Air separation units: technology on the move!BRONSWERK
Several industries require pure nitrogen, oxygen or argon for their production processes. Cryogenic Air Separation is the process that enables the separation of these compounds. Interested in this technology? Have a look at this content and contact us if we can help!
Most modern ammonia processes are based on steam-reforming of natural gas or naphtha.
The 3 main technology suppliers are Uhde (Uhde/JM Partnership), Topsoe & KBR.
The process steps are very similar in all cases.
Other suppliers are Linde (LAC) & Ammonia Casale.
In the plant, ammonia is produced from synthesis gas containing hydrogen and nitrogen in the ratio of approximately 3:1. Besides these components, the synthesis gas contains inert gases such as argon and methane to a limited extent. The source of H2 is demineralized water and the hydrocarbons in the natural gas. The source of N2 is the atmospheric air. The source of CO2 is the hydrocarbons in the natural gas feed. Product ammonia and CO2 is sent to urea plant. The present article intended the description of ammonia plant for natural gas based plants and the possible material balance of some section.
Air separation units: technology on the move!BRONSWERK
Several industries require pure nitrogen, oxygen or argon for their production processes. Cryogenic Air Separation is the process that enables the separation of these compounds. Interested in this technology? Have a look at this content and contact us if we can help!
Most modern ammonia processes are based on steam-reforming of natural gas or naphtha.
The 3 main technology suppliers are Uhde (Uhde/JM Partnership), Topsoe & KBR.
The process steps are very similar in all cases.
Other suppliers are Linde (LAC) & Ammonia Casale.
In the plant, ammonia is produced from synthesis gas containing hydrogen and nitrogen in the ratio of approximately 3:1. Besides these components, the synthesis gas contains inert gases such as argon and methane to a limited extent. The source of H2 is demineralized water and the hydrocarbons in the natural gas. The source of N2 is the atmospheric air. The source of CO2 is the hydrocarbons in the natural gas feed. Product ammonia and CO2 is sent to urea plant. The present article intended the description of ammonia plant for natural gas based plants and the possible material balance of some section.
This is great Presentation with 3D effects which is all about production of ammonia from natural gas.
I am damn sure you will be getting everything here searching for.
its better to download it and then run in powerpoint 2013.
A case study on Process Condensate Stripper in Ammonia Plant by Prem Baboo.pdfPremBaboo4
A trouble shooting case study in Fertilizers unit, India.Solving the problem of Feed/Effluent Exchanger E-3321A/B in Process Condensate stripping section of Ammonia plant by Analytical approach. The problem solved by in house experts without changing the heat exchangers while others plant change the heat exchangers. Number of modification done and huge amount of energy saved. The paper intended how to save energy by changing heat exchanger and pressure of PC Stripper. The treated process condensate was earlier cooled by CW in final cooler from about 90ºC to 40ºC. This available heat of PC is being recovered by exchanging heat with DM water in a plate heat exchanger. The pressure of PC stripper has been raised to about 1.5 kg/cm²g to make the extra heat recovery possible. Now pressure is 41.5 kg/cm2. A new Plate heat exchanger was procured & installed for the heat recovery.
Episode 3 : Production of Synthesis Gas by Steam Methane ReformingSAJJAD KHUDHUR ABBAS
Episode 3 : Production of Synthesis Gas by Steam Methane Reforming
History of Synthesis Gas
In 1780, Felice Fontana discovered that combustible gas develops if water vapor is passed over carbon at temperatures over 500 °C. This CO and H2 containing gas was called water gas and mainly used for lighting purposes in the19th century.
As of the beginning of the 20th century, H2/CO-mixtures were used for syntheses of hydrocarbons and then, as a consequence, also called synthesis gas.
Haber and Bosch discovered the synthesis of ammonia from H2 and N2 in 1910 and the first industrial ammonia synthesis plant was commissioned in 1913.
The production of liquid hydrocarbons and oxygenates from syngas conversion over iron catalysts was discovered in 1923 by Fischer and Tropsch.
