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International Journal of Civil Engineering and Technology (IJCIET)
Volume 7, Issue 2, March-April 2016, pp. 315–320, Article ID: IJCIET_07_02_027
Available online at
http://www.iaeme.com/IJCIET/issues.asp?JType=IJCIET&VType=7&IType=2
Journal Impact Factor (2016): 9.7820 (Calculated by GISI) www.jifactor.com
ISSN Print: 0976-6308 and ISSN Online: 0976-6316
© IAEME Publication
EXPERIMENTAL INVESTIGATION ON
BEHAVIOUR OF NANO CONCRETE
R. Sakthivel
Research Scholar Karpagam University, Coimbatore, India
Dr. N. Balasundaram
Head of Department, Civil Engineering,
Karpagam University, Coimbatore, India
ABSTRACT
The influence of Nano-Silica on various properties of concrete is obtained
by replacing the cement with various percentages of Nano-Silica. Nano-Silica
is used as a partial replacement for cement in the range of 2.5%, 3%, and
3.5% for M25 mix. Specimens are casted using Nano-Silica concrete.
Laboratory tests were conducted to determine the compressive strength, split
tensile and flexural strength of Nano-Silica concrete at the age of 7 and 28
days. Results indicate that the concrete, by using Nano-Silica powder, was
able to increase its compressive strength. However, the density is reduced
compared to standard mix of concrete. The replacement of cement with 3%
Nano-Silica results in higher strength and reduction in the permeability than
the controlled concrete. The replacement of cement with Nano-Silica more
than 3% results in the reduction of various properties of Nano-Silica concrete.
Key words: Nano-Silica Powder, Strength, Concrete, Plasticizers.
Cite this Article: R. Sakthivel and Dr. N. Balasundaram. Experimental
Investigation on Behaviour of Nano Concrete, International Journal of Civil
Engineering and Technology, 7(2), 2016, pp. 315–320.
http://www.iaeme.com/IJCIET/issues.asp?JType=IJCIET&VType=7&IType=2
1. INTRODUCTION
Concrete is the most common material used in the construction. It is a highly
homogeneous material produced by mixture of finely powdered cement, aggregates of
various sizes and water with inherent physical, chemical and mechanical properties. A
reaction between the cement and water yields calcium silicate hydrate, which gives
concrete strength and other mechanical properties of concrete as well as some by-
products including calcium hydroxide [CH],‘gel pores’ etc.
Concrete is a construction material composed of Portland cement and water
combined with sand, gravel, crushed stone, or other inert material such as expanded
R. Sakthivel and Dr. N. Balasundaram
http://www.iaeme.com/IJCIET/index.asp 316 editor@iaeme.com
slag or vermiculite. The cement and water form a paste which hardens by chemical
reaction into a strong, stone-like mass. The inert materials are called aggregates, and
for economy no more cement paste is used than is necessary to coat all the aggregate
surfaces and fill all the voids.
Super plasticizers
A super plasticizer is used to improve the workability of fresh Nano concrete. The
dosage of super plasticizer also has an effect on the compressive strength of concrete.
It also gives good surface finish and reduces setting time. It is generally
acknowledged that the slump loss of fresh concrete at the construction site is one of
the principal reasons associated with problems related to the strength and durability of
concrete.
To produce high workability concrete without loss of strength. To promote high
early and ultimate strengths by taking advantage of water reduction whilst
maintaining workability.
To produce high quality concrete of improved durability and permeability. At
higher dosages, advantages can be taken of the retardation of initial setting time of
concrete especially in large pours.
NANOTECHNOLOGY
Nano Technology applied to concrete includes the use of nanomaterial’s like Nano
silica, Nano fibres etc. By adding the Nanomaterial’s, concrete composites with
superior properties can be produced. Addition of Nano silica (NS) in concretes and
mortars results in more efficient hydration of cement. Due to the pozzolanic activity,
additional calcium silicate hydrates are formed to generate more strength and to
reduce free calcium hydroxide. This also helps in reducing the cement requirement,
NS improves the microstructure and reduces the water permeability of concrete thus
making it more durable. Concretes with strengths as high as 100 MPa with high
workability, anti-bleeding properties and short de-moulding time can be produced.
Nano silica can be used as an additive to eco concrete mixtures.
