This document summarizes the development of a novel zeolite synthesized from fly ash for treating wastewater. The synthesis process involves mixing fly ash with sodium hydroxide and refluxing for 98 hours at 383K until the pH becomes neutral. This combination of conventional and microwave synthesis methods increases the zeolite's porosity and cation exchange capacity (CEC) for effective wastewater treatment. Testing shows the zeolite effectively removes various metal cations like iron(III) from wastewater through ion exchange and absorption processes. With further optimization of synthesis parameters like time, temperature and base concentration, this fly ash-based zeolite could be developed into an efficient material for wastewater treatment.