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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1150
EFFECT OF MIXING AND COMPACTION TEMPERATURES ON THE INDIRECT TENSILE
STRENGTH AND FATIGUE BEHAVIOUR OF BITUMINOUS CONCRETE MIX PREPARED
USING POLYMER MODIFIED BITUMEN
SHARANABASAPPA KORI
----------------------------------------------------------------***------------------------------------------------------------------
ABSTRACT - Bituminous mixes are used in the surface layer of road and airfield pavements. The mix is composed usually of
aggregate and bitumen. The design of bituminous paving mix, as with the design of other engineering materials is largely a
matter of selecting and proportioning of constituent materials to obtain the desired properties in the finished pavement
structure.
In the present study, an attempt is made to evaluate the effects of Mixing and Compaction temperature on the Marshall
Properties, Indirect Tensile Strength and Fatigue behaviour of Bituminous Concrete Mix prepared using Polymer Modified
Bitumen. The present study includes an aggregate gradation of Bituminous Concrete Mix Grading-2 as per MoRT&H
specifications (4th revision), Polymer Modified Bitumen (PMB-70) as binder. The design of Bituminous Concrete Mix prepared
using Polymer Modified Bitumen as per IRC SP 53-2002 specifications.
Based on the experimental work and analysis carried out in the present study, an ideal mixing temperature of 160oC
and compaction temperature of 140oC is suggested for the preparation of Bituminous Concrete Mix prepared using Polymer
Modified Bitumen.
1. INTRODUCTION
1.1 GENERAL
Bituminous materials are extensively used for roadway construction, primarily because of their excellent binding
characteristics and water proofing properties relatively at low cost. The bituminous mix design aims to determine the
proportion of bitumen, filler, fine aggregates and coarse aggregates to produce a mix which is workable, strong, durable and
economical. Significant variation in daily and seasonal temperature of pavement induces early development of distress
conditions (ravelling, undulation, rutting, cracking, bleeding, and potholing) of bituminous pavement. Another major concern
for distress of road surface is overloading of commercial vehicles and increased traffic density.
SBS is a styrene-butadiene-styrene made by the co-polymerization of butadiene and styrene. Butadiene and styrene
block copolymer, to form a styrene (S) - butadiene (B) - benzene Ethylene (S) of the structure, as thermoplastic elastomeric.
SBS has the advantages of rubber and plastic, at room temperature with a rubber elastic, like rubber, as high temperatures can
melt flow, a plastic material. SBS formed within the bitumen, greatly improving the performance of bitumen.
Binder viscosity varies with temperature and different binders require different temperatures to achieve the same
handling properties. Polymer modified binders, in particular, increase in viscosity at a much faster rate on cooling than normal
paving grade bitumen.
1.2 OBJECTIVES OF THE PRESENT STUDY
 To assess the physical properties of aggregate as per MoRT&H requirements.
 To assess the physical properties of Polymer Modified Bitumen [PMB-70 (SBS)] as per IRC SP: 53-2002 requirements.
 To determine the optimum bitumen content of Bituminous Concrete Mix prepared using Polymer Modified Bitumen by
Marshall Method of mix design.
 To assess the Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at optimum
bitumen content by varying mixing and compaction temperatures.
 To conduct Indirect Tensile Strength Test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
optimum bitumen content by varying mixing and compaction temperatures.
 To conduct Indirect Tensile Fatigue Test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
25oC keeping constant mixing temperature, varying compaction temperature and stress level.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1151
 To carryout Linear Regression analysis for the data obtained from Indirect Tensile Fatigue Test conducted on
Bituminous Concrete Mix prepared using Polymer Modified Bitumen.
2. LITERATURE REVIEW
2.1 GENERAL
The durability of asphaltic concrete is greatly influenced by the environmental changes during the year between hot
and cold temperatures and between day and night. High temperatures can soften the bitumen and consequently reduce the
stiffness of asphaltic concrete making the mix more susceptible to rutting. On the other hand, low temperature can increase
the stiffness of bitumen and reduce the flexibility of the asphaltic concrete, hence, inducing fatigue failure. As a result, cracking
of the pavement surface may develop which adversely affects the performance of the asphaltic concrete. Thus, high
temperature stiffness and low temperature flexibility are important properties in bituminous mixtures respectively to avert
rutting and cracking.
2.2 PRACTICAL MIX DESIGN MODEL FOR ASPHALT MIXTURE.(5)
This paper describes an “Optimisation of asphalt mixture design to ensure favourable behaviour at low and high air
temperatures” is aimed to find a practical model for the optimisation of asphalt mixture composition which will be related to
the target functional properties of asphalt pavement relevant for various climate and traffic conditions in the field.
2.3 DETERMINATION OF MIXING AND COMPACTING TEMPERATURES FOR HOT MIX ASPHALT.(3)
This paper gives the typical mixing and compacting temperature has been normally set as 160°C and 140°C respectively
based on experience for the lab procedure purpose. With the newly revised Specification of Roadwork 2007, new bitumen
grade had been introduced including grade 60-70 and some other types of modified bitumen. The objective of this study is to
determine the appropriate mixing and compacting temperature for the bitumen grades by viscosity and correlation with other
physical properties of bitumen. Rotational Brookfield Viscometer was used to determine the correct temperature for viscosity
at 165°C and 135°C and at viscosity ranges of 0.17±0.02 and 0.28±0.03 Pa s for mixing and compacting, respectively as per
ASTM D 2493
3. EXPERIMENTAL INVESTIGATIONS
3.1 GENERAL
In the present study the aggregate gradation Grading-2 adopted for Bituminous Concrete as per Table 500-18
recommended by MORT&H (IVth Revision) specifications. Basic Engineering tests on aggregates and binder were conducted in
the laboratory to assess their properties.
Marshall Method of mix design was adopted to carryout mix design for Bituminous Concrete Mix prepared using
Polymer Modified Bitumen. Marshall Stability and Indirect Tensile Strength tests were conducted on Bituminous Concrete Mix
prepared using Polymer Modified Bitumen by varying mixing and compaction temperatures. For the selected mixing and
compaction temperatures Indirect Tensile Fatigue test was conducted at 25oC by varying stress level.
3.2 CONSTITUENTS OF A MIX (Aggregates, Bitumen & Cement)
Table 3.1: Physical Properties of Aggregates
Description of Aggregate Tests Test Results
Requirements as per Table 500-17 of MoRT&H
Specifications
Aggregate Impact value (%) 18.94 Max 24%
Flakiness and Elongation Index (Combined)
(%)
28.97 Max 30%
Los Angeles Abrasion value (%) 19.44 Max 30%
Water Absorption (%) 0.5 Max 2%
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1152
Table 3.2: Test Results of Polymer Modified Bitumen PMB-70(SBS) and Requirements
Test Test Results
Requirements as per IRC SP:53-
2002
Penetration at 25°C, 100gm,
5 Seconds, 0.1mm
68.67 50-90
Softening Point (Ring & Ball), °C 58.5 Minimum 55
Ductility at 27oC 100+ +60
Flash point, COC, °C 252 Minimum 220
Elastic Recovery of Half Thread in Ductilometer at 15°C, % 78 Minimum 75
Separation, Difference in Softening point (Ring & Ball),°C 2 Maximum 3
Viscosity at 150oC, Poise 3.59 2-6
Thin Film Oven Test ( TFOT ) on Residue
Loss in mass, % 0.64 Maximum 1
Increase in Softening point
(Ring & Ball), °C
4 Maximum 6
Reduction in Penetration of Residue at 25°C, % 23.29 Maximum 35
Elastic Recovery of Half Thread in Ductilometer at 25°C, % 60 Minimum 50
Table 3.3: Specific Gravity of Materials
Description of materials Specific Gravity
Coarse aggregate 2.67
Fine aggregate 2.72
Mineral filler (cement) 3.12
Polymer Modified Bitumen PMB-70(SBS) 1.02
Table 3.4: Aggregate Gradation for Bituminous Concrete Mix (Grading-2) as per MoRT&H Specification
IS Sieve Size, mm % Passing (Specified) % Passing (Mid Limit)
19 100 100
13.2 79-100 89.5
9.5 70-88 79
4.75 53-71 62
2.36 42-58 50
1.18 34-48 41
0.60 26-38 32
0.30 18-28 23
0.15 12-20 16
0.075 4-10 7
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1153
3.3 MARSHALL METHOD OF MIX DESIGN
There are two major features of Marshall Stability method of designing mixes are:
 Density Voids Analysis
 Stability Flow Test.
