Overflows and Gravity Drainage Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 OUTLINE OF THE PROBLEM
5 DESIGNING FOR FLOODED FLOW
6 DESIGNING NON-FLOODED PIPELINES
6.1 Vertical Pipework
6.2 From the Side of a Vessel
6.3 Established (uniform) Flow in Near-horizontal Pipes
6.4 Non-uniform Flow
7 NON-FLOODED FLOW IN COMPLEX SYSTEMS
8 ENTRAINING FLOW
9 SIMPLE TANK OVERFLOWS
9.1 Venting of the Tank
10 BIBLIOGRAPHY
11 NOMENCLATURE
TABLE
1 GEOMETRICAL FUNCTIONS OF PART-FULL PIPES
FIGURES
1 TYPICAL SEQUENCE OF SURGING FLOW
2 DESIGNING FOR FLOODED FLOW
3 CAPACITY OF SLOPING PIPELINES
4 OVERFLOW FROM SIDE OF VESSEL
5 METHODS OF AVOIDING LARGE CIRCULAR SIDE
OVERFLOWS
6 CAPACITY OF A GENTLY SLOPING PIPE AS A FUNCTION OF LIQUID DEPTH
7 COMPLEX PIPE SYSTEMS
8 REMOVAL OF ENTRAINED GASES
DESIGN OF VENT GAS COLLECTION AND DESTRUCTION SYSTEMS Gerard B. Hawkins
DESIGN OF VENT GAS COLLECTION AND DESTRUCTION SYSTEMS
CONTENTS
1 INTRODUCTION
1.1 Purpose
1.2 Scope of this Guide
1.3 Use of the Guide
2 ENVIRONMENTAL ISSUES
2.1 Principal Concerns
2.2 Mechanisms for Ozone Formation
2.3 Photochemical Ozone Creation Potential
2.4 Health and Environmental Effects
2.5 Air Quality Standards for Ground Level Concentrations of Ozone, Targets for Reduction of VOC Discharges and Statutory Discharge Limits
3 VENTS REDUCTION PHILOSOPHY
3.1 Reduction at Source
3.2 End-of-pipe Treatment
4 METHODOLOGY FOR COLLECTION & ASSESSMENT OF PROCESS FLOW DATA
4.1 General
4.2 Identification of Vent Sources
4.3 Characterization of Vents
4.4 Quantification of Process Vent Flows
4.5 Component Flammability Data Collection
4.6 Identification of Operating Scenarios
4.7 Quantification of Flammability Characteristics for Combined Vents
4.8 Identification, Quantification and Assessment of Possibility of Air Ingress Routes
4.9 Tabulation of Data
4.10 Hazard Study and Risk Assessment
4.11 Note on Aqueous / Organic Wastes
4.12 Complexity of Systems
4.13 Summary
5 SAFE DESIGN OF VENT COLLECTION HEADER SYSTEMS
5.1 General
5.2 Process Design of Vent Headers
5.3 Liquid in Vent Headers
5.4 Materials of Construction
5.5 Static Electricity Hazard
5.6 Diversion Systems
5.7 Snuffing Systems
6 SAFE DESIGN OF THERMAL OXIDISERS
6.1 Introduction
6.2 Design Basis
6.3 Types of High Temperature Thermal Oxidizer
6.4 Refractories
6.5 Flue Gas Treatment
6.6 Control and Safety Systems
6.7 Project Program
6.8 Commissioning
6.9 Operational and Maintenance Management
APPENDICES
A GLOSSARY
B FLAMMABILITY
C EXAMPLE PROFORMA
D REFERENCES
DOCUMENTS REFERRED TO IN THIS PROCESS GUIDE
TABLE
1 PHOTOCHEMICAL OZONE CREATION POTENTIAL REFERENCED
TO ETHYLENE AS UNITY
FIGURES
1 SCHEMATIC OF TYPICAL VENT COLLECTION AND THERMAL OXIDIZER SYSTEM
2 TYPICAL KNOCK-OUT POT WITH LUTED DRAIN
3 SCHEMATIC OF DIVERSION SYSTEM
4 CONVENTIONAL VERTICAL THERMAL OXIDIZER
5 CONVENTIONAL OXIDIZER WITH INTEGRAL WATER SPARGER
6 THERMAL OXIDIZER WITH STAGED AIR INJECTION
7 DOWN-FIRED UNIT WITH WATER BATH QUENCH
8 FLAMELESS THERMAL OXIDATION UNIT
9 THERMAL OXIDIZER WITH REGENERATIVE HEAT RECOVERY
10 TYPICAL PROJECT PROGRAM
11 TYPICAL FLAMMABILITY DIAGRAM
12 EFFECT OF DILUTION WITH AIR
13 EFFECT OF DILUTION WITH AIR ON 100 Rm³ OF FLAMMABLE GAS
Introduction to Pressure Surge in Liquid Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 CAUSES OF PRESSURE SURGE
4.1 Start-up
5 CONSEQUENCES OF PRESSURE SURGES
6 PRELIMINARY CALCULATIONS
6.1 Estimation of the Sonic Velocity
6.2 Pipeline Period
7 CALCULATION OF PEAK PRESSURES
7.1 Rigid Liquid Column Theory
7.2 Sudden Changes in Flowrate
7.3 Moderately Rapid Changes in Flowrate
7.4 Reflections and Attenuations
7.5 Vapor Cavity Formation
7.6 Complex Piping Systems
8 FORCES ON PIPE SUPPORTS.
9 METHODS OF REDUCING THE EFFECTS OF
PRESSURE SURGE
9.1 Flowrate
9.2 Pipe Diameter
9.3 Valve Selection and Operation
9.4 Pump Start-up/Shut-down
9.5 Surge Tanks and Accumulators
9.6 Vacuum Breakers
9.7 Changes to Equipment
10 DETAILED ANALYSIS
10.1 Data Requirements
10.2 Interpretation of Results
11 GUIDELINES FOR CALCULATIONS
12 EXAMPLES OF PRESSURE SURGE INCIDENTS
12.1 Caustic Soda Pipeline Movement
12.2 Ammonia Pipe Movement
12.3 Propylene Reactor Start-up
12.4 Cooling Water Failure
12.5 Dry Riser Fire Sprinkler Systems
12.6 Cast Iron Fire Main Pressurization
DESIGN OF VENT GAS COLLECTION AND DESTRUCTION SYSTEMS Gerard B. Hawkins
DESIGN OF VENT GAS COLLECTION AND DESTRUCTION SYSTEMS
CONTENTS
1 INTRODUCTION
1.1 Purpose
1.2 Scope of this Guide
1.3 Use of the Guide
2 ENVIRONMENTAL ISSUES
2.1 Principal Concerns
2.2 Mechanisms for Ozone Formation
2.3 Photochemical Ozone Creation Potential
2.4 Health and Environmental Effects
2.5 Air Quality Standards for Ground Level Concentrations of Ozone, Targets for Reduction of VOC Discharges and Statutory Discharge Limits
3 VENTS REDUCTION PHILOSOPHY
3.1 Reduction at Source
3.2 End-of-pipe Treatment
4 METHODOLOGY FOR COLLECTION & ASSESSMENT OF PROCESS FLOW DATA
4.1 General
4.2 Identification of Vent Sources
4.3 Characterization of Vents
4.4 Quantification of Process Vent Flows
4.5 Component Flammability Data Collection
4.6 Identification of Operating Scenarios
4.7 Quantification of Flammability Characteristics for Combined Vents
4.8 Identification, Quantification and Assessment of Possibility of Air Ingress Routes
4.9 Tabulation of Data
4.10 Hazard Study and Risk Assessment
4.11 Note on Aqueous / Organic Wastes
4.12 Complexity of Systems
4.13 Summary
5 SAFE DESIGN OF VENT COLLECTION HEADER SYSTEMS
5.1 General
5.2 Process Design of Vent Headers
5.3 Liquid in Vent Headers
5.4 Materials of Construction
5.5 Static Electricity Hazard
5.6 Diversion Systems
5.7 Snuffing Systems
6 SAFE DESIGN OF THERMAL OXIDISERS
6.1 Introduction
6.2 Design Basis
6.3 Types of High Temperature Thermal Oxidizer
6.4 Refractories
6.5 Flue Gas Treatment
6.6 Control and Safety Systems
6.7 Project Program
6.8 Commissioning
6.9 Operational and Maintenance Management
APPENDICES
A GLOSSARY
B FLAMMABILITY
C EXAMPLE PROFORMA
D REFERENCES
DOCUMENTS REFERRED TO IN THIS PROCESS GUIDE
TABLE
1 PHOTOCHEMICAL OZONE CREATION POTENTIAL REFERENCED
TO ETHYLENE AS UNITY
FIGURES
1 SCHEMATIC OF TYPICAL VENT COLLECTION AND THERMAL OXIDIZER SYSTEM
2 TYPICAL KNOCK-OUT POT WITH LUTED DRAIN
3 SCHEMATIC OF DIVERSION SYSTEM
4 CONVENTIONAL VERTICAL THERMAL OXIDIZER
5 CONVENTIONAL OXIDIZER WITH INTEGRAL WATER SPARGER
6 THERMAL OXIDIZER WITH STAGED AIR INJECTION
7 DOWN-FIRED UNIT WITH WATER BATH QUENCH
8 FLAMELESS THERMAL OXIDATION UNIT
9 THERMAL OXIDIZER WITH REGENERATIVE HEAT RECOVERY
10 TYPICAL PROJECT PROGRAM
11 TYPICAL FLAMMABILITY DIAGRAM
12 EFFECT OF DILUTION WITH AIR
13 EFFECT OF DILUTION WITH AIR ON 100 Rm³ OF FLAMMABLE GAS
Introduction to Pressure Surge in Liquid Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 CAUSES OF PRESSURE SURGE
