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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 576
EXPERIMENTAL ANALYSIS OF FRACTURE TOUGHNESS AND
MICROSTRUCTURE ANALYSIS OF ALUMINIUM6061 REINFORCED WITH
ROCK DUST PARTICULATES
Dr. Syed Ahamed1, Shilpa P C2, Roshan J D3
1Associate Professor, Dept. of mechanical Engineering, University B D T College of Engineering, Davangere.
2,3Dept. of mechanical Engineering, University B D T College of Engineering, Davangere.
---------------------------------------------------------------------***----------------------------------------------------------------------
Abstract – For the last few years there has been a rapid
increase in the utilization of aluminium alloys, particularly in
the automobile industries, due to low weight, density,
coefficient of thermal expansion, and high strength, wear
resistance. Among the materials of tribological importance,
Aluminium metal matrix composites have received extensive
attention for practical as well as fundamental reasons.
Aluminium alloys and aluminium- based metal matrix
composites have found applications in the manufacture of
various automotive engine components.
In our study, a stir casting process is used to fabricate
aluminum composites reinforced with various volume
fractions of rock dust (0, 4, 8, 12 & 16wt %) particulates.
Mechanical properties of unreinforced MMCs were examined.
Optical microscope is used to study the micro structural
characterization of the composites. It is observed that the
fracture toughness of the MMCs increased the reinforcement
volume fraction. It is observed that compare to that of base
aluminium alloy, the casted composite gives the better
mechanical properties 16%rock dust is the best.
Key Words: mechanical properties,FractureToughness,
Aluminum 6061, automotive engine components, stir
casting technique, etc.
1. INTRODUCTION
A composite material is defined as a structural material
created synthetically or artificially by combining two or
more materials having dissimilar characteristics. The
constituents are combined at macroscopic level and are not
soluble in each other. One constituent is called as Matrix
phase and the other is called Reinforcing phase. Reinforcing
phase is embedded in the matrix to give the desired
characteristics.
Ironically, given the growing knowledge with synthetic
products and the ever-increasing range of applications, the
term defines a clear definition. Loose words such as
components composed of two or more clearly identifiable
components are used to describe real composites such as
wood, organic components such as facial fabric, plant
aggregates, minerals, and rock.
Reinforcing phase: fibers, flakes, particulates, whiskers etc.
Matrix phase: continuous phase two ions.
2. OBJECTIVES
The goals of the proposed work are to:
ď‚· Investigation of Fracture toughness.
ď‚· Investigation brief microstructure analysis.
3. MATERIAL USED AND PROPERTIES
Composite material is made of Al6061-rock dust. The
mechanical properties and chemical composition of Al6061
as shown in the tables.
TABLE.1 Material Properties.
Properties Aluminium-6061 Alloy
Melting point (°C) 720
Density (g/cmÂł) 2.7
Linear thermal expansion
(k-1)
2.32*10-5
Poisson’s Ratio 0.33
Modulus of elasticity (GPa) 68.9
Thermal Conductivity (W/mK) 151-202
TABLE.2 Chemical Composition
4. EXPERIMENTAL WORK
The simplest and the most cost effective method of liquid
state fabrication is stir casting. In this work stir casting
technique is employed to fabricate, which is a liquid state
method of composite materials fabrication, in which a
dispersed phase (reinforcementparticulates)ismixedwitha
molten metal by means of stirring. The base metal Al6061
was melted at 7200C in an induction furnace. Anappropriate
amount (4 wt% of the base metal) of rock dust powder was
added slowly to the molten metal. Simultaneously, the
molten metal was stirred thoroughly at a constant speed
with a stirrer. The high temperature molten metal was
poured into the pre-heated (6000C) cast iron molds to get the
required specimens. Figure 1 shows the induction furnace
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 577
setup. The same procedure is followed to produce 8%, 12%,
and 16%.
Fig 1: Induction Furnace.
5. TESTINGS
The specimens were machined asperASTME399standards.
Test was carried out on a computerized SENBspecimenCNC
wire cut EDM .The toughness test specimens are shown in
fig.3
Fig 2: Toughness Test Specimen
6. RESULTS AND DISCUSSION
A. Fracture toughness Test
The fracture toughness testresultsaregiventhelinearstrain
fracture toughness (K1c) of metal was investigated using
pre-cracked fatigue specimens. The specimens were
prepared and tests performed as per ASTM E399 standards.
