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Fatigue damage of adhesive layers – 
experiments and models. 
by 
Tomas Walander, Alexander Eklind, Thomas 
Carlberger, Ulf Stigh 
1 
Tamonash Jana 
001411202019
2 
Introduction 
Generation of macroscopic cracks due to fatigue. 
Use of adhesive materials in Industry.
3 
Adhesives 
1. DOW Betamate5096 
(BM5096) 
 A Rubber Based Stiff 
Structural Adhesive 
 Epoxy Resin 
 Nominal Layer 
Thickness- 0.3 mm 
2. DOW BetaForce 
2850 (BF2850) 
Polyurethane (PUR) 
based Adhesive 
Soft modular 
Adhesive 
Nominal Layer 
Thickness- 1 mm
4 
Methodology 
1st Approach - Paris’ law combined with the Energy 
Release Rate G : 
For a linear elastic specimen with a single crack tip loaded 
with a prescribed load F 
(1) 
b=width of the specimen, Complience C=Δ/F, 
a=Crack length
5 
As suggested by Berry(1963) 
p,q=Compliance calibration parameters 
Now 
Substituting dC/da in eqn (1) 
⇒ 
(2) 
(3) 
(4)
6 
 Experimental values of Δ, F, and number of elapsed 
Cycles N are obtained. 
Using Eqtn (3) and (4), G vs. a is evaluated for each 
experiment 
Hence the parameters c and n of ‘Paris’ Law’ are 
evaluated. 
(5)
7 
The relation used for determining da/dN 
using experimental data is 
afit =fitted crack length 
(6)
8 
2nd Approach - Damage Mechanics Approach : 
The damage evolution law is given by 
(7) 
D=Damage variable, σ= Peel stress, kn= elastic stiffness ; 
alternatively 
(8) 
α, β =Damage law parameters, σth = fatigue threshold value 
in stress
 The damage laws are implemented as a User Material 
subroutine (UMAT) in Abaqus with the cohesive elements to 
simulate the experiments. 
9 
The model does only consider damage in peel loading.
10 
Experiment
 Specimens are manufactured according to the dimensions 
in the table below. 
 By repeated experiments, the static stress-deformation 
relations for Mode I loading are first determined for each 
adhesive. 
 For the rubber adhesive, the method of Andersson and 
Stigh (2004) is used; for the PUR adhesive, the method of 
Tamuzs et al. (2004) is used. 
11
Stress-deformation relations for Rubber adhesive 
12
13 
Stress-deformation relations for PUR adhesive
A fatigue test rig is developed consisting of a solid bar with 
six individual loads cells. 
14 
The rig is mounted in a servo hydraulic tensile test 
machine. 
The experiments are controlled with the initial value of 
Load ratio=0.1 
The experiments are performed at 4 Hz for up to three 
million load cycles.
15 
Experimental data and simulations of F vs N for 
Rubber adhesive
Experimental data and simulations of F vs N for PUR 
16 
adhesive
17 
Evaluated a vs. N for Rubber adhesive
18 
Evaluated a vs. N for PUR adhesive
19 
Evaluated G vs. N for Rubber adhesive
20 
Evaluated G vs. N for PUR adhesive
21 
Result Analysis and Parameter Identification 
The end value of G is used as an engineering estimate of 
the threshold value Gth for fatigue crack growth. 
The corresponding threshold value in stress σth is 
determined as the value of stress corresponding to the point 
where G= Gth. 
The parameters α and β in Eq. (8) are determined by fitting 
results from 
numerical simulations to the experimental results in a log-log 
plot of (da/dN) vs. G.
22 
Parameters obtained by evaluation
23 
Conclusion 
Fracture mechanics using Paris’ law provides simpler 
parameter estimation than damage mechanics approach. 
The local modelling of fatigue damage using damage 
mechanics provides a more physical model of the fatigue 
properties. 
