Evaporator Equipment used in evaporation, the process of boiling a liquid in order to reduce its volume  Need Reduces transportation cost Storage costs  Prepare for the next Unit operation – drying,  crystallisation etc. Reduces deteriorative chemical reactions  Better microbiological stability  Recovery of solvent http://avibert.blogspot.com
Evaporator Driving force: Temperature difference  in between steam chest temperature and product temperature. Result : Volatile solvent is removed from the feed. Solution (volatile solvent + non volatile solute) Concentrate (Higher solute Conc.) http://avibert.blogspot.com
Examples Concentration of milk to produce condensed milk Concentration of juices Concentration of NaOH, NaCl from aqueous solutions to produce salt. Ether recovery from fat extraction http://avibert.blogspot.com
Basic Parts of an Evaporator Heat-exchanger  Vacuum  Vapour separator  Condenser  http://avibert.blogspot.com
Evaporator Vapor out Feed in Steam in (Saturated vapor) Product out Condensate out (Saturated Liquid) Vapor Separator Heat Exchanger Vaccum for non condensable Condensor unit Coolant In Coolant out http://avibert.blogspot.com
Evaporator Type  Batch Pan  Rising Film  Falling Film  Multiple Effect Evaporators http://avibert.blogspot.com
Processing Factors Conc of solute in feed Conc of solute in product/concentrate Pressure and Temp. of the system Depends on temperature sensitivity of material. Boiling point elevation http://avibert.blogspot.com
Processing Factors Steam pressure and temperature Material of construction  Foaming Low heat transfer rate Entrainment loss http://avibert.blogspot.com
Heat Transfer Coefficient, h A coefficient which indicates the amount of heat flow that is exchanged across a unit area of a medium or system in a unit amount of time with a unit of temperature difference between the boundary of the system.  S.I. unit W m -2  K -1. http://avibert.blogspot.com
Overall Heat Transfer Coefficient, U In cases of combined heat transfer for a heat exchanger, there are two values for h.  Convective heat transfer coefficient  for the fluid film inside the tubes  Convective heat  transfer coefficient for the  fluid  film  outside  the  tubes.      The  thermal  conductivity  (k)  and thickness (Dx) of the tube wall must also be accounted for.   So an additional term (Uo), called the overall heat transfer coefficient, must be used instead.   http://avibert.blogspot.com
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Steam Trap Function Discharge condensate, air and other incondensable gases from a steam system while not permitting the escape of live steam  http://avibert.blogspot.com
Ball Float Steam Trap http://avibert.blogspot.com
Reduces the ferocity of discharge and sound. Sound levels can be reduced by up to 80%.  http://avibert.blogspot.com
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Vapor Out m v h v Steam in  m s h s Condensate out m c h c Water in m w h w Q E Q L http://avibert.blogspot.com
Lab Calculation Calculate U, overall heat transfer coefficient for the evaporator Perform a mass balance and energy balance Calculate discrepancy  http://avibert.blogspot.com
Mass Balance Feed Side: m (kg/s) m (feed in) = m (Vapor) Steam Side m (steam)= m (condensate collected) + m (flash) http://avibert.blogspot.com
Flash Steam Loss The amount of flash steam produced during the pressure reduction can be expressed as: w = (H il  - H fl ) / H fe   where w = ratio of flash steam generated (kg flash steam / kg condensate) H il  = initial liquid enthalpy (kJ/kg) H fl  = final liquid enthalpy (kJ/kg) H fe  = enthalpy of evaporation (kJ/kg) http://avibert.blogspot.com
Energy Balance H (kJ/kg) Energy from the steam to the water Q E The Heat Loss from the vessel to the room, Q L Amount of heat in condensing steam Q S Q S =  Q E +  Q L http://avibert.blogspot.com
Measurements Q S and  Q E  Mass Flow rate- condensate, feed water T,P will give H Specific Enthalpy Q =  mH Q L Surface area Surface temperature Q L  =hA  ∆ T Q E  = UA  ∆ T http://avibert.blogspot.com
Further Reference Transport Processes and Separation process principle by: Christie. J. Geankoplis Animations on evaporator visit: www.rpaulsingh.com  and click animations then evaporator http://avibert.blogspot.com
Multiple-effect Evaporator Water is boiled in a sequence of vessels, each held at a lower pressure than the last.  Because the boiling point of water decreases as pressure decreases, the vapor boiled off in one vessel can be used to heat the next Generally the first vessel (at the highest pressure) requires an external source of heat  http://avibert.blogspot.com
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Thank You http://avibert.blogspot.com

Evaporator

  • 1.