Figure 3.1: Marshall Stability Test
3.4 INDIRECT TENSILE STRENGTH TEST
Figure 3.2: Indirect Tensile Strength Test
3.5 INDIRECT TENSILE FATIGUE TEST
Indirect Tensile Fatigue Test apparatus
Salient features of the equipment
Capacity - 2 Tons
Load type - Half Sine
Major component - LVDT (Linear Variable Differential Transducers)
- Load cell
- Loading frame
- Temperature controlled chamber
- Position controller
- Data acquisition system
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1154
Figure 3.3: Indirect Tensile Fatigue Test
4. ANALYSIS OF DATA
4.1 GENERAL
Marshall Stability test was carried out on Bituminous Concrete Mix specimens prepared using Polymer Modified
Bitumen to determine the optimum bitumen content, Marshall Stability and volumetric properties of the mix.
The Marshall properties and Indirect Tensile Strength values of Bituminous Concrete Mix prepared using Polymer
Modified Bitumen were calculated by varying mixing and compaction temperatures. Indirect Tensile Fatigue Test was carried
out on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at 25oC keeping constant mixing temperature,
varying compaction temperature and stress level.
Table 4.1: Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen
Bitumen
content, %
Marshall
stability, kgs
Flow,
mm
Bulk
density,
g/cc
Total air
voids, %
Voids Filled with
Bitumen, %
Voids in Mineral
Aggregates, %
5.0 1818.14 2.56 2.38 5.39 68.41 17.06
5.5 1838.93 3.20 2.39 4.42 74.45 17.31
6.0 1700.51 3.56 2.38 3.98 77.90 18.00
6.5 1579.84 3.68 2.37 3.92 79.41 19.02
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1155
Figure 4.1: Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen to determine
the optimum bitumen content
1500
1600
1700
1800
1900
4.5 5.0 5.5 6.0 6.5 7.0
Stability,kgs
Bitumen, %
Stability v/s Bitumen
2.0
2.5
3.0
3.5
4.0
4.5 5.0 5.5 6.0 6.5 7.0
Flow,mm
Bitumen, %
Flow v/s Bitumen
2.365
2.370
2.375
2.380
2.385
2.390
4.5 5.0 5.5 6.0 6.5 7.0
Bulkdensity,g/cc
Bitumen, %
Bulk density v/s Bitumen
3.5
4.0
4.5
5.0
5.5
6.0
4.5 5.0 5.5 6.0 6.5 7.0
Airvoids,%
Bitumen, %
Air voids v/s Bitumen
66
69
72
75
78
81
4.5 5.0 5.5 6.0 6.5 7.0
VoidsfilledwithBitumen,%
Bitumen, %
Voids filled with Bitumen v/s
Bitumen
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1156
4.2 DETERMINATION OF OPTIMUM BITUMEN CONTENT
The optimum bitumen content for mix is determined by taking the average values of three bitumen content
corresponding to Maximum Stability, Maximum Bulk Density and 4% Air Voids in Total Mix. From the graphs shown in figure
4.1, Bitumen content corresponding To Maximum Stability, Maximum Bulk Density and 4% Air Voids in Total Mix is 5.4%,
5.5% and 6% respectively.
The Optimum Bitumen Content (OBC) for mix is the average of three values
OBC = (5.4+5.5+6) / 3 = 5.63 %
4.3 MARSHALL PROPERTIES OF BITUMINOUS CONCRETE MIX PREPARED USING POLYMER MODIFIED BITUMEN AT
OPTIMUM BITUMEN CONTENT
The Bituminous Concrete Mix specimens prepared using Polymer Modified Bitumen was subjected to Marshall Stability
test at optimum bitumen content. Marshall Properties at optimum binder content and test results are presented in table 4.2.
Table 4.2: Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at Optimum
Bitumen Content
SL. No. Marshall Properties Test Results Requirements as per IRC SP 53 2002
1 Optimum Bitumen Content, % 5.63 -----
2 Marshall Stability, kgs 1776.83 1200
3 Marshall Flow, mm 3.60 2.5 - 4.0%
4 Marshall Quotient, kg/mm 493.56 250-500
5 Air voids(Vv), % 4.43 3.0 - 5.0%
6 Bulk density, g/cc 2.38 -----
7 Voids in Mineral Aggregates (VMA), % 17.59 -----
8 Voids filled with Bitumen (VFB), % 74.82 -----
4.4 COMPARISON OF MARSHALL PROPERTIES BY VARYING MIXING AND COMPACTION TEMPERATURES
Comparison of Marshall Properties V/S Compaction Temperature of Bituminous Concrete Mix prepared using Polymer
Modified Bitumen for Mixing Temperature 140°C, 150°C, 160°C, 170°C and 180°C are shown in figure 4.2.
800
1000
1200
1400
1600
1800
80 100 120 140
Stability,kg
Compaction temperature, ºc
Stability v/s Compaction
temperature
140
150
160
170
180
2
2.3
2.6
2.9
3.2
3.5
3.8
80 100 120 140
Flow,mm
Compaction temperature, ºc
Flow v/s Compaction temperature
140
150
160
170
180
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1157
Figure 4.2: Comparison of Marshall Properties V/S Compaction Temperature of Bituminous Concrete Mix prepared
using Polymer Modified Bitumen for Mixing Temperature 140°C, 150°C, 160°C, 170°C and 180°C
4.5 COMPARISON OF INDIRECT TENSILE STRENGTH BY VARYING MIXING AND COMPACTION TEMPERATURES
4.6
Comparison of Indirect Tensile Strength v/s Compaction Temperature of Bituminous Concrete Mix prepared using
Polymer Modified Bitumen at mixing temperature 140°C, 150°C, 160°C, and 170°C is shown in figure 4.3.