2. OBJECTIVE
 The main objective of this project is to determine experimental investigation on
behavior of Nano material with various ratios. Nano technology can modify the
molecular structure of the concrete material to improve the material properties. Effect
of Nano silica dosages on compressive strength, tensile strength, Flexural strength of
concrete.
 The Nano materials such as Nano silica (SiO2) of varying percentage are used to
determine the strength of concrete specimens. (Cube, cylinder & prism) between
control concrete and Nano material %.
3. METHODOLOGY
The main aim of this project is to determine experimental investigation on behavior of
Nano material with various ratios. Controlled concrete slabs. The following steps are
involved.
 Initially the materials used are tested and the test results are shown in table 1.
 Cubes, cylinders and prisms are casted for varying percentage of Nano silica and they
are used for determining the compressive strength split tensile strength and flexural
strength of concrete using varying percentage of Nano silica
Experimental Investigation on Behaviour of Nano Concrete
http://www.iaeme.com/IJCIET/index.asp 317 editor@iaeme.com
 Tests are conducted using compression testing machine and also cylinders are tested
using split tensile testing machine.
 After determining the test results suitable percentage of Nano silica is determined to
cast the Nano silica.
 . The replacement of cement with 3% Nano-Silica results in higher strength and
reduction in the permeability than the controlled concrete.
 The experimental works were conducted on concrete laboratory by applying load.
The following flow chart shows the methodology of this project
4. EXPERIMENTAL WORKS
The preliminary tests were conducted on cement, fine aggregate, coarse aggregate and
the test results were obtained. Based on the results obtained the mix proportion for M
25 concrete is done.
The properties of materials tested are as follows,
Table 1 Properties of Cement, FA, CA
Property Cement FA CA
Fineness 1% 4.72 8.21
Consistency 30%
Initial setting time 35 mins
Specific gravity 3.15 2.67 2.78
Mix Proportion For M25 Concrete
Cement = 320 Kg/m3
Collection of Materials
Collection of literatures
Mix design of Concrete
Casting of Cubes,
Cylinder, Prism
Curing and Testing
Results and discussions
R. Sakthivel and Dr. N. Balasundaram
http://www.iaeme.com/IJCIET/index.asp 318 editor@iaeme.com
Fine aggregate = 794 Kg/m3
Coarse aggregate = 1204 Kg/m3
Water-cement ratio = 0.45
Water content = 140 Kg/m3
C: FA: CA = 1:1.52:2.75
The mix proportion for M25 concrete is calculated using IS 456:2000, IS
10262:2009. Superplastizicer is also added to increase the workability of concrete.
Test Specimens
The compressive stress, split tensile strength and flexural strength of concrete are
determined by casting cubes of size 150x150x150 mm, cylinders of size 300x150 mm
and prisms of size 500mmx100mmx100mm and allowed for 7 and 28 days curing and
the test results were obtained for various percentage of Nano silica.
Table 2 compressive stress of controlled concrete cubes and Nano silica cube
specimen
Compressive stress in 7
days (N/mm2
)
Compressive stress in
28 days (N/mm2
)
CC 18.99 27.60
NS 2.5% 25.95 29.15
NS 3% 27.75 34.80
NS 3.5% 26.66 32.50
Figure 1 shows the compressive stress of cubes
Note: CC- controlled concrete, NS- Nano silica
Table 2 Split Tensile Strength Of controlled concrete Cylinders and Nano silica concrete
cylinders
specimen
Split tensile strength in
7 days (N/mm2
)
Split tensile strength in
28 days (N/mm2
)
CC 2.87 3.51
NS 2.5% 3.26 3.98
NS 3% 3.82 4.64
NS 3.5% 3.45 4.31
0
5
10
15
20
25
30
35
CC NS 2.5% NS 3% NS 3.5%
7 days
28 days
Experimental Investigation on Behaviour of Nano Concrete
http://www.iaeme.com/IJCIET/index.asp 319 editor@iaeme.com
Figure 2 shows the split tensile strength of cylinders
Note: CC- controlled concrete, NS- Nano silica
Table 3 Flexural Strength Of controlled concrete prisms and Nano silica concrete prisms
specimen
Flexural strength in 7
days (N/mm2
)
Flexural strength in 28
days (N/mm2
)
CC 2.08 2.61
NS 2.5% 2.78 3.12
NS 3% 3.94 4.92
NS 3.5% 3.81 4.21
Figure 3 shows the flexural strength of concrete
Note: CC- controlled concrete, NS- Nano silica
Based on the test results obtained the strength of the concrete increases from 2.5%
to 3% and it decreases gradually to 3.5%. The replacement of cement with 3% Nano-
Silica results in higher strength and reduction in the permeability than the controlled
concrete. The replacement of cement with Nano-Silica more than 3% results in the
reduction of various properties of Nano-Silica concrete.