4.1 Start-up
5 CONSEQUENCES OF PRESSURE SURGES
6 PRELIMINARY CALCULATIONS
6.1 Estimation of the Sonic Velocity
6.2 Pipeline Period
7 CALCULATION OF PEAK PRESSURES
7.1 Rigid Liquid Column Theory
7.2 Sudden Changes in Flowrate
7.3 Moderately Rapid Changes in Flowrate
7.4 Reflections and Attenuations
7.5 Vapor Cavity Formation
7.6 Complex Piping Systems
8 FORCES ON PIPE SUPPORTS.
9 METHODS OF REDUCING THE EFFECTS OF
PRESSURE SURGE
9.1 Flowrate
9.2 Pipe Diameter
9.3 Valve Selection and Operation
9.4 Pump Start-up/Shut-down
9.5 Surge Tanks and Accumulators
9.6 Vacuum Breakers
9.7 Changes to Equipment
10 DETAILED ANALYSIS
10.1 Data Requirements
10.2 Interpretation of Results
11 GUIDELINES FOR CALCULATIONS
12 EXAMPLES OF PRESSURE SURGE INCIDENTS
12.1 Caustic Soda Pipeline Movement
12.2 Ammonia Pipe Movement
12.3 Propylene Reactor Start-up
12.4 Cooling Water Failure
12.5 Dry Riser Fire Sprinkler Systems
12.6 Cast Iron Fire Main Pressurization
Pipeline Design for Isothermal, Laminar Flow of Non-Newtonian FluidsGerard B. Hawkins
Pipeline Design for Isothermal, Laminar Flow of Non-Newtonian Fluids
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 RHEOLOGICAL BEHAVIOR OF PURELY VISCOUS
NON-NEWTONIAN FLUIDS
4.1 Experimental Characterization
4.2 Rheological Models
5 PRESSURE DROP-FLOW RATE RELATIONSHIPS
BASED DIRECTLY ON EXPERIMENTAL DATA
5.1 Use of Shear Stress – Shear Rate Data
5.2 Tubular Viscometer Data
6 PRESSURE DROP – FLOW RATE RELATIONSHIPS BASED ON RHEOLOGICAL MODELS
7 LOSSES IN PIPE FITTINGS
7.1 Entrances Losses
7.2 Expansion Effects
7.3 Contraction Losses
7.4 Valves
7.5 Bends
8 EFFECT OF WALL SLIP
9 VELOCITY PROFILES
9.1 Velocity Profile from Experimental Flow-Curve
9.2 Velocity Profile from Rheological Model
9.3 Residence Time Distribution
10 CHECKS ON THE VALIDITY OF THE
DESIGN PROCEDURES
10.1 Rheological Behavior
10.2 Validity of Experimental Data
10.2 Check on Laminar Flow
11 NOMENCLATURE
12 REFERENCES
FIGURES
1 FLOW CURVES FOR PURELY VISCOUS FLUIDS
2 PLOTS OF D∆P/4L VERSUS 32Q/ɳD3 FOR PURELY VISCOUS FLUIDS
3 LOG-LOG PLOT OF t VERSUS ý
4 FLOW CURVE FOR A BINGHAM PLASTIC
5 LOG-LOG PLOT FOR A GENERALIZED BINGHAM
PLASTIC
6 CORRELATION OF ENTRANCE LOSS
7 CORRELATION OF EXPANSION LOSS
8 EFFECT OF “WALL SLIP” ON VELOCITY PROFILE
9 D∆P/4L VERSUS Q/ɳR3 WITH WALL SLIP
10 EVALUATION OFUs WITH Ʈw
11 VARIATION OF Us WITH Ʈw
12 PLOT OF D∆P/4L VERSUS 8 (ū- Us)/D FOR
CONDITIONS OF WALL SLIP
13 CUMULATIVE RESIDENCE TIME DISTRIBUTION
TO POWER LAW FLUIDS
14 EFFECTS OF TUBE LENGTH AND DIAMETER ON
RELATIONSHIP BETWEEN D∆P/4L AND 32Q/ɳD3
Pressure Relief Systems
BACKGROUND TO RELIEF SYSTEM DESIGN Vol.1 of 6
The Guide has been written to advise those involved in the design and engineering of pressure relief systems. It takes the user from the initial identification of potential causes of overpressure or under pressure through the process design of relief systems to the detailed mechanical design. "Hazard Studies" and quantitative hazards analysis are not described; these are seen as complementary activities. Typical users of the Guide will use some Parts in detail and others in overview.
CENTRIFUGAL COMPRESSOR SETTLE OUT CONDITIONS TUTORIALVijay Sarathy
Centrifugal Compressors are a preferred choice in gas transportation industry, mainly due to their ability to cater to varying loads. In the event of a compressor shutdown as a planned event, i.e., normal shutdown (NSD), the anti-surge valve is opened to recycle gas from the discharge back to the suction (thereby moving the operating point away from the surge line) and the compressor is tripped via the driver (electric motor or Gas turbine / Steam Turbine). In the case of an unplanned event, i.e., emergency shutdown such as power failure, the compressor trips first followed by the anti-surge valve opening. In doing so, the gas content in the suction side & discharge side mix.
Therefore, settle out conditions is explained as the equilibrium pressure and temperature reached in the compressor piping and equipment volume following a compressor shutdown
Air / Steam Regeneration Procedure for Primary Reforming CcatalystGerard B. Hawkins
VULCAN Series VSG-Z101 Primary Reforming
Air steam regeneration procedures can be used either on start-up of a reformer after it has cooled, or can be done in the shut down process.
AIR STEAM REGENERATION ON SHUT DOWN
AIR STEAM REGENERATION ON START-UP
This 5 day training course is designed to give you a comprehensive account of methods and techniques used in modern well testing and analysis. Subsequently to outlining well test objectives and general methodologies applied, the course will provide real case studies and practice using modern software for Pressure Transient Analysis. These exercises will demonstrate clearly the limitations, assumptions and applicability of various techniques applied in the field.
This presentation is a brief descriptive procedure of simulating in aspen flare system analyser (otherwise called as flarenet). It gives a step by step instructions to develop a flare network scheme in the simulator
Distillation Towers (Columns) presentation on Types, governing Equations and ...Hassan ElBanhawi
Based on my 8 years of experience in Oil & Gas industry I can claim that you can find here All what you need to know about Columns. This is an introduction to understand more about their:-
-Types
-Basic Principles and equations
-Distillation System
-P&ID Symbols
-Worked Example
You can find also more at:
http://hassanelbanhawi.com/staticequipment/columns/
All the data and the illustrative figures presented here can be found through two reference books:-
ENGINEERING DATA BOOK by Gas Processors Suppliers Association
Process Technology - Equipment and Systems by Charles E. Thomas
Thank you.
Compressors presentation on Types, Classification and governing EquationsHassan ElBanhawi
Based on my 8 years of experience in Oil & Gas industry I can claim that you can find here All what you need to know about Compressors. This is an introduction to understand more about their:-
-Types.
-Selection.
-Performance.
-Worked Example.
-Excel Sheets for Calculation.
You can find also more at:
http://hassanelbanhawi.com/rotatingequipment/compressors/
All the data and the illustrative figures presented here can be found through two reference books:-
ENGINEERING DATA BOOK by Gas Processors Suppliers Association
Process Technology - Equipment and Systems by Charles E. Thomas
Thank you.
Air Cooled Heat Exchanger Design
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 SUITABILITY FOR AIR COOLING
4.1 Options Available For Cooling
4.2 Choice of Cooling System
5 SPECIFICATION OF AN AIR COOLED HEAT
EXCHANGER
5.1 Description and Terminology
5.2 General
5.3 Thermal Duty and Design Margins
5.4 Process Pressure Drop
5.5 Design Ambient Conditions
5.6 Process Physical Properties
5.7 Mechanical Design Constraints
5.8 Arrangement
5.9 Air Side Fouling
5.10 Economic Factors in Design
6 CONTROL
7 PRESSURE RELIEF
8 ASSESSMENT OF OFFERS
8.1 General
8.2 Manual Checking Of Designs
8.3 Computer Assessment
8.4 Bid Comparison
9 FOULING AND CORROSION
9.1 Fouling
9.2 Corrosion
10 OPERATION AND MAINTENANCE
10.1 Performance Testing
10.2 Air-Side Cleaning
10.3 Mechanical Maintenance
10.4 Tube side Access
11 REFERENCES
Gas-Solid-Liquid Mixing Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 SELECTION OF EQUIPMENT
5 THREE-PHASE MASS TRANSFER WITH CHEMICAL REACTION
6 STIRRED VESSEL DESIGN
6.1 Agitator Design
6.2 Design for Solids Suspension
6.3 Vessel Design
6.4 Gas-Liquid Mass Transfer Coefficient and Surface Area
7 THREE-PHASE FLUIDIZED BEDS
7.1 Gas and Liquid Hold-Up
7.2 Calculation Procedure
7.3 Bubble Size
7.4 Mass Transfer
7.5 Heat Transfer
7.6 Elutriation
8 SLURRY REACTORS
8.1 Gas Rate
8.2 Mass Transfer
9 NOMENCLATURE
10 BIBLIOGRAPHY
Pipeline Design for Isothermal, Laminar Flow of Non-Newtonian FluidsGerard B. Hawkins
Pipeline Design for Isothermal, Laminar Flow of Non-Newtonian Fluids
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 RHEOLOGICAL BEHAVIOR OF PURELY VISCOUS
NON-NEWTONIAN FLUIDS
4.1 Experimental Characterization
4.2 Rheological Models
5 PRESSURE DROP-FLOW RATE RELATIONSHIPS
BASED DIRECTLY ON EXPERIMENTAL DATA
5.1 Use of Shear Stress – Shear Rate Data
5.2 Tubular Viscometer Data
6 PRESSURE DROP – FLOW RATE RELATIONSHIPS BASED ON RHEOLOGICAL MODELS
7 LOSSES IN PIPE FITTINGS
7.1 Entrances Losses
7.2 Expansion Effects
7.3 Contraction Losses
7.4 Valves
7.5 Bends
8 EFFECT OF WALL SLIP
9 VELOCITY PROFILES
9.1 Velocity Profile from Experimental Flow-Curve
9.2 Velocity Profile from Rheological Model
9.3 Residence Time Distribution
10 CHECKS ON THE VALIDITY OF THE
DESIGN PROCEDURES
10.1 Rheological Behavior
10.2 Validity of Experimental Data
10.2 Check on Laminar Flow
11 NOMENCLATURE
12 REFERENCES
FIGURES
1 FLOW CURVES FOR PURELY VISCOUS FLUIDS
2 PLOTS OF D∆P/4L VERSUS 32Q/ɳD3 FOR PURELY VISCOUS FLUIDS
3 LOG-LOG PLOT OF t VERSUS ý
4 FLOW CURVE FOR A BINGHAM PLASTIC
5 LOG-LOG PLOT FOR A GENERALIZED BINGHAM
PLASTIC
6 CORRELATION OF ENTRANCE LOSS
7 CORRELATION OF EXPANSION LOSS
8 EFFECT OF “WALL SLIP” ON VELOCITY PROFILE
9 D∆P/4L VERSUS Q/ɳR3 WITH WALL SLIP
10 EVALUATION OFUs WITH Ʈw
11 VARIATION OF Us WITH Ʈw
12 PLOT OF D∆P/4L VERSUS 8 (ū- Us)/D FOR
CONDITIONS OF WALL SLIP
13 CUMULATIVE RESIDENCE TIME DISTRIBUTION
TO POWER LAW FLUIDS
14 EFFECTS OF TUBE LENGTH AND DIAMETER ON
RELATIONSHIP BETWEEN D∆P/4L AND 32Q/ɳD3
Pressure Relief Systems
BACKGROUND TO RELIEF SYSTEM DESIGN Vol.1 of 6
The Guide has been written to advise those involved in the design and engineering of pressure relief systems. It takes the user from the initial identification of potential causes of overpressure or under pressure through the process design of relief systems to the detailed mechanical design. "Hazard Studies" and quantitative hazards analysis are not described; these are seen as complementary activities. Typical users of the Guide will use some Parts in detail and others in overview.
