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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1808
Development of a New Solid Insulation paper with the use of
Phenol Formaldehyde Resin Material for a Oil-Immersed Transformer
Kulbeer Singh1, Harinder Singh Sandhu 2
1Student, Department of Electrical Engineering, AIET Faridkot, Punjab, India
2Assistant Professor, Department of Electrical Engineering, AIET Faridkot, Punjab, India.
----------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - The utilization of paper as a insulation
material in various engineering applications is more due
to its mechanical and electrical properties. As paper is
flexible therefore it has been designed as insulation
material in electrical engineering for various parts and
components. The raw electrical insulation material used
for conventional transformer is kraft paper and further
modification is done by layering of phenol formaldehyde
resin through certain procedure. The electrical and
mechanical properties of newly modified paper are
improved as compared to the existing one.
Key Words: Kraft paper; Phenol Formaldehyde Resin;
Electric Strength in oil; Electric strength in air.
1. INTRODUCTION
The transformer is like a heart of the power system.
Transformers are vital components of electric power
generation, transmission, allocation and widely held of
transformers consists of liquid dielectrics such as
hydrocarbon oil and solid insulation as paper. Most of
the transformers are oil-immersed type and their
insulation is provided by mainly dielectric mineral oil
and solid insulation paper. Insulation paper which is
widely used in oil-immersed transformers is made of
natural cellulose [1, 2]. A few insulation materials were
known for low temperature power applications in early
days. Paper was one of the first insulation material used
in high voltage technology. A combination of electrical
stress and the degradation of insulation are constantly
happening, as one of the major causes of insulation
failure is general wear and tear. But nowadays insulation
papers with improved electrical and mechanical
properties are developed and Kraft paper is one of the
widely used insulating materials in transformers.
A lot of the research work has been done by researchers
on the modification for improvement of insulation of oil
[3–5]. But research to improve the insulation of paper is
not approached to desirable levels, which is also a very
important concern in regard to improve the efficiency
and life of a transformer. As life of transformer totally
depends on insulation.
2. USE OF PHENOL FORMALDEHYDE RESIN
It is commonly used in products of rubber. The phenol
formaldehyde resin ensures good solubility in
hydrocarbons and serves as indispensable modifying
agent for chloroprene rubber. The bonding with the
cellulose paper is like a lamination. When particles of
Phenol Formaldehyde Resin are used in layering, they
can be attached to the cellulose surface. This effect may
greatly change the dielectric properties of oil-
impregnated insulation paper. Therefore, high density
Formaldehyde resin is used for the layering process. The
results show that this newly prepared paper by layering
will improve insulation properties.
3. SAMPLE PREPARATION
Layering is best way to add up new properties in existing
one paper. The samples are prepared by layering with
the help of brush in small step movements.
Fig -1: Kraft Paper Sheet
The transformer paper(3mil) is collected from the firm
named as Kraft paper. Two samples are prepared first by
one side layering and second one with double side
layering. The results of these two samples are compared
with unmodified fresh paper to get desired results.
Identification of sample is:
TP- without Layering
TP1- One side layered
TP2- Both side layer
All the three samples of transformer paper are prepared
from a sheet of 100x30 cm2. Thickness of whole sheet is
3 mil.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1809
4. EXPERIMENTAL WORK
The diagram of the electrodes for measuring the
breakdown voltage is shown in Figure 2. A copper bar
was used to connect the HV electrode with the HVAC
power supply. The diameter and height of the high-
voltage (HV) and ground electrodes were both 25 mm. In
this test, transformer oil was used for the dielectric in
the stainless steel box.
Fig -2: Diagram of electrodes
The experiment was performed for finding the electric
strength of paper in oil and air. The oil gap was formed
in the 3 cm-diameter whole of the 3 mm-thick
paperboard. The thickness of the experimental papers is
about 75, 90,104 microns respectively. The external
diameter of the paperboard was 6 cm. Circles of 4cm
diameter of paper sheet were cut. All samples were put
into the vacuum chamber and were dried at 90 °C for 48
h, and then the mineral oil at 40 °C was infused into the
glass bottles in the vacuum chamber to immerse samples
for 24 h.
