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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3114
Experimental Investigation on the Usage of Vermiculite Waste in
Concrete
M.Manoharan1, R.Haripraba2, S.Muthulakshmi3, N.Aanandh4
1Assistant Professor, Dept. of Civil Engineering, Rajalakshmi Engineering College, Chennai, Tamilnadu, India
2Assistant Professor, Dept. of Civil Engineering, Arulmigu Meenakshi Amman College of Engineering,
Thiruvannamalai, Tamilnadu, India
3Assistant Professor, Dept. of Civil Engineering, Rajalakshmi Engineering College, Chennai, Tamilnadu, India
4Assistant Professor, Dept. of Civil Engineering, Rajalakshmi Engineering College, Chennai, Tamilnadu, India
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract –Concrete is one of the most extensively used
construction material in the worldwithtwobilliontonsplaced
worldwide each year. It is used because of its easy workability
and strength. Aggregates are the major ingredients which
occupy 60 to 80 percent of the total volume of concrete and
greatly influence its properties, mix proportionsandeconomy.
In order to reduce the cost of construction and to protect the
natural resources, there is a need to use alternative and
sustainable construction materials. Vermiculite, which is a
waste mineral from the wire lining industry, can be used as
partial replacement for fine aggregates in concrete. Use of
Vermiculite in concrete enhances the shrinkage and crack
resistance, fire resistance, reduces environmental impact and
also reduces the construction cost. Important characteristics
of a good quality aggregate include resistance to abrasion,
resistance to freeze/thaw action, resistance to sulphates,
correct shape and surface texture, proper gradation, density,
and compressive and flexural strength. The main objective of
this research is to study the strength parameters such as
compressive strength, split tensile and flexural strength of
concrete using vermiculite as partial replacement with 5%,
10% and 20% by weight. Several tests such as compressive
strength, tensile strength and flexural strength test on
concrete cubes and beam casted with vermiculite were
conducted. The results showed that 10% of fine aggregates
replaced by Vermiculite gave the best results. Vermiculitecan
be used as one of the best replacement for sand and moreover
the weight of the concrete is greatly reduced in large extent.
Key Words: Compressive strength, density, flexural
strength, freeze/thaw action, sustainable materials,
tensile strength, Vermiculite.
1. INTRODUCTION
Concrete is a widely used construction material because of
its good workability. It is mostly consists of aggregates,
namely fine and coarse aggregates. Nowadays, sand is
heavily depleted and it leads to an alarming state. Natural
sand cannot be replaced by any other materials due to its
significant properties. Due to the sudden decrease of sand,
manufacturing sand came into existenceforthereplacement
of river sand. Several alternatives for natural sand are being
tested and reports are being published. Among the
alternatives, Vermiculite, a mineral whichistobeusedasthe
replacement of fine aggregates partially up to some extent.
Vermiculite is a hydrous phyllosilicate mineral.Itundergoes
significant expansion when heated. Duetosufficientheating,
Exfoliation occurs in Vermiculite and the effect is routinely
produced in furnaces. It is a light weight material, hence if it
is added as an ingredient of concrete, greatly reduces the
self-weight of the structure.
Vermiculite is used in many commercial sectors namely,
1. Brake lining industries
2. Calcium Silicate boards
3. Soil conditioner
4. Waste treatment
5. Cementitious fire proofing products etc.
Table -1: Properties of Vermiculite
Chemical Analysis
Silicon (SiO2) 39.40%
Magnesium (MgO) 25.20%
Aluminium (Al2O3) 8.80%
Potassium (K2O) 4.50%
Calcium (CaO) 1.80%
Carbonate (CO2) 1.40%
Titanium (TiO2) 0.80%
Fluorine (F) 0.50%
Physical Properties
Melting Point (°C) 1330
Specific Heat
(1kJ/kg.K)
1.08
Specific Gravity
(Crude)
2.5
Mohs Hardness (Crude) 1-2
pH (ISO 787-9) 7-8
% Loss at 105°C
(Expanded Product)
< 0.5
% Loss at 1000°C
(Expanded Product)
< 6
Many researchers have worked on Vermiculite concrete,
replacing by weight of cement up to some percentage.
