Paper dryers are occasionally shut down for periods of time ranging from a few hours to many months. It important that proper procedures be followed when shutting down dryers to be sure that the process is complete and appropriate for the duration of the shutdown.
Basics of Self-Supported Rotary Joint Installation on Steam-Heated Paper DryersKadant Inc.
Long service life of rotary joints and adjacent flexible hoses can be achieved by following basic installation guidelines. This is particularly important with self-supported rotary pressure joints that are used for paper dryers. General installation guidelines are provided.
Carbide Doctor Blades on Ceramic Press RollsKadant Inc.
Ceramic press rolls have become popular choices for improving papermaking efficiency and product quality. The proper selection and use of ceramic-tipped doctor blades and cleaning shower systems is critical in getting the highest performance from these rolls.
This document provides an overview of the paper manufacturing process. It discusses (1) preparing wood through debarking, chipping, and screening, (2) cooking the wood chips using chemicals like sodium hydroxide and sodium sulfide to break down lignin, (3) washing, screening, and bleaching the pulp to remove remaining lignin and impurities, and (4) the final paper making process of forming sheets from the pulp. Key aspects of bleaching include oxygen delignification to reduce lignin content followed by chlorine dioxide or chlorine-free bleaching to achieve a bright, high quality pulp for paper production.
Dryer Surface Temperature Response CharacteristicsKadant Inc.
This paper reviews data on thermal response of a dryer cylinder to changes in heat load (sheet break simulation) and to changes in dryer steam pressures. It also shows the improvements that are possible with the application of Turbulator® bars and advanced dryer section control.
Troubleshooting Flooding of Paper DryersKadant Inc.
The document discusses causes and troubleshooting of paper dryer flooding. It describes how condensate forms and needs to be drained from the dryer. Flooding occurs when drainage is insufficient and condensate builds up. Potential causes include issues with the syphon shoe design or installation, erosion of parts, or leaks that interfere with proper drainage. Troubleshooting involves checking for problems with the mechanical components or steam supply system that could disrupt the drainage process.
Glitter is recent developed printing. Glitter is a unique, clear digital print and cut material for full-color printing that adds the bold look of sparkly glitter. Glitters add on the garment with paste and fixed by heat on a specific area.
The document provides an overview of modern papermaking processes. It covers various paper and board grades, their compositions, and the properties contributed by different fiber types. The papermaking process is described, including stock preparation, forming, pressing, drying, and finishing. Recovered fiber usage and deinking processes are also discussed. Key factors that influence paper quality such as fiber length and type are explained.
Paper dryers are occasionally shut down for periods of time ranging from a few hours to many months. It important that proper procedures be followed when shutting down dryers to be sure that the process is complete and appropriate for the duration of the shutdown.
Basics of Self-Supported Rotary Joint Installation on Steam-Heated Paper DryersKadant Inc.
Long service life of rotary joints and adjacent flexible hoses can be achieved by following basic installation guidelines. This is particularly important with self-supported rotary pressure joints that are used for paper dryers. General installation guidelines are provided.
Carbide Doctor Blades on Ceramic Press RollsKadant Inc.
Ceramic press rolls have become popular choices for improving papermaking efficiency and product quality. The proper selection and use of ceramic-tipped doctor blades and cleaning shower systems is critical in getting the highest performance from these rolls.
This document provides an overview of the paper manufacturing process. It discusses (1) preparing wood through debarking, chipping, and screening, (2) cooking the wood chips using chemicals like sodium hydroxide and sodium sulfide to break down lignin, (3) washing, screening, and bleaching the pulp to remove remaining lignin and impurities, and (4) the final paper making process of forming sheets from the pulp. Key aspects of bleaching include oxygen delignification to reduce lignin content followed by chlorine dioxide or chlorine-free bleaching to achieve a bright, high quality pulp for paper production.
Dryer Surface Temperature Response CharacteristicsKadant Inc.
This paper reviews data on thermal response of a dryer cylinder to changes in heat load (sheet break simulation) and to changes in dryer steam pressures. It also shows the improvements that are possible with the application of Turbulator® bars and advanced dryer section control.
Troubleshooting Flooding of Paper DryersKadant Inc.
The document discusses causes and troubleshooting of paper dryer flooding. It describes how condensate forms and needs to be drained from the dryer. Flooding occurs when drainage is insufficient and condensate builds up. Potential causes include issues with the syphon shoe design or installation, erosion of parts, or leaks that interfere with proper drainage. Troubleshooting involves checking for problems with the mechanical components or steam supply system that could disrupt the drainage process.