CNC wire cut Electronic discharge machine (EDM) used to
form notch on the specimen. Single edge notch bending
(SENB) specimen employed in performing K1c test. Total 5
specimens were prepared for 5 different compositions of
aluminium 6061 and rock dust (0%, 4%, 8%, 12%, and
16%).
Table 3: Maximum cyclic load for pre-cracking the
specimen
Table 4: Experimental results of critical Fracture
toughness (Kq) and maximum fracture Toughness (Kmax)
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 578
Fig 4: Experimental results of critical Fracture toughness
(Kq) and maximum fracture toughness (Kmax)
The charts shown in figures are K1c Load V / s COD
curves for all 5 compositions of aluminium 6061 and rock
dust composite. 5 percent of the linear secant row is traced
to the P-COD curve and at junction we can find out the Pq
fracture charge. The base metal fracture charge(Pq)is1,829
KN and the largest fracture charge (Pmax) is 2,073 KN and
the fracture charge (Pq) is 2,357 KN and the maximum
fracture charge (Pmax) is 2,552 for Al6061-12 percent rock
dust. Experimental evaluation of peak fracture toughness
(Kmax) is 19.5611 and critical fracture toughness (K1c) is
18.2126 for 12 percent rock dust weight. Obviously, the
results show that the fracture's toughness increases with a
maximum weight proportion of rock dust. From the
outcomes, it is recognized that the material's brittleness
improves with a rise in weight percentage of rock dust. The
sudden fracture happens with 16 percent rock dust for the
Al-6061.
B. Microstructure Analysis
The Figures shows microstructure of the casted specimens.
The microstructure of the specimens is investigated by
optical microscope with differentzoomingconditions.These
micrographs confirm that there was a uniform distribution
of rock dust particles in the base matrix; and it clearlyshows
that voids and discontinuitiesarereducedasincreasein rock
dust percentage.
Fig 5: AL6061-ROCK DUST (0%) at 10X and 40X
Fig 6: AL6061-ROCK DUST (4%) at 10X & 40X
Fig 7: AL6061-ROCK DUST (8%) at 10X & 40X
Figure highlights the almost uniform distribution of rock
dust particles in a matrix alloy. The rock dust's average
particle size is 150 meshes. Most rock dust particle shapeisin
nature angular and sub-angular. It is discovered that the area
fraction also improves as the proportion of strengthening
rises as shown in the optical micrograph.Italsoobserved that
owing to enhanced interfacial bonding of reinforcement with
aluminum matrix alloy this can be attributed to enhanced
hardness and wear resistance. By preheatingparticlesofrock
dust before adding them to the matrix material, good
interfacial bondingcanbeachieved.Fromthemicrostructures
shown in the figures above, we can say that all
Microstructures consist of fine precipitates of alloy elements
dispersed in the aluminum matrix along the grain boundary.
The tough particles in the rock dust help with the material's
wear resistance. The microstructureofthe productsisheavily
influenced by various mechanical characteristics such as
hardness, strength,toughness,etc.Microstructureassessment
is commonly used in the materials quality control sectors.
7. CONCLUSIONS
1. The aluminium alloy composites containing
different amounts of rock dust particles were
produced by stir casting method successfully.
2. Rock dust particles distribute evenly in the
matrix phase.
3. The experimental and theoretical results of
critical fracture toughness (kq) and maximum
fracture toughness (Kmax) results are increases
with increase of reinforcement in metal matrix
composite.
4. Maximum fracture toughness (Kmax)
experimental assessment is 19.9396 and critical
fracture toughness (K1c) is 19.0125 for 16% rock
dust weight.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 579
REFERENCES
[1]. S. Rama Rao, G. Padmanabhan, “Fabrication and
mechanical properties of aluminium-boron carbide
composites”, International Journal of Materials and
Biomaterials Applications.
[2]. M. Marimuthu, L. John Berchmans ―Preparation
and Characterization of B4C Particulate Reinforced Al-
Mg Alloy Matrix Composites‖. International Journal of
Modern Engineering Research (IJMER), Vol. 3, Issue. 6,
Nov - Dec. 2013 pp-3723-3729.