5. TEST APPARATUS
According to clause 5 of IEC publication 243 the test is
carried out in air and oil. The electrodes shall be in
accordance with Sub-clauses 6.1.1 or 6.1.3 of the
publication. The preferred electrodes are the 25/75 mm
electrodes. The faces of the electrodes shall be parallel
and free from pits or other imperfections. All test pieces
should be sufficiently large to avoid flash-over. The
number of tests may be made on one test piece. The
application of voltage is in accordance with the Sub-
clause of IEC publication 243. Criterion of breakdown,
see clause of that publication. Nine tests made according
to standard.
Fig -3: BDV Tester
6. RESULTS
The maximum voltage which can material bear without
causing breakdown or damage, usually expressed in
kilovolts per unit of thickness. The test is performed for
air and oil separately. The sample size used for the
testing is 4 cm-diameter circles. The results are little bit
improved in air after the layering of paper and much
improved in oil. It is clear from the reading that modified
paper is electrically very strong in oil under the load
conditions. But its good sign for us the electric strength
is gradually increased in oil. The readings noted from the
testing procedure to determine Dielectric Strength for
fresh and modified papers after layering with the
specified methodology prescribed in [7] are tabulated
below. The actual results are obtained by calculating the
mean value of three breakdowns reading for same
sample.
Table -1: Readings of samples
Property Units TP TP1 TP2
Dielectric Strength in
air
kV/mm 11 14.1 16.4
Dielectric Strength in
oil kv/mm
kV/mm 45 58.5 70.3
7. DISCUSSIONS
The graphs are plotted for comparison of original sample
TP with modified papers TP1 TP2. After results it is
obtained that electric strength of paper in oil has been
improved very well. But Electric Strength in air is
increased little bit that is not much important.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1810
The graph shown in Figures are of Dielectric Strength of
papers in air and oil respectively. These Figures
represents the values obtained for Dielectric Strength. It
is recorded by the procedure followed in laboratory at
room temperature on the sample of fresh and modified
insulating papers w.r.t. kV/mm of Dielectric Strength.
The layering of Phenol Formaldehyde Resin improves
the dielectric strength of paper in both air and oil. The
graph shows the ascending trend for the Dielectric
Strength as we move from left to right .
8. CONCLUSIONS
In summary, it is easy to implement method as
implemented to improve the Dielectric properties of the
Kraft paper. Additional test of physical & dielectric
properties were also performed on fresh and modified
paper to examine the full potential of the Kraft paper,
and it was found that Dielectric breakdown
characteristics of modified Kraft with phenol
formaldehyde resin in oil and air have the better results
as compared to the original fresh samples of Kraft paper.
REFERENCES
[1] T. V. Oommen and T. A. Prevost, “Cellulose insulation
in oil-filled power transformers—part II—maintaining
insulation integrity and life,” IEEE Electrical Insulation
Magazine, vol. 22, no. 2, pp. 5–14, 2006.
[2] P. KopWansky, L. Tomco, and K. Marton, “The DC
dielectric breakdown strength of magnetic fluids based
on transformer oil,” Journal of Magnetism and Magnetic
Materials, vol. 289, no. 1, pp. 415–418, 2005.
[3] P. Pang and P. Englezos, “Application of pretreated
ground calcium carbonate in mechanical pulp
suspensions,” Pulp and Paper Canada, vol. 104, no. 6, pp.
37–39, 2003.
[4] M. Ohashi, S. Kawakami, Y. Yokogawa, and G. C. Lai,
“Spherical aluminum nitride fillers for heat-conducting
plastic packages,” Journal of the American Ceramic
Society, vol. 88, no. 9, pp. 2615–2618, 2005.
[5] Enis Tuncer, Georgios Polizos, Isidor Sauers, and D.
Randy James, “Electrical insulation paper and its physical
properties at cryogenic temperatures” IEEE transaction
on applied superconductivity Volume: 21, issue 3, page
1438-1440 June 2011.
[6] Masood, M. U. Zuberi and E. Husain, “ Breakdown
strength of solid dielectrics in liquid nitrogen” IEEE
transactions on dielectrics and electrical insulation vol.
15, no 4, page 1051-1055 august 2008.
[7] T A Prevost, T V. Oommen, "Cellulose insulation in
oil-filled power transformers: Part I- History and
development [J]", IEEE Electrical Insulation Magazine,
vol. 1, no. 22, pp. 28-35, 2006.
[8] Akira Miyoshi, “ A method for thermally upgrading
insulating paper using alkyl-naphthalene oil. IEEE
transactions on electrical insulation, Volume: EI-11,
issue 3, Sept. 1976.