5. CONCLUSION
That the compressive strength of concrete initially increased up to 3% of Nano-Silica
and with further increase in the Nano-Silica content the compressive strength of
0
1
2
3
4
5
CC NS 2.5% NS 3% NS 3.5%
7 days
28 days
0
1
2
3
4
5
CC NS 2.5% NS 3% NS 3.5%
7 days
28 days
R. Sakthivel and Dr. N. Balasundaram
http://www.iaeme.com/IJCIET/index.asp 320 editor@iaeme.com
concrete decreases. Concrete containing lower percentages (3%) of Nano-Silica
possess higher values of compressive strength than that of controlled concrete.A
considerable increase in flexural strength and split tensile strength of Nano-Silica
concrete was observed compared to controlled concrete.
Based on the experimental results, use of Nano-Silica as partial replacement of
cement in small quantities is advantageous on the performance of concrete. Nano-
Silica added in small quantities can improve the strength and permeability resistance.
It can also be concluded that the permeability of concrete decreases with the increase
in the percentage of Nano-Silica up to 3% due to the effect of Nano-Silica filling the
voids in concrete.
The initial and final setting times of cement mortar containing Nano-silica was
found to decrease with increase in the replacement percentage. Use of Nano – silica in
the concrete reduces the co2 emission.
REFERENCES
[1] IS: 456-2000, Indian Standard “Plain and Reinforced Concrete”, Code of
Practice 2000. Bureau of Indian Standards, New Delhi 110002.
[2] IS: 516-1959, Indian Standard “Methods of testing for strength of concrete”,
Code of Practice. Bureau of Indian Standards, New Delhi 110002.
[3] IS: 10262-2009, Indian Standard “Recommended Guidelines for Concrete Mix
Design”, Code of Practice 2009. Bureau of Indian Standards, New Delhi
110002.
[4] IS: 383-1970, Indian Standard “Specification For Coarse And Fine Aggregates
From Natural Sources For Concrete”, Code of Practice 1970. Bureau of Indian
Standards, New Delhi 110002.
[5] IS: 12269-1999, Indian Standard “Specification For 53 Grade Ordinary Portland
Cement”, Code of Practice 1999. Bureau of Indian Standards, New Delhi
110002.
[6] M.S.Shetty, “Concrete Technology”, S.Chand and company ltd., New Delhi.
[7] Strength Efficiency Factor For Nano Silica At Different Age, C. K. Sridhar, S.
B. Vanakudre, International Journal of Engineering and Advanced Technology
(IJEAT) ISSN: 2249 – 8958, Volume-3 Issue-6, August 2014.
[8] Comparative Studies on High Strength Concrete Mixes Using Micro Silica and
Nanosilica, Siva Sai, International Journal of Engineering and Technical
Research (IJETR) ISSN: 2321-0869, Volume-1, Issue-7, September 2013.
[9] Experimental Investigation on The Properties of Nanosilica Concrete, Dr. D. V.
Prasada Rao, Associate Professor, Department of Civil Engineering, Sri
Venkateswara University College of Engineering, Andhra Pradesh, International
Journal of Civil Engineering and Technology (IJCIET) ISSN 0976 – 6308
(Print) Volume 5, Issue 6, June (2014), pp. 116-124.
[10] Experimental Investigation on Nanomaterial Concrete, Saloma, Lecturer,
Faculty of Civil Engineering, Sriwijaya University, International Journal of Civil
& Environmental Engineering (IJENS 137403-5858 Vol: 13, No: 03, pp.15-20,
June 2013),
[11] Study And Performance of High Strength Concrete Using With Nano Silica and
Silica Fume, Seelanani Janardhana, Siddartha Educational Academy Group of
Institutions, Tirupathi, Andhra Pradesh, International Journal of Civil
Engineering and Technology (IJCIET_06_11_019, Volume-6, Issue 11, pp. 184-
196, Nov 2015).