[3]. Bhargavi Rebba, N.Ramanaiah, ―Studies on
Mechanical Properties of 2024 Al – B4C Composites”.
Advanced Materials Manufacturing & Characterization
Vol 4 Issue 1 (2014).
[4]. K.S.Sridhar Raja, V.K.Bupesh Raja, ― Effect of boron
carbide particle in wear characteristic ofcastaluminium
a356 composite”, IOSR Journal of Mechanical and Civil
Engineering (IOSR-JMCE) e- ISSN: 2278-1684, p-ISSN :
2320–334X PP 73-77.
[5]. Narayana Yuvaraj,Sivanandam Aravindan
,Vipin,―Fabrication of Al5083/B4C surface composite
byfriction stir processing and its tribological
characterization”, JMRTEC- 154, Journal of Material
Research and Technology.
[6]. V. Auradi, Rajesh G.L and S. A. Kori, “Processing of
B4C Particulate Reinforced 6061 Aluminum Matrix
Composites by melt stirring involving two-step
addition”, 3rd International Conference on Materials
Processing and Characterization (ICMPC 2014).
[7]. Srinivasu R , Sambasiva RaoA,MadhusudhanReddy
G , Srinivasa Rao K “Friction stir surfacing of cast A356
aluminium silicon alloy with boron carbide and
molybdenum disulphide powders”, Elsevier,2014.
[8]. Ehsan Ghasali, Masoud Alizadeh, Touradj
Ebadzadeh, Amir hossein Pakseresht,Ali Rahbari,
―Investigation on micro structural and mechanical
properties of B4C–aluminum matrix composites
prepared by microwave sintering‖, Journal of Material
Research and Technology.
[9]. V. Daniel Jebin, D. Shivalingappa J. Jenix Rino, “Wear
behavior of AL6063-Alumina Metal Matrix Composite‖,
International Journal of Science and Research (IJSR),
India.
[10]. Siddesh Kumar N G, V M Ravindranth, G S Shiva
Shankar, ―Mechanical and Wear Behaviour of
aluminium metal matrix hybrid composite”,
International Conference on AdvancesinManufacturing
and Materials Engineering, AMME 2014.

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IRJET- Experimental Analysis of Fracture Toughness and Microstructure Analysis of Aluminium6061 Reinforced with Rock Dust Particulates

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 576 EXPERIMENTAL ANALYSIS OF FRACTURE TOUGHNESS AND MICROSTRUCTURE ANALYSIS OF ALUMINIUM6061 REINFORCED WITH ROCK DUST PARTICULATES Dr. Syed Ahamed1, Shilpa P C2, Roshan J D3 1Associate Professor, Dept. of mechanical Engineering, University B D T College of Engineering, Davangere. 2,3Dept. of mechanical Engineering, University B D T College of Engineering, Davangere. ---------------------------------------------------------------------***---------------------------------------------------------------------- Abstract – For the last few years there has been a rapid increase in the utilization of aluminium alloys, particularly in the automobile industries, due to low weight, density, coefficient of thermal expansion, and high strength, wear resistance. Among the materials of tribological importance, Aluminium metal matrix composites have received extensive attention for practical as well as fundamental reasons. Aluminium alloys and aluminium- based metal matrix composites have found applications in the manufacture of various automotive engine components. In our study, a stir casting process is used to fabricate aluminum composites reinforced with various volume fractions of rock dust (0, 4, 8, 12 & 16wt %) particulates. Mechanical properties of unreinforced MMCs were examined. Optical microscope is used to study the micro structural characterization of the composites. It is observed that the fracture toughness of the MMCs increased the reinforcement volume fraction. It is observed that compare to that of base aluminium alloy, the casted composite gives the better mechanical properties 16%rock dust is the best. Key Words: mechanical properties,FractureToughness, Aluminum 6061, automotive engine components, stir casting technique, etc. 1. INTRODUCTION A composite material is defined as a structural material created synthetically or artificially by combining two or more materials having dissimilar characteristics. The constituents are combined at macroscopic level and are not soluble in each other. One constituent is called as Matrix phase and the other is called Reinforcing phase. Reinforcing phase is embedded in the matrix to give the desired characteristics. Ironically, given the growing knowledge with synthetic products and the ever-increasing range of applications, the term defines a clear definition. Loose words such as components composed of two or more clearly identifiable components are used to describe real composites such as wood, organic components such as facial fabric, plant aggregates, minerals, and rock. Reinforcing phase: fibers, flakes, particulates, whiskers etc. Matrix phase: continuous phase two ions. 2. OBJECTIVES The goals of the proposed work are to: ď‚· Investigation of Fracture toughness. ď‚· Investigation brief microstructure analysis. 