The following equation, by considering Ordinary Portland Cement (OPC) was given MLWA = (Cf X CS X αmax) / (S X ΦLWA) ------------ (i) Where, MLWA = mass of (dry) LWAs requiredperunitvolume of concrete (kg/m3) Cf = cement factor or binder content (kg/m3) CS = chemical shrinkage of concrete (g of water / g of cement) αmax = maximum expected degree of cement hydration S = degree of saturation of LWAs (0 to 1) ΦLWA = absorption (desorption)capacityofLWAs(kgwater/ kg dry LWAs) Correct approach to get ΦLWA is to use the measured desorption capacity of the LWAs at Relative Humidity of 92%. Practically, LWAs are saturated initially. Afterwards, they undergo desorption duringtheinternal curing(Bentzet al. 2005) [30]. Typical coefficients forchemical shrinkagefor an OPC concrete are between 0.06 & 0.08 at room temperature. The maximum expected degreeofhydrationof cement under saturated condition (αmax) can be considered as [(w/c)/0.36], for w/c ratio below 0.36. However, the maximum expected degree of hydration can be estimated as 1 for (w/c) ratio > 0.36. It is necessary that the LWAs should be distributed throughouttheconcretemass.Therefore,Fine Light Weight Aggregates (FLWAs) are preferred to Coarse Light Weight Aggregates (CLWAs). The advantage of FLWAs is the lesser distance between the aggregates. It will provide beneficial effects of IC to a large paste volume.
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2413 2.2 Role of Water-Filled LWAs Plastic shrinkage cracking is reduced due to IC because water from the LWAs replenishes thewaterwhichislostdue to evaporation (fig. 2). Immediately after the concrete gets placed, the system is in a fluid state. Cement grains & aggregates try to settle because of gravity. The pore fluid (water) is forced to the surface. During theinitial period,this bleed water forms a thin layer over the concrete surface. Water evaporates from the concrete surface at a fairly constant rate (provided the environmental exposure conditions are constant). This is known as constant rate period of drying [31]. During this period, the concrete continues to consolidateinthevertical direction.Thisresults in to the settlement of surface. However,aftercertainperiod, the rate of settlement drastically reduces because the particles begin to come in each other’s contact. Assuming that the evaporation rate is relatively high, the bleed water layer will be lost from the concrete surface. Fig. 2: A conceptual illustration of the role of water- filled lightweight aggregate at the surface of a concrete exposed to drying immediately after placement (Henkensiefken, Briatka, Bentz, Nantung, & Weiss, 2010). A slower rate of evaporation is seen when the water available to evaporate reduces. This is referred to as the falling rate period [31]. During this period, water between the particles is drawn because of evaporation.Thisresultsin to capillary stress development. This leads to further consolidation & it may subsequently cause concrete cracking. In the case of conventional concrete, the stresses will increase drastically during this period; however, in the system with IC, water is supplied by the pre-wettedLWAs to compensate for the evaporating water from the concrete surface. Due to this, capillary stresses are low during the falling rate period. Low consolidation & lower potential for plastic shrinkage cracking are the results. National Institute of Standards & Technology (NIST) [8] verified the water removal from LWAs while the surrounding cement paste remains saturated, using 3-dimentional x-ray absorption microtomography measurements. On the other hand, it is seen that in a sealed system which was not exposed to drying, the water remained in the LWAs until it was drawn out to the surrounding cement paste due to capillary forces generated during hydration [32]. Though pre-wetted LWAs are useful in decreasing the potential for cracking dueto plasticshrinkage& reducing the crack width, any water consumed in this phase will not be available later to decrease the autogenous &/or drying shrinkage. Water lost at a high RH (RH > 96%) corresponds to the pores in the LWAs as large as > 25 nm. Water lost at high RH is preferred for self-curing. The water leaves the pores of the LWAs provided that enough suction pressure exists. However, this favorable desorption behaviour is not characteristic of all the LWAs (Lura 2004) [33].Thedistance of water travelled from the surfaces of internal reservoirs was estimated by Bentz et. al. [34] in terms of hydration age. Early age (< 1 day): 20 mm, middle age (1day to 3 days): 5 mm, late (3 to 7 days): 1mm, worst case (> 28 days): 0.25 mm. Self-curing results in to producing a denser microstructure with fewer & smaller unhydratedcementparticles&fewer& smaller capillary pores. The microstructureoftheInterfacial Transition Zones (ITZ) around LWAs & normal weight aggregates (NWAs) are different (Fig. 3). In the case of NWAs, a wall effect exists because of inherent size differences between cement particles & aggregates. Thereis a deficiency of cement particles & a surplus of water (porosity) near the aggregate surface; so, a higher (w/c) within the ITZ. Sel-curing is useful for mitigating autogenous shrinkage (chemical shrinkage), which decreases the internal RH in the hydrating concrete. This increasesshrinkage& earlyage cracking (Bentz et.al., 2005) [34]. Fig. 3: Diffrence in the moisture movement between Porous Light Weight Aggrgates (LWAs) & Normal Weight Aggregates (NWAs).