CENTRIFUGAL COMPRESSOR SETTLE OUT CONDITIONS TUTORIALVijay Sarathy
Centrifugal Compressors are a preferred choice in gas transportation industry, mainly due to their ability to cater to varying loads. In the event of a compressor shutdown as a planned event, i.e., normal shutdown (NSD), the anti-surge valve is opened to recycle gas from the discharge back to the suction (thereby moving the operating point away from the surge line) and the compressor is tripped via the driver (electric motor or Gas turbine / Steam Turbine). In the case of an unplanned event, i.e., emergency shutdown such as power failure, the compressor trips first followed by the anti-surge valve opening. In doing so, the gas content in the suction side & discharge side mix.
Therefore, settle out conditions is explained as the equilibrium pressure and temperature reached in the compressor piping and equipment volume following a compressor shutdown
Air / Steam Regeneration Procedure for Primary Reforming CcatalystGerard B. Hawkins
VULCAN Series VSG-Z101 Primary Reforming
Air steam regeneration procedures can be used either on start-up of a reformer after it has cooled, or can be done in the shut down process.
AIR STEAM REGENERATION ON SHUT DOWN
AIR STEAM REGENERATION ON START-UP
This 5 day training course is designed to give you a comprehensive account of methods and techniques used in modern well testing and analysis. Subsequently to outlining well test objectives and general methodologies applied, the course will provide real case studies and practice using modern software for Pressure Transient Analysis. These exercises will demonstrate clearly the limitations, assumptions and applicability of various techniques applied in the field.
This presentation is a brief descriptive procedure of simulating in aspen flare system analyser (otherwise called as flarenet). It gives a step by step instructions to develop a flare network scheme in the simulator
Distillation Towers (Columns) presentation on Types, governing Equations and ...Hassan ElBanhawi
Based on my 8 years of experience in Oil & Gas industry I can claim that you can find here All what you need to know about Columns. This is an introduction to understand more about their:-
-Types
-Basic Principles and equations
-Distillation System
-P&ID Symbols
-Worked Example
You can find also more at:
http://hassanelbanhawi.com/staticequipment/columns/
All the data and the illustrative figures presented here can be found through two reference books:-
ENGINEERING DATA BOOK by Gas Processors Suppliers Association
Process Technology - Equipment and Systems by Charles E. Thomas
Thank you.
Compressors presentation on Types, Classification and governing EquationsHassan ElBanhawi
Based on my 8 years of experience in Oil & Gas industry I can claim that you can find here All what you need to know about Compressors. This is an introduction to understand more about their:-
-Types.
-Selection.
-Performance.
-Worked Example.
-Excel Sheets for Calculation.
You can find also more at:
http://hassanelbanhawi.com/rotatingequipment/compressors/
All the data and the illustrative figures presented here can be found through two reference books:-
ENGINEERING DATA BOOK by Gas Processors Suppliers Association
Process Technology - Equipment and Systems by Charles E. Thomas
Thank you.
Air Cooled Heat Exchanger Design
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 SUITABILITY FOR AIR COOLING
4.1 Options Available For Cooling
4.2 Choice of Cooling System
5 SPECIFICATION OF AN AIR COOLED HEAT
EXCHANGER
5.1 Description and Terminology
5.2 General
5.3 Thermal Duty and Design Margins
5.4 Process Pressure Drop
5.5 Design Ambient Conditions
5.6 Process Physical Properties
5.7 Mechanical Design Constraints
5.8 Arrangement
5.9 Air Side Fouling
5.10 Economic Factors in Design
6 CONTROL
7 PRESSURE RELIEF
8 ASSESSMENT OF OFFERS
8.1 General
8.2 Manual Checking Of Designs
8.3 Computer Assessment
8.4 Bid Comparison
9 FOULING AND CORROSION
9.1 Fouling
9.2 Corrosion
10 OPERATION AND MAINTENANCE
10.1 Performance Testing
10.2 Air-Side Cleaning
10.3 Mechanical Maintenance
10.4 Tube side Access
11 REFERENCES
Gas-Solid-Liquid Mixing Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 SELECTION OF EQUIPMENT
5 THREE-PHASE MASS TRANSFER WITH CHEMICAL REACTION
6 STIRRED VESSEL DESIGN
6.1 Agitator Design
6.2 Design for Solids Suspension
6.3 Vessel Design
6.4 Gas-Liquid Mass Transfer Coefficient and Surface Area
7 THREE-PHASE FLUIDIZED BEDS
7.1 Gas and Liquid Hold-Up
7.2 Calculation Procedure
7.3 Bubble Size
7.4 Mass Transfer
7.5 Heat Transfer
7.6 Elutriation
8 SLURRY REACTORS
8.1 Gas Rate
8.2 Mass Transfer
9 NOMENCLATURE
10 BIBLIOGRAPHY
Hydrogen Compressors
Engineering Design Guide
1 SCOPE
2 PHYSICAL ROPERTIES
2.1 Data for Pure Hydrogen
2.2 Influence of Impurities
3 MATERIALS OF CONSTRUCTION
3.1 Hydrogen from Electrolytic Cells
3.2 Pure Hydrogen
4 DESIGN
4.1 Pulsation
4.2 Bypass
5 TESTING OR COMMISSIONING RECIPROCATING COMPRESSORS
6 LUBRICATION
7 LAYOUT
8 REFERENCES
FIGURES
1 MOLLIER CHART - HYDROGEN
2 COMPRESSIBILITY CHART
3 NELSON DIAGRAM
4 WATER CONTENT IN HYDROGEN FOR OIL-LUBRICATED COMPRESSORS AS GRAMM/M2 SWEPT CYLINDER AREA
Batch Distillation
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 BACKGROUND TO THE DESIGN
4.1 General
4.2 Choice of batch/continuous operation
4.3 Boiling point curve and cut policy
4.4 Method of design
4.5 Scope of calculations required for design
5 SIMPLE BATCH DISTILLATION
6 FRACTIONAL BATCH DISTILLATION
6.1 General
6.2 Approximate methods
6.3 Rigorous design - use of a computer model
6.4 Other factors influencing the design
6.4.1 Occupation
6.4.2 Choice of Batch Rectification or Stripping
6.4.3 Batch size
6.4.4 Initial estimate of cut policy
6.4.5 Liquid Holdup
6.4.6 Total reflux operation and heating-up time
6.4.7 Column operating pressure
6.5 Optimum Design of the Batch Still
6.6 Special design problems
7 GENERAL ASPECTS OF EQUIPMENT DESIGN
7.1 Kettle reboilers
7.2 Column Internals
7.3 Condensers and reflux split boxes
8 PROCESS CONTROL AND INSTRUMENTATION IN
BATCH DISTILLATION
9 MECHANICAL DESIGN FEATURES
10 BIBLIOGRAPHY
APPENDICES
A McCABE - THIELE METHOD - TYPICAL EXAMPLE
Large Water Pumps
CONTENTS
1 SCOPE
SECTION ONE: INTEGRATION OF PUMPS INTO THE PROCESS
2 PROPERTIES OF FLUID
2.1 Cooling Water
2.2 Brine
2.3 Estuary Water
2.4 Harbor Water
2.5 Oil-field water
3 CALCULATION OF DUTY
4 CHOICE OF TYPE AND NUMBER OF PUMPS
4.1 Type of Pump
4.2 Points to Consider
4.3 Number of Pumps
5 RECOMMENDED LINE DIAGRAM
5.1 Check List for Each Pump
6 RECOMMENDED LAYOUT
SECTION TWO: CONSTRUCTION FEATURES
7 HORIZONTAL, AXIALLY SPLIT CASING PUMPS
7.1 Pressure Casing
7.2 Bolting
7.3 Flanges and Connections
7.4 Rotating Elements
7.5 Wear Rings
7.6 Running Clearances
7.7 Mechanical Seals
7.8 Packed Glands
7.9 Bearings and Bearing Housings
7.10 Lubrication
7.11 Couplings
7.12 Guards
7.13 Baseplates
7.14 Flywheels
8 VERTICAL PUMPS
8.1 General
8.2 Pressure Casing
8.3 Bolting
8.4 Flanges and Connections
8.5 Rotating Element
8.6 Packed Glands
8.7 Bearings and Bearing Housings
8.8 Pump Head
8.9 Column Pipes
8.10 Line Shaft and Couplings
8.11 Reverse Rotation
8.12 Gearboxes
9 MATERIALS
9.1 Castings
9.2 Casings
9.3 Impellers
9.4 Shafts
9.5 Shaft Sleeves
9.6 Bolts and Nuts
10 DRIVERS