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EXPERIMENTAL INVESTIGATION ON BEHAVIOUR OF NANO CONCRETE

  • 1. http://www.iaeme.com/IJCIET/index.asp 315 editor@iaeme.com International Journal of Civil Engineering and Technology (IJCIET) Volume 7, Issue 2, March-April 2016, pp. 315–320, Article ID: IJCIET_07_02_027 Available online at http://www.iaeme.com/IJCIET/issues.asp?JType=IJCIET&VType=7&IType=2 Journal Impact Factor (2016): 9.7820 (Calculated by GISI) www.jifactor.com ISSN Print: 0976-6308 and ISSN Online: 0976-6316 © IAEME Publication EXPERIMENTAL INVESTIGATION ON BEHAVIOUR OF NANO CONCRETE R. Sakthivel Research Scholar Karpagam University, Coimbatore, India Dr. N. Balasundaram Head of Department, Civil Engineering, Karpagam University, Coimbatore, India ABSTRACT The influence of Nano-Silica on various properties of concrete is obtained by replacing the cement with various percentages of Nano-Silica. Nano-Silica is used as a partial replacement for cement in the range of 2.5%, 3%, and 3.5% for M25 mix. Specimens are casted using Nano-Silica concrete. Laboratory tests were conducted to determine the compressive strength, split tensile and flexural strength of Nano-Silica concrete at the age of 7 and 28 days. Results indicate that the concrete, by using Nano-Silica powder, was able to increase its compressive strength. However, the density is reduced compared to standard mix of concrete. The replacement of cement with 3% Nano-Silica results in higher strength and reduction in the permeability than the controlled concrete. The replacement of cement with Nano-Silica more than 3% results in the reduction of various properties of Nano-Silica concrete. Key words: Nano-Silica Powder, Strength, Concrete, Plasticizers. Cite this Article: R. Sakthivel and Dr. N. Balasundaram. Experimental Investigation on Behaviour of Nano Concrete, International Journal of Civil Engineering and Technology, 7(2), 2016, pp. 315–320. http://www.iaeme.com/IJCIET/issues.asp?JType=IJCIET&VType=7&IType=2 1. INTRODUCTION Concrete is the most common material used in the construction. It is a highly homogeneous material produced by mixture of finely powdered cement, aggregates of various sizes and water with inherent physical, chemical and mechanical properties. A reaction between the cement and water yields calcium silicate hydrate, which gives concrete strength and other mechanical properties of concrete as well as some by- products including calcium hydroxide [CH],‘gel pores’ etc. Concrete is a construction material composed of Portland cement and water combined with sand, gravel, crushed stone, or other inert material such as expanded
  • 2. R. Sakthivel and Dr. N. Balasundaram http://www.iaeme.com/IJCIET/index.asp 316 editor@iaeme.com slag or vermiculite. The cement and water form a paste which hardens by chemical reaction into a strong, stone-like mass. The inert materials are called aggregates, and for economy no more cement paste is used than is necessary to coat all the aggregate surfaces and fill all the voids. Super plasticizers A super plasticizer is used to improve the workability of fresh Nano concrete. The dosage of super plasticizer also has an effect on the compressive strength of concrete. It also gives good surface finish and reduces setting time. It is generally acknowledged that the slump loss of fresh concrete at the construction site is one of the principal reasons associated with problems related to the strength and durability of concrete. To produce high workability concrete without loss of strength. To promote high early and ultimate strengths by taking advantage of water reduction whilst maintaining workability. To produce high quality concrete of improved durability and permeability. At higher dosages, advantages can be taken of the retardation of initial setting time of concrete especially in large pours. NANOTECHNOLOGY Nano Technology applied to concrete includes the use of nanomaterial’s like Nano silica, Nano fibres etc. By adding the Nanomaterial’s, concrete composites with superior properties can be produced. Addition of Nano silica (NS) in concretes and mortars results in more efficient hydration of cement. Due to the pozzolanic activity, additional calcium silicate hydrates are formed to generate more strength and to reduce free calcium hydroxide. This also helps in reducing the cement requirement, NS improves the microstructure and reduces the water permeability of concrete thus making it more durable. Concretes with strengths as high as 100 MPa with high workability, anti-bleeding properties and short de-moulding time can be produced. Nano silica can be used as an additive to eco concrete mixtures. 