Glitter is recent developed printing. Glitter is a unique, clear digital print and cut material for full-color printing that adds the bold look of sparkly glitter. Glitters add on the garment with paste and fixed by heat on a specific area.
The document provides an overview of modern papermaking processes. It covers various paper and board grades, their compositions, and the properties contributed by different fiber types. The papermaking process is described, including stock preparation, forming, pressing, drying, and finishing. Recovered fiber usage and deinking processes are also discussed. Key factors that influence paper quality such as fiber length and type are explained.
Vibration Characteristics in Cantilever Stationary SyphonsKadant Inc.
Most high-speed paper machine dryers operate with stationary cantilever syphons and dryer bars. Modern cantilever stationary syphons are rigidly mounted to the dryer bearing housings and they provide a reliable system of support. Dryer bars provide for high rates of heat transfer with excellent heat transfer and profile uniformity.
Thermocompressors use high-pressure steam to raise the pressure of low-pressure steam for use in dryers. They must be properly sized to match the application, as oversized thermocompressors can operate with inadequate control and vent excess steam. Installing dryer bars on low-speed dryers can reduce energy consumption by lowering the machine's rimming speed and reducing drive load. Monitoring dryer section ventilation systems by checking temperature rises and drops can indicate issues that increase energy usage like dirty filters or un draining steam coils. Non-contact dryers that do not touch the paper sheet should be disconnected from steam service to prevent wasted blow-through steam.
Benefits of online porosity measurement feb 2018Pekka Komulainen
Online porosity measurement provides a way to optimize papermaking processes and ensure consistent paper quality. Porosity is influenced by many process parameters from stock preparation to the drying section. Maintaining a constant porosity indicates that the papermaking process is performing well and producing paper with consistent physical properties. While online and laboratory porosity measurements can differ due to factors like web speed and dwell time, monitoring porosity online allows the identification of quality issues and process deviations.
Pulp and Paper Manufacturing and Treatment Of Waste Water
is About:
What is Fiber?
Lignin?Hemicellouse?
Real Explanation of Photosynthesis?
SEM (Scanning Electronic Microscope) Pictures of Trees
Can Plants Survive in Green Light?
How the Pulp is Produced from The Trees (Video) ?
Can We Use Other Than Trees for Pulp Preparation?
Some Information about Locally Located oldest Paper Mills
How the Waste Water Treated from Industries?
The document describes the key components and processes of a paper machine. It discusses the wet end which includes stock preparation and transport to the headbox. It then explains the headbox, wire section for initial dewatering, press section for further dewatering including conventional, German and shoe presses. Drying sections are described next for heating and drying the paper web. A size press is included to make the surface water repellent before winding the finished paper onto large reels. Water is circulated throughout the entire papermaking process.
The document describes the process of paper production, including:
1) Wood fibers are the main raw material and are unlocked from surrounding tissue through mechanical or chemical processes to produce pulp.
2) The pulp is refined, additives are mixed in, and the slurry is formed into a continuous web on a paper machine where water is removed through several sections.
3) Key factors that determine paper properties are fiber length and orientation, degree of refining, and additives used. The paper making process produces a fiber-oriented sheet with different characteristics on each side.
The document describes a cylinder dryer machine used for drying fabrics. It uses indirect drying through heated stainless steel cylinders. The fabric moves over several heated drums where it is dried at temperatures of 120-130°C using steam at pressures of 1-3 atm. This is an efficient and low-cost drying method suitable for intermediate drying of flat fabrics that cannot withstand high tension. The main components of the cylinder dryer are the hollow cylinders, guide rollers, free rollers and pin rollers. Proper maintenance such as checking motor RPM, even heating of cylinders, and ensuring smooth roller movement is important.
This document discusses water saving technology in the textile industry. It proposes using solophenyl dyes for dyeing cotton and cotton-polyester blends, which can save significant amounts of water compared to conventional reactive dyes. For 100% cotton fabrics, solophenyl dyes can reduce water consumption from 60-80 liters/kg to 20-30 liters/kg. For cotton-polyester blends, a one-batch dyeing process using solophenyl dyes has the potential to save water consumption from 120-140 liters/kg down to 30-40 liters/kg. Adopting these new dyeing techniques could help textile factories minimize their environmental impact and reduce production costs.
production of denim fabrics using rope dyeing and slasher dyeing methods: a c...Yousuf Ali
This document compares the slasher and rope methods of denim production. It finds that the rope method requires more floor space and manpower but produces denim at a higher rate with less breakage and wastage than the slasher method. Key differences are that the rope method allows for stripe fabrics, has better tensile strength and color fastness, but higher costs. The slasher method uses higher counts and has more consistent shades but higher breakage rates.