10.1 Electric Motor Drives
11 BIBLIOGRAPHY
APPENDICES:
A COOLING WATER - EUROPEAN SITE
B TIDAL RIVER ESTUARY
C FLYWHEEL INERTIA FOR PRESSURE SURGE ABATEMENT
D RESIN COATING OF CASINGS FOR WATER PUMPS
E AREA RATIO METHOD
F NOTES ON PUMP IMPELLERS CASTINGS
G LIMIT ON SHAFT DIAMETER FOR HORIZONTAL PUMPS HAVING
ONE DOUBLE-ENTRY IMPELLER SUPPORTED BETWEEN BEARINGS
H FORCES AND BENDING MOMENTS ON RISING MAIN ASSEMBLY
I POWER COSTS
J PUTATIVE COST COMPARISON SHEET
K TECHNICAL COMPARISON SHEETS
FIGURES
2.1 VAPOR TEMPERATURE CURVES
2.2 DENSITY TEMPERATURE CURVES
3.1 TYPICAL HEAD OF PUMPS
3.2 TOTAL HEAD OF VERTICAL IMMERSED PUMP
3.3 TYPICAL TIDAL RIVER ESTUARY LEVELS
3.5 SUBMERGENCE LIMITS
4.1 TYPES OF PUMP
4.2 GUIDE TO PUMP TYPE AND SPEED
5.1 TYPICAL LINE DIAGRAM
6 GUIDE TO SUCTION PIPEWORK DESIGN
7 CASING AND IMPELLER DETAILS
8.1 DRY WELL AND WET WELL PUMP INSTALLATIONS
8.2 BELLMOUTH DIMENSIONS FOR VERTICAL INTAKES
8.3 MAXIMUM SPACING BETWEEN SHAFT GUIDE BUSHING
8.4 LINE SHAFT COUPLING
9 TYPICAL VOLUTE CASING
10 TYPICAL CASE WEAR RINGS
11 SEAL AREA
TABLES
1 LIQUID PROPERTIES SODIUM CHLORIDE (25% W/W)
2 LIQUID PROPERTIES SODIUM CHLORIDE (20% W/W)
3 LIQUID PROPERTIES SODIUM CHLORIDE (16.25% W/W)
4 LIQUID PROPERTIES SODIUM CHLORIDE (15% W/W)
5 LIQUID PROPERTIES SODIUM CHLORIDE (10% W/W)
6 LIQUID PROPERTIES SODIUM CHLORIDE (5% W/W)
7 GUIDE TO PUMP TYPE AND SPEED
8 RECOMMENDED CAST MATERIALS FOR USE IN THE PUMP INDUSTRY
GRAPHS
1 GUIDE TO ROTOR INERTIA
2 LIMITS BETWEEN BEARINGS
DOCUMENTS REFERRED TO IN THIS ENGINEERING DEPARTMENT DESIGN GUIDE
Boiler Water Circulation Pumps
1 SCOPE
2 CHOICE OF TYPE AND NUMBER OF PUMPS
2.1 Need for Continuous Flow
2.2 Pump Reliability
3 CHOICE OF DRIVER
4 DUTY CALCULATIONS
5 CHOICE OF SEAL
5.1 Mechanical Seals
5.2 Soft-packed Glands
5.3 Construction Features
5.4 Guarding
6 CONSTRUCTION FEATURES
6.1 Vertical Glandless Wet-stator Motor Pumps
7 LAYOUT
7.1 Non-return Valves
7.2 Reducers at Pump Connections
7.3 Glandless Pumps for System Pressures
Exceeding 60 bar abs
7.4 Access round Glandless Pumps
7.5 Cooling Water Supply
8 RECOMMENDED LINE DIAGRAMS
8.1 Horizontal Pumps in Category 1
8.2 Vertical Wet-stator Motor Pumps in Category
APPENDICES
A PROPERTIES OF WATER AT THE SATURATION LINE
B ANNEX TO API 610, 6TH EDITION 1981:
VERTICAL GLANDLESS WET-STATOR MOTOR PUMPS
C ANNEX TO API 610, 6TH EDITION 1981:
HORIZONTAL BACK PULL-OUT PUMPS FOR BOILER
WATER CIRCULATION DUTY
FIGURES
3.1 NPSH CORRECTION FOR WATER
3.2 VELOCITY OF SOUND IN WATER AT 50 BAR
(NO BUBBLES)
3.3 VELOCITY OF SOUND IN WATER AT 50 BAR
(WITH 3% VAPOR CONTENT)
8.1 RECOMMENDED LINE DIAGRAM HORIZONTAL PUMPS - CATEGORY 1
8.2 RECOMMENDED LINE DIAGRAM HORIZONTAL PUMPS - SOFT PACKED GLAND INSTALLATION
8.3 RECOMMENDED LINE DIAGRAM HORIZONTAL PUMPS - MECHANICAL SEAL INSTALLATION
8.4 RECOMMENDED LINE DIAGRAM VERTICAL WET STATOR PUMPS - CATEGORY 2
BIBLIOGRAPHY
Turbulent Heat Transfer to Non Newtonian Fluids in Circular TubesGerard B. Hawkins
Turbulent Heat Transfer to Non Newtonian Fluids in Circular Tubes
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 THE INTEGRATION OF THE ENERGY EQUATION
5 THE EDDY VISCOSITY FOR NON-NEWTONIAN AND DRAG REDUCING FLUIDS
6 THE CALCULATION OF HEAT TRANSFER
COEFFICIENTS FOR NON-NEWTONIAN AND DRAG
REDUCING FLUIDS IN TURBULENT PIPE FLOW
6.1 General
6.2 Drag Reducing Fibre Suspensions
6.3 Transition Delay
7 NOMENCLATURE
8 BIBLIOGRAPHY
Integration of Special Purpose Reciprocating Compressors into a ProcessGerard B. Hawkins
1 SCOPE
2 CHOICE OF COMPRESSOR TYPE
2.1 Parameters
2.2 Preliminary Choice of Machine Type
2.3 Review of Other Types of Compressor
3 CHOICE OF NUMBER OF COMPRESSORS
3.1 Influence of Reliability Classification
3.2 Driver Considerations
3.3 Deterioration of Standby Machines
4 EFFECTS OF PROCESS GAS COMPOSITION
4.1 Particulate Contamination
4.2 Droplets in Suspension
4.3 Polymer Deposit
4.4 Molecular Weight Variation
4.5 Compressibility Variation
4.6 Gas Dryness
4.7 Gas Solution in Lubricating Oil for Cylinder and Gland
5 THROUGHPUT REGULATION
5.1 Inlet Line Throttle Valve
5.2 Inlet Line Cut-off Valve
5.3 Compressor Inlet Valve Lifter
5.4 Clearance Volume Variation
5.5 Speed Variation
5.6 Bypass
5.7 Hybrid Regulation Systems
6 PRINCIPAL FEATURES
6.1 Calculate Discharge Gas Temperature
6.2 Choice of Number of Stages
6.3 Configuration
6.4 Valve Operation Limit on Piston Speed
6.5 Limits for Mean Piston Speed
6.6 Estimation of Volumetric Efficiency
6.7 Estimation of Crankshaft Rotational Speed
6.8 Calculation of Piston Diameter
6.9 Choice of Number of Cylinders
7 DRIVER TYPE
7.1 Electric Motors
7.2 Steam Turbines
7.3 Special Drivers
8 VESSELS
APPENDICES
A RELIABILITY CLASSIFICATION
B CONDITIONS FOR LUBRICATED CYLINDERS AND GLANDS
C ESTIMATE OF LUBE OIL CONTAMINATION OF PROCESS GAS
D INFLUENCE OF GAS COMPOSITION AND MACHINE CONSTRUCTION
ON FILLED PTFE PISTON RING SEALS
E LIMITS ON GAS TEMPERATURES
FIGURES
1 SELECTION CHART
2 DESIGN SEQUENCE 1 - ESTIMATE NUMBER OF STAGES
3 DESIGN SEQUENCE 2 - ESTIMATE CYLINDER SIZES
How to Use the GBHE Mixing Guides
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 THE MIXING GUIDES
4.1 Mixing Guides
4.2 GBHE Mixing and Agitation Manual
5 DEVICE SELECTION
6 MIXING QUESTIONNAIRE
6.1 What is being mixed?
6.2 Why is it being mixed?
6.3 How is it to be mixed?
6.4 Is Heat Transfer Important?
6.5 Is Mixing Time Important?
6.6 Is Inventory Important?
6.7 Is Subsequent Phase Separation Important?
6.8 What Quantities?
6.9 What are the Selection Criteria?
6.10 What Data are required?
7 BASICS
7.1 Bulk Movement
7.2 Shear and Elongation
7.3 Turbulent Diffusion
7.4 Molecular Diffusion
7.5 Mixing Mechanisms
APPENDICES
A ROTATING MIXING DEVICES
B MIXING DEVICES WITHOUT MOVING PARTS
Centrifugal Compressors
SECTION ONE - ANTI-SURGE PROTECTION AND THROUGHPUT REGULATION
0 INTRODUCTION
1 SCOPE
2 MACHINE CHARACTERISTICS
2.1 Characteristics of a Single Compressor Stage
2.2 Characteristic of a Multiple Stage Having More
Than One Impeller
2.3 Use of Compressor Characteristics in Throughput
Regulation Schemes
3 MECHANISM AND EFFECTS OF SURGE
3.1 Basic Flow Instabilities
3.2 Occurrence of Surge
3.3 Intensity of Surge
3.4 Effects of Surge
3.5 Avoidance of Surge
3.6 Recovery from Surge
4 CONTROL SCHEMES INCLUDING SURGE PROTECTION
4.1 Output Control
4.2 Surge Protection
4.3 Surge Detection and Recovery
5 DYNAMIC CONSIDERATIONS
5.1 Interaction
5.2 Speed of Response of Antisurge Control System
6 SYSTEM EQUIPMENT SPECIFICATIONS
6.1 The Antisurge Control Valve
6.2 Non-return Valve
6.3 Pressure and flow measurement
6.4 Signal transmission
6.5 Controllers
7 TESTING
7.1 Determination of the Surge Line
7.2 Records
8 INLET GUIDE VANE UNITS
8.1 Application
8.2 Effect on Power Consumption of the Compressor
8.3 Effect of Gas Conditions, Properties and Contaminants
8.4 Aerodynamic Considerations
8.5 Control System Linearity
8.6 Actuator Specification
8.7 Avoidance of Surge
8.8 Features of Link Mechanisms
8.9 Limit Stops and Shear Links
APPENDICES
A LIST OF SYMBOLS AND PREFERRED UNITS
B WORKED EXAMPLE 1 COMPRESSOR WITH VARIABLE INLET PRESSURE AND VARIABLE GAS COMPOSITION
C WORKED EXAMPLE 2 A CONSTANT SPEED ~ STAGE COMPRESSOR WITH INTER-COOLING
D WORKED EXAMPLE 3 DYNAMIC RESPONSE OF THE ANTISURGE PROTECTION SYSTEM FOR A SERVICE AIR COMPRESSOR RUNNING AT CONSTANT SPEED
