Prepare by : Milan Chovatiya
B.Pharm Sem -3
Guide by: Mrs. Pooja Khanpara
APIP, Jamnagar
 Synonym
 Biological source
 Geographical source
 Preparation of Starch
 Description of starch
 Chemical constituents
 Identification
 Uses
 Adulterants
 Synonyms : Amylum
 Biological source :
 Consists of polysaccharides granules
obtained from grains of maize (Zea mays
L.)Rice(Oryza savita) or wheat (Triticum
aestivum L.)
 Family :
Gramineae or from tubers of potato (Solanum
tuberosum L.),family solanaceae.
 Most of tropical as well as , subtropical
countries prepare starch commercially.
India.
 Depending upon the raw material to be used
for processing or type of starch to be
produced.
 Different processes:
are used for commercial manufacture of
starch
1. Washing and softening are involved
2. Grinding and sieving
3. Tabling or centrifugation
4. De-watering and drying of starch
5. The recovery of by-products
 Potato starch : Potatoes are washed, crushed
or cut and converted to a slurry filtered .
Milky slurry containing starch is purified by
centrifugation , washed , dried and sent to the
market.
 Rice starch : Broken pieces of rice soaked in
water with the sodium hydroxide 0.5% solution.
• Crushed, centrifugation , dried.
 Pulverised and packed.
 Maize and corn starch : Grains are washed
, softened , sulphur dioxide is passes to
prevent fermentation, milling.
• The germs (embryo) are separated.
• Antibiotics like penicillin, germs oil ( corn oil)
are produced as by-products.
• Sieving, washing are done.
• The starch being heavier, dried in dryer and
starch is prepared.
 Wheat starch : Wheat flour is dough ,kept
for a time, threshed or grind on grooved
rollers, with watering shaking to take out
starch, dried and packed.
 Starch occurs as fine powder or irregular,
angular masses.
 Colour : Rice starch - white ,
wheat - cream and potato - slightly
yellowish.
 Odour : Odourless
 Taste Mucilaginous
 Size and shape : Different
types as under:
1. Rice starch : The granules are (i)
simple – polyhedral, 2-12 micron in
diameter.(ii) compound granules are
ovoid, 12 to 30 μ × 7 to 12 μ in size,
with 2 to 150 component.
2. Wheat starch : Simple, lenticular ,
circular or oval in shape, 5 to 50 μ in
diameter.
The granules contain hilum at the centre
and the concentric faintly marked
straiations .
Rarely compound granules with 2-4
components.
3. Maize starch : Polyhedral or rounded, 5
to 31 μ in diameter, with distinct cavity in
center, and 2 to5 rays cleft.
4. Potato starch : Simple granules. Sub-
spherical, flattend.
• Irregularly avoid in shape. 30 to 100 μ in
size.
• Hilum is present near narrower red with
well marked concentric striations.
• Starch is insoluble in water and alcohol.
 That contain two polysaccharides viz.
(i) amylose (β – amylose ) and
amylopectin (α – amylose ) in the
proportion of 1:2.
 Amylose is water soluble while
amylopectin is water insoluble.
 Swell in water
 Responsible for the gelatinising
property of starch.
 1. Boil 1 g of starch with 15 ml of
water and cool. The translucent
viscous jelly is produced.
 2. The above jelly turns deep blue
by the addition of solution of iodine.
The blue colour disappears on
warming and reappears on cooling.
 Used as a nutritive, demulcent, protective
and as an absorbent.
 Used in the preparation of dusting talcum
powder for application over the skin.
 As antidote in iodine poisoning, as a
disintegrating agent in pills and tablets, and
as diluent in dry extracts of crude drug.
 It is a diagnostic aid in the identification of
crude drugs.
 Glycerin of starch is used as an
emollient and as a base for
suppositories.
 Also a starting material for the
commercial manufacture of liquid
glucose, dextrose and dextrin.
 Starch is industrially used for the
sizing of paper and cloth.
 Tapioca starch or Cassava or Brazilian
arrowroot- This starch is obtained
from Manihot
esculenta (Euphorbiaceae) and is
used as substitute for starch.

