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IRJET- Removal of Turbidity from Dairy Waste Water using Natural Coagulants
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IRJET- Removal of Turbidity from Dairy Waste Water using Natural Coagulants
1.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5455 Removal of Turbidity from Dairy Waste Water Using Natural Coagulants Vinaykumar S N1, Pavankumar P N2, A Brahma Prakash Sah3, Basavaraj Chandrashekar Reddy4 1,2 Asst.prof, Dept of Civil Engineering, City Engineering College, Bangalore, Karnataka, India 3,4Student, City Engineering College, Bangalore, Karnataka, India ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - The water is treated using natural coagulants i.e. Chickpea (cicerariethinum), Hyacinth bean (dolichos lablab), Drumstick seed (moringa oliefera), Tamarind seeds (Tamarind Indica) and Fenugreek (trigonella foenum graecum), so that chemical usage in the treatment is reduced and hence there is a reduction in the treatment cost. The most of the natural coagulants used in the process are chosen such that they either waste or can be obtained at a cheaper rate. This will also help reduce the waste generation. There might be any harmful effects on the plants and animals when the water is treated through the chemical and discharged into water body and if used for gardening, if not the effect might be of long term. Even this harmful could be avoided using the natural coagulants. Keywords: Coagulants, Chickpea, Hyacinth bean, Fenugreek, Drumstick seed, Tamarind seed. 1. INTRODUCTION Water is the most ubiquitous material in nature and most vital for domestic purposes such as drinking, cooking, washing, bathing etc. Nearly 70 percent of the world is covered by water in which only 2.5 percent of it is fresh, the rest is saline and ocean-based. Even then, just 1 percent of our freshwater is easily accessible. The problem of water crisis is due to water pollution. Sewage produced by industries should be treated in an effective manner to reduce the pollution content in the waste. This method needs huge investment, therefore to reduce the cost of treatment, we should try to find coagulants which are efficient, and at the same time it is cheap too. Hence we have chosen natural coagulants, due to which the treatment cost would be reduced. The water which is supplied by any supply board treats the water using the chemical coagulants. There may have an adverse effect on health of animals and plants if used in excess or might show long term effect in future. There are many advanced methods to treat the water but those are expansive too. 2. OBJECTIVE To use various eco friendly natural coagulants materials for the dairy waste water treatment. To remove the suspended impurities from the diary waste water. To find out the optimum time, speed intensity and coagulant dosage. To study the coagulation efficiency of natural coagulants in turbid water. To investigate physical characteristics of dairy waste water discharged by the milk processing unit. 3. BACKGROUND 3.1 DAIRY PRODUCTS MANUFACTURING PROCESS Source: M.N.Rao, A.K Datta, “Industrial wastewater treatment”, third edition, oxford & IBH publishing Co Pvt.Ltd. 3.2 CHARACTERISTICS OF TYPICAL DAIRY WASTE WATER PARAMETERS Dairy effluents contain dissolved sugars proteins and fats and possibly residues of additives. The key parameters are biochemical oxygen demand (BOD), chemical oxygen demand (COD), total suspended solids, and total dissolved solids. Cream, butter, cheese, and whey production are major sources of BOD in wastewater. The dairy wastewater may contain pathogens from contaminated
2.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5456 materials or production processes. A dairy often generates odors and, in some cases, dust, which need to be controlled. Most of the solid wastes can be processed into other products and by-products. Table 1 Characteristics of typical dairy waste water parameters Items Value pH 7.2 Alkalinity 600 mg/l as CaCO3 Total Dissolved Solids 1060 mg/l Suspended Solids 760 mg/l BOD 1240 mg/l COD 84 mg/l Total Nitrogen 84 mg/l Phosphorus 11.7 mg/l Oil and grease 290 mg/l Chloride 105 mg/l Source: M.N.Rao, A.K Datta, “Industrial wastewater treatment”, third edition, oxford & IBH publishing Co Pvt.Ltd. 3.3 DAIRY WASTE WATER TREATMENT PROCEDURE Figure 1 Dairy waste water treatment procedure Source: M.N.Rao, A.K Datta, “Industrial wastewater treatment”, third edition, oxford & IBH publishing Co Pvt.Ltd. 4. MATERILAS AND EQUIPEMENTS 4.1MATERIALS The natural coagulants are collected from the local market of Bangalore, Karnataka, India. 4.1.1 Drumstick seeds (scientific name: Arachis hypogaea): Figure 2 Drumstick seeds 4.1.2 Chickpea (scientific name: Cicer arietinum): Figure 3 Chickpea 4.1.3 Fenugreek (scientific name: Trigonella Foenum Graecum): Figure 4 Fenugreek
3.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5457 4.1.4 Hyacinth bean (scientific name: Dolichos Lablab): Figure 5 Hyacinth bean 4.1.5 Tamarind seeds (scientific name: Tamarind Indica): Figure 6 Tamarind seeds 4.2 EQUIPEMENTS 4.2.1 pH meter Figure 7 pH meter 4.2.2 Turbidity Figure 8 Turbidity 4.2.3 Jar test apparatus Figure 9 Jar test apparatus 5. METHODOLOGY All the natural coagulants are collected and dried in the sunlight. Then all the seeds are ground to fine powder of approximate size 600 µm sieve. The diary waste water is collected from the local market of Bangalore, Karnataka. The analysis of waste water sample using the various parameters such as TDS, COD, BOD etc. The optimization for natural coagulants dosage was performed using the jar test apparatus. The apparatus permitted six beakers to be agitated all together 0.5L of diary waste water were doused with 3, 3.5, 4, 4.5, 5 ml of natural coagulants was stirred for rapidly for 1min at 100 rpm followed by 10, 20 and 30 min & slow stirring for flocculation to settle at bottom. Floc are settled for 1hr and treated sample is taken for analysis. These procedures are repeated several times so that optimum pH, speed, time and dosage of coagulants can be calculated.