Potassium permanganate spray is done on jeans to take a bright effect on sand blast area. One important thing about potassium permanganate spray is, this is usually a sporting process to increase the effect of sand blast and which is one of the most important process i denim washing.
This document discusses strategies for optimizing vacuum in the wire part of a paper machine to conserve energy. It notes that increasing vacuum and dwell time can increase dryness up to a point, after which gains are minimal. Recommendations include applying vacuum in increasing order with the highest vacuum in the last box and reducing open area and peak vacuum where dryness is not significantly affected. Reducing dwell time from excessive levels like 150ms down to 10-15ms can substantially reduce air flow needs and energy consumption. Replacing vacuum pumps or installing more efficient options like roots blowers or variable frequency drives can achieve further savings. Proper design optimization of vacuum and the wire table offers significant potential for increased energy efficiency and improved wire life.
Dimas DP Nugroho presented on pulping technology fundamentals. He has an engineering background in chemical engineering and the pulp and paper industry. He has worked in various roles in pulp mills in Indonesia and conducted research in Canada. The presentation covered the pulping processes of kraft, mechanical, semi-chemical, and dissolving pulps. It discussed the steps of wood handling, chipping, cooking, washing, bleaching, and drying of pulp. Key process parameters that control pulp quality at each stage were also summarized.
Dryer doctors have a number of purposes in a paper machine dryer section: sheet shedding, dryer surface cleaning, threading, and air handling and control. Paper dryer doctors are often overlooked in the papermaking process, but they need proper attention to maintain efficient dryer operation.
Disperse dyes are used to dye polyester fabrics. They are not soluble in water and must be dispersed using a dispersing agent. There are various types of disperse dyes classified by their energy level, which determines their suitability for different dyeing processes like high temperature exhaust dyeing or printing. Key factors for disperse dyes include good dispersion stability, build-up, and fastness properties. Dyeing processes for polyester include batchwise, high temperature, carrier, and continuous dyeing. When dyeing polyester/cellulose blends, both portions can be dyed together or separately in one or two baths. Continuous dyeing uses pad-steam methods with thermosol fixation. Pro
The document summarizes the key steps and components in the paper manufacturing process using a paper machine. It describes the basic components of the paper machine including the headbox, which deposits the pulp slurry onto the wire screen, and the fourdrinier wet end, where water is removed from the web through gravity, foils, and suction before entering the press and dryer sections. It provides details on key components in the wet end like the slice, forming board, table rolls, and couch roll that work to remove water and form the paper web.
The document discusses the properties and dyeing of aramid fibers such as Technora, Conex, and Kevlar. It describes how aramid fibers have good heat resistance, strength and chemical resistance but are difficult to dye. Pretreating the fibers with liquid ammonia or using polar solvents can increase dye uptake. The document also examines different dyeing methods and how parameters like temperature, time and solvent selection affect the dyeing process and properties of the dyed fibers.
The ninth lecture in the module Particle Technology, delivered to second year students who have already studied basic fluid mechanics. The different mechanisms for the removal of dust from gases are covered and the design equations used for control, modelling and understanding of the equipment are presented and derived. Examples of industrial equipment for gas cleaning are included.
Crescentformer general process. tissue machine VoithNelson Izaguirre
CRESCENT FORMER
The Crescent Former is the culmination of technological improvements derived from our experience in the manufacturing of four machines since the 1960s (Plain Wire; Sloped Wire; Twin Wire C-Former; and Twin Wire S-Former). The first Crescent Former was invented in the 1970s by the multinational Kimberly Clark which held the patent until the Nineties.
Our technological innovations and more than 50 years of experience in the field of tissue ensure the highest levels of performance from the Recard Crescent Former.
Each Recard Crescent Former is designed to optimize the real operating speed of your production line. We have achieved performance of over 2000 meters per minute.
This document provides information on the Benfield process for removing carbon dioxide from gas streams. It discusses key aspects of the process including:
- Absorption of CO2 into a potassium carbonate solution and regeneration of the solution by heating.
- Use of an activator like DEA to improve CO2 absorption.
- Comparison with other CO2 removal processes like Rectisol and considerations for process selection.
