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© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1252
Experimental Investigation on Durability Properties of Silica Fume
blended High Strength Concrete
D Nirosha1, Jaya Priya Yerragudi2,S Ashish kumar3, J Hemavathi 4,V S Theja Karthikeya 5, N
Vijaya kumar6,
1-6Department of Civil Engineering, Annamacharya Institute of Technology and Sciences, Tirupati, - 517520
--------------------------------------------------------------***----------------------------------------------------------------
Abstract:
The most adaptable building material is concrete, which is created by combining cement, sand, and aggregate with
water. After water, concrete is the material that is utilised the most globally. Concrete has a high fire resistance and
durability. Yet, the design of the mix, the curing procedure, and the calibre of the materials employed all affect the quality and
strength of the concrete. There are now many different kinds of high-strength materials available, including high-strength
concrete, thanks to the development of new technologies and materials. The compressive strength of high-strength concrete is
claimed to be much higher than that of regular concrete.
This study is mainly focused on the strength properties as well as the durability properties of silica fume based High
strength concrete. In this study, SF is kept at a replacement level of 15% in the manufacture of HSC for three different mixes
i.e. M60, M70 and M80. In this study, the strength properties viz., compressive strength of HSC was determined at an age of 7,
14 and 28 days of curing and the durability properties viz., Sorpitivity test were studied at 7, 14 and 28 days of curing.
Keywords: High Strength Concrete, Silica fume, Durability properties, Sorpitivity test.
1) Introduction:
1.1 General
In place of normal concrete, high-strength
concrete (HSC) is increasingly being employed in a
number of building applications [1]. This is because to the
unique characteristics of HSC, such as its high
compressive strength, improved durability, and reduced
permeability. HSC was created by the use of cutting-edge
ingredients and procedures such as silica fume, fly ash,
and superplasticizers, which increase the mechanical
properties and durability of the concrete [2]. One benefit
of employing HSC instead of ordinary concrete is the use
of smaller cross-sections, which results in less material
being utilised and cheaper prices. Moreover, the use of
HSC may result in structural components that are lighter
and thinner, thereby increasing architectural expression
and design flexibility [3].
In this instance, HSC has been used in place of
regular concrete to replace the pozzolanic components.
Silica fume, a by-product of the manufacture of silicon or
ferro silicon, is the primary pozzolanic material used in
this experiment [4]. Replacement of silica fume is kept at
15 For the successful and economical use of pozzolanic
materials, the relationship between pozzolanic material
and cement must be studied [5]. A construction made of
concrete should be capable of housing humans for an
extended period of time without sacrificing the
material's intrinsic properties [6]. Durability is the long-
term need that tenants place on the structure [7]. The
strength and durability traits, specifically, Sorpitivity, are
the subject of the current investigation.
1.2 Objective of the study:
This investigation relates mainly to the
production of high strength concrete (HSC) using SF
(Silica Fume). In this study, the replacement level of SF
kept at 15%. Based on the context of this project, the
research comprised the following stages:
 To develop a mixture proportioning process to
manufacture High strength concrete replacing
Portland cement with Silica fume (Micro silica).
 To study compressive strength of SF based HSC
after 7, 14 and 28 days of curing.
 To study the absorption rate of water
(Sorpitivity test) by HSC after 7,14 and 28 days
of curing.
2) Materials used
2.1 Cement:
ULTRATECH-53 grade ordinary Portland cement
conforming to IS: 12269 -2015 was used in this study for
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1253
the manufacture of concrete. The physical and chemical
properties of OPC 53 grade are shown in table 1 and its
specific gravity is noted to be 3.15.
Table 1: Properties of cement
2.2 Fine Aggregate:
In this study, natural river sand was used as fine
aggregate. The bulk specific gravity in oven-dry
condition and water absorption of the sand is observed
as 2.6 and 1% respectively. The Fineness modulus of
sand is observed as 2.69
2.3 Course Aggregate:
In this study, we used natural aggregates of crushed
stone of size 10mm as coarse aggregates. The bulk
specific gravity in over dry conditions and water
absorption of the coarse aggregates of 10mm size are
observed as 2.6 and 0.3% respectively.
2.4 Silica fume:
The pozzolanic material used in this study is silica fume.
Silica fume known as micro silica is one of the by-
products of the manufacture of silicon or ferrosilicon
metal. It is an amorphous silicon dioxide. In this, the
cement is replaced by silica fume at 15%.