4.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5458 6. RESULTS AND DISCUSSION 6.1 TREATMENT USING NATURAL COAGULENT PREPRATION OF NATURAL COAGULENT The seeds pod of cicerariethinum, dolichos lablab, moringa oliefera, tamridindica and trigonella foenum graecum are collected and dried naturally by sunlight. And seeds are removed from pod manually. The dried seeds were grounded to powder by domestic blenders. The powder was sieved through 600 µm sieve. 6.2 INITIAL PARAMETERS OF DAIRY WASTE WATER The raw waste was collected from Bangalore local market is tested for its initial parameter to find the degree of pollution in the effluent. This will help us the find the amount of treatment done at the final stage by comparing it with the initial parameter. Table 2 Initial parameters of dairy waste water Item Value pH 8.88 Turbidity 188 NTU COD 2448 mg/l BOD 1110 mg/l Electricity Conductivity 6.61 Total Dissolved Solids 4292 mg/l 6.3 JAR TEST The jar test is performed to obtain the optimum dosage of coagulant, speed, time and pH. Using this optimum values the water will be treated to get the best treatment of water possible. 6.3.1 OPTIMUM DOSAGE OF COAGULANTS Table 3 Result of optimum dosage of coagulants Coagulant Optimum dosage in mg/l Moringa Oliefera 4 Cicer arietinum 4.5 Trigonella Foenum Graecum 4 Dolichos Lablab 4 Tamrid Indica 5 From the above graph optimum dosage can be obtained. The graph also shows that tamrid indica removes maximum turbidity from the waste that is 58.5 NTU for optimum dosage of 5mg/l. 6.3.2 OPTIMUM TIME Table 4 Results of optimum time Coagulant Optimum Time in min Moringa Oliefera 30 Cicer arietinum 30 Trigonella Foenum Graecum 30 Dolichos Lablab 30 Tamrid Indica 30 From the optimum time graph, It shows that Tamrid Indica is more efficient than any other coagulant. It removed around 58.5 NTU of turbidity for the optimum time of 30mins. 0 20 40 60 80 100 120 140 160 180 200 3 3.5 4 4.5 5 5.5 10 15 20 25 TurbidityinNTU Dosage in mg/l Optimum Dosage of Coagulants Moringa Oliefera Cicer Arietinum Trigonella Foenum Graecum Dolichos lablab Tamrid Indica
5.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5459 6.3.3 OPTIMUM SPEED Optimum speed at which coagulants could effectively treat the water could be found from the graph. Maximum turbidity is removed by Tamrid Indica that is around 58.5 NTU at an optimum speed of 40 rpm. Table 5 Results of optimum speed Coagulant Optimum Speed in RPM Moringa Oliefera 40 Cicer Arietinum 40 Trigonella Foenum Graecum 40 Dolichos Lablab 40 Tamrid Indica 40 6.3.4 OPTIMUM pH Table 6 Results of optimum pH Coagulant Optimum pH Moringa Oliefera 9 Cicerariethinum 9 Trigonella Foenum Graecum 9 Dolichos Lablab 9 Tamrid Indica 9 From the above graph optimum pH can be obtained. This graph also shows that natural coagulants are more effective in alkaline medium. Even in this case Tamrid Indica has cleared maximum of turbidity that is about 58.5 NTU. 0 20 40 60 80 100 120 10 20 30 40 TurbidityinNTU Time in min Moringa oliefera Cicer Arietinum Trigonello Foenum graecum Dolichos lablab Tamrid indica 0 20 40 60 80 100 120 10 20 30 40 50 TurbidityinNTU Speed in RPMMoringa Oliefera Cicer Arietinum Trigonello Foenum Graecum Dolichos lablab Tamrid Indica 0 20 40 60 80 100 120 140 4 7 9 TurbidityinNTU pHMoringa oliefera Cicer arietinum Trigonella foenum graecum Dolichos lablab Tamrid Indica