E EXAMPLE OF INLET GUIDE VANE REGULATION
FIGURES
2.1 TYPICAL COMPRESSOR STAGE CHARACTERISTIC PLOTTED WITH FLOW AT DISCHARGE CONDITIONS
2.2 TYPICAL COMPRESSOR STAGE CHARACTERISTIC PLOTTED WITH FLOW AT INLET CONDITIONS
2.3 PERFORMANCE CHARACTERISTICS OF A COMPRESSOR STAGE AT VARYING SPEEDS
2.4 SYSTEM WORKING POINT DEFINED BY INTERSECTION OF PROCESS AND COMPRESSOR CHARACTERISTICS
2.5 DISCHARGE THROTTLE REGULATION
2.6 BYPASS REGULATION
2.7 INLET THROTTLE REGULATION
2.8 INLET GUIDE VANE REGULATION
2.9 VARIABLE SPEED REGULATION
3.1 GAS PULSATION LEVELS FOR A CENTRIFUGAL COMPRESSOR
3.2 REPRESENTATION OF CYCLIC FLOW DURING SURGE OF LONG PERIOD
3.3 TYPICAL WAVEFORM OF DISCHARGE PRESSURE DURING SURGE
3.4 MULTIPLE SURGE LINE FOR A MULTISTAGE CENTRIFUGAL COMPRESSOR
3.5 TYPICAL MULTIPLE SURGE LINES FOR SINGLE STAGE AXIAL-FLOW COMPRESSOR
4.1 GENERAL SCHEMATIC FOR COMPRESSORS OPERATING IN PARALLEL TO FEED MULTIPLE USER PLANTS
4.2 ILLUSTRATION OF SAFETY MARGIN BETWEEN SURGE POINT AND SURGE PROTECTION POINT AT WHICH ANTISURGE SYSTEM IS ACTIVATED
4.3 ANTISURGE SYSTEM FOR COMPRESSOR WITH FLAT PERFO ..........
Distillation Sequences, Complex Columns and Heat IntegrationGerard B. Hawkins
Distillation Sequences, Complex Columns and Heat Integration
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 SEQUENCING OF SIMPLE COLUMNS
4.1 Sidestream Columns
4.2 Multi-Feed Columns
5 SIMPLE COLUMN SEQUENCING AND HEAT
INTEGRATION INTERACTIONS
5.1 Energy Quantity and Quality
5.2 Heat Integration within the Total Flowsheet
6 COMPLEX COLUMN ARRANGEMENTS
6.1 Indirect Sequence with Vapor Link
6.2 Sidestream Systems
6.3 Pre-Fractionator Systems
7 COMPLEX COLUMNS AND HEAT INTEGRATION
INTERACTIONS
FIGURES
1 DIRECT AND INDIRECT SEQUENCES
2 A SINGLE SIDESTREAM COLUMN REPLACING 2
SIMPLE COLUMNS
3 A TYPICAL MULTI-FEED COLUMN
4 TYPICAL GRAND COMPOSITION CURVE
5 TYPICAL INDIRECT SEQUENCE WITH VAPOUR LINK
6 SIDESTREAM STRIPPER AND SIDESTREAM
RECTIFIER
7 SIMPLEST PRE-FRACTIONATOR SYSTEM
8 SIMPLEST PRE-FRACTIONATOR SYSTEM
9 PETLYUK COLUMN
Gas Mixing
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 RECOMMENDATIONS FOR GAS MIXING:
PLUG FLOW
5 RECOMMENDATIONS FOR GAS MIXING:
BACKMIXED INITIAL ZONE
6 BIBLIOGRAPHY
Filtration
0 INTRODUCTION
1 The Theory Underlying Filtration Processes
1.1 The Mechanism of Simple Filtration Systems
1.1.2 Cake Filtration
1.1.3 Complete Blocking
1.1.4 Standard Blocking
1.1.5 Intermediate Blocking
1.2 Cake Filtration – Models and Mechanisms
1.2.1 Classical Theory for the Permeability of Porous Cakes and Beds
1.2.2 The Rate of Filtration through a Compressible Cake – The Standard Filtration Equation
1.2.3 The Compression or Consolidation of Filter Cakes – Ultimate degree of dewatering
1.2.4 The Rate of Consolidation
1.2.5 Useful Semi-Empirical Relations for Constant Pressure and Constant Rate Cake Filtration
1.2.6 Constant Pressure Filtration
1.2.7 Constant Rate Filtration
1.2.8 Multiphase Theory of Filtration
1.3 Crossflow Filtration
2 The Range and Selection of Filtration Equipment Technology
2.1 Scale
2.2 Solids Recovery, Liquids Clarification or Feed stream Concentration
2.3 Rate of Sedimentation
2.4 Rate of Cake Formation and Drainage
2.5 Batch vs Continuous Operation
2.6 Solids Loading
2.7 Further Processing
2.8 Aseptic or “Hygienic” Operation
2.9 Miscellaneous
2.10 Shear versus Compressional Deformation
2.11 Pressure versus Vacuum
3 Suspension Conditioning Prior to Filtration
3.1 Simple Filtration Aids
3.2 Mechanical Treatments
4 Post-Filtration Treatments and Further Downstream Processing
4.1 Washing
4.1.1 Air-Blowing
4.1.2 Drying
5 Testing and Characterization of Suspensions
5.1 Introduction – Suspension
5.2 Properties relevant to Filtration Performance
5.2.1 Pre-Filtration Properties of Suspension
5.2.2 Properties of Filter Cake
5.2.3 Laboratory Scale Filtration Rigs
5.3 Means of Monitoring Flocculant Dosage
5.4 Filter Cake Testing
5.4.1 Strength Testing (See also piston press described earlier)
5.4.2 Cake Permeability or Resistance
5.4.3 Rate of Cake Formation
6 Examples of the Application of the Forgoing Principles
6.1 Dewatering of Calcium Carbonate Slurries
6.2 Dewatering of Organic Products – Procion Dyestuffs
6.3 Filtration of Biological Systems – Harvesting a Filamentous Organism
References
Tables
Figures
Process Synthesis
INTRODUCTION
1 A SUGGESTED GENERAL APPROACH
2 EXAMPLES OF PROCESS SELECTION
2.1 Harvesting and Thickening of Single Cell Protein
2.2 Dewatering of a Specialty Latex
3 REFERENCES
TABLES
1 THE ADVANTAGES AND DISADVANTAGES OF DIFFERENT RANGE OF PH FOR “PROTEIN” ORGANISM FLOCCULATION
2 THE ADVANTAGES AND DISADVANTAGES OF VARYING EXTENTS OF CELL BREAKAGES
3 PREDICTED AND OBSERVED FILTER CAKE SOLIDS CONTENTS FOR THE VARIOUS LATICES AFTER COAGULATION
FIGURES
1 THE “PROTEIN” BACTERIAL HARVESTING SYSTEM
2 PROCESS FOR MANUFACTURE OF CALCIUM CARBONATE FILTERS
3 H-ACID ISOLATION
4 A SUGGESTED APPROACH TO DETERMINING FEASIBLE PROCESS OPTIONS, AND OPERATING CONDITIONS FOR SEPARATION OF FINE SOLIDS FROM SUSPENSION
5 MODULI VERSUS SOLIDS CONTENT FORTYPICAL FORWARD FLOCCULATED “PROTEIN” SUSPENSIONS
6 DECISION TREE FOR SELECTION OF AS1 HARVESTING CONDITIONS WHEN PRINCIPAL CONSTRAINT CONCERNS THE DEGREE OF THICKENING REQUIRED IN THE CONCENTRATE
7 DECISION TREE FOR SELECTION OF AS1 HARVESTING CONDITIONS WHEN PRINCIPAL CONSTRAINT CONCERNS THE USE OF FLOTATION AS A UNIT OPERATION FOR THICKENING
8 DECISION TREE FOR SELECTION OF AS1 HARVESTING CONDITIONS WHEN PRINCIPAL CONSTRAINT CONCERNS THE QUALITY OF THE RECYCLED LIQUOR
9 MODULUS SOLIDS CONTENT CURVES FOR THEVARIOUS COAGULATED LATICES
Integration of Reciprocating Metering Pumps Into A ProcessGerard B. Hawkins
Integration of Reciprocating Metering Pumps into a Process
Engineering Design Guide
1 SCOPE
2 PRELIMINARY CHOICE OF PUMP
SECTION A - TYPE/FLOW/PRESSURE/SPEED RATING
Al Pumping Pressure
A2 Pump Flowrate and Capacity
A3 Guide to Pump Speed & Type
A4 Metering Criteria
A5 Pressure Pulsation
A6 Over Delivery
SECTION B - INLET CONDITIONS
B1 Calculation of Basic NPSH
B2 Correction for Frictional Head
B3 Correction for Acceleration Head
B4 Calculation of Available NPSH
B5 Corrections to NPSH for Fluid Properties
B6 Estimation of NPSH Required
B7 Priming
SECTION C - POWER RATING
C1 Pump Efficiency
C2 Calculation of Absorbed Power
C3 Determination of Driver Power Rating
SECTION D - CASING PRESSURE RATING
Dl Calculation of Maximum Discharge Pressure
D2 Discharge Pressure Relief Rating
D3 Calculation of Pump Head Outlet Losses
D4 Casing Hydrostatic Test Pressure
APPENDICES
A RELIABILITY CLASSIFICATION
FIGURES
A3.1 ESTIMATE OF CRANK SPEED
A3.3 SELECTION OF PUMPING HEAD TYPE
B5.1 ESTIMATE OF VISCOSITY OF FINE SUSPENSIONS
B6 ESTIMATE OF NPSH REQUIRED
C1.1 GRAPH - VOLUMETRIC EFFICIENCY VS MEAN DIFFERENTIAL PRESSURE
Fluid Separation
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 A SEPARATION LOGIC TREE
5 METHODS OF DISTILLATION
5.1 Fractional Distillation
5.2 Azeotropic Distillation
5.3 Extractive Distillation
6 LIQUID-LIQUID EXTRACTION
7 OTHER COMMERCIAL METHODS OF SEPARATION
7.1 Adsorption
7.2 Fractional Crystallization
7.3 Ion Exchange
7.4 Membrane Processes
7.4.1 Ultrafiltration
7.4.2 Reverse Osmosis
7.4.3 Pervaporation
7.4.4 Liquid Membranes
7.4.5 Gas Permeation
7.4.6 Dialysis
7.4.7 Electrodialysis
7.5 Supercritical Fluid Extraction
7.6 Dissociation Extraction
7.7 Foam Fractionation
7.8 Clathration
7.9 Chromatography
8. OTHER METHODS OF SEPARATION
8.1 Precipitation
8.2 Paper Chromatography
8.3 Ligand Specific Chromatography
8.4 Electrophoresis
8.5 Isoelectric Focusing
8.6 Thermal Diffusion
8.7 Sedimentation Ultracentrifugation
8.8 Isopycnic Ultracentrifugation
8.9 Molecular Distillation
8.10 Gel Filtration
APPENDICES
A AT A GLANCE CHART BASED ON FENSKE, UNDERWOOD
B A GENERALIZED y - x DIAGRAM
C TEMPERATURE - COMPOSITION DIAGRAMS FOR
AZEOTROPIC MIXTURES
D A TYPICAL y - x DIAGRAM FOR EXTRACTIVE DISTILLATION (SOLVENT FREE BASIS)
E RAPID ESTIMATION OF LIQUID-LIQUID EXTRACTION REQUIREMENTS
F LIQUID - LIQUID EXTRACTION - THE USE OF EXTRACT REFLUX
G SELECTIVITIES REQUIRED FOR EQUAL PLANT COSTS
FIGURE
1 SEPARATION LOGIC TREE
Use and Applications of Membranes
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 GENERAL
4.1 What is a Membrane Process?
4.2 What does a Membrane look like?
4.3 Why use Membranes?
4.4 Membrane Types and Polymers Used
5 REVERSE OSMOSIS
5.1 Principles of Reverse Osmosis
5.2 Limitations
5.3 Performance
5.4 Costs
5.5 Worked Example
5.6 Applications
6 MICROFILTRATION AND ULTRAFILTRATION
6.1 Microfiltration
6.2 Ultrafiltration
7 PERVAPORATION
7.1 Classes of Application
7.2 Characteristics
7.3 Costs
7.4 Example - Lurgi Design
7.5 Application - Stripping Organics from Water
8 GAS SEPARATION AND VAPOR PERMEATION
8.1 Gas Separation
8.2 Vapor Permeation
9 LESS COMMON MEMBRANE PROCESSES
9.1 Dialysis
9.2 Electrodialysis
9.3 Electrolysis
9.4 Salt Splitting
10 BIBLIOGRAPHY
TABLES
1 UTILITY CONSUMPTION AND COST COMPARISON
Similar to Overflows and Gravity Drainage Systems (20)
Pressure Relief Systems Vol 2
Causes of Relief Situations
This Volume 2 is a guide to the qualitative identification of common causes of overpressure in process equipment. It cannot be exhaustive; the process engineer and relief systems team should look for any credible situation in addition to those given in this Part which could lead to a need for pressure relief (a relief situation).
