This document describes the synthesis of 7-hydroxy-4-methyl coumarin via the Pechmann reaction. The Pechmann reaction involves the condensation of resorcinol with ethyl acetoacetate in concentrated sulfuric acid. The reaction mechanism proceeds through the initial formation of a β-hydroxy ester intermediate, which then cyclizes and dehydrates to form the coumarin product. Following the described procedure yields 4.3g of a pale yellow solid product, which is 49% of the theoretical yield. Characterization by TLC shows the product has a different Rf value than the starting materials, indicating formation of 7-hydroxy-4-methyl coumarin.