Much of the syngas conversion processes were being developed in Germany during the first and second world wars at a time when natural resources were becoming scare and alternative routes for hydrogen production, ammonia synthesis, and transportation fuels were a necessity.
In 1943/44, this was applied for large-scale production of artificial fuels from synthesis gas in Germany.
Calculation of an Ammonia Plant Energy Consumption: Gerard B. Hawkins
Calculation of an Ammonia Plant Energy Consumption:
Case Study: #06023300
Plant Note Book Series: PNBS-0602
CONTENTS
0 SCOPE
1 CALCULATION OF NATURAL GAS PROCESS FEED CONSUMPTION
2 CALCULATION OF NATURAL GAS PROCESS FUEL CONSUMPTION
3 CALCULATION OF NATURAL GAS CONSUMPTION FOR PILOT BURNERS OF FLARES
4 CALCULATION OF DEMIN. WATER FROM DEMIN. UNIT
5 CALCULATION OF DEMIN. WATER TO PACKAGE BOILERS
6 CALCULATION OF MP STEAM EXPORT
7 CALCULATION OF LP STEAM IMPORT
8 DETERMINATION OF ELECTRIC POWER CONSUMPTION
9 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT ISBL
10 ADJUSTMENT OF ELECTRIC POWER CONSUMPTION FOR TEST RUN CONDITIONS
11 CALCULATION OF AMMONIA SHARE IN MP STEAM CONSUMPTION IN UTILITIES
12 CALCULATION OF AMMONIA SHARE IN ELECTRIC POWER CONSUMPTION IN UTILITIES
13 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT OSBL
14 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT
Selection of amine solvents for CO2 capture from natural gas power plant - presentation by Jiafei Zhang in the Natural Gas CCS session at the UKCCSRC Cardiff Biannual Meeting, 10-11 September 2014
A common apparatus used in gas absorption, distillation and liq-liq extraction. Design and construction of packed towers, types of tower, packing materials, liquid distributers, types of packing...
This is great Presentation with 3D effects which is all about production of ammonia from natural gas.
I am damn sure you will be getting everything here searching for.
its better to download it and then run in powerpoint 2013.
A case study on Process Condensate Stripper in Ammonia Plant by Prem Baboo.pdfPremBaboo4
A trouble shooting case study in Fertilizers unit, India.Solving the problem of Feed/Effluent Exchanger E-3321A/B in Process Condensate stripping section of Ammonia plant by Analytical approach. The problem solved by in house experts without changing the heat exchangers while others plant change the heat exchangers. Number of modification done and huge amount of energy saved. The paper intended how to save energy by changing heat exchanger and pressure of PC Stripper. The treated process condensate was earlier cooled by CW in final cooler from about 90ºC to 40ºC. This available heat of PC is being recovered by exchanging heat with DM water in a plate heat exchanger. The pressure of PC stripper has been raised to about 1.5 kg/cm²g to make the extra heat recovery possible. Now pressure is 41.5 kg/cm2. A new Plate heat exchanger was procured & installed for the heat recovery.
Episode 3 : Production of Synthesis Gas by Steam Methane ReformingSAJJAD KHUDHUR ABBAS
Episode 3 : Production of Synthesis Gas by Steam Methane Reforming
History of Synthesis Gas
In 1780, Felice Fontana discovered that combustible gas develops if water vapor is passed over carbon at temperatures over 500 °C. This CO and H2 containing gas was called water gas and mainly used for lighting purposes in the19th century.
As of the beginning of the 20th century, H2/CO-mixtures were used for syntheses of hydrocarbons and then, as a consequence, also called synthesis gas.
Haber and Bosch discovered the synthesis of ammonia from H2 and N2 in 1910 and the first industrial ammonia synthesis plant was commissioned in 1913.
The production of liquid hydrocarbons and oxygenates from syngas conversion over iron catalysts was discovered in 1923 by Fischer and Tropsch.