Reference [1] observed that an increase in 13% of
compressive strength while Vermiculite is replaced 5% by
the weight of cement. Reference [2] showed that Concrete
gives more compressive strengthwhilecementisreplacedby
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3115
Vermiculite. Usage of Vermiculite gives a good impact on the
strength parameters as wellas greatreductioninself-weight.
From references [3], [5], [6] & [7], it was observed that the
vermiculite act as a high heat resisting material. References
[4] & [8] showed that the lightweight material can be
prepared from vermiculite with good heat insulating
property.
Fig -1: Vermiculite
2. TEST ON MATERIALS USED
Ordinary Portland cement of 43 grade confirming to IS:
8112-1989, is used in this study. Aggregate is an essentially
used construction material and inert material which
contains 70 to 80 % volume of the concrete. Hence, if you
want to study about the concrete, it is essential to know
about the properties of aggregates because of its major
volume.
Therefore, it should be completely tested before using for
construction. Not only the aggregates should be strong and
durable but should also have proper shape and size to act as
monolithically in the structural components. Hence, it’s
essential to conduct several tests on aggregates in order to
ensure the quality of aggregates and check their. The
following are the test results conducted for the ingredients
of concrete:
Table -2: Test results of Cement
S.No. Property Value
1 Normal Consistency 33%
2 Initial Setting Time
(minutes)
35
3 Final Setting Time
(minutes)
483
4 Specific Gravity 3.13
5 Fineness Of Cement 1.1
Table -3: Test results of Fine and Coarse Aggregate
S.No. Property
Fine
Aggregate
Coarse
Aggregate
1. Specific Gravity 2.65 2.85
2. Fineness Modulus 2.80 6.19
3. Water Absorption 1 % 0.6 %
Table -4: Test results of Vermiculite
3. METHODOLOGY
Based on the guidelines for mix proportions provided in IS:
10262-2009, mix proportion for M25 grade of concrete was
arrived as 1:1.41:2.81 with water/cement ratio of 0.45.
Table -5: Mix proportions of concrete for 1 m3
Cement
Fine
aggregate
Coarse
aggregate
Water
438 kg 614.93 kg 1228.21 kg 197.16
lit1 1.41 2.81 0.45
Workability is a main factor which directly connects the
strength of concrete. The standard value has to be checked
out for the functional strength of the concrete. The fresh
concrete is prepared based on the ratio above said and
slump cone test is conducted to determinetheworkability of
concrete.
Table -6: Slump Cone test result
Workability Replacement of Vermiculite in
%0 5 10 20
Slump 52
mm
52
mm
55
mm
58
mm
4. RESULTS AND DISCUSSIONS
4.1 Compressive Strength
The compressive strength test was conducted on 3
specimens for each % replacement as per the
recommendations of IS: 516-1959. The specimens were
tested on the compression testing machine and the values
are tabulated below.
S. No. Property Value
1. Specific Gravity 2.34
2. Fineness Modulus 2.43
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3116
Table -7: Compressive Strength Test Results
S.
No.
Curing
days
% of
Vermiculite
Compressive
Strength (N/mm2)
1 7 days
0 23.56
5 24.44
10 24.89
20 24.00
2 14 days
0 27.11
5 27.56
10 28.89
20 27.78
3 28 days
0 31.11
5 31.78
10 33.11
20 32.22
The above table clearly shows that the compressivestrength
of 10% replaced vermiculite produced good result.Based on
the above results, a graph was shown below.
0
5
10
15
20
25
30
35
0 5 10 20
CompressiveStrengthin
N/mm2
% of Vermiculite
7 Days
14 Days
28 Days
Chart -1: Compressive Strength graph
4.2 Split Tensile Strength
The split tensile strength test was conducted on 3 cylinder
specimens for each % replacement as per the
recommendations of IS: 5816-1999. The specimens were
tested on the compression testing machine and the values
are tabulated below.