- Parameters that affect the absorption and regeneration steps like pressure, temperature, and flow rates.
- Causes and prevention of corrosion in the system through vanadium addition and factors that can cause foaming of the solution.
1. Fine, dusty clinker leads to segregation in the kiln and non-uniform clinker beds in coolers due to differences in particle size and density.
2. When high-velocity cooling air hits closely-packed fine clinker dust, the air is heated, expands, and fluidizes the dust causing it to flow rapidly down the cooler in a "red river."
3. Newer cooler designs use stationary inclined grates and mechanical air flow regulators to better control air distribution and reduce issues caused by red rivers of fine, hot clinker dust.
NONLINEAR MODEL PREDICTIVE CONTROL FOR OPERATION OF A POST COMBUSTION ABSORPT...Modelon
This document summarizes research on developing a nonlinear model predictive control (NMPC) strategy for optimizing the operation of a post-combustion carbon capture unit. Key points:
1) Researchers created a detailed Modelica model of an amine-based carbon capture process but reduced it to improve computational efficiency for real-time optimization.
2) The reduced model was validated against experimental plant data and found to accurately capture system dynamics and behavior.
3) JModelica.org was used to perform offline optimizations of the reduced model, minimizing costs while satisfying operational constraints.
4) Preliminary results showed the NMPC approach was able to optimize reboiler duty and maintain a target carbon
The document provides an overview of reservoir simulation and performance analysis methods. It discusses static and dynamic reservoir modeling, including history matching and prediction. The key points covered are:
1) Reservoir simulation involves building static and dynamic reservoir models to match historical production and predict future performance.
2) History matching is used to validate the simulation model by comparing calculated pressures, saturations, and production to historical data.
3) After achieving a match, the model can be used to predict future field performance under different development scenarios and identify new infill locations.
Vibration Characteristics in Cantilever Stationary SyphonsKadant Inc.
Most high-speed paper machine dryers operate with stationary cantilever syphons and dryer bars. Modern cantilever stationary syphons are rigidly mounted to the dryer bearing housings and they provide a reliable system of support. Dryer bars provide for high rates of heat transfer with excellent heat transfer and profile uniformity.
Thermocompressors use high-pressure steam to raise the pressure of low-pressure steam for use in dryers. They must be properly sized to match the application, as oversized thermocompressors can operate with inadequate control and vent excess steam. Installing dryer bars on low-speed dryers can reduce energy consumption by lowering the machine's rimming speed and reducing drive load. Monitoring dryer section ventilation systems by checking temperature rises and drops can indicate issues that increase energy usage like dirty filters or un draining steam coils. Non-contact dryers that do not touch the paper sheet should be disconnected from steam service to prevent wasted blow-through steam.
Benefits of online porosity measurement feb 2018Pekka Komulainen
Online porosity measurement provides a way to optimize papermaking processes and ensure consistent paper quality. Porosity is influenced by many process parameters from stock preparation to the drying section. Maintaining a constant porosity indicates that the papermaking process is performing well and producing paper with consistent physical properties. While online and laboratory porosity measurements can differ due to factors like web speed and dwell time, monitoring porosity online allows the identification of quality issues and process deviations.
Pulp and Paper Manufacturing and Treatment Of Waste Water
is About:
What is Fiber?
Lignin?Hemicellouse?
Real Explanation of Photosynthesis?
SEM (Scanning Electronic Microscope) Pictures of Trees
Can Plants Survive in Green Light?
How the Pulp is Produced from The Trees (Video) ?
Can We Use Other Than Trees for Pulp Preparation?
Some Information about Locally Located oldest Paper Mills
How the Waste Water Treated from Industries?
The document describes the key components and processes of a paper machine. It discusses the wet end which includes stock preparation and transport to the headbox. It then explains the headbox, wire section for initial dewatering, press section for further dewatering including conventional, German and shoe presses. Drying sections are described next for heating and drying the paper web. A size press is included to make the surface water repellent before winding the finished paper onto large reels. Water is circulated throughout the entire papermaking process.
The document describes the process of paper production, including:
1) Wood fibers are the main raw material and are unlocked from surrounding tissue through mechanical or chemical processes to produce pulp.
2) The pulp is refined, additives are mixed in, and the slurry is formed into a continuous web on a paper machine where water is removed through several sections.
3) Key factors that determine paper properties are fiber length and orientation, degree of refining, and additives used. The paper making process produces a fiber-oriented sheet with different characteristics on each side.