[9] G.L Atkinson, and W.R. Thoms , “An epoxy-paper
insulation system for high voltage applications” IEEE
transactions on electrical insulation Volume: EI-2,
issue:1, page 18-24 April 1967.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1811

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IRJET- Development of a New Solid Insulation paper with the use of Phenol Formaldehyde Resin Material for a Oil-Immersed Transformer

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1808 Development of a New Solid Insulation paper with the use of Phenol Formaldehyde Resin Material for a Oil-Immersed Transformer Kulbeer Singh1, Harinder Singh Sandhu 2 1Student, Department of Electrical Engineering, AIET Faridkot, Punjab, India 2Assistant Professor, Department of Electrical Engineering, AIET Faridkot, Punjab, India. ----------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - The utilization of paper as a insulation material in various engineering applications is more due to its mechanical and electrical properties. As paper is flexible therefore it has been designed as insulation material in electrical engineering for various parts and components. The raw electrical insulation material used for conventional transformer is kraft paper and further modification is done by layering of phenol formaldehyde resin through certain procedure. The electrical and mechanical properties of newly modified paper are improved as compared to the existing one. Key Words: Kraft paper; Phenol Formaldehyde Resin; Electric Strength in oil; Electric strength in air. 1. INTRODUCTION The transformer is like a heart of the power system. Transformers are vital components of electric power generation, transmission, allocation and widely held of transformers consists of liquid dielectrics such as hydrocarbon oil and solid insulation as paper. Most of the transformers are oil-immersed type and their insulation is provided by mainly dielectric mineral oil and solid insulation paper. Insulation paper which is widely used in oil-immersed transformers is made of natural cellulose [1, 2]. A few insulation materials were known for low temperature power applications in early days. Paper was one of the first insulation material used in high voltage technology. A combination of electrical stress and the degradation of insulation are constantly happening, as one of the major causes of insulation failure is general wear and tear. But nowadays insulation papers with improved electrical and mechanical properties are developed and Kraft paper is one of the widely used insulating materials in transformers. A lot of the research work has been done by researchers on the modification for improvement of insulation of oil [3–5]. But research to improve the insulation of paper is not approached to desirable levels, which is also a very important concern in regard to improve the efficiency and life of a transformer. As life of transformer totally depends on insulation. 2. USE OF PHENOL FORMALDEHYDE RESIN It is commonly used in products of rubber. The phenol formaldehyde resin ensures good solubility in hydrocarbons and serves as indispensable modifying agent for chloroprene rubber. The bonding with the cellulose paper is like a lamination. When particles of Phenol Formaldehyde Resin are used in layering, they can be attached to the cellulose surface. This effect may greatly change the dielectric properties of oil- impregnated insulation paper. Therefore, high density Formaldehyde resin is used for the layering process. The results show that this newly prepared paper by layering will improve insulation properties. 3. SAMPLE PREPARATION Layering is best way to add up new properties in existing one paper. The samples are prepared by layering with the help of brush in small step movements. Fig -1: Kraft Paper Sheet The transformer paper(3mil) is collected from the firm named as Kraft paper. Two samples are prepared first by one side layering and second one with double side layering. The results of these two samples are compared with unmodified fresh paper to get desired results. Identification of sample is: TP- without Layering TP1- One side layered TP2- Both side layer All the three samples of transformer paper are prepared from a sheet of 100x30 cm2. Thickness of whole sheet is 3 mil.