Much of the syngas conversion processes were being developed in Germany during the first and second world wars at a time when natural resources were becoming scare and alternative routes for hydrogen production, ammonia synthesis, and transportation fuels were a necessity.
In 1943/44, this was applied for large-scale production of artificial fuels from synthesis gas in Germany.
Calculation of an Ammonia Plant Energy Consumption: Gerard B. Hawkins
Calculation of an Ammonia Plant Energy Consumption:
Case Study: #06023300
Plant Note Book Series: PNBS-0602
CONTENTS
0 SCOPE
1 CALCULATION OF NATURAL GAS PROCESS FEED CONSUMPTION
2 CALCULATION OF NATURAL GAS PROCESS FUEL CONSUMPTION
3 CALCULATION OF NATURAL GAS CONSUMPTION FOR PILOT BURNERS OF FLARES
4 CALCULATION OF DEMIN. WATER FROM DEMIN. UNIT
5 CALCULATION OF DEMIN. WATER TO PACKAGE BOILERS
6 CALCULATION OF MP STEAM EXPORT
7 CALCULATION OF LP STEAM IMPORT
8 DETERMINATION OF ELECTRIC POWER CONSUMPTION
9 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT ISBL
10 ADJUSTMENT OF ELECTRIC POWER CONSUMPTION FOR TEST RUN CONDITIONS
11 CALCULATION OF AMMONIA SHARE IN MP STEAM CONSUMPTION IN UTILITIES
12 CALCULATION OF AMMONIA SHARE IN ELECTRIC POWER CONSUMPTION IN UTILITIES
13 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT OSBL
14 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT
Selection of amine solvents for CO2 capture from natural gas power plant - presentation by Jiafei Zhang in the Natural Gas CCS session at the UKCCSRC Cardiff Biannual Meeting, 10-11 September 2014
A common apparatus used in gas absorption, distillation and liq-liq extraction. Design and construction of packed towers, types of tower, packing materials, liquid distributers, types of packing...
Analysis of Steady State Cryogenic Air Separation Unit and Simulation of Fixe...Dr. Amarjeet Singh
Atmospheric dry air contains approximately 78%
nitrogen, 21% oxygen, and 1% argon plus low concentrations
of noble gases like carbon dioxide, hydrocarbons and other
impurities. An air separation unit divides atmospheric air
into the three pure gaseous components (nitrogen, oxygen
and argon). Nitrogen, oxygen and argon are used by industry
in large quantities and hence termed industrial gases. The
current work aim is to simulate the cryogenic air separation
unit including adsorber and cryogenic distillation. Simulation
of absorber is carried out using ADSIM of Aspen Tech to
remove carbon dioxide (CO2
) and water vapour (H2O). The
breakthrough curves of carbon dioxide (CO2
) and water
vapour on 5A molecular sieve and activated alumina
respectively are found at different Reynolds number. The
study helps to find out schedule time adsorber/desorber unit.
ASPEN Plus simulator is used to simulate cryogenic air
separation into nitrogen, oxygen and argon.
Comparison of Alternate Methods for Generating Nitrogen for Industrial Proces...Classic Controls, Inc.
Nitrogen is used extensively throughout various industries because of its properties as an inert gas. The volume of its use can make nitrogen cost a significant line item on an operation's expense report.
The article compares three methods of generating nitrogen and examines the relative costs of each.
It will help to the students of Mechanical Engineering. These notes are according to HVAC Subject. Some important topics are here for your good understanding. These are written in easy language, u can understand easily.
Furnaces in Refinery and Petrochemicals
Process furnaces
Crude distillation unit
Reaction Heaters
Reformer Heater
Heater Performance objectives
Reasons to save Energy
Heater Types
Radiant section
Convection section
Crossover section
Burners
Centrifugal Pump
Type of pumps
Centrifugal Pump working
Centrifugal Pump calculation
How to choose pump
Characteristics curves
Pump head compensation
Cavitation and NPSH
Priming
Multi stage centrifugal Pump
Pump safety
Effluent Treatment Plant
What is ETP
Need fo ETP
Design of ETP
Design of ETP
Sludge treatment process
Flowchart of ETP
Case study of ETP
ETP plant operation
Textile plant ETP
Equalization
Sedimentation
Settlers
Sludge treatment process
Flowchart of ETP
Case study of ETP
ETP plant operation
Textile plant ETP
Equalization
Sedimentation
Settlers
PH adjustment
Rotating equipment maintenance.