The document describes a cylinder dryer machine used for drying fabrics. It uses indirect drying through heated stainless steel cylinders. The fabric moves over several heated drums where it is dried at temperatures of 120-130°C using steam at pressures of 1-3 atm. This is an efficient and low-cost drying method suitable for intermediate drying of flat fabrics that cannot withstand high tension. The main components of the cylinder dryer are the hollow cylinders, guide rollers, free rollers and pin rollers. Proper maintenance such as checking motor RPM, even heating of cylinders, and ensuring smooth roller movement is important.
This document discusses water saving technology in the textile industry. It proposes using solophenyl dyes for dyeing cotton and cotton-polyester blends, which can save significant amounts of water compared to conventional reactive dyes. For 100% cotton fabrics, solophenyl dyes can reduce water consumption from 60-80 liters/kg to 20-30 liters/kg. For cotton-polyester blends, a one-batch dyeing process using solophenyl dyes has the potential to save water consumption from 120-140 liters/kg down to 30-40 liters/kg. Adopting these new dyeing techniques could help textile factories minimize their environmental impact and reduce production costs.
production of denim fabrics using rope dyeing and slasher dyeing methods: a c...Yousuf Ali
This document compares the slasher and rope methods of denim production. It finds that the rope method requires more floor space and manpower but produces denim at a higher rate with less breakage and wastage than the slasher method. Key differences are that the rope method allows for stripe fabrics, has better tensile strength and color fastness, but higher costs. The slasher method uses higher counts and has more consistent shades but higher breakage rates.
Potassium permanganate spray is done on jeans to take a bright effect on sand blast area. One important thing about potassium permanganate spray is, this is usually a sporting process to increase the effect of sand blast and which is one of the most important process i denim washing.
This document discusses strategies for optimizing vacuum in the wire part of a paper machine to conserve energy. It notes that increasing vacuum and dwell time can increase dryness up to a point, after which gains are minimal. Recommendations include applying vacuum in increasing order with the highest vacuum in the last box and reducing open area and peak vacuum where dryness is not significantly affected. Reducing dwell time from excessive levels like 150ms down to 10-15ms can substantially reduce air flow needs and energy consumption. Replacing vacuum pumps or installing more efficient options like roots blowers or variable frequency drives can achieve further savings. Proper design optimization of vacuum and the wire table offers significant potential for increased energy efficiency and improved wire life.
Dimas DP Nugroho presented on pulping technology fundamentals. He has an engineering background in chemical engineering and the pulp and paper industry. He has worked in various roles in pulp mills in Indonesia and conducted research in Canada. The presentation covered the pulping processes of kraft, mechanical, semi-chemical, and dissolving pulps. It discussed the steps of wood handling, chipping, cooking, washing, bleaching, and drying of pulp. Key process parameters that control pulp quality at each stage were also summarized.
Dryer doctors have a number of purposes in a paper machine dryer section: sheet shedding, dryer surface cleaning, threading, and air handling and control. Paper dryer doctors are often overlooked in the papermaking process, but they need proper attention to maintain efficient dryer operation.
Disperse dyes are used to dye polyester fabrics. They are not soluble in water and must be dispersed using a dispersing agent. There are various types of disperse dyes classified by their energy level, which determines their suitability for different dyeing processes like high temperature exhaust dyeing or printing. Key factors for disperse dyes include good dispersion stability, build-up, and fastness properties. Dyeing processes for polyester include batchwise, high temperature, carrier, and continuous dyeing. When dyeing polyester/cellulose blends, both portions can be dyed together or separately in one or two baths. Continuous dyeing uses pad-steam methods with thermosol fixation. Pro
The document summarizes the key steps and components in the paper manufacturing process using a paper machine. It describes the basic components of the paper machine including the headbox, which deposits the pulp slurry onto the wire screen, and the fourdrinier wet end, where water is removed from the web through gravity, foils, and suction before entering the press and dryer sections. It provides details on key components in the wet end like the slice, forming board, table rolls, and couch roll that work to remove water and form the paper web.
The document discusses the properties and dyeing of aramid fibers such as Technora, Conex, and Kevlar. It describes how aramid fibers have good heat resistance, strength and chemical resistance but are difficult to dye. Pretreating the fibers with liquid ammonia or using polar solvents can increase dye uptake. The document also examines different dyeing methods and how parameters like temperature, time and solvent selection affect the dyeing process and properties of the dyed fibers.