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1809 4. EXPERIMENTAL WORK The diagram of the electrodes for measuring the breakdown voltage is shown in Figure 2. A copper bar was used to connect the HV electrode with the HVAC power supply. The diameter and height of the high- voltage (HV) and ground electrodes were both 25 mm. In this test, transformer oil was used for the dielectric in the stainless steel box. Fig -2: Diagram of electrodes The experiment was performed for finding the electric strength of paper in oil and air. The oil gap was formed in the 3 cm-diameter whole of the 3 mm-thick paperboard. The thickness of the experimental papers is about 75, 90,104 microns respectively. The external diameter of the paperboard was 6 cm. Circles of 4cm diameter of paper sheet were cut. All samples were put into the vacuum chamber and were dried at 90 °C for 48 h, and then the mineral oil at 40 °C was infused into the glass bottles in the vacuum chamber to immerse samples for 24 h. 5. TEST APPARATUS According to clause 5 of IEC publication 243 the test is carried out in air and oil. The electrodes shall be in accordance with Sub-clauses 6.1.1 or 6.1.3 of the publication. The preferred electrodes are the 25/75 mm electrodes. The faces of the electrodes shall be parallel and free from pits or other imperfections. All test pieces should be sufficiently large to avoid flash-over. The number of tests may be made on one test piece. The application of voltage is in accordance with the Sub- clause of IEC publication 243. Criterion of breakdown, see clause of that publication. Nine tests made according to standard. Fig -3: BDV Tester 6. RESULTS The maximum voltage which can material bear without causing breakdown or damage, usually expressed in kilovolts per unit of thickness. The test is performed for air and oil separately. The sample size used for the testing is 4 cm-diameter circles. The results are little bit improved in air after the layering of paper and much improved in oil. It is clear from the reading that modified paper is electrically very strong in oil under the load conditions. But its good sign for us the electric strength is gradually increased in oil. The readings noted from the testing procedure to determine Dielectric Strength for fresh and modified papers after layering with the specified methodology prescribed in [7] are tabulated below. The actual results are obtained by calculating the mean value of three breakdowns reading for same sample. Table -1: Readings of samples Property Units TP TP1 TP2 Dielectric Strength in air kV/mm 11 14.1 16.4 Dielectric Strength in oil kv/mm kV/mm 45 58.5 70.3 7. DISCUSSIONS The graphs are plotted for comparison of original sample TP with modified papers TP1 TP2. After results it is obtained that electric strength of paper in oil has been improved very well. But Electric Strength in air is increased little bit that is not much important.
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1810 The graph shown in Figures are of Dielectric Strength of papers in air and oil respectively. These Figures represents the values obtained for Dielectric Strength. It is recorded by the procedure followed in laboratory at room temperature on the sample of fresh and modified insulating papers w.r.t. kV/mm of Dielectric Strength. The layering of Phenol Formaldehyde Resin improves the dielectric strength of paper in both air and oil. The graph shows the ascending trend for the Dielectric Strength as we move from left to right . 8. CONCLUSIONS In summary, it is easy to implement method as implemented to improve the Dielectric properties of the Kraft paper. Additional test of physical & dielectric properties were also performed on fresh and modified paper to examine the full potential of the Kraft paper, and it was found that Dielectric breakdown characteristics of modified Kraft with phenol formaldehyde resin in oil and air have the better results as compared to the original fresh samples of Kraft paper. REFERENCES [1] T. V. Oommen and T. A. Prevost, “Cellulose insulation in oil-filled power transformers—part II—maintaining insulation integrity and life,” IEEE Electrical Insulation Magazine, vol. 22, no. 2, pp. 5–14, 2006. [2] P. KopWansky, L. Tomco, and K. Marton, “The DC dielectric breakdown strength of magnetic fluids based on transformer oil,” Journal of Magnetism and Magnetic Materials, vol. 289, no. 1, pp. 415–418, 2005. [3] P. Pang and P. Englezos, “Application of pretreated ground calcium carbonate in mechanical pulp suspensions,” Pulp and Paper Canada, vol. 104, no. 6, pp. 37–39, 2003. [4] M. Ohashi, S. Kawakami, Y. Yokogawa, and G. C. Lai, “Spherical aluminum nitride fillers for heat-conducting plastic packages,” Journal of the American Ceramic Society, vol. 88, no. 9, pp. 2615–2618, 2005. [5] Enis Tuncer, Georgios Polizos, Isidor Sauers, and D. Randy James, “Electrical insulation paper and its physical properties at cryogenic temperatures” IEEE transaction on applied superconductivity Volume: 21, issue 3, page 1438-1440 June 2011. [6] Masood, M. U. Zuberi and E. Husain, “ Breakdown strength of solid dielectrics in liquid nitrogen” IEEE transactions on dielectrics and electrical insulation vol. 15, no 4, page 1051-1055 august 2008. [7] T A Prevost, T V. Oommen, "Cellulose insulation in oil-filled power transformers: Part I- History and development [J]", IEEE Electrical Insulation Magazine, vol. 1, no. 22, pp. 28-35, 2006. [8] Akira Miyoshi, “ A method for thermally upgrading insulating paper using alkyl-naphthalene oil. IEEE transactions on electrical insulation, Volume: EI-11, issue 3, Sept. 1976. [9] G.L Atkinson, and W.R. Thoms , “An epoxy-paper insulation system for high voltage applications” IEEE transactions on electrical insulation Volume: EI-2, issue:1, page 18-24 April 1967.
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 03 | Mar-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1811