Table 8: Split Tensile Strength Test Results
S.
No.
Curing
days
% of
Vermiculite
Tensile Strength
(N/mm2)
1 7 days
0 2.33
5 2.44
10 2.89
20 2.78
2 14 days 0 2.78
5 2.89
10 3.33
20 3.11
3 28 days
0 3.56
5 3.89
10 4.33
20 4.00
0
1
2
3
4
5
0 5 10 20
SplitTensileStrengthin
N/mm2 % of Vermiculite
7 Days
14 Days
28 Days
Chart -2: Split Tensile Strength graph
The above table and graph clearly showed that the tensile
strength of 10% replaced vermiculite produced maximum
strength.
4.3 Flexural Strength Test
The beams are designed and the reinforcement bars are
placed accordingly. The flexural strengthtestwasconducted
on the beam specimens which was casted using
reinforcement bars for each % replacement as per the
recommendations of IS: 516-1959. The specimens were
tested on the loading frames as shown below and the values
are tabulated.
Fig -2: Flexural Strength Test
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072
© 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3117
Table -9: Flexural Strength Test Results
S.
No.
Curing
days
% of
Vermiculite
Flexural
Strength
(N/mm2)
1 28 days
0 63.58
5 63.25
10 68.36
20 65.89
60
62
64
66
68
70
0 5 10 20
FlexuralStrengthin
N/mm2
% of Vermiculite
28 Days
Chart -3: Flexural Strength graph
0
20
40
60
80
0 5 10 20
StrengthinN/mm2
% of Vermiculite
Compressive
Strength
Split Tensile
Strength
Flexural
Strength
Chart -4: Cumulative Strength Test graph
From the above table and graph, the result obtained as 10%
replaced vermiculite produced maximum strength.
5. CONCLUSION
This study was conducted to evaluate the effect of using
Vermiculite as the partial replacement of fine aggregate in
concrete composites and also gave an idea by using these
materials within specific range. Several tests were
conducted on the materials of the concrete composites and
the reports were observed. With the results obtained, we
conclude that 10% of fine aggregates replaced by
Vermiculite will give best result. It wasalsosuggestedthat in
order to reduce the weight of concrete and improvement in
the alternation of sand, Vermiculite is used as oneofthebest
replacement and moreover the weight of the concrete is
greatly reduce in large usage.
REFERENCES
1. James S. Webber, “Study the effect of vermiculite on
concrete”, Wadsworth Centre, NYS Department of
Health, New York, 2011.
2. Faut Koksal, O.Genecel, W. Brostow and H.E. Hagg
lobland “ Effect of high temperature on mechanical and
physical properties of light weight cement based
refractory including expanded vermiculite”, Materials
Research Innovations, W.S.Maney &Son Ltd. 2012,
Received 11 July 2011; accepted 9 September 2011,
pages 7-13.
3. A.M. Papadopoulos, “State of art in thermal insulation
materials and aims for future developments”, Energy
and Buildings, 2005, Pages 3777-86.
4. M. Akao, A. Yamazaki, Y. Fukuda, “Vermiculite board for
novel building material”, Journal of Material Science
Letters, Volume 22, 2003, Pages 1483-1485.
5. Norman M.P. Low, “TheThermal insulatingpropertiesof
Vermiculite”, Journal of Building Physics, Volume 8,
Issue 2, 1984, Pages 107-115.
6. Norman M.P. Low, “Vermiculite- A promising material
for high-temperature”, Refractories & Industrial
Ceramics, Volume 44- No.3, 2003.
7. S.A. Suvorov, V.V. Skurikhin, “High-Temperature heat
insulating materials-basedonVermiculite”,Refractories
& Industrial Ceramics, 2002, Pages 43383-389.
8. P.M. Carkner, “Lightweight insulating concrete and
methods for using same”, U.S.Patent no.6290769.
9. IS: 10262-2009, Bureau of Indian standard- Concrete
Mix Proportioning – Guidelines (first revision) and IS:
456-2000.