2.5 Super plasticizer:
In this study, superplasticizer we used Poly- carboxylate
ether which is used to reduce the water content in the
manufacture of high-strength concrete. This is one of the
essentially utilized superplasticizers in concrete cement.
2.6 Water:
One of the main components while manufacturing high-
strength concrete. In this research, we used potable and
drinking water for casting and curing purposes as per
the IS 456-2000 coal provisions.
3) Mixing, Casting, and Curing:
 Mixing: Mixing as per mix design, the silica fume
is added at a percentage of 15% by replacing
cement with silica fume for three different
grades of concrete viz., M60, M70, and M80
grades of concrete.
 Casting: For this research work, we proceeded
with the casting of 36 cubes of size 100mm *
100mm * 100mm and 36 cylinders of size 50mm
* 100mm. These specimens are undergone
various tests such as compressive strength and
durability tests namely the Sorpitivity test.
 Curing: After completion of the casting, the
specimens are left for curing. The curing
duration may be varied for different tests of
specimens. For the compressive strength test
and Sorpitivity test, the curing duration is for 7
days, 14 days, and 28 days.
Mix proportions:
The main objective of this research work is to enhance
the compressive strength and durability properties by
adding blended materials such as silica fume. As per IS:
10262-2019 guidelines, the mix design is prepared. Here
we used M60, M70, and M80 grade concrete shown in
table 3, which shows the percentages of cement, fine
aggregate, and coarse aggregate by 1:1.97:3.24,
1:1.53:2.48 and 1:1.685:2.75 with water/cement ratio of
0.398, 0.348 and 0.251 each respectively.
Table 2: Mix proportions of concrete.
4) Experimental setup:
The cubes and cylindrical specimens were cured
as designated above-mentioned conditions and tests
were carried out as per IS: 516-1959 for the testing of
strength, and IS 1124 (1974) for the Sorpitivity test.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1254
4.1 Compressive strength test:
The cubes of size 100mm* 100mm* 100mm are
tested under the compression testing machine as per IS:
516-1959 under saturated conditions by completely
wrapping out the moisture content on the surface period
of 7 days, 14 days, and 28 days. The relation between
cement and silica fume was done with a silica fume
percentage of 15%.
Fig 1(a): Compressive strength test setup
Fig 1(b): Compressive strength reading
4.2 Sorpitivity test:
The cylinders of size 100mm*50mm of grades
M60, M70 and M80 are firstly oven dried after curing at a
surface period of 7 days, 14 days, and 28 days. Later
these specimens are tested by applying epoxy resin to
them as per the code IS 1124 (1974). Then these
specimens’ weights are noted and then placed in the
water for about thirty minutes after thirty minutes the
specimens are removed from the water and then dried
for 30 seconds and then weighed and the test is repeated
for about 6 to 8 trials where any two consecutive
weights of specimens are equal. After obtaining the
weights of the specimens,
the rate of penetration of water into the concrete is
calculated.
The Sorptivity rate is calculated by using the
formula:
Sorpitivity rate, S = √
Where, S = Sorpitivity rate
= Change in weights
A = Area of the specimen
= Density of water
t = time taken for the last testing
Fig 2(a): Weighing of specimen
Fig 2(b): Setup for Sorpitivity testing.
5) Results:
5.1 Compressive Strength:
The compressive strength test results are shown
in chart 1. It is seen that concrete of grade M60 attained
the minimum compressive strength values when
compared to the other two mixes after 7 days, 14 days
and 28 days of curing. The mixes of M70 and M80 have
attained the maximum compressive strength values of
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1255
53.94 MPa and 59.89 MPa when compared to mixes of
M60 (47.75 MPa) after 7 days of curing. The mixes of
M70 and M80 have attained the maximum compressive
strength values of 71.37 MPa and 80.09 MPa when
Chart 1: The comparisons of compressive strength
values for different grades of concrete at different ages.
compared to mixes of M60 (63.42 MPa) after 14 days of
curing. The mixes of M70 and M80 have attained the
maximum compressive strength values of 79.32 MPa and
88.89 MPa when compared to mixes of M60 (71.26 MPa)
after 28 days of curing.
5.2 Sorpitivity test:
The Sorpitivity test results are shown in the
chart 2. It is clearly observed that concrete mix of grade
M80 attained the less Sorpitivity values when compared
to those of the other two mixes after 7, 14 and 28 days of
curing.