2. OBJECTIVE  The main objective of this project is to determine experimental investigation on behavior of Nano material with various ratios. Nano technology can modify the molecular structure of the concrete material to improve the material properties. Effect of Nano silica dosages on compressive strength, tensile strength, Flexural strength of concrete.  The Nano materials such as Nano silica (SiO2) of varying percentage are used to determine the strength of concrete specimens. (Cube, cylinder & prism) between control concrete and Nano material %. 3. METHODOLOGY The main aim of this project is to determine experimental investigation on behavior of Nano material with various ratios. Controlled concrete slabs. The following steps are involved.  Initially the materials used are tested and the test results are shown in table 1.  Cubes, cylinders and prisms are casted for varying percentage of Nano silica and they are used for determining the compressive strength split tensile strength and flexural strength of concrete using varying percentage of Nano silica
  • 3. Experimental Investigation on Behaviour of Nano Concrete http://www.iaeme.com/IJCIET/index.asp 317 editor@iaeme.com  Tests are conducted using compression testing machine and also cylinders are tested using split tensile testing machine.  After determining the test results suitable percentage of Nano silica is determined to cast the Nano silica.  . The replacement of cement with 3% Nano-Silica results in higher strength and reduction in the permeability than the controlled concrete.  The experimental works were conducted on concrete laboratory by applying load. The following flow chart shows the methodology of this project 4. EXPERIMENTAL WORKS The preliminary tests were conducted on cement, fine aggregate, coarse aggregate and the test results were obtained. Based on the results obtained the mix proportion for M 25 concrete is done. The properties of materials tested are as follows, Table 1 Properties of Cement, FA, CA Property Cement FA CA Fineness 1% 4.72 8.21 Consistency 30% Initial setting time 35 mins Specific gravity 3.15 2.67 2.78 Mix Proportion For M25 Concrete Cement = 320 Kg/m3 Collection of Materials Collection of literatures Mix design of Concrete Casting of Cubes, Cylinder, Prism Curing and Testing Results and discussions
  • 4. R. Sakthivel and Dr. N. Balasundaram http://www.iaeme.com/IJCIET/index.asp 318 editor@iaeme.com Fine aggregate = 794 Kg/m3 Coarse aggregate = 1204 Kg/m3 Water-cement ratio = 0.45 Water content = 140 Kg/m3 C: FA: CA = 1:1.52:2.75 The mix proportion for M25 concrete is calculated using IS 456:2000, IS 10262:2009. Superplastizicer is also added to increase the workability of concrete. Test Specimens The compressive stress, split tensile strength and flexural strength of concrete are determined by casting cubes of size 150x150x150 mm, cylinders of size 300x150 mm and prisms of size 500mmx100mmx100mm and allowed for 7 and 28 days curing and the test results were obtained for various percentage of Nano silica. Table 2 compressive stress of controlled concrete cubes and Nano silica cube specimen Compressive stress in 7 days (N/mm2 ) Compressive stress in 28 days (N/mm2 ) CC 18.99 27.60 NS 2.5% 25.95 29.15 NS 3% 27.75 34.80 NS 3.5% 26.66 32.50 Figure 1 shows the compressive stress of cubes Note: CC- controlled concrete, NS- Nano silica Table 2 Split Tensile Strength Of controlled concrete Cylinders and Nano silica concrete cylinders specimen Split tensile strength in 7 days (N/mm2 ) Split tensile strength in 28 days (N/mm2 ) CC 2.87 3.51 NS 2.5% 3.26 3.98 NS 3% 3.82 4.64 NS 3.5% 3.45 4.31 0 5 10 15 20 25 30 35 CC NS 2.5% NS 3% NS 3.5% 7 days 28 days