GAS DISPERSION - A Definitive Guide to Accidental Releases of Heavy GasesGerard B. Hawkins
GAS DISPERSION - A Definitive Guide to Accidental Releases of Heavy Gases
This Process Safety Guide has been written with the aim of assisting process engineers, hazard analysts and environmental advisers in carrying out gas dispersion calculations. The Guide aims to provide assistance by:
• Improving awareness of the range of dispersion models available within GBHE, and providing guidance in choosing the most appropriate model for a particular application.
• Providing guidance to ensure that source terms and other model inputs are correctly specified, and the models are used within their range of applicability.
• Providing guidance to deal with particular topics in gas dispersion such as dense gas dispersion, complex terrain, and modeling the chemistry of oxides of nitrogen.
• Providing general background on air quality and dispersion modeling issues such as meteorology and air quality standards.
• Providing example calculations for real practical problems.
SCOPE
The gas dispersion guide contains the following Parts:
1 Fundamentals of meteorology.
2 Overview of air quality standards.
3 Comparison between different air quality models.
4 Designing a stack.
5 Dense gas dispersion.
6 Calculation of source terms.
7 Building wake effects.
8 Overview of the chemistry of the oxides of nitrogen.
9 Overview of the ADMS complex terrain module.
10 Overview of the ADMS deposition module.
11 ADMS examples.
12 Modeling odorous releases.
13 Bibliography of useful gas dispersion books and reports.
14 Glossary of gas dispersion modeling terms.
Appendix A : Modeling Wind Generation of Particulates.
APPENDIX B TABLE OF PROPERTY VALUES FOR SPECIFIC CHEMICALS
Theory of Carbon Formation in Steam Reforming
Contents
1 Introduction
2 Underpinning Theory
2.1 Conceptualization
2.2 Reforming Reactions
2.3 Carbon Formation Chemistry
2.3.1 Natural Gas
2.3.2 Carbon Formation for Naphtha Feeds
2.3.3 Carbon Gasification
2.4 Heat Transfer
3 Causes
3.1 Effects of Carbon Formation
3.2 Types of Carbon
4 What are the Effects of Carbon Formation?
4.1 Why does Carbon Formation Get Worse?
4.1.1 So what is the Next Step?
4.2 Consequences of Carbon Formation
4.3 Why does Carbon Form where it does?
4.3.1 Effect on Process Gas Temperature
4.4 Why does Carbon Formation Propagate Down the Tube?
4.4.1 Effect on Radiation on the Fluegas Side
4.5 Why does Carbon Formation propagate Up the Tube?
5 How do we Prevent Carbon Formation
5.1 The Role of Potash
5.2 Inclusion of Pre-reformer
5.3 Primary Reformer Catalyst Parameters
5.3.1 Activity
5.3.2 Heat Transfer
5.3.3 Increased Steam to Carbon Ratio
6 Steam Out
6.1 Why does increasing the Steam to Carbon Ratio Not Work?
6.2 Why does reducing the Feed Rate not help?
6.3 Fundamental Principles of Steam Outs
TABLES
1 Heat Transfer Coefficients in a Typical Reformer
2 Typical Catalyst Loading Options
FIGURES
1 Hot Bands
2 Conceptual Pellet
3 Naphtha Carbon Formation
4 Heat Transfer within an Reformer
5 Types of Carbon Formation
6 Effect of Carbon on Nickel Crystallites
7 Absorption of Heat
8 Comparison of "Base Case" v Carbon Forming Tube
9 Carbon Formation Vicious Circle
10 Temperature Profiles
11 Carbon Pinch Point
12 Carbon Formation
13 Effect on Process Gas Temperature
14 How does Carbon Propagate into an Unaffected Zone?
15 Movement of the Carbon Forming Region
16 Effect of Hot Bands on Radiative Heat Transfer
17 Effect of Potash on Carbon Formation
18 Application of a Pre-reformer
19 Effect of Activity on Carbon Formation
Calculation of an Ammonia Plant Energy Consumption: Gerard B. Hawkins
Calculation of an Ammonia Plant Energy Consumption:
Case Study: #06023300
Plant Note Book Series: PNBS-0602
CONTENTS
0 SCOPE
1 CALCULATION OF NATURAL GAS PROCESS FEED CONSUMPTION
2 CALCULATION OF NATURAL GAS PROCESS FUEL CONSUMPTION
3 CALCULATION OF NATURAL GAS CONSUMPTION FOR PILOT BURNERS OF FLARES
4 CALCULATION OF DEMIN. WATER FROM DEMIN. UNIT
5 CALCULATION OF DEMIN. WATER TO PACKAGE BOILERS
6 CALCULATION OF MP STEAM EXPORT
7 CALCULATION OF LP STEAM IMPORT
8 DETERMINATION OF ELECTRIC POWER CONSUMPTION
9 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT ISBL
10 ADJUSTMENT OF ELECTRIC POWER CONSUMPTION FOR TEST RUN CONDITIONS
11 CALCULATION OF AMMONIA SHARE IN MP STEAM CONSUMPTION IN UTILITIES
12 CALCULATION OF AMMONIA SHARE IN ELECTRIC POWER CONSUMPTION IN UTILITIES
13 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT OSBL
14 DETERMINATION OF THE TOTAL ENERGY CONSUMPTION OF THE AMMONIA PLANT
Ammonia Plant Technology
Pre-Commissioning Best Practices
GBHE-APT-0102
PICKLING & PASSIVATION
CONTENTS
1 PURPOSE OF THE WORK
2 CHEMICAL CONCEPT
3 TECHNICAL CONCEPT
4 WASTES & SAFETY CONCEPT
5 TARGET RESULTS
6 THE GENERAL CLEANING SEQUENCE MANAGEMENT
6.6.1 Pre-cleaning or “Physical Cleaning
6.6.2 Pre-rinsing
6.6.3 Chemical Cleaning
6.6.4 Critical Factors in Cleaning Success
6.6.5 Rinsing
6.6.6 Inspection and Re-Cleaning, if Necessary
7 Systems to be treated by Pickling/Passivation
Ammonia Plant Technology
Pre-Commissioning Best Practices
Piping and Vessels Flushing and Cleaning Procedure
CONTENTS
1 Scope
2 Aim/purpose
3 Responsibilities
4 Procedure
4.1 Main cleaning methods
4.1.1 Mechanical cleaning
4.1.2 Cleaning with air
4.1.3 Cleaning with steam (for steam networks only)
4.1.4 Cleaning with water
4.2 Choice of the cleaning method
4.3 Cleaning preparation
4.4 Protection of the devices included in the network
4.5 Protection of devices in the vicinity of the network
4.6 Water flushing procedure
4.6.1 Specific problems of water flushing
4.6.2 Preparation for water flushing
4.6.3 Performing a water flush
4.6.4 Cleanliness criteria
4.7 Air blowing procedure
4.7.1 Specific problems of air blowing
4.7.2 Preparation for air blowing
4.7.3 Performing air blowing
4.7.4 Cleanliness checks
4.8 Steam blowing procedure
4.8.1 Specific problems of steam blowing
4.8.2 Preparation for steam blowing
4.8.3 Performing steam blowing
4.8.4 Cleanliness checks
4.9 Chemical cleaning procedure
4.9.1 Specific problems of cleaning with a chemical solution
4.9.2 Preparation for chemical cleaning
4.9.3 Performing a chemical cleaning
4.9.4 Cleanliness criteria
4.10 Re-assembly - general guideline
4.11 Preservation of flushed piping
PRACTICAL GUIDE ON THE SELECTION OF PROCESS TECHNOLOGY FOR THE TREATMENT OF A...Gerard B. Hawkins
PRACTICAL GUIDE ON THE SELECTION OF PROCESS TECHNOLOGY FOR THE TREATMENT OF AQUEOUS ORGANIC EFFLUENT STREAMS
CONTENTS
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
3.1 IPU
3.2 AOS
3.3 BODs
3.4 COD
3.5 TOC
3.6 Toxicity
3.7 Refractory Organics/Hard COD
3.8 Heavy Metals
3.9 EA
3.10 Biological Treatment Terms
3.11 BATNEEC
3.12 BPEO
3.13 EQS/LV
3.14 IPC
3.15 VOC
3.16 F/M Ratio
3.17 MLSS
3.18 MLVSS
4 DESIGN/ECONOMIC GUIDELINES
5 EUROPEAN LEGISLATION
5.1 General
5.2 Integrated Pollution Control (IPC)
5.3 Best Available Techniques Not Entailing Excessive Costs (BATNEEC)
5.4 Best Practicable Environmental Option (BPEO)
5.5 Environmental Quality Standards(EQS)
6 IPU EXIT CONCENTRATION
7 SITE/LOCAL REQUIREMENTS
8 PROCESS SELECTION PROCEDURE
8.1 Waste Minimization Techniques (WMT)
8.2 AOS Stream Definition
8.3 Technical Check List
8.4 Preliminary Selection of Suitable Technologies
8.5 Process Sequences
8.6 Economic Evaluation
8.7 Process Selection
APPENDICES
A DIRECTIVE 76/464/EEC - LIST 1
B DIRECTIVE 76/464/EEC - LIST 2
C THE EUROPEAN COMMISSION PRIORITY CANDIDATE LIST
D THE UK RED LIST
E CURRENT VALUES FOR EUROPEAN COMMUNITY ENVIRONMENTAL QUALITY STANDARDS AND CORRESPONDING LIMIT VALUES
F ESTABLISHED TECHNOLOGIES
G EMERGING TECHNOLOGY
H PROPRIETARY/LESS COMMON TECHNOLOGIES
J COMPARATIVE COST DATA
PRACTICAL GUIDE ON THE REDUCTION OF DISCHARGES TO ATMOSPHERE OF VOLATILE ORGA...Gerard B. Hawkins
PRACTICAL GUIDE ON THE REDUCTION OF DISCHARGES TO ATMOSPHERE OF VOLATILE ORGANIC COMPOUNDS (VOCs)
FOREWORD
CONTENTS
1 INTRODUCTION
2 THE NEED FOR VOC CONTROL
3 CONTROL AT SOURCE
3.1 Choice or Solvent
3.2 Venting Arrangements
3.3 Nitrogen Blanketing
3.4 Pump Versus Pneumatic Transfer
3.5 Batch Charging
3.6 Reduction of Volumetric Flow
3.7 Stock Tank Design
4 DISCHARGE MEASUREMENT
4.1 By Inference or Calculation
4.2 Flow Monitoring Equipment
4.3 Analytical Instruments
4.4 Vent Emissions Database
5 ABATEMENT TECHNOLOGY
5.1 Available Options
5.2 Selection of Preferred Option
5.3 Condensation
5.4 Adsorption
5.5 Absorption
5.6 Thermal Incineration
5.7 Catalytic Oxidation
5.8 Biological Filtration
5.9 Combinations of Process technologies
5.10 Processes Under Development
6 GLOSSARY OF TERMS
7 REFERENCES
Appendix 1. Photochemical Ozone Creation Potentials
Appendix 2. Examples of Adsorption Preliminary Calculations
Appendix 3. Example of Thermal Incineration Heat and Mass Balance
Appendix 4. Cost Correlations
Getting the Most Out of Your Refinery Hydrogen PlantGerard B. Hawkins
Getting the Most Out of Your Refinery Hydrogen Plant
Contents
Summary
1 Introduction
2 "On-purpose" Hydrogen Production
3 Operational Aspects
4 Uprating Options on the Steam Reformer
4.1 Steam Reforming Catalysts and Tube Metallurgy
4.2 Oxygen-blown Secondary Reformer
4.3 Pre-reforming
4.4 Post-reforming
5 Downstream Units
6 Summary of Uprating Options
7 Conclusions
EMERGENCY ISOLATION OF CHEMICAL PLANTS
CONTENTS
1 Introduction
2 When should Emergency Isolation Valves be Installed
3 Emergency Isolation Valves and Associated Equipment
3.1 Installations on existing plant
3.2 Actuators
3.3 Power to close or power to open
3.4 The need for testing
3.5 Hand operated Emergency Valves
3.6 The need to stop pumps in an emergency
3.7 Location of Operating Buttons
3.8 Use of control valves for Isolation
4 Detection of Leaks and Fires
5 Precautions during Maintenance
6 Training Operators to use Emergency Isolation Valves
7 Emergency Isolation when no remotely operated valve is available
