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1.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 587 STUDY ON VARIOUS BIO-MEDICAL WASTE USING FTIR ANALYSIS M. Balamurugan1, R. Balaji2, K. Mohan Raj3, G. Anbarasu4 1(Assistant Professor, Department of Mechanical Engineering, Sri Venkateshwaraa College of Engineering and Technology, Puducherry, India) 2,3,4(UG Final year Student, Department of Mechanical Engineering, Sri Venkateshwaraa College of Engineering and Technology, Puducherry, India) ----------------------------------------------------------------------***--------------------------------------------------------------------- Abstract – As the Population of increases day by day the government of India facing problem in power demand. To overcome the power demand, we propose an idea of Bio-medical waste management. Using Biomass, waste can convert into useful power source. By using Fourier Infra-red analysis, we can able to get the chemical composition and also we can easily able to conclude the biomass which yield much useful bio product from waste. Keyword- Biomass, waste management, medical waste, FTIR. 1. Introduction The waste management of medical waste is not treated properly, may be hazardous to people and environment. As the incineration of medical waste is not developed in India, it is necessary to know the products during incineration and others process. According to Bio-medical waste management rule in 2016, the medical waste categories in four bags yellow, red, blue and white colour bags. From these categories red colour bag was selected under survey in hospital. The two samples have selected glucose bottle and glove. Medical incineration plant refers not just to the mass burn, but also to type of thermal treatment systems for discarded materials that waste resources and generate pollutants. These include systems based upon combustion, pyrolysis, and thermal gasification. In biomass conversion method combustions process due to the tremendous diversity of medical waste sources. It is important to build comprehensive medical waste models that can predict product specification and yields. The lack of data, combining with the large variety and complexity of medical wastes. Medical waste characteristics can be clarified for conversion method of each medical waste is studied. 1.1 FTIR analysis Fourier transform infrared spectrometry (short FT-IR) is one of techniques that are used today for measuring the intensity of infrared radiation as a function of frequency or wavelength. Infrared radiation is invisible electromagnetic radiation just below the red colour of visible electromagnetic spectrum, with wavelength range from 700 nm to 1mm. FTIR results can be used to evaluate the functional groups and prove the existence of some emissions, which provides plenty of information of mixed gases, can be used to identify the composition of mixture, as well as be used to quantify CO2, CO, CH2, C2H4, HCN, and NH2, etc. Table 1 BAGS DAY 1 DAY 2 DAY 3 DAY 4 DAY 5 DAY 6 YELLOW 40Kg 38Kg 40Kg 41Kg 40Kg 46Kg RED 10Kg 10Kg 12Kg 12Kg 8Kg 11Kg BLUE 3Kg 2Kg 3Kg 3Kg 2Kg 2Kg WHITE 2Kg 1Kg 1Kg 1Kg 3Kg 3Kg 1.2 Experiments materials The experimental material according to survey in hospital as shown in table 1 and 2. The red colour bag is selected for sample for analysis From survey, we selected red colour bag for sample materials. Material found in red colour bag: ● Glucose bottles ● Syringe
2.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 588 ● Tubes ● Gloves and other plastics Table 2 MATERIALS DAY Kg MONTH Kg YEAR Kg GLUCOSE BOTTLE 4 120 1460 SYRINGE 3 90 1095 TUBES 1.5 45 547.5 GLOVES AND OTHERS 1.5 45 547.5 TOTAL 10 300 3650 1.3 Survey Conclusion We conclude that two sample materials selected for doing FTIR analysis. ● Glucose ● Gloves 2. Result of FTIR When the absorbance at different wavenumber can be obtained to analyse the composition of gas at this moment; at the same time, when the wavenumber is fixed absorbance information at different time can also be obtained. This wave number to analyse certain component as a function of time. The FTIR result of a bottle shows many peaks of different value in concern with transmittance (%) and (cm-1). Despite of many micro peaks there is a smooth stretch between the values of 3370.6 and 2416.1. The smooth stretch shows the traces of alkenes. Some small sharp and blunt peaks are also absorbed between the values of 2340.4 and 1720.9. It shows the presence of carboxylic acids esters. The largest peaks has the value of 714.2. It implies the presence of alkyl group. Fig.3.1 (a) FTIR result of bottle The FTIR result of gloves shows many peaks of different values in concern with transmittance (%) and (cm-1). In concern with the gloves results of FTIR there are two flat regions. They are 3020 and 1735. It implies the presence of alkyl halides and anhydrides. Huge number of tiny peaks is also absorbed. It shows the presence of many combinations of compounds. It assures the presence of Nitriles, Amines and Amides.