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2414 Due to this, strength & durability get hampered badly. To combat the shrinkage thatresultsfromself-desiccation& the associated drop in internal RH, the minimum amount of water needed to supply IC is equal to the volume of water that is needed to fill the empty pore space that results from autogenous shrinkage associated with cement hydration. Internal RH is a measure of the amountofinternal waterthat is available for cement hydration in the cement paste. Concretes containingLWAs haveincreasedinternal RH.They reduce autogenous shrinkage & therefore reduce total shrinkage. Due to this, there is a decresaed potential for cracking. IC are suited for the concrete mixes with relatively low w/cm ratios (ratios < 0.36) (Villarreal and Crocker, 2007). [35]. 2.3 Ready Mixed Concrete (RMC) Plant: Practical Feasibility of LWA Concrete for Internal Curing The Ready-Mixed Concrete producers find it difficult to use LWAs . The practical challenege for them is to maintain a proper saturation to ensure that lightweight concrete will pump. However, this diffuclty can be overcome by using a sprinkler system, a saturation pit, a pug mill or by vacuum saturating the aggregate. Fine Light Weight Aggreagtes (FLWAs) are preferred over Coarse Light Weight Aggreates (CLWAs). But, FLWAs exhibit cohesivepropertieswhenthey are wet. This may lead to a difficulty of handling them in a batching plant owing to the fact that they may stick or make a bridge over the gate. However, an auger-screw gate on the hopper instead of the typical clam-gate can be used. Alternatively, batching the material as received & determining water absorption before concrete sets, can be carried out. But, this raises many questions. If the assumed amount of water absorption by LWAs is wrong, the (w/c) ratio of the concrete mix would be wrong. This would lead to the concrete with much different properties than expected. There is another issue of pumping the concrete. The water quantity to be forced into the LWAs during pumping needs to be determined at first. As the LWAs absorb water until set, the slump test may not indicate the normal slump. Since extra water would be placed in the mixture for absorption, this water would increase the concrete slump & appear wetter than it would be if the LWAs were pre-soaked. This may necessitate a proper correction to be applied to the observed slump value. 3. CONCLUSIONS The benefits of Internal Curing using LWAs are as below:  The use of LWAs decraseses the water absorption. This leads to a good quality concrete.  Shrinkage cracking can be delayed or prevented ifa sufficient volume of LWAs is incorporated in to the concrete.  Plastic shrinkage cracking can be reduced or eliminated by adding the required amountofLWAs. In order to effectively utilize theadvantagesofIC&makingit practically feasible for producing such a concrete on large scale in RMC plant, certain aspects need attentionforfurther development.  IC is normally used for High Performance Concrete (HPC) with low (w/c) ratio, to mitigate autogenous shrinkage. For high (w/c) ratio concretes,problems other than autogenous shrinkage such as plastic shrinkage cracking & water absorption exist. More research is required to extend IC to high (w/c)ratio mixes.  Mixture proportioningmethodshavefocusedonthe autogenous shrinkage caused by the chemical shrinkage of cement. This consideration is vital in internal curing applications. But this should not be the only consideration.  Aggregate desorption needs more attention rather than aggregate absorption.  Volume of LWAs is an important factor. Along with it, aggregate size & grading must also be given due importance while proportioning the mix.  Issues related to utilizing the pre-wetted LWAs in a concrete batching plant must be given due importance. The materials can be batched dry.  In RMC plant, a method for finding the quantity of water absorbed (& subsequently desorbed) needs to be developed.  During pumping, the water will be absorbed by the LWAs. So, an extra amount of water has to be added to the concrete mix.  This addition of extra amount of water makes it imperative to develop a new worakability test or modify the slump test to cater to the practical requirement. REFERENCES 1. L'Hermite, R.G., Volume changes of concrete, in 4th International Symposium on theChemistryofCement.1960: Washington D.C. 2. La Chatelier, H., Sur les changements de volume qui accompagent le durcissement des ciments, in Bulletin Societe de l'encouragement pour l'industrie nationale.1900: Paris, France. 3. Couch, J., P. Lura, O.M. Jensen, and J. Weiss. Use of acoustic emission to detect cavitation andsolidification(timezero) in cement pastes, in International RILEM Conference on Volume Changes of Hardening Concrete: Testing and Mitigation, Lyngby, Denmark (2006), pp. 393 - 400.