  • 5. Experimental Investigation on Behaviour of Nano Concrete http://www.iaeme.com/IJCIET/index.asp 319 editor@iaeme.com Figure 2 shows the split tensile strength of cylinders Note: CC- controlled concrete, NS- Nano silica Table 3 Flexural Strength Of controlled concrete prisms and Nano silica concrete prisms specimen Flexural strength in 7 days (N/mm2 ) Flexural strength in 28 days (N/mm2 ) CC 2.08 2.61 NS 2.5% 2.78 3.12 NS 3% 3.94 4.92 NS 3.5% 3.81 4.21 Figure 3 shows the flexural strength of concrete Note: CC- controlled concrete, NS- Nano silica Based on the test results obtained the strength of the concrete increases from 2.5% to 3% and it decreases gradually to 3.5%. The replacement of cement with 3% Nano- Silica results in higher strength and reduction in the permeability than the controlled concrete. The replacement of cement with Nano-Silica more than 3% results in the reduction of various properties of Nano-Silica concrete. 5. CONCLUSION That the compressive strength of concrete initially increased up to 3% of Nano-Silica and with further increase in the Nano-Silica content the compressive strength of 0 1 2 3 4 5 CC NS 2.5% NS 3% NS 3.5% 7 days 28 days 0 1 2 3 4 5 CC NS 2.5% NS 3% NS 3.5% 7 days 28 days
  • 6. R. Sakthivel and Dr. N. Balasundaram http://www.iaeme.com/IJCIET/index.asp 320 editor@iaeme.com concrete decreases. Concrete containing lower percentages (3%) of Nano-Silica possess higher values of compressive strength than that of controlled concrete.A considerable increase in flexural strength and split tensile strength of Nano-Silica concrete was observed compared to controlled concrete. Based on the experimental results, use of Nano-Silica as partial replacement of cement in small quantities is advantageous on the performance of concrete. Nano- Silica added in small quantities can improve the strength and permeability resistance. It can also be concluded that the permeability of concrete decreases with the increase in the percentage of Nano-Silica up to 3% due to the effect of Nano-Silica filling the voids in concrete. The initial and final setting times of cement mortar containing Nano-silica was found to decrease with increase in the replacement percentage. Use of Nano – silica in the concrete reduces the co2 emission. REFERENCES [1] IS: 456-2000, Indian Standard “Plain and Reinforced Concrete”, Code of Practice 2000. Bureau of Indian Standards, New Delhi 110002. [2] IS: 516-1959, Indian Standard “Methods of testing for strength of concrete”, Code of Practice. Bureau of Indian Standards, New Delhi 110002. [3] IS: 10262-2009, Indian Standard “Recommended Guidelines for Concrete Mix Design”, Code of Practice 2009. Bureau of Indian Standards, New Delhi 110002. [4] IS: 383-1970, Indian Standard “Specification For Coarse And Fine Aggregates From Natural Sources For Concrete”, Code of Practice 1970. Bureau of Indian Standards, New Delhi 110002. [5] IS: 12269-1999, Indian Standard “Specification For 53 Grade Ordinary Portland Cement”, Code of Practice 1999. Bureau of Indian Standards, New Delhi 110002. [6] M.S.Shetty, “Concrete Technology”, S.Chand and company ltd., New Delhi. [7] Strength Efficiency Factor For Nano Silica At Different Age, C. K. Sridhar, S. B. Vanakudre, International Journal of Engineering and Advanced Technology (IJEAT) ISSN: 2249 – 8958, Volume-3 Issue-6, August 2014. [8] Comparative Studies on High Strength Concrete Mixes Using Micro Silica and Nanosilica, Siva Sai, International Journal of Engineering and Technical Research (IJETR) ISSN: 2321-0869, Volume-1, Issue-7, September 2013. [9] Experimental Investigation on The Properties of Nanosilica Concrete, Dr. D. V. Prasada Rao, Associate Professor, Department of Civil Engineering, Sri Venkateswara University College of Engineering, Andhra Pradesh, International Journal of Civil Engineering and Technology (IJCIET) ISSN 0976 – 6308 (Print) Volume 5, Issue 6, June (2014), pp. 116-124. [10] Experimental Investigation on Nanomaterial Concrete, Saloma, Lecturer, Faculty of Civil Engineering, Sriwijaya University, International Journal of Civil & Environmental Engineering (IJENS 137403-5858 Vol: 13, No: 03, pp.15-20, June 2013), [11] Study And Performance of High Strength Concrete Using With Nano Silica and Silica Fume, Seelanani Janardhana, Siddartha Educational Academy Group of Institutions, Tirupathi, Andhra Pradesh, International Journal of Civil Engineering and Technology (IJCIET_06_11_019, Volume-6, Issue 11, pp. 184- 196, Nov 2015).