The experimental results contain substantial scatter for the 
rubber based adhesive. Thus, a large 
number of repeated experiments are necessary to give useful 
data and properties.
24 
Thank You

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Fatigue damage of adhesive layers.

  • 1. Fatigue damage of adhesive layers – experiments and models. by Tomas Walander, Alexander Eklind, Thomas Carlberger, Ulf Stigh 1 Tamonash Jana 001411202019
  • 2. 2 Introduction Generation of macroscopic cracks due to fatigue. Use of adhesive materials in Industry.
  • 3. 3 Adhesives 1. DOW Betamate5096 (BM5096)  A Rubber Based Stiff Structural Adhesive  Epoxy Resin  Nominal Layer Thickness- 0.3 mm 2. DOW BetaForce 2850 (BF2850) Polyurethane (PUR) based Adhesive Soft modular Adhesive Nominal Layer Thickness- 1 mm
  • 4. 4 Methodology 1st Approach - Paris’ law combined with the Energy Release Rate G : For a linear elastic specimen with a single crack tip loaded with a prescribed load F (1) b=width of the specimen, Complience C=Δ/F, a=Crack length
  • 5. 5 As suggested by Berry(1963) p,q=Compliance calibration parameters Now Substituting dC/da in eqn (1) ⇒ (2) (3) (4)
  • 6. 6  Experimental values of Δ, F, and number of elapsed Cycles N are obtained. Using Eqtn (3) and (4), G vs. a is evaluated for each experiment Hence the parameters c and n of ‘Paris’ Law’ are evaluated. (5)
  • 7. 7 The relation used for determining da/dN using experimental data is afit =fitted crack length (6)
  • 8. 8 2nd Approach - Damage Mechanics Approach : The damage evolution law is given by (7) D=Damage variable, σ= Peel stress, kn= elastic stiffness ; alternatively (8) α, β =Damage law parameters, σth = fatigue threshold value in stress
  • 9.  The damage laws are implemented as a User Material subroutine (UMAT) in Abaqus with the cohesive elements to simulate the experiments. 9 The model does only consider damage in peel loading.
  • 11.  Specimens are manufactured according to the dimensions in the table below.  By repeated experiments, the static stress-deformation relations for Mode I loading are first determined for each adhesive.  For the rubber adhesive, the method of Andersson and Stigh (2004) is used; for the PUR adhesive, the method of Tamuzs et al. (2004) is used. 11
  • 12. Stress-deformation relations for Rubber adhesive 12
  • 14. A fatigue test rig is developed consisting of a solid bar with six individual loads cells. 14 The rig is mounted in a servo hydraulic tensile test machine. The experiments are controlled with the initial value of Load ratio=0.1 The experiments are performed at 4 Hz for up to three million load cycles.
  • 15. 15 Experimental data and simulations of F vs N for Rubber adhesive
  • 16. Experimental data and simulations of F vs N for PUR 16 adhesive
  • 17. 17 Evaluated a vs. N for Rubber adhesive
  • 18. 18 Evaluated a vs. N for PUR adhesive
  • 19. 19 Evaluated G vs. N for Rubber adhesive
  • 20. 20 Evaluated G vs. N for PUR adhesive
  • 21. 21 Result Analysis and Parameter Identification The end value of G is used as an engineering estimate of the threshold value Gth for fatigue crack growth. The corresponding threshold value in stress σth is determined as the value of stress corresponding to the point where G= Gth. The parameters α and β in Eq. (8) are determined by fitting results from numerical simulations to the experimental results in a log-log plot of (da/dN) vs. G.
  • 22. 22 Parameters obtained by evaluation
  • 23. 23 Conclusion Fracture mechanics using Paris’ law provides simpler parameter estimation than damage mechanics approach. The local modelling of fatigue damage using damage mechanics provides a more physical model of the fatigue properties. The experimental results contain substantial scatter for the rubber based adhesive. Thus, a large number of repeated experiments are necessary to give useful data and properties.