10. IS: 516-1959, Methods of Tests for Strength of Concrete
(Eighteenth Revision JUNE 2006).

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IRJET- Experimental Investigation on the Usage of Vermiculite Waste in Concrete

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3114 Experimental Investigation on the Usage of Vermiculite Waste in Concrete M.Manoharan1, R.Haripraba2, S.Muthulakshmi3, N.Aanandh4 1Assistant Professor, Dept. of Civil Engineering, Rajalakshmi Engineering College, Chennai, Tamilnadu, India 2Assistant Professor, Dept. of Civil Engineering, Arulmigu Meenakshi Amman College of Engineering, Thiruvannamalai, Tamilnadu, India 3Assistant Professor, Dept. of Civil Engineering, Rajalakshmi Engineering College, Chennai, Tamilnadu, India 4Assistant Professor, Dept. of Civil Engineering, Rajalakshmi Engineering College, Chennai, Tamilnadu, India ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract –Concrete is one of the most extensively used construction material in the worldwithtwobilliontonsplaced worldwide each year. It is used because of its easy workability and strength. Aggregates are the major ingredients which occupy 60 to 80 percent of the total volume of concrete and greatly influence its properties, mix proportionsandeconomy. In order to reduce the cost of construction and to protect the natural resources, there is a need to use alternative and sustainable construction materials. Vermiculite, which is a waste mineral from the wire lining industry, can be used as partial replacement for fine aggregates in concrete. Use of Vermiculite in concrete enhances the shrinkage and crack resistance, fire resistance, reduces environmental impact and also reduces the construction cost. Important characteristics of a good quality aggregate include resistance to abrasion, resistance to freeze/thaw action, resistance to sulphates, correct shape and surface texture, proper gradation, density, and compressive and flexural strength. The main objective of this research is to study the strength parameters such as compressive strength, split tensile and flexural strength of concrete using vermiculite as partial replacement with 5%, 10% and 20% by weight. Several tests such as compressive strength, tensile strength and flexural strength test on concrete cubes and beam casted with vermiculite were conducted. The results showed that 10% of fine aggregates replaced by Vermiculite gave the best results. Vermiculitecan be used as one of the best replacement for sand and moreover the weight of the concrete is greatly reduced in large extent. Key Words: Compressive strength, density, flexural strength, freeze/thaw action, sustainable materials, tensile strength, Vermiculite. 1. INTRODUCTION Concrete is a widely used construction material because of its good workability. It is mostly consists of aggregates, namely fine and coarse aggregates. Nowadays, sand is heavily depleted and it leads to an alarming state. Natural sand cannot be replaced by any other materials due to its significant properties. Due to the sudden decrease of sand, manufacturing sand came into existenceforthereplacement of river sand. Several alternatives for natural sand are being tested and reports are being published. Among the alternatives, Vermiculite, a mineral whichistobeusedasthe replacement of fine aggregates partially up to some extent. Vermiculite is a hydrous phyllosilicate mineral.Itundergoes significant expansion when heated. Duetosufficientheating, Exfoliation occurs in Vermiculite and the effect is routinely produced in furnaces. It is a light weight material, hence if it is added as an ingredient of concrete, greatly reduces the self-weight of the structure. Vermiculite is used in many commercial sectors namely, 1. Brake lining industries 2. Calcium Silicate boards 3. Soil conditioner 4. Waste treatment 5. Cementitious fire proofing products etc. Table -1: Properties of Vermiculite Chemical Analysis Silicon (SiO2) 39.40% Magnesium (MgO) 25.20% Aluminium (Al2O3) 8.80% Potassium (K2O) 4.50% Calcium (CaO) 1.80% Carbonate (CO2) 1.40% Titanium (TiO2) 0.80% Fluorine (F) 0.50% Physical Properties Melting Point (°C) 1330 Specific Heat (1kJ/kg.K) 1.08 Specific Gravity (Crude) 2.5 Mohs Hardness (Crude) 1-2 pH (ISO 787-9) 7-8 % Loss at 105°C (Expanded Product) < 0.5 % Loss at 1000°C (Expanded Product) < 6 Many researchers have worked on Vermiculite concrete, replacing by weight of cement up to some percentage. Reference [1] observed that an increase in 13% of compressive strength while Vermiculite is replaced 5% by the weight of cement. Reference [2] showed that Concrete gives more compressive strengthwhilecementisreplacedby
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3115 Vermiculite. Usage of Vermiculite gives a good impact on the strength parameters as wellas greatreductioninself-weight. From references [3], [5], [6] & [7], it was observed that the vermiculite act as a high heat resisting material. References [4] & [8] showed that the lightweight material can be prepared from vermiculite with good heat insulating property. Fig -1: Vermiculite 2. TEST ON MATERIALS USED Ordinary Portland cement of 43 grade confirming to IS: 8112-1989, is used in this study. Aggregate is an essentially used construction material and inert material which contains 70 to 80 % volume of the concrete. Hence, if you want to study about the concrete, it is essential to know about the properties of aggregates because of its major volume. Therefore, it should be completely tested before using for construction. Not only the aggregates should be strong and durable but should also have proper shape and size to act as monolithically in the structural components. Hence, it’s essential to conduct several tests on aggregates in order to ensure the quality of aggregates and check their. The following are the test results conducted for the ingredients of concrete: Table -2: Test results of Cement S.No. Property Value 1 Normal Consistency 33% 2 Initial Setting Time (minutes) 35 3 Final Setting Time (minutes) 483 4 Specific Gravity 3.13 5 Fineness Of Cement 1.1 Table -3: Test results of Fine and Coarse Aggregate S.No. Property Fine Aggregate Coarse Aggregate 1. Specific Gravity 2.65 2.85 2. Fineness Modulus 2.80 6.19 3. Water Absorption 1 % 0.6 % Table -4: Test results of Vermiculite 3. METHODOLOGY Based on the guidelines for mix proportions provided in IS: 10262-2009, mix proportion for M25 grade of concrete was arrived as 1:1.41:2.81 with water/cement ratio of 0.45. Table -5: Mix proportions of concrete for 1 m3 Cement Fine aggregate Coarse aggregate Water 438 kg 614.93 kg 1228.21 kg 197.16 lit1 1.41 2.81 0.45 Workability is a main factor which directly connects the strength of concrete. The standard value has to be checked out for the functional strength of the concrete. The fresh concrete is prepared based on the ratio above said and slump cone test is conducted to determinetheworkability of concrete. Table -6: Slump Cone test result Workability Replacement of Vermiculite in %0 5 10 20 Slump 52 mm 52 mm 55 mm 58 mm 4. RESULTS AND DISCUSSIONS 4.1 Compressive Strength The compressive strength test was conducted on 3 specimens for each % replacement as per the recommendations of IS: 516-1959. The specimens were tested on the compression testing machine and the values are tabulated below. S. No. Property Value 1. Specific Gravity 2.34 2. Fineness Modulus 2.43