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2415 4. Bentz, D.P., P.M. Halleck, A.S. Grader, and J.W. Roberts, Water movement during internal curing: Direct observation using x-ray microtomography, ConcreteInternational,2006. 28(10): pp. 39-45. 5. Lura, P., O. Jensen, and S.-I. Igarashi, Experimental observation of internal water curing of concrete, Materials and Structures, 2007. 40(2): pp. 211-220. 6. Lura, P., D. Bentz, D. Lange, K. Kovler, A. Bentur, and K. van Breugel, Measurement of water transport from saturated pumice aggregates to hardeningcementpaste, Materialsand Structures, 2006. 39(9): pp. 861-868. 7. Jensen, O.M. and P.F.Hansen, Autogenousdeformationand rh-change in perspective, Cement and Concrete Research, 2001. 31(12): pp. 1859-1865. 8. Henkensiefken, R., P. Briatka, D. Bentz, T. Nantung, and J. Weiss, Plastic shrinkage cracking in internally cured mixtures made with pre-wetted lightweight aggregate, Concrete International, 2009. 9. Henkensiefken, R., T. Nantung, D.P. Bentz, and J. Weiss, Volume change and cracking in internally cured mixtures made with saturated lightweightaggregateundersealed and unsealed conditions, Cement and Concrete Composites, 2008(Accepted). 10. Henkensiefken, R., J. Castro, D. Bentz, T. Nantung, and J. Weiss, Water absorption in internally cured mortar made with water-filled lightweight aggregate, Cement and Concrete Research, 2009(Accepted). 11. S. Mindess, J.F.Young, and D. Darwin, Concrete, (2nd edition, Prentice-Hall, 2003. p. 287). 12. P.K. Mehta, P. K. and P.J.M Monteriro, Concrete – Microstructure, Properties and Materials, (Third Edition, Tata McGraw Hill, 2009). 13. A.M. Neville, Properties of concrete, (FourthImpression, Pearson Education, 2009). 14. T.C. Powers, L.E. Copeland, H.M. Mann, Capillary continuity or discontinuity in cement pastes, The Research Bulletin of the Portland Cement Association 1 (2) (1959) 38–48 Bulletin 110. 15. P. Klieger, Early High Strength Concrete for Prestressing, Proceedings WorldConferenceonPrestressedConcrete,(pp. A5-1 to A5-14), San Francisco, 1957. 16. R.H. Campbell and R.E. Tobin, CoreandCylinderStrength of Natural and Lightweight Concrete, ACI Journal, Vol. 64, April 1967, pp. 190-195. 17. R.E. Philleo, Concrete Science and Reality, Materials Science of Concrete II, J. P. Skalny and S. Mindess, eds., American Ceramic Society, Westerville, 1991, pp. 1-8. 18. ACI Committee 308. Guidetocuringconcrete(ACI308R– 01, Re-approved 2008). American Concrete Institute, Farmington Hills, Mich, 2001, p. 31. 19. Igor De la Varga , Javier Castro, Dale Bentz and Jason Weiss, Application of internalcuring for mixtures containing high volumes of fly ash, Cement and Concrete Composites , Volume 34, Issue 9, October 2012, Pages 1001–1008. 20. Dale P. Bentz and W. Jason Weiss,Internal Curing:A2010 State-of-the-Art Review,National Institute of Standards and Technology, NISTIR 7765, U.S. Department of Commerce, February 2011. 