Figure 4.3: Comparison of Indirect Tensile Strength v/s Compaction Temperature of Bituminous Concrete Mix
prepared using Polymer Modified Bitumen at mixing temperature 140°C, 150°C, 160°C, and 170°C
2.26
2.29
2.32
2.35
2.38
80 100 120 140
Bulkdensity,g/cc
Compaction temperature, ºc
Bulk density v/s Compaction temperature
140
150
160
170
180
3.0
4.5
6.0
7.5
9.0
80 90 100 110 120 130 140 150
Airvoids,%
Compaction temperature, ºc
Air voids v/s Compaction temperature
140
150
160
170
180
55
60
65
70
75
80
80 100 120 140
VoidsFilledWith
Bitumen,%
Compaction temperature, ºc
Voids Filled With Bitumen v/s
Compaction temperature
140
150
160
170
180
16
17
18
19
20
21
22
80 100 120 140
VoidsinMineral
Aggregate,%
Compaction temperature, ºc
Voids in Mineral Aggregate v/s
Compaction temperature
140
150
160
170
180
0.5
0.7
0.9
1.1
1.3
80 90 100 110 120 130 140 150
Indirecttensilestrength,
N/mm2
Compaction Temperature, o C
Indirect Tensile Strength v/s Compaction
Temperature
1
4
0
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1158
4.7 INDIRECT TENSILE FATIGUE TEST ON BITUMINOUS CONCRETE MIX PREPARED USING POLYMER MODIFIED
BITUMEN AT 25oC KEEPING CONSTANT MIXING TEMPERATURE, VARYING COMPACTION TEMPERATURE AND
STRESS LEVEL
Indirect Tensile Fatigue Tests were conducted on cylindrical specimens of Bituminous Concrete Mix. Indirect Tensile
Fatigue Test was conducted at 25oC test temperature on Bituminous Concrete Mix prepared using Polymer Modified Bitumen
keeping constant mixing temperature (160oC), varying compaction temperature (110oC, 120oC, 130oC and 140oC) and stress
levels (10%, 20%, 30% and 40%). The test results are presented in table 4.3, 4.4, 4.5, 4.6.
Table 4.3: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
constant mixing temperature 160oC and compaction temperature 110oC by varying Stress Level at 25oC test
temperature
Stress
Level, %
Load, N
Height of
specimen, mm
Stress,
Mpa
Resilient
Horizontal
Deformation, mm
Resilient
Modulus,
Mpa
Initial
Tensile
Strain,
Micro
Fatigue
Life, No. of
cycles
10 1152 66.25 0.11069 0.03082 349.80 648.66 6156
10 1152 66.5 0.11027 0.03122 344.02 657.08 5854
20 2304 67 0.21889 0.06256 340.80 1316.69 1588
20 2304 66.5 0.22054 0.06408 335.22 1348.68 1392
30 3456 67.75 0.32470 0.09532 331.80 2006.18 480
30 3456 67.5 0.32591 0.09612 330.25 2023.02 446
40 4608 67.75 0.43294 0.12864 327.81 2707.46 208
40 4608 67.75 0.43294 0.12925 326.26 2720.30 188
Table 4.4: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
constant mixing temperature 160oC and compaction temperature 120oC by varying Stress Level at 25oC test
temperature
Stress
Level, %
Load, N
Height of
specimen, mm
Stress,
Mpa
Resilient
Horizontal
Deformation, mm
Resilient
Modulus, Mpa
Initial
Tensile
Strain,
Micro
Fatigue
Life, No. of
cycles
10 1255 65.5 0.12196 0.02533 468.98 533.12 6472
10 1255 66.25 0.12058 0.02595 452.60 546.16 6198
20 2511 66.5 0.24035 0.05856 399.78 1232.50 2326
20 2511 66.75 0.23945 0.05943 392.45 1250.81 2282
30 3767 67 0.35789 0.09232 377.59 1943.04 542
30 3767 67.5 0.35523 0.09286 372.61 1954.41 524
40 5022 67.75 0.47184 0.12456 368.96 2621.59 224
40 5022 67.5 0.47358 0.12694 363.38 2671.68 188
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1159
Table 4.5: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
constant mixing temperature 160oC and compaction temperature 130oC by varying Stress Level at 25oC test
temperature
Stress
Level, %
Load, N
Height of
specimen, mm
Stress,
Mpa
Resilient
Horizontal
Deformation, mm
Resilient
Modulus,
Mpa
Initial
Tensile
Strain,
Micro
Fatigue
Life, No. of
cycles
10 1290 66 0.12441 0.02167 559.21 456.08 7124
10 1290 66 0.12441 0.02233 542.69 469.97 6878
20 2580 66.5 0.24696 0.05315 452.57 1118.64 2952
20 2580 66 0.24883 0.05422 447.00 1141.16 2796
30 3870 67.25 0.36630 0.08331 428.27 1753.41 590
30 3870 67.5 0.36495 0.08362 425.10 1759.93 558
40 5160 67 0.49023 0.11505 415.03 2421.43 262
40 5160 66.75 0.49206 0.11693 409.89 2461.00 234
Table 4.6: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
constant mixing temperature 160oC and compaction temperature 140oC by varying Stress Level at 25oC test
temperature
Stress
Level, %
Load, N
Height of
specimen, mm
Stress,
Mpa
Resilient
Horizontal
Deformation, mm
Resilient
Modulus, Mpa
Initial
Tensile
Strain,
Micro
Fatigue
Life, No. of
cycles
10 1331 66.25 0.12788 0.01763 706.53 371.06 8158
10 1331 66.25 0.12788 0.01801 691.62 379.05 7856
20 2662 66.5 0.25481 0.03782 656.23 795.99 3952
20 2662 66.25 0.25577 0.03987 624.84 839.14 3788
30 3993 66.5 0.38221 0.06439 578.16 1355.20 906
30 3993 66.75 0.38078 0.06836 542.55 1438.76 792
40 5324 67 0.50581 0.10376 474.82 2183.82 456
40 5324 67.25 0.50393 0.10498 467.55 2209.49 374
4.8 LINEAR REGRESSION ANALYSIS
Linear regression analysis was carried out for data obtained from Indirect Tensile Fatigue Tests conducted at 25oC test
temperature on Bituminous Concrete Mix prepared using Polymer Modified Bitumen and the details are presented in table 4.7
and graphs are shown in figure 4.4, 4.5, 4.6, 4.7.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
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Table 4.7: Linear regression analysis for the data obtained from Indirect Tensile Fatigue Test
Compaction
Temperature
Relationship R2 value Equations
110oC
Fatigue Life Stress Level
0.7757 y= -184.48x + 6651
120oC 0.8537 y = -201.58x + 7384
130oC 0.875 y = -225.59x + 8314
140oC 0.9031 y= -257.97x + 9734.5
110oC
Fatigue Life Tensile Stress
0.7797 y = -17236x + 6729.2
120oC 0.8569 y= -17246x + 7477.2
130oC 0.8724 y = -18493x + 8356.5
140oC 0.9073 y= -20567x + 9812.8
110oC
Fatigue Life Resilient Modulus
0.8404 y = 274.1x – 89987
120oC 0.9858 y = 64.91x – 23590
130oC 0.9713 y = 48.86x – 19800
140oC 0.8349 y = 31.995x – 15681
110oC
Fatigue Life
Initial Tensile
Strain
0.8125 y= -4.0105x + 8084.1
120oC 0.8545 y = -2.8692x + 6918.5
130oC 0.8709 y = -3.4292x + 7638.7
140oC 0.8125 y= -4.0105x + 8084.1
Figure 4.4: Fatigue Life v/s Stress Level of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and
Stress Level at 25o
C
y110 = -184.48x + 6651
R² = 0.7757
y120 = -201.58x + 7384
R² = 0.8537
y 130= -225.59x + 8314
R² = 0.875
y140 = -257.97x + 9734.5
R² = 0.9031
0
1000
2000
3000
4000
5000
6000
7000
8000
9000
0 10 20 30 40 50
FatigueLife,No.ofcycles
Stress Level, %
Fatigue Life v/s Stress Level
110
120
130
140
Linear (110)
Linear (120)
Linear (130)
Linear (140)
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
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Figure 4.5: Fatigue Life v/s Tensile Stress of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at
constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and
Stress Level at 25oC
Figure 4.6: Fatigue Life v/s Resilient Modulus of Bituminous Concrete Mix prepared using Polymer Modified Bitumen
at constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and
Stress Level at 25oC
y110 = -17236x + 6729.2
R² = 0.7797
y120 = -17246x + 7477.2
R² = 0.8569
y130 = -18493x + 8356.5
R² = 0.8724
y140 = -20567x + 9812.8
R² = 0.9073
0
1000
2000
3000
4000
5000
6000
7000
8000
9000
0.0 0.1 0.2 0.3 0.4 0.5 0.6
FatigueLife,No.ofcycles
Tensile stress, Mpa
Fatigue Life v/s Tensile stress
110
120
130
140
Linear (110)
Linear (120)
Linear (130)
Linear (140)
y110 = 274.1x - 89987
R² = 0.8404
y120 = 64.91x - 23590
R² = 0.9858
y 130= 48.86x - 19800
R² = 0.9713
y140 = 31.995x - 15681
R² = 0.8349
0
1000
2000
3000
4000
5000
6000
7000
8000
9000
0 100 200 300 400 500 600 700 800
FatigueLife,No.ofcycles
Resilient Modulus, Mpa
Fatigue Life v/s Resilient Modulus
110
120
130
140
Linear (110)
Linear (120)
Linear (130)
Linear (140)
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1162
Figure 4.7: Fatigue Life v/s Initial Tensile Strain of Bituminous Concrete Mix prepared using Polymer Modified
Bitumen at constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and
140oC) and Stress Level at 25oC
DISCUSSIONS AND CONCLUSIONS
5.1 DISCUSSIONS
 It is observed from Table 4.1, the Optimum Bitumen Content obtained for Bituminous Concrete Mix prepared using
Polymer Modified Bitumen is 5.63%.