Chart 2: The comparisons of Sorpitivity test values for
different grades of concrete at different ages.
The concrete mix of grade M60 has attained the
maximum Sorpitivity value of 2.12 after 7 days of curing.
The mixes M70 and M80 attained the Sorpitivity values
1.88 and 1.76 respectively which are less when
compared to the mix M60 after 7 days of curing.
Likewise, for the age of 14 days, the concrete mix of
grade M60 has attained the maximum Sorpitivity value
of 1.89. The mixes M70 and M80 attained the Sorpitivity
values 1.62 and 1.53 respectively which are less when
compared to the mix M60 after 14 days of curing.
Likewise, for the age of 28 days, the concrete mix of
grade M60 has attained the maximum Sorpitivity value
of 1.64. The mixes M70 and M80 attained the Sorpitivity
values 1.35 and 1.21 respectively which are less when
compared to the mix M60 after 28 days of curing.
6) Conclusions:
Based on the test results, the following conclusions
are drawn:
1. The increase in compressive strength has been
observed in the mixes M60, M70 and M80
grades of concrete. It is clearly observed that as
the grade of concrete is high then, the higher is
the compressive strength.
2. As the age of curing increases, the compressive
strength also increases gradually.
3. As the grade of concrete increases, the
Sorpitivity value decreases and it is seen that as
the curing period of concrete is increasing, the
Sorpitivity values are decreasing.
7) References:
1. I. A. Sharaky,F. A. Megahed, M.H. Seleem,
A. M. Badawy The infuence of silica fume, nano
silica and mixing method on the strength
and durability of concrete.
2. Byung Wan Jo, Sumit Chakraborty, Seung-Tae
Lee, and Yun Sung Lee Durability Study of Silica
Fume-mortar exposed to the Combined Sulfate
and Chloride-rich Solution.
3. Byung Wan Jo, Muhammad Ali Sikandar, Sumit
Chakraborty, Zafar Baloch Investigation of the
acid and sulfate resistance performances of
hydrogen-rich water-based mortars.
4. Riyadh A. I. Albattat, Zahra Jamshidzadeh, Ali
Alasadi Assessment of compressive strength and
durability of silica fume-based concrete in acidic
environment
5. B. Krishna Kumari Bai and M. Kanta Rao the
effect of fly ash, SF and its combinations on
strength and durability properties on HSC.

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Experimental Investigation on Durability Properties of Silica Fume blended High Strength Concrete

  • 1. © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1252 Experimental Investigation on Durability Properties of Silica Fume blended High Strength Concrete D Nirosha1, Jaya Priya Yerragudi2,S Ashish kumar3, J Hemavathi 4,V S Theja Karthikeya 5, N Vijaya kumar6, 1-6Department of Civil Engineering, Annamacharya Institute of Technology and Sciences, Tirupati, - 517520 --------------------------------------------------------------***---------------------------------------------------------------- Abstract: The most adaptable building material is concrete, which is created by combining cement, sand, and aggregate with water. After water, concrete is the material that is utilised the most globally. Concrete has a high fire resistance and durability. Yet, the design of the mix, the curing procedure, and the calibre of the materials employed all affect the quality and strength of the concrete. There are now many different kinds of high-strength materials available, including high-strength concrete, thanks to the development of new technologies and materials. The compressive strength of high-strength concrete is claimed to be much higher than that of regular concrete. This study is mainly focused on the strength properties as well as the durability properties of silica fume based High strength concrete. In this study, SF is kept at a replacement level of 15% in the manufacture of HSC for three different mixes i.e. M60, M70 and M80. In this study, the strength properties viz., compressive strength of HSC was determined at an age of 7, 14 and 28 days of curing and the durability properties viz., Sorpitivity test were studied at 7, 14 and 28 days of curing. Keywords: High Strength Concrete, Silica fume, Durability properties, Sorpitivity test. 1) Introduction: 1.1 General In place of normal concrete, high-strength concrete (HSC) is increasingly being employed in a number of building applications [1]. This is because to the unique characteristics of HSC, such as its high compressive strength, improved durability, and reduced permeability. HSC was created by the use of cutting-edge ingredients and procedures such as silica fume, fly ash, and superplasticizers, which increase the mechanical properties and durability of the concrete [2]. One benefit of employing HSC instead of ordinary concrete is the use of smaller