PUMPS
COMPRESSORS
AGITATORS
FANS / BLOWERS
TURBINES
VACUUM PUMPS
VALVES
Type of Seals
Stuffing
SINGLE MECHANICAL SEAL Pusher Type
Bellows Mechanical Seal
Double Mechanical Seal
STEAM TRAPS
Steam trap is a type of automatic valve that filters out
condensate (i.e. condensed steam) and non-condensable gases
such as air without letting steam escape.
Steam ejector working principle
An ejector is a device used to suck the gas or vapour from the desired vessel or system. An ejector is similar to an of vacuum pump or compressor. The major difference between the ejector and the vacuum pump or compressor is it had no moving parts. Hence it is relatively low-cost and easy to operate and maintenance free equipment.
Piping and Instrument Diagram
Piping and Instrument Diagram Standard Symbols Detailed Documentation provides a standard set of shapes & symbols for documenting P&ID and PFD,
including standard shapes of instrument, valves, pump, heating exchanges, mixers, crushers, vessels, compressors, filters, motors and connecting shapes.
Permit To Work
Types of Permit To Work
Hot Work Permit
Confined Space Entry Permit
Electrical Permit
Excavation Permit
Radiography Permit
Crane Critical Lifts Permit
Man Basket Operation
Permit Issuer Responsibilities
Permit Receiver Responsibilities
HSE Permit Coordinator
Responsibilities
Revalidation of the Permit
Work Permit Flow Chart
Heat exchangers
TUBE AND SHELL
PLATE HEAT EXCHANGER
FLOW OF ARRANGEMENT
REGENERATIVE HEAT EXCHANGER
log mean temperature difference (LMTD)
Number of Transfer Units (NTU) Method
EFFECTIVENESS OF HEAT EXCHANGER
Hybrid optimization of pumped hydro system and solar- Engr. Abdul-Azeez.pdffxintegritypublishin
Advancements in technology unveil a myriad of electrical and electronic breakthroughs geared towards efficiently harnessing limited resources to meet human energy demands. The optimization of hybrid solar PV panels and pumped hydro energy supply systems plays a pivotal role in utilizing natural resources effectively. This initiative not only benefits humanity but also fosters environmental sustainability. The study investigated the design optimization of these hybrid systems, focusing on understanding solar radiation patterns, identifying geographical influences on solar radiation, formulating a mathematical model for system optimization, and determining the optimal configuration of PV panels and pumped hydro storage. Through a comparative analysis approach and eight weeks of data collection, the study addressed key research questions related to solar radiation patterns and optimal system design. The findings highlighted regions with heightened solar radiation levels, showcasing substantial potential for power generation and emphasizing the system's efficiency. Optimizing system design significantly boosted power generation, promoted renewable energy utilization, and enhanced energy storage capacity. The study underscored the benefits of optimizing hybrid solar PV panels and pumped hydro energy supply systems for sustainable energy usage. Optimizing the design of solar PV panels and pumped hydro energy supply systems as examined across diverse climatic conditions in a developing country, not only enhances power generation but also improves the integration of renewable energy sources and boosts energy storage capacities, particularly beneficial for less economically prosperous regions. Additionally, the study provides valuable insights for advancing energy research in economically viable areas. Recommendations included conducting site-specific assessments, utilizing advanced modeling tools, implementing regular maintenance protocols, and enhancing communication among system components.
Welcome to WIPAC Monthly the magazine brought to you by the LinkedIn Group Water Industry Process Automation & Control.