 It is observed from Table 4.2, the Marshall Stability, Marshall Flow, Marshall Quotient, Bulk Density, Air Voids, VMA and
VFB of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at optimum bitumen content were 1776.83
kg, 3.6 mm, 493.56 kg/mm, 2.38 g/cc, 4.43%, 17.59% and 74.82% respectively.
Marshall Stability
 The Marshall Stability of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually increases with
increase in compaction temperature by 38% from 90oC to 140oC.
 The Marshall Stability of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in
mixing temperature by 14% from 140oC to 160oC and substantial increase by 2.4% from 160oC to 170oC as further
increase in mixing temperature of 180oC there is sudden reduction in the stability by 23%.
Marshall Flow
 The Flow of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually decreases with increase in
compaction temperature by 31.8% from 90oC to 140oC.
 The Flow of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in mixing
temperature by 25.9% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden
reduction in the Flow by 4.8%.
y110 = -4.0105x + 8084.1
R² = 0.8125
y 120= -2.8692x + 6918.5
R² = 0.8545
y130 = -3.4292x + 7638.7
R² = 0.8709
y140 = -4.0105x + 8084.1
R² = 0.8125
0
1000
2000
3000
4000
5000
6000
7000
8000
9000
0 500 1000 1500 2000 2500 3000
FatigueLife,No.ofcycles
Initial Tensile strain, Micro
Fatigue Life v/s Initial Tensile strain
110
120
130
140
Linear (110)
Linear (120)
Linear (130)
Linear (140)
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1163
Bulk Density
 The Bulk Density of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually increases with
increase in compaction temperature by 3.5% from 90oC to 140oC.
 The Bulk Density of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in
mixing temperature by 0.9% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden
reduction in the Bulk Density by 1.2%.
Air Voids
 The Air Voids of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually decreases with increase
in compaction temperature by 39.1% from 90oC to 140oC.
 The Air Voids of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases with increase in mixing
temperature by 17.7% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden increase
in the Air Voids by 29.2%.
Voids in Mineral Aggregate
 The Voids in Mineral Aggregate of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually
decreases with increase in compaction temperature by 13.4% from 90oC to 140oC.
 The Voids in Mineral Aggregate of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases with
increase in mixing temperature by 4.3% from 140oC to 170oC as further increase in mixing temperature of 180oC there
is sudden increase in the Voids in Mineral Aggregate by 7.6%.
Voids filled with Bitumen
 The Voids filled with bitumen of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually
increases with increase in compaction temperature by 16.4% from 90oC to 140oC.
 The Voids filled with bitumen of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with
increase in mixing temperature by 5.2% from 140oC to 170oC as further increase in mixing temperature of 180oC there
is sudden reduction in the Voids filled with bitumen by 9.6%.
Indirect Tensile Strength Test
 The Indirect Tensile Strength of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually
increases with increase in compaction temperature by 36% from 90oC to 140oC.
 The Indirect Tensile Strength of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with
increase in mixing temperature by 13% from 140oC to 160oC as further increase in mixing temperature of 170oC there is
sudden reduction in the Indirect Tensile Strength by 10%.
Indirect Tensile Fatigue Test
 The Fatigue Life of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in
compaction temperature from 110oC to 140oC by 25.01% at 10% stress level, 61.54% at 20% stress level, 45.35% at
30% stress level and 52.06% at 40% stress level.
 The Resilient Modulus of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase
in compaction temperature from 110oC to 140oC by 50.37% at 10% stress level, 47.21% at 20% stress level, 40.87% at
30% stress level and 30.59% at 40% stress level.
 The Initial Tensile Strain of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases with
increase in compaction temperature from 110oC to 140oC by 42.55% at 10% stress level, 38.66% at 20% stress level,
30.66% at 30% stress level and 19.06% at 40% stress level.
5.2 CONCLUSIONS
 The Physical Properties of Aggregate satisfy the requirements as per Table 500-17 of MoRT&H specification.
 The Physical Properties of Polymer Modified Bitumen PMB-70 (SBS) satisfy the requirements as per IRC SP 53-2002.
 The Optimum Bitumen Content obtained for Polymer Modified Bituminous Concrete is 5.63%.
 There is considerable increase in the Marshall Stability as the mixing and compaction temperature increases and there
is substantial reduction in the Marshall Stability with further increase in the mixing and compaction temperature.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1164
 There is considerable increase in the Indirect Tensile Strength as the mixing and compaction temperature increases and
there is substantial reduction in the Indirect Tensile Strength with further increase in the mixing and compaction
temperature.
 Fatigue Life of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases as compaction
temperature increases.
 Resilient Modulus of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases as compaction
temperature increases.
 Initial Tensile Strain of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases as compaction
temperature increases.
 Based on the experimental work and analysis carried out in the present study, an ideal mixing temperature of 160oC
and compaction temperature of 140oC is suggested for the preparation of Bituminous Concrete Mix prepared using
Polymer Modified Bitumen-(70).
REFERENCES
1. Jian-Shiuh Chen, Min-Chih Liao and Ming-Shen Shiah “Asphalt Modified by Styrene-Butadiene-Styrene Tri-Block
Copolymer: Morphology and Model”.