21. D.P. Bentz, P.M. Halleck, A.S. Grader, and J.W. Roberts, Four-Dimensional X-ray Micro tomography Study of Water Movement during Internal Curing, Proceedings of the International RILEM Conference - Volume Changes of Hardening Concrete: Testing and Mitigation, Eds. O.M. Jensen, P. Lura, and K. Kovler, RILEM Publications S.A.R.L., 11-20, 2006 22. Castro, J., Keiser, L., Golias, M., and Weiss, J., Absorption and Desorption Properties of FineLightweightAggregatefor Application to Internally Cured Concrete Mixtures, Cement and Concrete Composites, 33(10), 1001-1008, 2011. 23. Darwin, D.; Lindquist, W. D.; McLeod, H. A. K.; and Browning, J., “Mineral Admixtures, Curing, and Concrete Shrinkage—An Update,” Concrete Technology, V. 1, No. 1, Oct. 2007, pp. 56-65. 24. T.A. Hammer, O. Bjontegaard and E.G. Sellevold, Internal Curing—Role of Absorbed Water in Aggregates, High- Performance Structural LightweightConcrete,SP-218,J. Ries and T. Holm, eds., American Concrete Institute, Farmington Hills, MI, 2004, pp. 131-142. 25. T.A. Hammer, O. Bjontegaard, and E.J. Sellevold, Internal Curing- Role of Absorbed Water in Aggregates, in ACI SP- 218, High PerformanceStructural LightweightConcrete, Eds. J.P. Ries and T.A. Holm, American Concrete Institute, Farmington Hills, MI, 131- 142, 2004. 26. ] Jason Weiss, Dale .P. Bentz, A. Schindler and Petro Lura, Internal Curing: Constructing more robust concrete, Structure Magazine, 10-14 January 2012. 27. Ryan Henkensiefken, Javier Castro, Haejin Kim, Dale Bentz, and Jason Weiss, Internal Curing Improves Concrete Performance throughout its Life, Concrete InFocus, 8 (5), 22- 30, September-October 2009.
  • 6. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 02 | Feb 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 2416 28. D.P. Bentz, K.A. Snyder, Protected paste volume in Concrete: Extension to Internal Curing using saturated lightweight fineaggregate,CementandConcreteResearch,V. 29,No. 11, Nov. 1999, pp. 1863-1867. 29. D.P. Bentz, and K.A. Snyder, Protected Paste Volume in Concrete: Extension to Internal Curing Using Saturated Lightweight Fine Aggregate,Cement and Concrete Research, 29 (11), 1863-1867, 1999. 30. Dale.P. Bentz, Petro Lura, and John W. Roberts, Mixture proportioning for internal curing, Concrete International, V. 27, No. 2, Feb. 2005, pp. 35-40. 31. Lura., P., Pease, B., Mazotta, G. B., Rajabipour, F., & Weiss, J., Influence of Shrinkage Reducing Admixtures on Development of Plastic Shrinkage Cracks, ACI Materials Journal, Vol. 104, pp. 187-194, (2007). 32. Henkensiefken, R., "Internal Curing in Cementitious Systems Made Using Saturated Lightweight Aggregate," Purdue University, 2008, 33. Pietro Lura, Dale P. Bentz, David A. Lange, Konstantin Kovler and Arnon Bentur, Pumice Aggregates for Internal Water Curing, Concrete Science and Engineering Proceedings. International RILEM Symposium,Evanston, IL, March 22-24, 2004, 137-151 pp., 2004. 34. D.P. Bentz, E.A.B. Koenders, S. Mönnig, H.W.Reinhardt,K. van Breugel, G. Ye,Materialsscience-basedmodelsinsupport of internal water curing RILEM report 41, 29-43. 35. V.H. Villarreal, Internal curing - real world ready mix production and applications: A practical approach to lightweight modified concrete, in Internal Curing of High Performance Concrete: Laboratory and Field Experiences, American Concrete Institute, Farmington Hills, MI (2008), pp. 45-56.