In this month's edition, along with this month's industry news to celebrate the 13 years since the group was created we have articles including
A case study of the used of Advanced Process Control at the Wastewater Treatment works at Lleida in Spain
A look back on an article on smart wastewater networks in order to see how the industry has measured up in the interim around the adoption of Digital Transformation in the Water Industry.
Cosmetic shop management system project report.pdfKamal Acharya
Buying new cosmetic products is difficult. It can even be scary for those who have sensitive skin and are prone to skin trouble. The information needed to alleviate this problem is on the back of each product, but it's thought to interpret those ingredient lists unless you have a background in chemistry.
Instead of buying and hoping for the best, we can use data science to help us predict which products may be good fits for us. It includes various function programs to do the above mentioned tasks.
Data file handling has been effectively used in the program.
The automated cosmetic shop management system should deal with the automation of general workflow and administration process of the shop. The main processes of the system focus on customer's request where the system is able to search the most appropriate products and deliver it to the customers. It should help the employees to quickly identify the list of cosmetic product that have reached the minimum quantity and also keep a track of expired date for each cosmetic product. It should help the employees to find the rack number in which the product is placed.It is also Faster and more efficient way.
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2. air separation
• An air separation plant separates atmospheric air into its primary
components, typically nitrogen and oxygen, and sometimes also argon and
other rare inert gases.
• The most common method for air separation is fractional distillation.
Cryogenic air separation units (ASUs) are built to provide nitrogen or
oxygen and often co-produce argon. Other methods such as
membrane, pressure swing adsorption (PSA) and vacuum pressure swing
adsorption (VPSA) are commercially used to separate a single component
from ordinary air. High purity oxygen, nitrogen, and argon used
for semiconductor device fabrication requires cryogenic distillation.
Similarly, the only viable source of the rare gases neon, krypton,
and xenon is the distillation of air using at least two distillation columns.
3.
4. Cryogenic distillation process
• Pure gases can be separated from air by first cooling it until it
liquefies, then selectively distilling the components at their various
boiling temperatures. The process can produce high purity gases but
is energy-intensive. This process was pioneered by Dr. Carl von
Linde in the early 20th century and is still used today to produce high
purity gases.
• The cryogenic separation process requires a very tight integration of
heat exchangers and separation columns to obtain a good efficiency
and all the energy for refrigeration is provided by the compression of
the air at the inlet of the unit.
5. • To achieve the low distillation temperatures an air separation unit requires
a refrigeration cycle that operates by means of the Joule–Thomson effect, and
the cold equipment has to be kept within an insulated enclosure (commonly
called a "cold box"). The cooling of the gases requires a large amount of energy to
make this refrigeration cycle work and is delivered by an air compressor. Modern
ASUs use expansion turbines for cooling; the output of the expander helps drive
the air compressor, for improved efficiency. The process consists of the following
main steps:
1. Before compression the air is pre-filtered of dust.
2. Air is compressed where the final delivery pressure is determined by recoveries
and the fluid state (gas or liquid) of the products. Typical pressures range
between 5 and 10 bar gauge. The air stream may also be compressed to
different pressures to enhance the efficiency of the ASU. During compression
water is condensed out in inter-stage coolers.
3. The process air is generally passed through a molecular sieve bed, which
removes any remaining water vapour, as well as carbon dioxide, which would
freeze and plug the cryogenic equipment. Molecular sieves are often designed
to remove any gaseous hydrocarbons from the air, since these can be a
problem in the subsequent air distillation that could lead to explosions. The
molecular sieves bed must be regenerated. This is done by installing multiple
units operating in alternating mode and using the dry co-produced waste gas to
desorb the water.
6. 4. Process air is passed through an integrated heat exchanger (usually a plate
fin heat exchanger) and cooled against product (and waste) cryogenic
streams. Part of the air liquefies to form a liquid that is enriched in oxygen.
The remaining gas is richer in nitrogen and is distilled to almost pure
nitrogen (typically < 1ppm) in a high pressure (HP) distillation column. The
condenser of this column requires refrigeration which is obtained from
expanding the more oxygen rich stream further across a valve or through
an Expander, (a reverse compressor).