2. K.Kantha Kumar and A.Veeraragavan “Optimizing the Bituminous Concrete Mixes for Fatigue Performance”.
3. Noorafidah Binti Ithnin “Determination of Mixing and Compacting Temperatures for Hot Mix Asphalt”.
4. Shivangi Gupta & A.Veeraragavan “Fatigue Behaviour of Polymer Modified Bituminous Concrete Mixtures”.
5. Sixth Framework Programme of Spens Project, Transport Research Europe “Practical Mix Design Model for Asphalt
Mixture”.
6. Specification of Ministry of Road Transport and Highways (MoRT&H) Government of India 4th Revision.
7. IRC SP 53-2002 specification for Modified bitumen.

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  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1150 EFFECT OF MIXING AND COMPACTION TEMPERATURES ON THE INDIRECT TENSILE STRENGTH AND FATIGUE BEHAVIOUR OF BITUMINOUS CONCRETE MIX PREPARED USING POLYMER MODIFIED BITUMEN SHARANABASAPPA KORI ----------------------------------------------------------------***------------------------------------------------------------------ ABSTRACT - Bituminous mixes are used in the surface layer of road and airfield pavements. The mix is composed usually of aggregate and bitumen. The design of bituminous paving mix, as with the design of other engineering materials is largely a matter of selecting and proportioning of constituent materials to obtain the desired properties in the finished pavement structure. In the present study, an attempt is made to evaluate the effects of Mixing and Compaction temperature on the Marshall Properties, Indirect Tensile Strength and Fatigue behaviour of Bituminous Concrete Mix prepared using Polymer Modified Bitumen. The present study includes an aggregate gradation of Bituminous Concrete Mix Grading-2 as per MoRT&H specifications (4th revision), Polymer Modified Bitumen (PMB-70) as binder. The design of Bituminous Concrete Mix prepared using Polymer Modified Bitumen as per IRC SP 53-2002 specifications. Based on the experimental work and analysis carried out in the present study, an ideal mixing temperature of 160oC and compaction temperature of 140oC is suggested for the preparation of Bituminous Concrete Mix prepared using Polymer Modified Bitumen. 1. INTRODUCTION 1.1 GENERAL Bituminous materials are extensively used for roadway construction, primarily because of their excellent binding characteristics and water proofing properties relatively at low cost. The bituminous mix design aims to determine the proportion of bitumen, filler, fine aggregates and coarse aggregates to produce a mix which is workable, strong, durable and economical. Significant variation in daily and seasonal temperature of pavement induces early development of distress conditions (ravelling, undulation, rutting, cracking, bleeding, and potholing) of bituminous pavement. Another major concern for distress of road surface is overloading of commercial vehicles and increased traffic density. SBS is a styrene-butadiene-styrene made by the co-polymerization of butadiene and styrene. Butadiene and styrene block copolymer, to form a styrene (S) - butadiene (B) - benzene Ethylene (S) of the structure, as thermoplastic elastomeric. SBS has the advantages of rubber and plastic, at room temperature with a rubber elastic, like rubber, as high temperatures can melt flow, a plastic material. SBS formed within the bitumen, greatly improving the performance of bitumen. Binder viscosity varies with temperature and different binders require different temperatures to achieve the same handling properties. Polymer modified binders, in particular, increase in viscosity at a much faster rate on cooling than normal paving grade bitumen. 1.2 OBJECTIVES OF THE PRESENT STUDY  To assess the physical properties of aggregate as per MoRT&H requirements.  To assess the physical properties of Polymer Modified Bitumen [PMB-70 (SBS)] as per IRC SP: 53-2002 requirements.  To determine the optimum bitumen content of Bituminous Concrete Mix prepared using Polymer Modified Bitumen by Marshall Method of mix design.  To assess the Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at optimum bitumen content by varying mixing and compaction temperatures.  To conduct Indirect Tensile Strength Test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at optimum bitumen content by varying mixing and compaction temperatures.  To conduct Indirect Tensile Fatigue Test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at 25oC keeping constant mixing temperature, varying compaction temperature and stress level.
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1151  To carryout Linear Regression analysis for the data obtained from Indirect Tensile Fatigue Test conducted on Bituminous Concrete Mix prepared using Polymer Modified Bitumen. 2. LITERATURE REVIEW 2.1 GENERAL The durability of asphaltic concrete is greatly influenced by the environmental changes during the year between hot and cold temperatures and between day and night. High temperatures can soften the bitumen and consequently reduce the stiffness of asphaltic concrete making the mix more susceptible to rutting. On the other hand, low temperature can increase the stiffness of bitumen and reduce the flexibility of the asphaltic concrete, hence, inducing fatigue failure. As a result, cracking of the pavement surface may develop which adversely affects the performance of the asphaltic concrete. Thus, high temperature stiffness and low temperature flexibility are important properties in bituminous mixtures respectively to avert rutting and cracking. 2.2 PRACTICAL MIX DESIGN MODEL FOR ASPHALT MIXTURE.(5) This paper describes an “Optimisation of asphalt mixture design to ensure favourable behaviour at low and high air temperatures” is aimed to find a practical model for the optimisation of asphalt mixture composition which will be related to the target functional properties of asphalt pavement relevant for various climate and traffic conditions in the field. 2.3 DETERMINATION OF MIXING AND COMPACTING TEMPERATURES FOR HOT MIX ASPHALT.