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Sulfur handling & melting
Sebastian Brechtel
Product & Strategy Manager
© Outotec – All rights reserved
Sulfur handling and melting – process steps
10/26/20152
• Sulfur storage
• Solid sulfur dosing
• Sulfur melting
• Sulfur filtration
• Leaf filter
• Polishing / Police filter
• Liquid sulfur storage
© Outotec – All rights reserved
Sulfur Handling & Melting
10/26/20153
Sulfur Melting in ext. Heat Exchanger & Filtration & Storage
© Outotec – All rights reserved
Sulfur Storage
10/26/20154
Bulk Storage
Liquid Sulfur Storage
45,000 t
© Outotec – All rights reserved
Sulfur storage under roof recommended
10/26/20155
• Higher CAPEX
• Safety concept needed
• Less impact on
environment
• Minimized pollution = loss
of sulfur
• Acidity control
© Outotec – All rights reserved
Solid Sulfur-Day Bin
Features
• Bin for two sulfur melters
• Two independent discharge systems for
each melter
• High flexibility
- Adjustable sulfur feed of each
melter
• Reduced Invest cost, only one
installation
• Additional buffer capacity
• More flexibility by feeding from
storage to day bin
10/26/20156
© Outotec – All rights reserved
Solid Sulfur-Day Bin
Alternative – Payloader
• Smaller capacity plants
• Man power required
10/26/20157
© Outotec – All rights reserved
Sulfur melting and filtration
Features
• Sulfur melting tank above ground
• No pits – why?
• Dead zones in rectangular
shaped pits
• Solids settling
• No heat and mass transfer in
dead zones
• Leakages not visible
= LARGE & INEFFICIENT
10/26/20158
© Outotec – All rights reserved
Sulfur melting and filtration
Features
• Sulfur melting tank above ground
• Tanks advantages
• Circular without dead zones
• Easy to agitate well
• High efficiency mass and heat
transfer
• Easier cleaning
Efficient:
40 t/h sulfur melting in tank of
7 m diameter
4 m height
10/26/20159
© Outotec – All rights reserved
Sulfur melting and filtration
Features
• Sulfur melting tank above ground
• No pits
• Front-end loader sulfur feed or
Sulfur day bin dosing
• Good access for maintenance
• Heating coils removable or
external shell and tube heat
exchanger
• One single agitator in melter
• Leaf filter & polishing filter
10/26/201510
© Outotec – All rights reserved
Sulfur Melting Tank - Dirty Sulfur
Features
• Full drainage of the tank possible for
maintenance
• Easier removal of non-molten , un-
desired solids collected at the lowest
part of the vessel
• Better access to equipment parts
• Removable heating coils
• Carbon steel with brick-lined section
in upper part of the melter
• Natural overflow to dirty sulfur pump
tank
10/26/201511
M
© Outotec – All rights reserved
Sulfur Melting Tank - Dirty Sulfur
10/26/201512
Flat Bottom
© Outotec – All rights reserved
Sulfur Melting Tank
Features
• minimized number of weld seams by
bending design
• heating bundle removable from top of
melter by filled up melter
• individual replacement of each heating
coil
10/26/201513
© Outotec – All rights reserved
Sulfur Leaf Filter
Features
• Hydraulic movement of Filter Shell
• Avoiding filter cake disposals on
movement
system , Hanging shell arrangement
prefered
• Solid filter plate support system
• Personal risk elimination by disposal
opening below filter frame
• All utility and sulfur connections at
fixed head except the shell heating
device
10/26/201514
© Outotec – All rights reserved
Police - / Polishing - Filter
10/26/201515
Features
Filter candle type
sinter material allows
high filtering efficiency,
steam and chemical
cleaning
© Outotec – All rights reserved
Ceramic vs. wounded glas fibre candles
10/26/201516
Pro
• Efficient
• High capacity
Con
• Cost
• Cleaning difficult
Pro
• Cost
Con
• Capacity
• Single use
© Outotec – All rights reserved
Ceramic vs. wounded glas fibre candles
10/26/201517
Design decision triggered by level of impurities
© Outotec – All rights reserved
Thank you for your attention ...