Starch

  • 1.
    Prepare by :Milan Chovatiya B.Pharm Sem -3 Guide by: Mrs. Pooja Khanpara APIP, Jamnagar
  • 2.
     Synonym  Biologicalsource  Geographical source  Preparation of Starch  Description of starch  Chemical constituents  Identification  Uses  Adulterants
  • 3.
     Synonyms :Amylum  Biological source :  Consists of polysaccharides granules obtained from grains of maize (Zea mays L.)Rice(Oryza savita) or wheat (Triticum aestivum L.)  Family : Gramineae or from tubers of potato (Solanum tuberosum L.),family solanaceae.
  • 4.
     Most oftropical as well as , subtropical countries prepare starch commercially. India.
  • 5.
     Depending uponthe raw material to be used for processing or type of starch to be produced.  Different processes: are used for commercial manufacture of starch 1. Washing and softening are involved 2. Grinding and sieving 3. Tabling or centrifugation 4. De-watering and drying of starch 5. The recovery of by-products
  • 6.
     Potato starch: Potatoes are washed, crushed or cut and converted to a slurry filtered . Milky slurry containing starch is purified by centrifugation , washed , dried and sent to the market.  Rice starch : Broken pieces of rice soaked in water with the sodium hydroxide 0.5% solution. • Crushed, centrifugation , dried.  Pulverised and packed.
  • 7.
     Maize andcorn starch : Grains are washed , softened , sulphur dioxide is passes to prevent fermentation, milling. • The germs (embryo) are separated. • Antibiotics like penicillin, germs oil ( corn oil) are produced as by-products. • Sieving, washing are done. • The starch being heavier, dried in dryer and starch is prepared.
  • 8.
     Wheat starch: Wheat flour is dough ,kept for a time, threshed or grind on grooved rollers, with watering shaking to take out starch, dried and packed.
  • 9.
     Starch occursas fine powder or irregular, angular masses.  Colour : Rice starch - white , wheat - cream and potato - slightly yellowish.  Odour : Odourless  Taste Mucilaginous  Size and shape : Different types as under:
  • 10.
    1. Rice starch: The granules are (i) simple – polyhedral, 2-12 micron in diameter.(ii) compound granules are ovoid, 12 to 30 μ × 7 to 12 μ in size, with 2 to 150 component. 2. Wheat starch : Simple, lenticular , circular or oval in shape, 5 to 50 μ in diameter. The granules contain hilum at the centre and the concentric faintly marked straiations . Rarely compound granules with 2-4 components.
  • 11.
    3. Maize starch: Polyhedral or rounded, 5 to 31 μ in diameter, with distinct cavity in center, and 2 to5 rays cleft. 4. Potato starch : Simple granules. Sub- spherical, flattend. • Irregularly avoid in shape. 30 to 100 μ in size. • Hilum is present near narrower red with well marked concentric striations. • Starch is insoluble in water and alcohol.
  • 12.
     That containtwo polysaccharides viz. (i) amylose (β – amylose ) and amylopectin (α – amylose ) in the proportion of 1:2.  Amylose is water soluble while amylopectin is water insoluble.  Swell in water  Responsible for the gelatinising property of starch.
  • 13.
     1. Boil1 g of starch with 15 ml of water and cool. The translucent viscous jelly is produced.  2. The above jelly turns deep blue by the addition of solution of iodine. The blue colour disappears on warming and reappears on cooling.
  • 14.
     Used asa nutritive, demulcent, protective and as an absorbent.  Used in the preparation of dusting talcum powder for application over the skin.  As antidote in iodine poisoning, as a disintegrating agent in pills and tablets, and as diluent in dry extracts of crude drug.  It is a diagnostic aid in the identification of crude drugs.
  • 15.
     Glycerin ofstarch is used as an emollient and as a base for suppositories.  Also a starting material for the commercial manufacture of liquid glucose, dextrose and dextrin.  Starch is industrially used for the sizing of paper and cloth.
  • 16.
     Tapioca starchor Cassava or Brazilian arrowroot- This starch is obtained from Manihot esculenta (Euphorbiaceae) and is used as substitute for starch.