(3) This paper gives the typical mixing and compacting temperature has been normally set as 160°C and 140°C respectively based on experience for the lab procedure purpose. With the newly revised Specification of Roadwork 2007, new bitumen grade had been introduced including grade 60-70 and some other types of modified bitumen. The objective of this study is to determine the appropriate mixing and compacting temperature for the bitumen grades by viscosity and correlation with other physical properties of bitumen. Rotational Brookfield Viscometer was used to determine the correct temperature for viscosity at 165°C and 135°C and at viscosity ranges of 0.17±0.02 and 0.28±0.03 Pa s for mixing and compacting, respectively as per ASTM D 2493 3. EXPERIMENTAL INVESTIGATIONS 3.1 GENERAL In the present study the aggregate gradation Grading-2 adopted for Bituminous Concrete as per Table 500-18 recommended by MORT&H (IVth Revision) specifications. Basic Engineering tests on aggregates and binder were conducted in the laboratory to assess their properties. Marshall Method of mix design was adopted to carryout mix design for Bituminous Concrete Mix prepared using Polymer Modified Bitumen. Marshall Stability and Indirect Tensile Strength tests were conducted on Bituminous Concrete Mix prepared using Polymer Modified Bitumen by varying mixing and compaction temperatures. For the selected mixing and compaction temperatures Indirect Tensile Fatigue test was conducted at 25oC by varying stress level. 3.2 CONSTITUENTS OF A MIX (Aggregates, Bitumen & Cement) Table 3.1: Physical Properties of Aggregates Description of Aggregate Tests Test Results Requirements as per Table 500-17 of MoRT&H Specifications Aggregate Impact value (%) 18.94 Max 24% Flakiness and Elongation Index (Combined) (%) 28.97 Max 30% Los Angeles Abrasion value (%) 19.44 Max 30% Water Absorption (%) 0.5 Max 2%
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1152 Table 3.2: Test Results of Polymer Modified Bitumen PMB-70(SBS) and Requirements Test Test Results Requirements as per IRC SP:53- 2002 Penetration at 25°C, 100gm, 5 Seconds, 0.1mm 68.67 50-90 Softening Point (Ring & Ball), °C 58.5 Minimum 55 Ductility at 27oC 100+ +60 Flash point, COC, °C 252 Minimum 220 Elastic Recovery of Half Thread in Ductilometer at 15°C, % 78 Minimum 75 Separation, Difference in Softening point (Ring & Ball),°C 2 Maximum 3 Viscosity at 150oC, Poise 3.59 2-6 Thin Film Oven Test ( TFOT ) on Residue Loss in mass, % 0.64 Maximum 1 Increase in Softening point (Ring & Ball), °C 4 Maximum 6 Reduction in Penetration of Residue at 25°C, % 23.29 Maximum 35 Elastic Recovery of Half Thread in Ductilometer at 25°C, % 60 Minimum 50 Table 3.3: Specific Gravity of Materials Description of materials Specific Gravity Coarse aggregate 2.67 Fine aggregate 2.72 Mineral filler (cement) 3.12 Polymer Modified Bitumen PMB-70(SBS) 1.02 Table 3.4: Aggregate Gradation for Bituminous Concrete Mix (Grading-2) as per MoRT&H Specification IS Sieve Size, mm % Passing (Specified) % Passing (Mid Limit) 19 100 100 13.2 79-100 89.5 9.5 70-88 79 4.75 53-71 62 2.36 42-58 50 1.18 34-48 41 0.60 26-38 32 0.30 18-28 23 0.15 12-20 16 0.075 4-10 7
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1153 3.3 MARSHALL METHOD OF MIX DESIGN There are two major features of Marshall Stability method of designing mixes are:  Density Voids Analysis  Stability Flow Test. Figure 3.1: Marshall Stability Test 3.4 INDIRECT TENSILE STRENGTH TEST Figure 3.2: Indirect Tensile Strength Test 3.5 INDIRECT TENSILE FATIGUE TEST Indirect Tensile Fatigue Test apparatus Salient features of the equipment Capacity - 2 Tons Load type - Half Sine Major component - LVDT (Linear Variable Differential Transducers) - Load cell - Loading frame - Temperature controlled chamber - Position controller - Data acquisition system
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1154 Figure 3.3: Indirect Tensile Fatigue Test 4. ANALYSIS OF DATA 4.1 GENERAL Marshall Stability test was carried out on Bituminous Concrete Mix specimens prepared using Polymer Modified Bitumen to determine the optimum bitumen content, Marshall Stability and volumetric properties of the mix. The Marshall properties and Indirect Tensile Strength values of Bituminous Concrete Mix prepared using Polymer Modified Bitumen were calculated by varying mixing and compaction temperatures. Indirect Tensile Fatigue Test was carried out on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at 25oC keeping constant mixing temperature, varying compaction temperature and stress level. Table 4.1: Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen Bitumen content, % Marshall stability, kgs Flow, mm Bulk density, g/cc Total air voids, % Voids Filled with Bitumen, % Voids in Mineral Aggregates, % 5.0 1818.14 2.56 2.38 5.39 68.41 17.06 5.5 1838.93 3.20 2.39 4.42 74.45 17.31 6.0 1700.51 3.56 2.38 3.98 77.90 18.00 6.5 1579.84 3.68 2.37 3.92 79.41 19.02
  • 6. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1155 Figure 4.1: Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen to determine the optimum bitumen content 1500 1600 1700 1800 1900 4.5 5.0 5.5 6.0 6.5 7.0 Stability,kgs Bitumen, % Stability v/s Bitumen 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0 Flow,mm Bitumen, % Flow v/s Bitumen 2.365 2.370 2.375 2.380 2.385 2.390 4.5 5.0 5.5 6.0 6.5 7.0 Bulkdensity,g/cc Bitumen, % Bulk density v/s Bitumen 3.5 4.0 4.5 5.0 5.5 6.0 4.5 5.0 5.5 6.0 6.5 7.0 Airvoids,% Bitumen, % Air voids v/s Bitumen 66 69 72 75 78 81 4.5 5.0 5.5 6.0 6.5 7.0 VoidsfilledwithBitumen,% Bitumen, % Voids filled with Bitumen v/s Bitumen
  • 7. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1156 4.2 DETERMINATION OF OPTIMUM BITUMEN CONTENT The optimum bitumen content for mix is determined by taking the average values of three bitumen content corresponding to Maximum Stability, Maximum Bulk Density and 4% Air Voids in Total Mix. From the graphs shown in figure 4.1, Bitumen content corresponding To Maximum Stability, Maximum Bulk Density and 4% Air Voids in Total Mix is 5.4%, 5.5% and 6% respectively. The Optimum Bitumen Content (OBC) for mix is the average of three values OBC = (5.4+5.5+6) / 3 = 5.63 % 4.3 MARSHALL PROPERTIES OF BITUMINOUS CONCRETE MIX PREPARED USING POLYMER MODIFIED BITUMEN AT OPTIMUM BITUMEN CONTENT The Bituminous Concrete Mix specimens prepared using Polymer Modified Bitumen was subjected to Marshall Stability test at optimum bitumen content. Marshall Properties at optimum binder content and test results are presented in table 4.2. Table 4.2: Marshall Properties of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at Optimum Bitumen Content SL. No. Marshall Properties Test Results Requirements as per IRC SP 53 2002 1 Optimum Bitumen Content, % 5.63 ----- 2 Marshall Stability, kgs 1776.83 1200 3 Marshall Flow, mm 3.60 2.5 - 4.0% 4 Marshall Quotient, kg/mm 493.56 250-500 5 Air voids(Vv), % 4.43 3.0 - 5.0% 6 Bulk density, g/cc 2.38 ----- 7 Voids in Mineral Aggregates (VMA), % 17.59 ----- 8 Voids filled with Bitumen (VFB), % 74.82 ----- 4.4 COMPARISON OF MARSHALL PROPERTIES BY VARYING MIXING AND COMPACTION TEMPERATURES Comparison of Marshall Properties V/S Compaction Temperature of Bituminous Concrete Mix prepared using Polymer Modified Bitumen for Mixing Temperature 140°C, 150°C, 160°C, 170°C and 180°C are shown in figure 4.2. 800 1000 1200 1400 1600 1800 80 100 120 140 Stability,kg Compaction temperature, ºc Stability v/s Compaction temperature 140 150 160 170 180 2 2.3 2.6 2.9 3.2 3.5 3.8 80 100 120 140 Flow,mm Compaction temperature, ºc Flow v/s Compaction temperature 140 150 160 170 180