3. MATERIAL USED AND PROPERTIES Composite material is made of Al6061-rock dust. The mechanical properties and chemical composition of Al6061 as shown in the tables. TABLE.1 Material Properties. Properties Aluminium-6061 Alloy Melting point (°C) 720 Density (g/cmÂł) 2.7 Linear thermal expansion (k-1) 2.32*10-5 Poisson’s Ratio 0.33 Modulus of elasticity (GPa) 68.9 Thermal Conductivity (W/mK) 151-202 TABLE.2 Chemical Composition 4. EXPERIMENTAL WORK The simplest and the most cost effective method of liquid state fabrication is stir casting. In this work stir casting technique is employed to fabricate, which is a liquid state method of composite materials fabrication, in which a dispersed phase (reinforcementparticulates)ismixedwitha molten metal by means of stirring. The base metal Al6061 was melted at 7200C in an induction furnace. Anappropriate amount (4 wt% of the base metal) of rock dust powder was added slowly to the molten metal. Simultaneously, the molten metal was stirred thoroughly at a constant speed with a stirrer. The high temperature molten metal was poured into the pre-heated (6000C) cast iron molds to get the required specimens. Figure 1 shows the induction furnace
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 577 setup. The same procedure is followed to produce 8%, 12%, and 16%. Fig 1: Induction Furnace. 5. TESTINGS The specimens were machined asperASTME399standards. Test was carried out on a computerized SENBspecimenCNC wire cut EDM .The toughness test specimens are shown in fig.3 Fig 2: Toughness Test Specimen 6. RESULTS AND DISCUSSION A. Fracture toughness Test The fracture toughness testresultsaregiventhelinearstrain fracture toughness (K1c) of metal was investigated using pre-cracked fatigue specimens. The specimens were prepared and tests performed as per ASTM E399 standards. CNC wire cut Electronic discharge machine (EDM) used to form notch on the specimen. Single edge notch bending (SENB) specimen employed in performing K1c test. Total 5 specimens were prepared for 5 different compositions of aluminium 6061 and rock dust (0%, 4%, 8%, 12%, and 16%). Table 3: Maximum cyclic load for pre-cracking the specimen Table 4: Experimental results of critical Fracture toughness (Kq) and maximum fracture Toughness (Kmax)
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 578 Fig 4: Experimental results of critical Fracture toughness (Kq) and maximum fracture toughness (Kmax) The charts shown in figures are K1c Load V / s COD curves for all 5 compositions of aluminium 6061 and rock dust composite. 5 percent of the linear secant row is traced to the P-COD curve and at junction we can find out the Pq fracture charge. The base metal fracture charge(Pq)is1,829 KN and the largest fracture charge (Pmax) is 2,073 KN and the fracture charge (Pq) is 2,357 KN and the maximum fracture charge (Pmax) is 2,552 for Al6061-12 percent rock dust. Experimental evaluation of peak fracture toughness (Kmax) is 19.5611 and critical fracture toughness (K1c) is 18.2126 for 12 percent rock dust weight. Obviously, the results show that the fracture's toughness increases with a maximum weight proportion of rock dust. From the outcomes, it is recognized that the material's brittleness improves with a rise in weight percentage of rock dust. The sudden fracture happens with 16 percent rock dust for the Al-6061. B. Microstructure Analysis The Figures shows microstructure of the casted specimens. The microstructure of the specimens is investigated by optical microscope with differentzoomingconditions.These micrographs confirm that there was a uniform distribution of rock dust particles