5. Alternatively the condenser may be cooled by interchanging heat with a
reboiler in a low pressure (LP) distillation column (operating at 1.2-1.3 bar
abs.) when the ASU is producing pure oxygen. To minimize the compression
cost the combined condenser/reboiler of the HP/LP columns must operate
with a temperature difference of only 1-2 K, requiring plate fin brazed
aluminium heat exchangers. Typical oxygen purities range in from 97.5% to
99.5% and influences the maximum recovery of oxygen. The refrigeration
required for producing liquid products is obtained using the Joule–Thomson
effect in an expander which feeds compressed air directly to the low
pressure column. Hence, a certain part of the air is not to be separated and
must leave the low pressure column as a waste stream from its upper
section.
7.
8. 6. Because the boiling point of argon (87.3 K at standard conditions)
lies between that of oxygen (90.2 K) and nitrogen (77.4 K), argon builds
up in the lower section of the low pressure column. When argon is
produced, a vapor side draw is taken from the low pressure column
where the argon concentration is highest. It is sent to another column
rectifying the argon to the desired purity from which liquid is returned
to the same location in the LP column. Use of modern structured
packings which have very low pressure drops enable argon with less
than 1 ppm impurities. Though argon is present in less to 1% of the
incoming, the air argon column requires a significant amount of energy
due to the high reflux ratio required (about 30) in the argon column.
Cooling of the argon column can be supplied from cold expanded rich
liquid or by liquid nitrogen.
7. Finally the products produced in gas form are warmed against the
incoming air to ambient temperatures. This requires a carefully crafted
heat integration that must allow for robustness against disturbances
(due to switch over of the molecular sieve beds). It may also require
additional external refrigeration during start-up.
9. • The separated products are sometimes supplied by pipeline to large
industrial users near the production plant. Long distance
transportation of products is by shipping liquid product for large
quantities or as dewar flasks or gas cylinders for small quantities.
10. Non-cryogenic processes
• Pressure swing adsorption provides separation of oxygen or nitrogen from air without
liquefaction. The process operates around ambient temperature; a zeolite (molecular
sponge) is exposed to high pressure air, then the air is released and an adsorbed film of
the desired gas is released. The size of compressor is much reduced over a liquefaction
plant, and portable oxygen concentrators are made in this manner to provide oxygen-
enriched air for medical purposes. Vacuum swing adsorption is a similar process; the
product gas is evolved from the zeolite at sub-atmospheric pressure.
• Membrane technologies can provide alternate, lower-energy approaches to air
separation. For example, a number of approaches are being explored for oxygen
generation. Polymeric membranes operating at ambient or warm temperatures, for
example, may be able to produce oxygen-enriched air (25-50% oxygen). Ceramic
membranes can provide high-purity oxygen (90% or more) but require higher
temperatures (800-900 deg C) to operate. These ceramic membranes include Ion
Transport Membranes (ITM) and Oxygen Transport Membranes (OTM). Air Products and
Chemicals Inc and Praxair are developing flat ITM and tubular OTM systems, .
11. • Membrane gas separation is used to provide oxygen poor and
nitrogen rich gases instead of air to fill the fuel tanks of jet liners, thus
greatly reducing the chances of accidental fires and explosions.
Conversely, membrane gas separation is currently used to provide
oxygen enriched air to pilots flying at great altitudes in aircraft
without pressurized cabins.
• Oxygen-enriched air can be obtained exploiting the different solubility
of oxygen and nitrogen. Oxygen is more soluble than nitrogen in
water, so if air is degassed from water, a stream of 35% oxygen can be
obtained.
12.
13. Applications
• Large amounts of oxygen are required for coal gasification projects;
cryogenic plants producing 3000 tons/day are found in some
projects.In steelmaking oxygen is required for the basic oxygen
steelmaking. Large amounts of nitrogen with low oxygen impurities
are used for inerting storage tanks of ships and tanks for petroleum
products, or for protecting edible oil products from oxidation.