    Evaporator Equipment usedin evaporation, the process of boiling a liquid in order to reduce its volume Need Reduces transportation cost Storage costs Prepare for the next Unit operation – drying, crystallisation etc. Reduces deteriorative chemical reactions Better microbiological stability Recovery of solvent http://avibert.blogspot.com
  • 2.
    Evaporator Driving force:Temperature difference in between steam chest temperature and product temperature. Result : Volatile solvent is removed from the feed. Solution (volatile solvent + non volatile solute) Concentrate (Higher solute Conc.) http://avibert.blogspot.com
  • 3.
    Examples Concentration ofmilk to produce condensed milk Concentration of juices Concentration of NaOH, NaCl from aqueous solutions to produce salt. Ether recovery from fat extraction http://avibert.blogspot.com
  • 4.
    Basic Parts ofan Evaporator Heat-exchanger Vacuum Vapour separator Condenser http://avibert.blogspot.com
  • 5.
    Evaporator Vapor outFeed in Steam in (Saturated vapor) Product out Condensate out (Saturated Liquid) Vapor Separator Heat Exchanger Vaccum for non condensable Condensor unit Coolant In Coolant out http://avibert.blogspot.com
  • 6.
    Evaporator Type Batch Pan Rising Film Falling Film Multiple Effect Evaporators http://avibert.blogspot.com
  • 7.
    Processing Factors Concof solute in feed Conc of solute in product/concentrate Pressure and Temp. of the system Depends on temperature sensitivity of material. Boiling point elevation http://avibert.blogspot.com
  • 8.
    Processing Factors Steampressure and temperature Material of construction Foaming Low heat transfer rate Entrainment loss http://avibert.blogspot.com
  • 9.
    Heat Transfer Coefficient,h A coefficient which indicates the amount of heat flow that is exchanged across a unit area of a medium or system in a unit amount of time with a unit of temperature difference between the boundary of the system. S.I. unit W m -2 K -1. http://avibert.blogspot.com
  • 10.
    Overall Heat TransferCoefficient, U In cases of combined heat transfer for a heat exchanger, there are two values for h. Convective heat transfer coefficient for the fluid film inside the tubes Convective heat transfer coefficient for the  fluid  film  outside  the  tubes.      The  thermal  conductivity  (k)  and thickness (Dx) of the tube wall must also be accounted for.   So an additional term (Uo), called the overall heat transfer coefficient, must be used instead.   http://avibert.blogspot.com
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    Steam Trap FunctionDischarge condensate, air and other incondensable gases from a steam system while not permitting the escape of live steam http://avibert.blogspot.com
  • 17.
    Ball Float SteamTrap http://avibert.blogspot.com
  • 18.
    Reduces the ferocityof discharge and sound. Sound levels can be reduced by up to 80%. http://avibert.blogspot.com
  • 19.
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  • 21.
    Vapor Out mv h v Steam in m s h s Condensate out m c h c Water in m w h w Q E Q L http://avibert.blogspot.com
  • 22.
    Lab Calculation CalculateU, overall heat transfer coefficient for the evaporator Perform a mass balance and energy balance Calculate discrepancy http://avibert.blogspot.com
  • 23.
    Mass Balance FeedSide: m (kg/s) m (feed in) = m (Vapor) Steam Side m (steam)= m (condensate collected) + m (flash) http://avibert.blogspot.com
  • 24.
    Flash Steam LossThe amount of flash steam produced during the pressure reduction can be expressed as: w = (H il - H fl ) / H fe where w = ratio of flash steam generated (kg flash steam / kg condensate) H il = initial liquid enthalpy (kJ/kg) H fl = final liquid enthalpy (kJ/kg) H fe = enthalpy of evaporation (kJ/kg) http://avibert.blogspot.com
  • 25.
    Energy Balance H(kJ/kg) Energy from the steam to the water Q E The Heat Loss from the vessel to the room, Q L Amount of heat in condensing steam Q S Q S = Q E + Q L http://avibert.blogspot.com
  • 26.
    Measurements Q Sand Q E Mass Flow rate- condensate, feed water T,P will give H Specific Enthalpy Q = mH Q L Surface area Surface temperature Q L =hA ∆ T Q E = UA ∆ T http://avibert.blogspot.com
  • 27.
    Further Reference TransportProcesses and Separation process principle by: Christie. J. Geankoplis Animations on evaporator visit: www.rpaulsingh.com and click animations then evaporator http://avibert.blogspot.com
  • 28.
    Multiple-effect Evaporator Wateris boiled in a sequence of vessels, each held at a lower pressure than the last. Because the boiling point of water decreases as pressure decreases, the vapor boiled off in one vessel can be used to heat the next Generally the first vessel (at the highest pressure) requires an external source of heat http://avibert.blogspot.com
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