3.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 589 Fig.3.1 (b) FTIR result of gloves 3. Conclusion The two medical wastes bottle and gloves contains esters, alkyl halides, anhydrides, nitrites, amines, amides and carboxylic acids. These can be used to produce multiple by products. Amines such as Novocaine are commonly used as anaesthetics, ephedra used as decongestant. Primary aromatic amines are used as a starting material for the manufacture of azo dyes. Nitrile rubber is a synthetic copolymer of acrylonitrile and butadiene. This form of rubber is highly resistant to chemicals and is used to make protective gloves, hoses and seals. References 1. A. Tarr (October 1971). "URBAN POLLUTION-Many long years ago". American Heritage Magazine. Ban horse drawn carriages. Retrieved November 13, 2016. 2. Chadwick, Edwin (1842). Report...from the Poor Law Commissioners on an Inquiry into the Sanitary Conditions of the Labouring Population of Great Britain 3. Pépin J, Abou Chakra CN, Pépin E, Nault V, Valiquette L. Evolution of the global burden of viral infections from unsafe medical injections, 2000-2010.PLoSOne. 2014 Jun 9;9(6):e99677. 4. WHO/UNICEF,2015. Water, sanitation and hygiene in health care facilities: status in low- and middle-income countries. World Health Organization, Geneva. 5. "Disposable Syringe Markets". TriMark Publications, LLC. June 2013. Archived from the original on 2014-09-11. 6. Bethany, Asked by. "Is it safe to reuse an insulin syringe? - CNN.com". Archived from the original on 2017-07-10. 7. "Disposable Medical Supplies Markets". TriMark Publications, LLC. July 2014. Archived from the original on 2014- 02-24 8. See M Le Page, ‘The Great Carbon Scam’ (21 September 2016) 231 New Scientist 20–21 9. Biomass Energy Center. Biomassenergycentre.org.uk. Retrieved on 2012-02-28. 10. Nagel, B.; Dellweg, H.; Gierasch, L. M. (1 January 1992). "Glossary for chemists of terms used in biotechnology (IUPAC Recommendations 1992)". Pure and Applied Chemistry. 64(1): 143–168. doi:10.1351/pac199264010143. 11. "Biomass - Energy Explained, Your Guide To Understanding Energy - Energy Information 12. S. Osvalda, Kinetics of pyrolysis combustion and gasification of three biomass fuels, Fuel Process. Technol. 88 (2007) 87–97. [2]
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of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 590 13. T.-H. Liou, Pyrolysis kinetics of electronic packaging material in a nitrogen atmosphere, J. Hazard. Mater. B103 (2003) 107–123. [3] 14. P.A. Bingham, R.J. Hand, S.D. Forder, A. Lavaysierre, Vitrified metal finishing wastes II. Thermal and structural characterization, J. Hazard. Mater. B122 (2005) 129–138. [4] 15. R. Font, A. Fullana, J. Conesa, Kinetic models for the pyrolysis and combustion of two types of sewage sludge, J. Anal. Appl. Pyrol. 74 (2005) 429–438. [5] 16. V. Kanokkantapong, T.F. Marhaba, B. Panyapinyophol, P. Pavasant, FTIR evaluation of functional groups involved in the formation of haloacetic acids during the chlorination of raw water, J. Hazard. Mater. B136 (2006) 188–196. [6] 17. G. Qian, D.D. Sun, J.H. Tay, Immobilization of mercury and zinc in an alkali-activated slag matrix, J. Hazard. Mater. B101 (2003) 65–77. [7] 18. M. Becidan, Ø. Skreiberg, J.E. Hustad, Products distribution and gas release in pyrolysis of thermally thick biomass residues samples, J. Anal. Appl. Pyrol. 