cross-sections, which results in less material being utilised and cheaper prices. Moreover, the use of HSC may result in structural components that are lighter and thinner, thereby increasing architectural expression and design flexibility [3]. In this instance, HSC has been used in place of regular concrete to replace the pozzolanic components. Silica fume, a by-product of the manufacture of silicon or ferro silicon, is the primary pozzolanic material used in this experiment [4]. Replacement of silica fume is kept at 15 For the successful and economical use of pozzolanic materials, the relationship between pozzolanic material and cement must be studied [5]. A construction made of concrete should be capable of housing humans for an extended period of time without sacrificing the material's intrinsic properties [6]. Durability is the long- term need that tenants place on the structure [7]. The strength and durability traits, specifically, Sorpitivity, are the subject of the current investigation. 1.2 Objective of the study: This investigation relates mainly to the production of high strength concrete (HSC) using SF (Silica Fume). In this study, the replacement level of SF kept at 15%. Based on the context of this project, the research comprised the following stages:  To develop a mixture proportioning process to manufacture High strength concrete replacing Portland cement with Silica fume (Micro silica).  To study compressive strength of SF based HSC after 7, 14 and 28 days of curing.  To study the absorption rate of water (Sorpitivity test) by HSC after 7,14 and 28 days of curing. 2) Materials used 2.1 Cement: ULTRATECH-53 grade ordinary Portland cement conforming to IS: 12269 -2015 was used in this study for International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1253 the manufacture of concrete. The physical and chemical properties of OPC 53 grade are shown in table 1 and its specific gravity is noted to be 3.15. Table 1: Properties of cement 2.2 Fine Aggregate: In this study, natural river sand was used as fine aggregate. The bulk specific gravity in oven-dry condition and water absorption of the sand is observed as 2.6 and 1% respectively. The Fineness modulus of sand is observed as 2.69 2.3 Course Aggregate: In this study, we used natural aggregates of crushed stone of size 10mm as coarse aggregates. The bulk specific gravity in over dry conditions and water absorption of the coarse aggregates of 10mm size are observed as 2.6 and 0.3% respectively. 2.4 Silica fume: The pozzolanic material used in this study is silica fume. Silica fume known as micro silica is one of the by- products of the manufacture of silicon or ferrosilicon metal. It is an amorphous silicon dioxide. In this, the cement is replaced by silica fume at 15%. 2.5 Super plasticizer: In this study, superplasticizer we used Poly- carboxylate ether which is used to reduce the water content in the manufacture of high-strength concrete. This is one of the essentially utilized superplasticizers in concrete cement. 2.6 Water: One of the main components while manufacturing high- strength concrete. In this research, we used potable and drinking water for casting and curing purposes as per the IS 456-2000 coal provisions. 3) Mixing, Casting, and Curing:  Mixing: Mixing as per mix design, the silica fume is added at a percentage of 15% by replacing cement with silica fume for three different grades of concrete viz., M60, M70, and M80 grades of concrete.  Casting: For this research work, we proceeded with the casting of 36 cubes of size 100mm * 100mm * 100mm and 36 cylinders of size 50mm * 100mm. These specimens are undergone various tests such as compressive strength and durability tests namely the Sorpitivity test.  Curing: After completion of the casting, the specimens are left for curing. The curing duration may be varied for different tests of specimens. For the compressive strength test and Sorpitivity test, the curing duration is for 7 days, 14 days, and 28 days. Mix proportions: The main objective of this research work is to enhance the compressive strength and durability properties by adding blended materials such as silica fume. As per IS: 10262-2019 guidelines, the mix design is prepared. Here we used M60, M70, and M80 grade concrete shown in table 3, which shows the percentages of cement, fine aggregate, and coarse aggregate by 1:1.97:3.24, 1:1.53:2.48 and 1:1.685:2.75 with water/cement ratio of 0.398, 0.348 and 0.251 each respectively. Table 2: Mix proportions of concrete. 4) Experimental setup: The cubes and cylindrical specimens were cured as designated above-mentioned conditions and tests were carried out as per IS: 516-1959 for the testing of strength, and IS 1124 (1974) for the Sorpitivity test.