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Sulfur Handling - Outotec - COBRAS 2015

  • 1. Sulfur handling & melting Sebastian Brechtel Product & Strategy Manager
  • 2. © Outotec – All rights reserved Sulfur handling and melting – process steps 10/26/20152 • Sulfur storage • Solid sulfur dosing • Sulfur melting • Sulfur filtration • Leaf filter • Polishing / Police filter • Liquid sulfur storage
  • 3. © Outotec – All rights reserved Sulfur Handling & Melting 10/26/20153 Sulfur Melting in ext. Heat Exchanger & Filtration & Storage
  • 4. © Outotec – All rights reserved Sulfur Storage 10/26/20154 Bulk Storage Liquid Sulfur Storage 45,000 t
  • 5. © Outotec – All rights reserved Sulfur storage under roof recommended 10/26/20155 • Higher CAPEX • Safety concept needed • Less impact on environment • Minimized pollution = loss of sulfur • Acidity control
  • 6. © Outotec – All rights reserved Solid Sulfur-Day Bin Features • Bin for two sulfur melters • Two independent discharge systems for each melter • High flexibility - Adjustable sulfur feed of each melter • Reduced Invest cost, only one installation • Additional buffer capacity • More flexibility by feeding from storage to day bin 10/26/20156
  • 7. © Outotec – All rights reserved Solid Sulfur-Day Bin Alternative – Payloader • Smaller capacity plants • Man power required 10/26/20157
  • 8. © Outotec – All rights reserved Sulfur melting and filtration Features • Sulfur melting tank above ground • No pits – why? • Dead zones in rectangular shaped pits • Solids settling • No heat and mass transfer in dead zones • Leakages not visible = LARGE & INEFFICIENT 10/26/20158
  • 9. © Outotec – All rights reserved Sulfur melting and filtration Features • Sulfur melting tank above ground • Tanks advantages • Circular without dead zones • Easy to agitate well • High efficiency mass and heat transfer • Easier cleaning Efficient: 40 t/h sulfur melting in tank of 7 m diameter 4 m height 10/26/20159
  • 10. © Outotec – All rights reserved Sulfur melting and filtration Features • Sulfur melting tank above ground • No pits • Front-end loader sulfur feed or Sulfur day bin dosing • Good access for maintenance • Heating coils removable or external shell and tube heat exchanger • One single agitator in melter • Leaf filter & polishing filter 10/26/201510
  • 11. © Outotec – All rights reserved Sulfur Melting Tank - Dirty Sulfur Features • Full drainage of the tank possible for maintenance • Easier removal of non-molten , un- desired solids collected at the lowest part of the vessel • Better access to equipment parts • Removable heating coils • Carbon steel with brick-lined section in upper part of the melter • Natural overflow to dirty sulfur pump tank 10/26/201511 M
  • 12. © Outotec – All rights reserved Sulfur Melting Tank - Dirty Sulfur 10/26/201512 Flat Bottom
  • 13. © Outotec – All rights reserved Sulfur Melting Tank Features • minimized number of weld seams by bending design • heating bundle removable from top of melter by filled up melter • individual replacement of each heating coil 10/26/201513
  • 14. © Outotec – All rights reserved Sulfur Leaf Filter Features • Hydraulic movement of Filter Shell • Avoiding filter cake disposals on movement system , Hanging shell arrangement prefered • Solid filter plate support system • Personal risk elimination by disposal opening below filter frame • All utility and sulfur connections at fixed head except the shell heating device 10/26/201514
  • 15. © Outotec – All rights reserved Police - / Polishing - Filter 10/26/201515 Features Filter candle type sinter material allows high filtering efficiency, steam and chemical cleaning
  • 16. © Outotec – All rights reserved Ceramic vs. wounded glas fibre candles 10/26/201516 Pro • Efficient • High capacity Con • Cost • Cleaning difficult Pro • Cost Con • Capacity • Single use
  • 17. © Outotec – All rights reserved Ceramic vs. wounded glas fibre candles 10/26/201517 Design decision triggered by level of impurities
  • 18. © Outotec – All rights reserved Thank you for your attention ...