References
Glossary
Appendix I Some Fires or Serious Escapes of Flammable Gases or Liquids that could have been controlled by Emergency Isolation Valves
Appendix II Some typical Installations
Amine Gas Treating Unit - Best Practices - Troubleshooting Guide Gerard B. Hawkins
Amine Gas Treating Unit Best Practices - Troubleshooting Guide for H2S/CO2 Amine Systems
Contents
Process Capabilities for gas treating process
Typical Amine Treating
Typical Amine System Improvements
Primary Equipment Overview
Inlet Gas Knockout
Absorber
Three Phase Flash Tank
Lean/Rich Heat Exchanger
Regenerator
Filtration
Amine Reclaimer
Operating Difficulties Overview
Foaming
Failure to Meet Gas Specification
Solvent Losses
Corrosion
Typical Amine System Improvements
Degradation of Amines and Alkanolamines during Sour Gas Treating
APPENDIX
Best Practices - Troubleshooting Guide
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Keynote at DIGIT West Expo, Glasgow on 29 May 2024.
Cheryl Hung, ochery.com
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Rapid and secure feature delivery is a goal across every application team and every branch of the DoD. The Navy’s DevSecOps platform, Party Barge, has achieved:
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Bob Boule
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The Art of the Pitch: WordPress Relationships and Sales
Overflows and Gravity Drainage Systems
1. GBH Enterprises, Ltd.
Process Engineering Guide:
GBHE-PEG-FLO-301
Overflows and Gravity Drainage
Systems
Information contained in this publication or as otherwise supplied to Users is
believed to be accurate and correct at time of going to press, and is given in
good faith, but it is for the User to satisfy itself of the suitability of the information
for its own particular purpose. GBHE gives no warranty as to the fitness of this
information for any particular purpose and any implied warranty or condition
(statutory or otherwise) is excluded except to the extent that exclusion is
prevented by law. GBHE accepts no liability resulting from reliance on this
information. Freedom under Patent, Copyright and Designs cannot be assumed.
Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / Shutdown
Activation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & Mass
Balance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst Performance
Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
2. Process Engineering Guide:
Overflows and Gravity
Drainage Systems
CONTENTS
Section
0
INTRODUCTION/PURPOSE
2
1
SCOPE
2
2
FIELD OF APPLICATION
2
3
DEFINITIONS
2
4
OUTLINE OF THE PROBLEM
2
5
DESIGNING FOR FLOODED FLOW
4
6
DESIGNING NON-FLOODED PIPELINES
5
6.1
6.2
6.3
6.4
Vertical Pipework
From the Side of a Vessel
Established (uniform) Flow in Near-horizontal Pipes
Non-uniform Flow
5
6
9
11
7
NON-FLOODED FLOW IN COMPLEX SYSTEMS
11
8
ENTRAINING FLOW
13
9
SIMPLE TANK OVERFLOWS
14
9.1
Venting of the Tank
14
10
BIBLIOGRAPHY
14
11
NOMENCLATURE
15
TABLE
1
GEOMETRICAL FUNCTIONS OF PART-FULL PIPES
9
FIGURES
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Balance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst Performance
Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
3. 1
TYPICAL SEQUENCE OF SURGING FLOW
3
2
DESIGNING FOR FLOODED FLOW
5
3
CAPACITY OF SLOPING PIPELINES
7
4
OVERFLOW FROM SIDE OF VESSEL
8
5
METHODS OF AVOIDING LARGE CIRCULAR SIDE
OVERFLOWS
8
CAPACITY OF A GENTLY SLOPING PIPE AS A FUNCTION
OF LIQUID DEPTH
10
7
COMPLEX PIPE SYSTEMS
12
8
REMOVAL OF ENTRAINED GASES
13
DOCUMENTS REFERRED TO IN THIS PROCESS
ENGINEERING GUIDE
16
6
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Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
4. 0
INTRODUCTION / PURPOSE
Gravity drainage systems occur frequently on chemical plants. Typical
examples are:
(a)
the condensate off-take from a condenser;
(b)
the liquid off-take from the base of an absorption column;
(c)
the emergency overflow from an atmospheric pressure storage
tank.
Gas entrained in a liquid flowing by gravity from a vessel will reduce the volume
of liquid flowing through the pipe and could cause surging flows.
1
SCOPE
This Process Engineering Guide (PEG) describes the problems which are
associated with gravity systems and recommends design criteria to avoid
such problems.
2
FIELD OF APPLICATION
This Guide applies to the process engineering community in GBH
Enterprises worldwide.
3
DEFINITIONS
For the purposes of this Guide no specific definitions apply.
4
OUTLINE OF THE PROBLEM
Whenever liquid flows by gravity out of a vessel or down a pipe there is a
potential problem of entrainment of gas by the liquid. Apart from any
process concerns:
(a) Entrained gas not only raises the pressure drop above the single
phase value but also reduces the static head available to drive the
flow. These effects can reduce the flow rate drastically below the
design value.
Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / Shutdown
Activation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & Mass
Balance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst Performance
Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
5. (b)
Entrained gas can give rise to unsteady flow conditions (surging)
which, in extreme cases, can result in equipment failure. Figure 1
shows a typical sequence which may occur for an absorption
column with an undersized liquid outlet.
A further description of gravity drainage problems and a review of
published information. For information on flow in partially filled nearhorizontal channels, consult a suitable fluid mechanics textbook
(e.g. see 10(a)).
Three approaches to the design of gravity systems are possible, namely:
(1)
The system can be designed to run full bore at all times. Single phase
criteria can then be used for pipework sizing.
(2)
The system can be designed to be self venting. Liquid velocities are kept
sufficiently low to allow any entrained gas to flow countercurrent to the
liquid flow.
(3)
Gas entrainment can be allowed to occur and the system designed to
accommodate potential problems.
In general, approach (1) can be expected to result in the smallest pipe sizes and
should be considered first. However, in many instances it is not possible to
ensure full pipe flow and the methods contained in Clauses 5, 6 and 7 should be
adopted.
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Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
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6. FIGURE 1
TYPICAL SEQUENCE OF SURGING FLOW
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Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
7. In this Guide, liquid flowrates are generally expressed in terms of a
dimensionless superficial volumetric flux j*L defined by:
This is similar in form to a Froude number. It is used in preference to the
Froude number, which has several different definitions depending on
circumstances.
Note:
At low pressures ρL >>ρG and g' ~ g
All equations in this Guide are based on units as shown in Clause 11.
5
DESIGNING FOR FLOODED FLOW
If at all times the pipeline runs full of liquid, then normal single phase
methods can be used for sizing the pipework. In order to avoid gas
entrainment, the liquid in the vessel should be maintained at such a level
as to keep the pipe inlet submerged, allowing for depression of the surface
near to the outlet.
Criteria for flooded outlets are as follows:
(a) For outlets from the base of vessels:
where h is the liquid depth in the vessel away from the region of the outlet.
This equation assumes irrotational flow. Vortexing can result in gas
entrainment even if the minimum depth is achieved (the ’bath plug’ effect).
A vortex breaker should be used to prevent this. A suitable design is
shown on Standard Sheet 11 0050. Detailed guidelines for the optimum
sizing of vortex breakers are contained in the documents quoted in 10(b)
and 10(c).
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Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
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8. (b) For outlets from the side of vessels
where h is the liquid height above the top of the outlet away from the
region of the outlet.
In order to ensure that the surface is maintained above the required level
some form of control may be necessary. This could be via a control valve
or a lute. Such devices will increase the system pressure drop and to
some extent reduce the benefits of going to flooded flow. If a lute
is used a siphon break may be necessary; pipework downstream of the
siphon break cannot be assumed to run flooded.
Single phase design criteria can also be applied to sections of gravity
drainage systems where it is certain the pipe is flooded. If these sections
are preceded by a self venting vertical section, a minimum length for
disengagement of 0.5 m should be provided before reducing the pipe
diameter to the single phase value.
Figure 2 shows some examples of systems designed for flooded flow.
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Activation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & Mass
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Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
9. Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / Shutdown
Activation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & Mass
Balance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst Performance
Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
10. 6
DESIGNING NON-FLOODED PIPELINES
6.1
Vertical Pipework
A slug of gas will be entrained in a liquid flowing down a vertical pipe if the
value of j*L exceeds about 0.32. For values of j*L less than this, the gas
slug will rise against the liquid flow. This forms the basis of the design
method for self venting flow, which is that j*L should be less than 0.3.