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3116 Table -7: Compressive Strength Test Results S. No. Curing days % of Vermiculite Compressive Strength (N/mm2) 1 7 days 0 23.56 5 24.44 10 24.89 20 24.00 2 14 days 0 27.11 5 27.56 10 28.89 20 27.78 3 28 days 0 31.11 5 31.78 10 33.11 20 32.22 The above table clearly shows that the compressivestrength of 10% replaced vermiculite produced good result.Based on the above results, a graph was shown below. 0 5 10 15 20 25 30 35 0 5 10 20 CompressiveStrengthin N/mm2 % of Vermiculite 7 Days 14 Days 28 Days Chart -1: Compressive Strength graph 4.2 Split Tensile Strength The split tensile strength test was conducted on 3 cylinder specimens for each % replacement as per the recommendations of IS: 5816-1999. The specimens were tested on the compression testing machine and the values are tabulated below. Table 8: Split Tensile Strength Test Results S. No. Curing days % of Vermiculite Tensile Strength (N/mm2) 1 7 days 0 2.33 5 2.44 10 2.89 20 2.78 2 14 days 0 2.78 5 2.89 10 3.33 20 3.11 3 28 days 0 3.56 5 3.89 10 4.33 20 4.00 0 1 2 3 4 5 0 5 10 20 SplitTensileStrengthin N/mm2 % of Vermiculite 7 Days 14 Days 28 Days Chart -2: Split Tensile Strength graph The above table and graph clearly showed that the tensile strength of 10% replaced vermiculite produced maximum strength. 4.3 Flexural Strength Test The beams are designed and the reinforcement bars are placed accordingly. The flexural strengthtestwasconducted on the beam specimens which was casted using reinforcement bars for each % replacement as per the recommendations of IS: 516-1959. The specimens were tested on the loading frames as shown below and the values are tabulated. Fig -2: Flexural Strength Test
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 06 Issue: 06 | June 2019 www.irjet.net p-ISSN: 2395-0072 © 2019, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 3117 Table -9: Flexural Strength Test Results S. No. Curing days % of Vermiculite Flexural Strength (N/mm2) 1 28 days 0 63.58 5 63.25 10 68.36 20 65.89 60 62 64 66 68 70 0 5 10 20 FlexuralStrengthin N/mm2 % of Vermiculite 28 Days Chart -3: Flexural Strength graph 0 20 40 60 80 0 5 10 20 StrengthinN/mm2 % of Vermiculite Compressive Strength Split Tensile Strength Flexural Strength Chart -4: Cumulative Strength Test graph From the above table and graph, the result obtained as 10% replaced vermiculite produced maximum strength. 5. CONCLUSION This study was conducted to evaluate the effect of using Vermiculite as the partial replacement of fine aggregate in concrete composites and also gave an idea by using these materials within specific range. Several tests were conducted on the materials of the concrete composites and the reports were observed. With the results obtained, we conclude that 10% of fine aggregates replaced by Vermiculite will give best result. It wasalsosuggestedthat in order to reduce the weight of concrete and improvement in the alternation of sand, Vermiculite is used as oneofthebest replacement and moreover the weight of the concrete is greatly reduce in large usage. REFERENCES 1. James S. Webber, “Study the effect of vermiculite on concrete”, Wadsworth Centre, NYS Department of Health, New York, 2011. 2. Faut Koksal, O.Genecel, W. Brostow and H.E. Hagg lobland “ Effect of high temperature on mechanical and physical properties of light weight cement based refractory including expanded vermiculite”, Materials Research Innovations, W.S.Maney &Son Ltd. 2012, Received 11 July 2011; accepted 9 September 2011, pages 7-13. 3. A.M. Papadopoulos, “State of art in thermal insulation materials and aims for future developments”, Energy and Buildings, 2005, Pages 3777-86. 4. M. Akao, A. Yamazaki, Y. Fukuda, “Vermiculite board for novel building material”, Journal of Material Science Letters, Volume 22, 2003, Pages 1483-1485. 5. Norman M.P. Low, “TheThermal insulatingpropertiesof Vermiculite”, Journal of Building Physics, Volume 8, Issue 2, 1984, Pages 107-115. 6. Norman M.P. Low, “Vermiculite- A promising material for high-temperature”, Refractories & Industrial Ceramics, Volume 44- No.3, 2003. 7. S.A. Suvorov, V.V. Skurikhin, “High-Temperature heat insulating materials-basedonVermiculite”,Refractories & Industrial Ceramics, 2002, Pages 43383-389. 8. P.M. Carkner, “Lightweight insulating concrete and methods for using same”, U.S.Patent no.6290769. 9. IS: 10262-2009, Bureau of Indian standard- Concrete Mix Proportioning – Guidelines (first revision) and IS: 456-2000. 10. IS: 516-1959, Methods of Tests for Strength of Concrete (Eighteenth Revision JUNE 2006).