6.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5460 6.4 FINAL PARAMETER AFTER TREATMENT Tests were conducted to find the reduction in the parameters of the effluent. The final parameters of the treated waste water at optimum dosage, time, speed, pH are as follows, 6.4.1 WHEN TREATED WITH MORINGA OLIEFERA Item Value pH 6.32 Turbidity 70 NTU COD 1112.7 mg/l BOD 462.5 mg/l Electricity Conductivity 4722 u/mm Total Dissolved Solids 3068 mg/l 6.4.2 WHEN TREATED WITH CICER ARIETHINUM Item Value pH 6.32 Turbidity 65.5 NTU COD 765 mg/l BOD 346.8 mg/l Electricity Conductivity 2874 u/mm Total Dissolved Solids 1860 mg/l 6.4.3 WHEN TREATED WITH TRIGONELLA FOENUM GRAECUM Item Value pH 6.32 Turbidity 72.7 NTU COD 1170 mg/l BOD 504.5 mg/l Electricity Conductivity 5085 u/mm Total Dissolved Solids 3301 mg/l 6.4.4 WHEN TREATED WITH DOLICHOS LABLAB Item Value pH 6.32 Turbidity 68.2 NTU COD 941.5 mg/l BOD 426.9 mg/l Electricity Conductivity 3888 u/mm Total Dissolved Solids 2520 mg/l 6.4.5 WHEN TREATED WITH TAMRINA INDICA Item Value pH 6.32 Turbidity 58.5 NTU COD 664 mg/l BOD 272.5 mg/l Electricity Conductivity 2727 u/mm Total Dissolved Solids 1474 mg/l 7. CONCLUSION The characteristics of untreated dairy waste water are pH 8.88, electric conductivity 6.61, COD 2448 mg/l, BOD 1110mg/l, turbidity 188 NTU and total dissolved solids 4292 mg/l. It could be concluded that Tamrina indica is the most effective coagulant since it removes the maximum turbidity than any other coagulant. It is also seen that the effluent parameter is maximum removed by Tamrina indica only . The second position in removing turbidity is secured by Cicer Ariethinum it has removed around 65.5 NTU of turbidity. And the third most effective turbidity remover is Dolichos lablab it removes around 68.2 NTU of Turbidity and the other parameter is also was removed effectively. Among the above mentioned natural coagulants, the maximum reduction of turbidity is 58.5 NTU, the maximum reduction of chemical oxygen demand is 664 mg/l, the maximum reduction bio chemical demand is 272.5, the maximum reduction of total dissolved solids is 1474 mg/l, the maximum of electrical conductivity is 2727 um/mm by Tamrina idindica and is more effective for the treatment of dairy waste water. ACKNOWLEDGEMENT We extend our sincerest gratitude to our guides Prof. Pavankumar P N, Prof. Vinaykumar S N and our well wishers who had constantly encouraged us and helped us in all situations whenever needed.
7.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 05 | May 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 5461 REFERENCES [1] G. Vijayaragavan T. Siva kumar and A. vimalkumar “Application plant based coagulants for waste water treatment IJAERS,vol 1 2011 [2] Chitteti Ramamurthy, Malige Uma Maheswari, Natarajan Selvaganabathy, Muthuvel Suresh Kumar, Venugopal Sujatha, ChinnasamyThirunavukkarasu [3] “Evaluation of eco-friendly coagulant from Trigonellafoenum-graecum seed”, Advances in Biological Chemistry, 2012, 2, 58-63 [4] Chitteti Ramamurthy, Malige Uma Maheswari, Natarajan Selvaganabathy, Muthuvel Suresh Kumar, Venugopal Sujatha, ChinnasamyThirunavukkarasu [5] “Evaluation of eco-friendly coagulant from Trigonellafoenum-graecum seed”, Advances in Biological Chemistry, 2012, 2, 58-63 [6] Source: M.N.Rao, A.K Datta, “Industrial wastewater treatment”, third edition, oxford & IBH publishing Co Pvt.Ltd. BIOGRAPHIES VINAYKUMAR S N, Asst.Professor Dept of Civil engineering in City Engineering College, B’lore. PAVANKUMAR P N, Asst.Professor Dept of Civil engineering in City Engineering College, B’lore. A BRAHMA PRAKASH SAH, Final year Student, BE Civil Engineering , City Engineering College, B’lore. BASAVARAJ CHANDRASHEKAR REDDY, Final year Student, BE Civil Engineering , City Engineering College, B’lore.
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