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1254 4.1 Compressive strength test: The cubes of size 100mm* 100mm* 100mm are tested under the compression testing machine as per IS: 516-1959 under saturated conditions by completely wrapping out the moisture content on the surface period of 7 days, 14 days, and 28 days. The relation between cement and silica fume was done with a silica fume percentage of 15%. Fig 1(a): Compressive strength test setup Fig 1(b): Compressive strength reading 4.2 Sorpitivity test: The cylinders of size 100mm*50mm of grades M60, M70 and M80 are firstly oven dried after curing at a surface period of 7 days, 14 days, and 28 days. Later these specimens are tested by applying epoxy resin to them as per the code IS 1124 (1974). Then these specimens’ weights are noted and then placed in the water for about thirty minutes after thirty minutes the specimens are removed from the water and then dried for 30 seconds and then weighed and the test is repeated for about 6 to 8 trials where any two consecutive weights of specimens are equal. After obtaining the weights of the specimens, the rate of penetration of water into the concrete is calculated. The Sorptivity rate is calculated by using the formula: Sorpitivity rate, S = √ Where, S = Sorpitivity rate = Change in weights A = Area of the specimen = Density of water t = time taken for the last testing Fig 2(a): Weighing of specimen Fig 2(b): Setup for Sorpitivity testing. 5) Results: 5.1 Compressive Strength: The compressive strength test results are shown in chart 1. It is seen that concrete of grade M60 attained the minimum compressive strength values when compared to the other two mixes after 7 days, 14 days and 28 days of curing. The mixes of M70 and M80 have attained the maximum compressive strength values of
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1255 53.94 MPa and 59.89 MPa when compared to mixes of M60 (47.75 MPa) after 7 days of curing. The mixes of M70 and M80 have attained the maximum compressive strength values of 71.37 MPa and 80.09 MPa when Chart 1: The comparisons of compressive strength values for different grades of concrete at different ages. compared to mixes of M60 (63.42 MPa) after 14 days of curing. The mixes of M70 and M80 have attained the maximum compressive strength values of 79.32 MPa and 88.89 MPa when compared to mixes of M60 (71.26 MPa) after 28 days of curing. 5.2 Sorpitivity test: The Sorpitivity test results are shown in the chart 2. It is clearly observed that concrete mix of grade M80 attained the less Sorpitivity values when compared to those of the other two mixes after 7, 14 and 28 days of curing. Chart 2: The comparisons of Sorpitivity test values for different grades of concrete at different ages. The concrete mix of grade M60 has attained the maximum Sorpitivity value of 2.12 after 7 days of curing. The mixes M70 and M80 attained the Sorpitivity values 1.88 and 1.76 respectively which are less when compared to the mix M60 after 7 days of curing. Likewise, for the age of 14 days, the concrete mix of grade M60 has attained the maximum Sorpitivity value of 1.89. The mixes M70 and M80 attained the Sorpitivity values 1.62 and 1.53 respectively which are less when compared to the mix M60 after 14 days of curing. Likewise, for the age of 28 days, the concrete mix of grade M60 has attained the maximum Sorpitivity value of 1.64. The mixes M70 and M80 attained the Sorpitivity values 1.35 and 1.21 respectively which are less when compared to the mix M60 after 28 days of curing. 6) Conclusions: Based on the test results, the following conclusions are drawn: 1. The increase in compressive strength has been observed in the mixes M60, M70 and M80 grades of concrete. It is clearly observed that as the grade of concrete is high then, the higher is the compressive strength. 2. As the age of curing increases, the compressive strength also increases gradually. 3. As the grade of concrete increases, the Sorpitivity value decreases and it is seen that as the curing period of concrete is increasing, the Sorpitivity values are decreasing. 7) References: 1. I. A. Sharaky,F. A. Megahed, M.H. Seleem, A. M. Badawy The infuence of silica fume, nano silica and mixing method on the strength and durability of concrete. 2. Byung Wan Jo, Sumit Chakraborty, Seung-Tae Lee, and Yun Sung Lee Durability Study of Silica Fume-mortar exposed to the Combined Sulfate and Chloride-rich Solution. 3. Byung Wan Jo, Muhammad Ali Sikandar, Sumit Chakraborty, Zafar Baloch Investigation of the acid and sulfate resistance performances of hydrogen-rich water-based mortars. 4. Riyadh A. I. Albattat, Zahra Jamshidzadeh, Ali Alasadi Assessment of compressive strength and durability of silica fume-based concrete in acidic environment 5. B. Krishna Kumari Bai and M. Kanta Rao the effect of fly ash, SF and its combinations on strength and durability properties on HSC.