  • 8. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1157 Figure 4.2: Comparison of Marshall Properties V/S Compaction Temperature of Bituminous Concrete Mix prepared using Polymer Modified Bitumen for Mixing Temperature 140°C, 150°C, 160°C, 170°C and 180°C 4.5 COMPARISON OF INDIRECT TENSILE STRENGTH BY VARYING MIXING AND COMPACTION TEMPERATURES 4.6 Comparison of Indirect Tensile Strength v/s Compaction Temperature of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at mixing temperature 140°C, 150°C, 160°C, and 170°C is shown in figure 4.3. Figure 4.3: Comparison of Indirect Tensile Strength v/s Compaction Temperature of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at mixing temperature 140°C, 150°C, 160°C, and 170°C 2.26 2.29 2.32 2.35 2.38 80 100 120 140 Bulkdensity,g/cc Compaction temperature, ºc Bulk density v/s Compaction temperature 140 150 160 170 180 3.0 4.5 6.0 7.5 9.0 80 90 100 110 120 130 140 150 Airvoids,% Compaction temperature, ºc Air voids v/s Compaction temperature 140 150 160 170 180 55 60 65 70 75 80 80 100 120 140 VoidsFilledWith Bitumen,% Compaction temperature, ºc Voids Filled With Bitumen v/s Compaction temperature 140 150 160 170 180 16 17 18 19 20 21 22 80 100 120 140 VoidsinMineral Aggregate,% Compaction temperature, ºc Voids in Mineral Aggregate v/s Compaction temperature 140 150 160 170 180 0.5 0.7 0.9 1.1 1.3 80 90 100 110 120 130 140 150 Indirecttensilestrength, N/mm2 Compaction Temperature, o C Indirect Tensile Strength v/s Compaction Temperature 1 4 0
  • 9. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1158 4.7 INDIRECT TENSILE FATIGUE TEST ON BITUMINOUS CONCRETE MIX PREPARED USING POLYMER MODIFIED BITUMEN AT 25oC KEEPING CONSTANT MIXING TEMPERATURE, VARYING COMPACTION TEMPERATURE AND STRESS LEVEL Indirect Tensile Fatigue Tests were conducted on cylindrical specimens of Bituminous Concrete Mix. Indirect Tensile Fatigue Test was conducted at 25oC test temperature on Bituminous Concrete Mix prepared using Polymer Modified Bitumen keeping constant mixing temperature (160oC), varying compaction temperature (110oC, 120oC, 130oC and 140oC) and stress levels (10%, 20%, 30% and 40%). The test results are presented in table 4.3, 4.4, 4.5, 4.6. Table 4.3: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and compaction temperature 110oC by varying Stress Level at 25oC test temperature Stress Level, % Load, N Height of specimen, mm Stress, Mpa Resilient Horizontal Deformation, mm Resilient Modulus, Mpa Initial Tensile Strain, Micro Fatigue Life, No. of cycles 10 1152 66.25 0.11069 0.03082 349.80 648.66 6156 10 1152 66.5 0.11027 0.03122 344.02 657.08 5854 20 2304 67 0.21889 0.06256 340.80 1316.69 1588 20 2304 66.5 0.22054 0.06408 335.22 1348.68 1392 30 3456 67.75 0.32470 0.09532 331.80 2006.18 480 30 3456 67.5 0.32591 0.09612 330.25 2023.02 446 40 4608 67.75 0.43294 0.12864 327.81 2707.46 208 40 4608 67.75 0.43294 0.12925 326.26 2720.30 188 Table 4.4: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and compaction temperature 120oC by varying Stress Level at 25oC test temperature Stress Level, % Load, N Height of specimen, mm Stress, Mpa Resilient Horizontal Deformation, mm Resilient Modulus, Mpa Initial Tensile Strain, Micro Fatigue Life, No. of cycles 10 1255 65.5 0.12196 0.02533 468.98 533.12 6472 10 1255 66.25 0.12058 0.02595 452.60 546.16 6198 20 2511 66.5 0.24035 0.05856 399.78 1232.50 2326 20 2511 66.75 0.23945 0.05943 392.45 1250.81 2282 30 3767 67 0.35789 0.09232 377.59 1943.04 542 30 3767 67.5 0.35523 0.09286 372.61 1954.41 524 40 5022 67.75 0.47184 0.12456 368.96 2621.59 224 40 5022 67.5 0.47358 0.12694 363.38 2671.68 188
  • 10. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1159 Table 4.5: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and compaction temperature 130oC by varying Stress Level at 25oC test temperature Stress Level, % Load, N Height of specimen, mm Stress, Mpa Resilient Horizontal Deformation, mm Resilient Modulus, Mpa Initial Tensile Strain, Micro Fatigue Life, No. of cycles 10 1290 66 0.12441 0.02167 559.21 456.08 7124 10 1290 66 0.12441 0.02233 542.69 469.97 6878 20 2580 66.5 0.24696 0.05315 452.57 1118.64 2952 20 2580 66 0.24883 0.05422 447.00 1141.16 2796 30 3870 67.25 0.36630 0.08331 428.27 1753.41 590 30 3870 67.5 0.36495 0.08362 425.10 1759.93 558 40 5160 67 0.49023 0.11505 415.03 2421.43 262 40 5160 66.75 0.49206 0.11693 409.89 2461.00 234 Table 4.6: Indirect Tensile Fatigue test on Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and compaction temperature 140oC by varying Stress Level at 25oC test temperature Stress Level, % Load, N Height of specimen, mm Stress, Mpa Resilient Horizontal Deformation, mm Resilient Modulus, Mpa Initial Tensile Strain, Micro Fatigue Life, No. of cycles 10 1331 66.25 0.12788 0.01763 706.53 371.06 8158 10 1331 66.25 0.12788 0.01801 691.62 379.05 7856 20 2662 66.5 0.25481 0.03782 656.23 795.99 3952 20 2662 66.25 0.25577 0.03987 624.84 839.14 3788 30 3993 66.5 0.38221 0.06439 578.16 1355.20 906 30 3993 66.75 0.38078 0.06836 542.55 1438.76 792 40 5324 67 0.50581 0.10376 474.82 2183.82 456 40 5324 67.25 0.50393 0.10498 467.55 2209.49 374 4.8 LINEAR REGRESSION ANALYSIS Linear regression analysis was carried out for data obtained from Indirect Tensile Fatigue Tests conducted at 25oC test temperature on Bituminous Concrete Mix prepared using Polymer Modified Bitumen and the details are presented in table 4.7 and graphs are shown in figure 4.4, 4.5, 4.6, 4.7.