The capacity of a pipe designed for j*L = 0.3 is shown on Curve 1 of
Figure 3.
Although designing to this criterion will avoid gross entrainment of gas in
the form of slugs, it will not prevent entrainment of small bubbles whose
Stokes Law velocity is less than the liquid velocity.
6.2
From the Side of a Vessel
If a liquid is flowing from the side of a vessel into a partly full circular pipe
inclined at more than a critical slope, the flow in the entrance region will be
’critical’, with a Froude number (defined as the ratio of the surface wave
speed to the actual liquid velocity) of one. With a value of j*L of 0.3, the
pipe entrance will be less than half full and the liquid level in the stagnant
region away from the overflow will be less than 80% of the pipe diameter
above the bottom of the pipe (see Figure 4). Thus the same design
criterion can be used as for vertical pipes.
The critical slope to ensure critical flow in the entrance region decreases
with pipe diameter and increases with the depth of liquid in the pipe.
However, for the range of pipe sizes used in practice, and assuming
typical pipe roughnesses, the critical slope is always less than 1:100.
For design purposes, a minimum slope of 1:40 is recommended for the
off-take pipework, although civil engineering installations such as drains
are often designed to a fall of 1:100.
The use of an overflow from near the top of a vessel, sized for a large
flowrate, requires the provision of considerable extra height on the vessel
above the maximum working level, which may be expensive.
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Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
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11. Two ways are suggested for avoiding this, namely:
(a) Provide a vertical stand-pipe within the vessel, sized by the methods
detailed in 6.1 (see also Figure 5(a)).
(b) Replace the circular side branch by a 'letter box' (see Figure 5(b)).
The liquid height over the base of such an outlet is given by the weir
formula:
where W is the width of the weir.
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Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
12. Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / Shutdown
Activation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & Mass
Balance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst Performance
Characterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /
Process Technology – Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology – Petrochemicals
Specializing in the Development & Commercialization of New Technology in the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
13. Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / Shutdown
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14. 6.3
Established (uniform) Flow in Near-horizontal Pipes
For a uniform (i.e. constant depth) flow in a partially filled inclined pipe, the
energy lost by friction is balanced by the potential energy change due to
the inclination of the pipe. The mean velocity is related to the inclination
and depth of flow by the equation:
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15. Figure 3 gives the volumetric capacity for established flow in half full and
three quarters full rough and smooth pipes. The curves were calculated
from equation (5) for pipes of slope 1:40 and a fluid with kinematic
viscosity of 10-6 m2/s (e.g. water at 20°C). The absolute roughness
used for the rough pipes was 0.25 mm (moderately rusty carbon steel).
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16. The results are not very sensitive to liquid viscosity; the capacity of a
rough pipe is increased by about 1% for an inviscid fluid, and reduced by
about 10% for a fluid with a kinematic viscosity of 10-5 m2/s.
Thus the curves can safely be used for most liquids.
Figure 6 shows the variation in capacity of a sloping pipe as a function of
relative depth. The peak capacity occurs for a relative depth of
approximately 0.95. Operating beyond the peak represents an unstable
situation, where an increase in depth causes a fall-off in capacity. It is
recommended that partially full pipes be limited to a relative depth of 0.75.
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17. FIGURE 6
CAPACITY OF A GENTLY SLOPING PIPE AS A FUNCTION OF
LIQUID DEPTH
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18. 6.4
Non-uniform Flow
The velocity of fluid in the off-take from a vessel designed to run half full (
j*L= 0.3) is less than the equilibrium value for a pipe with a slope greater
than the critical value. The liquid accelerates down the pipe, the depth
falling with distance towards the depth corresponding to established flow
at the given flowrate.
This reduction in depth with distance gives the possibility of reducing the
pipe size for long near-horizontal pipes. To do this safely, it is necessary
to solve the energy equation to determine the change in relative depth
with distance. The following design method is based on this approach.
(a) Size the off-take branch on the side of the vessel for j*L = 0.3 (Curve 1
of Figure 3). If this is a non-standard pipe size, choose the next standard
size above the calculated value. Continue this size for at least ten pipe
diameters.
(b) Determine the pipe diameter corresponding to half full established flow for
the required flowrate (use Curve 2A or 2B of Figure 3). Again select the
nearest standard size above the calculated value.
(c) Reduce the pipe size from the off-take size to the established size using
an eccentric reducer such that there is no change in the slope of the
bottom of the pipe. The reducer should have a minimum length of twice
the upstream diameter.
If this procedure is followed for pipes of slope 1:40, the liquid depth straight
after the reducer will not exceed 75% of the reduced pipe diameter.
For long inclined pipes it may be worth considering a second reduction down
to the size corresponding to an established flow relative depth of 0.75. This
reduction can take place after a further fifty diameters.
For short pipe runs the additional cost of tapered reducers, especially if made
with a gentle angle as recommended, which may be non-standard, or with
lined pipe, may exceed the savings achieved by use of smaller bore
pipework. In such cases the pipe should be run in the large size throughout.
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19. 7
NON-FLOODED FLOW IN COMPLEX SYSTEMS
There is little information available on non-flooded flow in systems
including bends, especially for changes from vertical to near horizontal
flow or vice versa. What evidence there is suggests that even if the pipe
diameter is chosen for self venting flow as detailed in Clause 6,
entrainment and surging may still occur due to the effects of the bends. As
a result the following design recommendations are only tentative.
All nominally horizontal sections should have a minimum slope of 1:40.
Bends in the ’horizontal’ plane are not expected to cause problems
provided the slope of 1:40 is continued round the bend and the bend is
gentle (say radius equals five diameters).
In the vertical plane, the number of bends should be reduced as far as
possible. Vertical sections should be replaced by gently sloping sections if
practicable. Bends should have a minimum radius of five diameters.
Vertical pipework, including bends from or to vertical sections, should be
sized for j*L < 0.3. Long inclined pipes can be sized for half full established
flow by the criteria given in 6.4, but should be increased back to the full
diameter before any vertical sections. Changes in diameter should be by
asymmetric tapered reducers of length equal to twice the larger diameter
and arranged such that the bottom of the reducer has a slope equal to that
of the pipework on either side. Figure 7 illustrates some of these points.
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21. Surging and similar problems caused by gas entrainment can sometimes
be reduced by providing a means for gas escape at key points. It may be
necessary to provide some form of gas/liquid separator at these points.
This may enable most of the pipework to be designed to a smaller size.
However, it should be remembered that it is not possible to predict the
degree of gas entrainment that would result and hence the pressure drop
cannot be calculated with any certainty. Two possible methods for the
removal of entrained gases are shown in Figure 8.
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22. 8
ENTRAINING FLOW
If the liquid flowrate is such that j*L exceeds 0.3 then the liquid will tend to
carry gas forward with it. The established film thickness for a falling film
flow can be calculated from the equation:
provided the film is thin compared with the pipe diameter. For j*L = 2 this
gives a relative film thickness of 0.11. However, in the entry region the film
thickness will be greater than this and bridging of the pipe may occur.
Simpson (see 10(d)), in experiments with a 13/16 inch vertical pipe, open
at the bottom and fed through a bend at the top, found the vertical pipe ran
full at j*L = 2. However, a simple vertical pipe of typical roughness, open at
both ends, with the frictional resistance balancing the gravitation, will run
full with a liquid flow equivalent to j*L = 10. Operation with j*L > 0.3 tends
to give intermittent flow with severe entrainment and slugging, especially if
there is no easy escape path for the gas. It is not recommended for other
than simple systems.
9
SIMPLE TANK OVERFLOWS
Although the self venting criterion represents a safe design basis, it often
results in a requirement for very large, and hence expensive, overflows. It
has been recognized for some time that there are many cases where such
a design is unnecessary, and a smaller size of overflow would suffice.
Because of this, and the absence of any firm guidelines, an experimental
program was undertaken using overflows of 2" diameter with water as the
liquid. Although it is recognized that this size is small compared with many
overflow systems, Dr P B Whalley of Oxford University, one of the world’s
leading authorities on two phase flow, considered that any extrapolation of
the conclusions to larger pipe sizes was likely to be conservative. This is
because slug flow in large diameter tubes tends to be unstable, and the
slug velocity tends to be greater than that given in 6.1. Note however that
sizeable bubbles of gas could still be dragged down by the liquid flow even
if full size slugs could not. The recommendations are based on this
consideration and the method is subject to the following constraints:
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23. (a) The overflow should be simple; that is, it should consist of a side outlet
followed immediately by a vertical pipe to grade. There may be a seal
pot on the base if required. Overflows which include several bends
and/or are proceeded by tortuous routes are excluded from this
method.
(b) Entrainment of gas from the tank into the overflow is allowable.
(b) Intermittent or variable flow in the overflow is permissible.
(c) Some variation in the level of liquid in the tank during the
overflow operation is acceptable.
(d) The tank is fitted with an adequate venting/in-breathing system
(see 9.1).
Provided that the above criteria are met, the overflow can be sized to have
half the diameter of an overflow sized for self venting flow at the same
flowrate by the method given in Clause 6.
If the above criteria cannot be met, it is recommended that the overflow be
designed to be self venting.
9.1
Venting of the Tank
A non-self venting overflow designed by the method detailed in Clause 9
can act as an efficient ejector, sucking gas from the vapor space above
the liquid level. It is therefore essential that adequate provision be made
for in-breathing. It is not possible to estimate with any certainty the
required in-breathing rate. However, a maximum can be placed upon it.
This is obtained by assuming that at some stage during the venting cycle
the overflow will be running full bore. The corresponding flowrate can be
obtained by balancing the head from the liquid level to the bottom of the
overflow against frictional losses in the pipework. It will be found that this
maximum flowrate is up to 30 times the mean rate. However, the provision
of a vent to allow inbreathing at this rate does not usually represent a
serious problem.
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24. 10
BIBLIOGRAPHY
(a) J K Vennard ’Elementary Fluid Mechanics’ 4th Edition,
Chapter 10, Wiley, 1962.
(b) F M Patterson, Oil & Gas Journal, August 4th, 1969, Page 118.
(c) S Waliullah, Chemical Engineering, May 9th, 1988, Page 108.
(d) L L Simpson ’Sizing Piping for Process Plants’ Chemical
Engineering, 75 No13, Page 19, 2 June 1968.
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25. 11
NOMENCLATURE
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26. DOCUMENTS REFERRED TO IN THIS PROCESS ENGINEERING GUIDE
This Process Engineering Guide makes reference to the following documents:
STANDARD SHEET
Vortex Breakers. Carbon Steel and Stainless Steel (referred to in Clause 5(a))
GBHE REPORT
Gravity Flow of Liquids in Pipes (referred to in Clause 4).
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