in the base matrix; and it clearlyshows that voids and discontinuitiesarereducedasincreasein rock dust percentage. Fig 5: AL6061-ROCK DUST (0%) at 10X and 40X Fig 6: AL6061-ROCK DUST (4%) at 10X & 40X Fig 7: AL6061-ROCK DUST (8%) at 10X & 40X Figure highlights the almost uniform distribution of rock dust particles in a matrix alloy. The rock dust's average particle size is 150 meshes. Most rock dust particle shapeisin nature angular and sub-angular. It is discovered that the area fraction also improves as the proportion of strengthening rises as shown in the optical micrograph.Italsoobserved that owing to enhanced interfacial bonding of reinforcement with aluminum matrix alloy this can be attributed to enhanced hardness and wear resistance. By preheatingparticlesofrock dust before adding them to the matrix material, good interfacial bondingcanbeachieved.Fromthemicrostructures shown in the figures above, we can say that all Microstructures consist of fine precipitates of alloy elements dispersed in the aluminum matrix along the grain boundary. The tough particles in the rock dust help with the material's wear resistance. The microstructureofthe productsisheavily influenced by various mechanical characteristics such as hardness, strength,toughness,etc.Microstructureassessment is commonly used in the materials quality control sectors. 7. CONCLUSIONS 1. The aluminium alloy composites containing different amounts of rock dust particles were produced by stir casting method successfully. 2. Rock dust particles distribute evenly in the matrix phase. 3. The experimental and theoretical results of critical fracture toughness (kq) and maximum fracture toughness (Kmax) results are increases with increase of reinforcement in metal matrix composite. 4. Maximum fracture toughness (Kmax) experimental assessment is 19.9396 and critical fracture toughness (K1c) is 19.0125 for 16% rock dust weight.
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 09 | Sep 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 579 REFERENCES [1]. S. Rama Rao, G. Padmanabhan, “Fabrication and mechanical properties of aluminium-boron carbide composites”, International Journal of Materials and Biomaterials Applications. [2]. M. Marimuthu, L. John Berchmans ―Preparation and Characterization of B4C Particulate Reinforced Al- Mg Alloy Matrix Composites‖. International Journal of Modern Engineering Research (IJMER), Vol. 3, Issue. 6, Nov - Dec. 2013 pp-3723-3729. [3]. Bhargavi Rebba, N.Ramanaiah, ―Studies on Mechanical Properties of 2024 Al – B4C Composites”. Advanced Materials Manufacturing & Characterization Vol 4 Issue 1 (2014). [4]. K.S.Sridhar Raja, V.K.Bupesh Raja, ― Effect of boron carbide particle in wear characteristic ofcastaluminium a356 composite”, IOSR Journal of Mechanical and Civil Engineering (IOSR-JMCE) e- ISSN: 2278-1684, p-ISSN : 2320–334X PP 73-77. [5]. Narayana Yuvaraj,Sivanandam Aravindan ,Vipin,―Fabrication of Al5083/B4C surface composite byfriction stir processing and its tribological characterization”, JMRTEC- 154, Journal of Material Research and Technology. [6]. V. Auradi, Rajesh G.L and S. A. Kori, “Processing of B4C Particulate Reinforced 6061 Aluminum Matrix Composites by melt stirring involving two-step addition”, 3rd International Conference on Materials Processing and Characterization (ICMPC 2014). [7]. Srinivasu R , Sambasiva RaoA,MadhusudhanReddy G , Srinivasa Rao K “Friction stir surfacing of cast A356 aluminium silicon alloy with boron carbide and molybdenum disulphide powders”, Elsevier,2014. [8]. Ehsan Ghasali, Masoud Alizadeh, Touradj Ebadzadeh, Amir hossein Pakseresht,Ali Rahbari, ―Investigation on micro structural and mechanical properties of B4C–aluminum matrix composites prepared by microwave sintering‖, Journal of Material Research and Technology. [9]. V. Daniel Jebin, D. Shivalingappa J. Jenix Rino, “Wear behavior of AL6063-Alumina Metal Matrix Composite‖, International Journal of Science and Research (IJSR), India. [10]. Siddesh Kumar N G, V M Ravindranth, G S Shiva Shankar, ―Mechanical and Wear Behaviour of aluminium metal matrix hybrid composite”, International Conference on AdvancesinManufacturing and Materials Engineering, AMME 2014.