  • 11. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1160 Table 4.7: Linear regression analysis for the data obtained from Indirect Tensile Fatigue Test Compaction Temperature Relationship R2 value Equations 110oC Fatigue Life Stress Level 0.7757 y= -184.48x + 6651 120oC 0.8537 y = -201.58x + 7384 130oC 0.875 y = -225.59x + 8314 140oC 0.9031 y= -257.97x + 9734.5 110oC Fatigue Life Tensile Stress 0.7797 y = -17236x + 6729.2 120oC 0.8569 y= -17246x + 7477.2 130oC 0.8724 y = -18493x + 8356.5 140oC 0.9073 y= -20567x + 9812.8 110oC Fatigue Life Resilient Modulus 0.8404 y = 274.1x – 89987 120oC 0.9858 y = 64.91x – 23590 130oC 0.9713 y = 48.86x – 19800 140oC 0.8349 y = 31.995x – 15681 110oC Fatigue Life Initial Tensile Strain 0.8125 y= -4.0105x + 8084.1 120oC 0.8545 y = -2.8692x + 6918.5 130oC 0.8709 y = -3.4292x + 7638.7 140oC 0.8125 y= -4.0105x + 8084.1 Figure 4.4: Fatigue Life v/s Stress Level of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and Stress Level at 25o C y110 = -184.48x + 6651 R² = 0.7757 y120 = -201.58x + 7384 R² = 0.8537 y 130= -225.59x + 8314 R² = 0.875 y140 = -257.97x + 9734.5 R² = 0.9031 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 0 10 20 30 40 50 FatigueLife,No.ofcycles Stress Level, % Fatigue Life v/s Stress Level 110 120 130 140 Linear (110) Linear (120) Linear (130) Linear (140)
  • 12. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1161 Figure 4.5: Fatigue Life v/s Tensile Stress of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and Stress Level at 25oC Figure 4.6: Fatigue Life v/s Resilient Modulus of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and Stress Level at 25oC y110 = -17236x + 6729.2 R² = 0.7797 y120 = -17246x + 7477.2 R² = 0.8569 y130 = -18493x + 8356.5 R² = 0.8724 y140 = -20567x + 9812.8 R² = 0.9073 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 0.0 0.1 0.2 0.3 0.4 0.5 0.6 FatigueLife,No.ofcycles Tensile stress, Mpa Fatigue Life v/s Tensile stress 110 120 130 140 Linear (110) Linear (120) Linear (130) Linear (140) y110 = 274.1x - 89987 R² = 0.8404 y120 = 64.91x - 23590 R² = 0.9858 y 130= 48.86x - 19800 R² = 0.9713 y140 = 31.995x - 15681 R² = 0.8349 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 0 100 200 300 400 500 600 700 800 FatigueLife,No.ofcycles Resilient Modulus, Mpa Fatigue Life v/s Resilient Modulus 110 120 130 140 Linear (110) Linear (120) Linear (130) Linear (140)
  • 13. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1162 Figure 4.7: Fatigue Life v/s Initial Tensile Strain of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at constant mixing temperature 160oC and by varying compaction temperature (110oC, 120oC, 130oC and 140oC) and Stress Level at 25oC DISCUSSIONS AND CONCLUSIONS 5.1 DISCUSSIONS  It is observed from Table 4.1, the Optimum Bitumen Content obtained for Bituminous Concrete Mix prepared using Polymer Modified Bitumen is 5.63%.  It is observed from Table 4.2, the Marshall Stability, Marshall Flow, Marshall Quotient, Bulk Density, Air Voids, VMA and VFB of Bituminous Concrete Mix prepared using Polymer Modified Bitumen at optimum bitumen content were 1776.83 kg, 3.6 mm, 493.56 kg/mm, 2.38 g/cc, 4.43%, 17.59% and 74.82% respectively. Marshall Stability  The Marshall Stability of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually increases with increase in compaction temperature by 38% from 90oC to 140oC.  The Marshall Stability of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in mixing temperature by 14% from 140oC to 160oC and substantial increase by 2.4% from 160oC to 170oC as further increase in mixing temperature of 180oC there is sudden reduction in the stability by 23%. Marshall Flow  The Flow of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually decreases with increase in compaction temperature by 31.8% from 90oC to 140oC.  The Flow of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in mixing temperature by 25.9% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden reduction in the Flow by 4.8%. y110 = -4.0105x + 8084.1 R² = 0.8125 y 120= -2.8692x + 6918.5 R² = 0.8545 y130 = -3.4292x + 7638.7 R² = 0.8709 y140 = -4.0105x + 8084.1 R² = 0.8125 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 0 500 1000 1500 2000 2500 3000 FatigueLife,No.ofcycles Initial Tensile strain, Micro Fatigue Life v/s Initial Tensile strain 110 120 130 140 Linear (110) Linear (120) Linear (130) Linear (140)
  • 14. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1163 Bulk Density  The Bulk Density of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually increases with increase in compaction temperature by 3.5% from 90oC to 140oC.  The Bulk Density of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in mixing temperature by 0.9% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden reduction in the Bulk Density by 1.2%. Air Voids  The Air Voids of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually decreases with increase in compaction temperature by 39.1% from 90oC to 140oC.  The Air Voids of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases with increase in mixing temperature by 17.7% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden increase in the Air Voids by 29.2%. Voids in Mineral Aggregate  The Voids in Mineral Aggregate of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually decreases with increase in compaction temperature by 13.4% from 90oC to 140oC.  The Voids in Mineral Aggregate of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases with increase in mixing temperature by 4.3% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden increase in the Voids in Mineral Aggregate by 7.6%. Voids filled with Bitumen  The Voids filled with bitumen of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually increases with increase in compaction temperature by 16.4% from 90oC to 140oC.  The Voids filled with bitumen of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in mixing temperature by 5.2% from 140oC to 170oC as further increase in mixing temperature of 180oC there is sudden reduction in the Voids filled with bitumen by 9.6%. Indirect Tensile Strength Test  The Indirect Tensile Strength of Bituminous Concrete Mix prepared using Polymer Modified Bitumen gradually increases with increase in compaction temperature by 36% from 90oC to 140oC.  The Indirect Tensile Strength of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in mixing temperature by 13% from 140oC to 160oC as further increase in mixing temperature of 170oC there is sudden reduction in the Indirect Tensile Strength by 10%. Indirect Tensile Fatigue Test  The Fatigue Life of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in compaction temperature from 110oC to 140oC by 25.01% at 10% stress level, 61.54% at 20% stress level, 45.35% at 30% stress level and 52.06% at 40% stress level.  The Resilient Modulus of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases with increase in compaction temperature from 110oC to 140oC by 50.37% at 10% stress level, 47.21% at 20% stress level, 40.87% at 30% stress level and 30.59% at 40% stress level.  The Initial Tensile Strain of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases with increase in compaction temperature from 110oC to 140oC by 42.55% at 10% stress level, 38.66% at 20% stress level, 30.66% at 30% stress level and 19.06% at 40% stress level. 5.2 CONCLUSIONS  The Physical Properties of Aggregate satisfy the requirements as per Table 500-17 of MoRT&H specification.  The Physical Properties of Polymer Modified Bitumen PMB-70 (SBS) satisfy the requirements as per IRC SP 53-2002.  The Optimum Bitumen Content obtained for Polymer Modified Bituminous Concrete is 5.63%.  There is considerable increase in the Marshall Stability as the mixing and compaction temperature increases and there is substantial reduction in the Marshall Stability with further increase in the mixing and compaction temperature.
  • 15. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 07 | July -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 1164  There is considerable increase in the Indirect Tensile Strength as the mixing and compaction temperature increases and there is substantial reduction in the Indirect Tensile Strength with further increase in the mixing and compaction temperature.  Fatigue Life of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases as compaction temperature increases.  Resilient Modulus of Bituminous Concrete Mix prepared using Polymer Modified Bitumen increases as compaction temperature increases.  Initial Tensile Strain of Bituminous Concrete Mix prepared using Polymer Modified Bitumen decreases as compaction temperature increases.  Based on the experimental work and analysis carried out in the present study, an ideal mixing temperature of 160oC and compaction temperature of 140oC is suggested for the preparation of Bituminous Concrete Mix prepared using Polymer Modified Bitumen-(70). REFERENCES 1. Jian-Shiuh Chen, Min-Chih Liao and Ming-Shen Shiah “Asphalt Modified by Styrene-Butadiene-Styrene Tri-Block Copolymer: Morphology and Model”. 2. K.Kantha Kumar and A.Veeraragavan “Optimizing the Bituminous Concrete Mixes for Fatigue Performance”. 3. Noorafidah Binti Ithnin “Determination of Mixing and Compacting Temperatures for Hot Mix Asphalt”. 4. Shivangi Gupta & A.Veeraragavan “Fatigue Behaviour of Polymer Modified Bituminous Concrete Mixtures”. 5. Sixth Framework Programme of Spens Project, Transport Research Europe “Practical Mix Design Model for Asphalt Mixture”. 6. Specification of Ministry of Road Transport and Highways (MoRT&H) Government of India 4th Revision. 7. IRC SP 53-2002 specification for Modified bitumen.