78 (2007) 207–213. [8] 19. S. Li, J. Lyons-Hart, J. Banyasz, K. Shafer, Real-time evolved gas analysis by FTIR method: an experimental study of cellulose pyrolysis, Fuel 80 (2001) 1809–1817. [9] 20. W. Jong, A. Pirone, M.A. Wojtowicz, Pyrolysis of miscanthus giganteus ´ and wood pellets: TG-FTIR analysis and reaction kinetics, Fuel 82 (2003) 1139–1147. [10] 21. R. Bassilakis, R.M. Carangelo, M.A. Wojtowicz, TG-FTIR analysis of ´ biomass pyrolysis, Fuel 80 (2001) 1765–1786. [11] 22. M.A. Wojtowicz, R. Bassilakis, W.W. Smith, et al., Modelling the evolution ´ of volatile species during tobacco pyrolysis, J. Anal. Appl. Pyrol. 66 (2003) 235–261. [12] 23. M. Herrera, M. Wilhelm, G. Matuschek, et al., Thermoanalytical and pyrolysis studies of nitrogen containing polymers, J. Anal. Appl. Pyrol. 58/59 (2001) 173–188. [13] 24. M.J. Fernandez-Berridi, N. Gonz ´ alez, A. Mugica, et al., Pyrolysis-FTIR ´ and TGA techniques as tools in the characterization of blends of natural rubber and SBR, Thermochim. Acta 444 (2006) 65–70. [14] 25. A. Lunghi, L. Gigante, P. Cardillo, V. Stefanoni, G. Pulga, R. Rota, Hazard assessment of substances produced from the accidental heating of chemical compounds, J. Hazard. Mater. A116 (2004) 11–21. [15] 26. cA.A. Rostami, M.R. Hajaligol, S.E. Wrenn, A biomass pyrolysis sub-model for CFD applications, Fuel 83 (2004) 1519–1525. 27. The public health implications of medical waste: a report to Congress. Atlanta: US Department of Health and Human Services, Public Health Service, Agency for Toxic Substances and Disease Registry, 1990; document no. PB91-100271 28. U.S. Congress, Office of Technology Assessment, Finding the Rx for Managing Medical Wastes, OTA-O-459 (Washington, DC: U.S. Government Printing Office, September 1990) 29. omass burning leads to Asian brown cloud, Chemical & Engineering News, 87, 4, 31 30. Heinimö, J.; Junginger, M. (2009). "Production and trading of biomass for energy – an overview of the global status" (PDF). Biomass and Bioenergy. 33 (9): 1310. doi:10.1016/j.biombioe.2009.05.017. Archived from the original (PDF) on 2013-05-31. 31. Use of biomass by help of the ORC process Archived July 21, 2011, at the Wayback Machine.. Gmk.info. Retrieved on 2012-02-28. 32. How False Solutions to Climate Change Will Worsen Global Warming. globaljusticeecology.org 33. Biofuel crops may worsen global warming: study. Ctv.ca (2008-02-09). Retrieved on 2012-02-28. 34. Biodiesel Will Not Drive Down Global Warming. Energy-daily.com (2007-04-24). Retrieved on 2012-02-28. 35. Forest volume-to-biomass models and estimates of mass for live and standing dead trees of U.S. forests Archived July 11, 2007, at the Wayback Machine.. (PDF) . Retrieved on 2012-02-28. 36. Ram. "SUSTAINABLE FOREST MANAGEMENT FOR DRY FORESTS OF SOUTH ASIA". Food and Agriculture Organization of the United Nations. Retrieved 11 August 2010. 37. http://www.who.int/csr/resources/publications/standardprecautions/en/
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of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 591 38. "Pre-Shred". Bondtech. Bondtech Corporation. Retrieved 4 September 2018. 39. https://www.gov.uk/healthcare-waste 40. NetRegs - Current legislation lists Archived September 27, 2007, at the Wayback Machine. 41. "Disposal of Medical Waste". Press Information Bureau. 25 July 2014. Retrieved 25 July 2014. 42. http://cpcb.nic.in/Bio_medical.php 43. ttp://www.siemens.com/entry/cc/features/greencityindex_international/all/en/pdf/report_northamerica_en.pf 44. "How the world should cope with its growing piles of rubbish". The Economist. Retrieved 2018-10-03. 45. http://web.mit.edu/urbanupgrading/urbanenvironment/resources/references/pdfs/DecisionMakers.pdf
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