The ninth lecture in the module Particle Technology, delivered to second year students who have already studied basic fluid mechanics. The different mechanisms for the removal of dust from gases are covered and the design equations used for control, modelling and understanding of the equipment are presented and derived. Examples of industrial equipment for gas cleaning are included.
Crescentformer general process. tissue machine VoithNelson Izaguirre
CRESCENT FORMER
The Crescent Former is the culmination of technological improvements derived from our experience in the manufacturing of four machines since the 1960s (Plain Wire; Sloped Wire; Twin Wire C-Former; and Twin Wire S-Former). The first Crescent Former was invented in the 1970s by the multinational Kimberly Clark which held the patent until the Nineties.
Our technological innovations and more than 50 years of experience in the field of tissue ensure the highest levels of performance from the Recard Crescent Former.
Each Recard Crescent Former is designed to optimize the real operating speed of your production line. We have achieved performance of over 2000 meters per minute.
This document provides information on the Benfield process for removing carbon dioxide from gas streams. It discusses key aspects of the process including:
- Absorption of CO2 into a potassium carbonate solution and regeneration of the solution by heating.
- Use of an activator like DEA to improve CO2 absorption.
- Comparison with other CO2 removal processes like Rectisol and considerations for process selection.
- Parameters that affect the absorption and regeneration steps like pressure, temperature, and flow rates.
- Causes and prevention of corrosion in the system through vanadium addition and factors that can cause foaming of the solution.
1. Fine, dusty clinker leads to segregation in the kiln and non-uniform clinker beds in coolers due to differences in particle size and density.
2. When high-velocity cooling air hits closely-packed fine clinker dust, the air is heated, expands, and fluidizes the dust causing it to flow rapidly down the cooler in a "red river."
3. Newer cooler designs use stationary inclined grates and mechanical air flow regulators to better control air distribution and reduce issues caused by red rivers of fine, hot clinker dust.
NONLINEAR MODEL PREDICTIVE CONTROL FOR OPERATION OF A POST COMBUSTION ABSORPT...Modelon
This document summarizes research on developing a nonlinear model predictive control (NMPC) strategy for optimizing the operation of a post-combustion carbon capture unit. Key points:
1) Researchers created a detailed Modelica model of an amine-based carbon capture process but reduced it to improve computational efficiency for real-time optimization.
2) The reduced model was validated against experimental plant data and found to accurately capture system dynamics and behavior.
3) JModelica.org was used to perform offline optimizations of the reduced model, minimizing costs while satisfying operational constraints.
4) Preliminary results showed the NMPC approach was able to optimize reboiler duty and maintain a target carbon
The document provides an overview of reservoir simulation and performance analysis methods. It discusses static and dynamic reservoir modeling, including history matching and prediction. The key points covered are:
1) Reservoir simulation involves building static and dynamic reservoir models to match historical production and predict future performance.
2) History matching is used to validate the simulation model by comparing calculated pressures, saturations, and production to historical data.
3) After achieving a match, the model can be used to predict future field performance under different development scenarios and identify new infill locations.
This Powerpoint describes what is Flow chemistry, what are its advantages over batch method, Continuous flow reactor and Applications of Continuous flow chemistry.
Numerical Simulation Slides for NBIL Presentation in Queens universityYashar Seyed Vahedein
The numerical simulation project conducted by NBIL aimed to predict the carbon nanotube manufacturing process using template-based chemical vapor deposition (TB-CVD). The simulation modeled the CVD reactor geometry, defined boundary conditions based on experimental data, and solved conservation equations to analyze flow behavior and species concentration over time. The results showed good agreement with experimental temperature data and provided insight into how varying process parameters like gas flow rate affected velocity profiles and mass fraction distributions within the reactor. This allows for optimization of the TB-CVD process to fabricate carbon nanotubes with higher efficiency.
The document discusses chemical process simulation and the use of process simulators. It provides an overview of process simulation techniques including sequential modular approach, equation oriented approach, and simultaneous modular approach. It also discusses typical process units that can be modeled, the development of simulation flowsheets, and commercial process simulators such as Aspen and ChemCad. Process simulation allows prediction of process performance, optimization of energy usage, and identification of bottlenecks.
The document discusses chemical process simulation. It provides background on using computer-aided simulation tools to analyze large-scale chemical processes under steady-state conditions. It describes the overall structure of process design and analysis using simulation, including flowsheet synthesis, material and energy balancing, equipment sizing and costing, and economic evaluation. It also discusses specific techniques for process simulation, including sequential modular, equation-oriented, and simultaneous modular approaches.
This document discusses various types of reactors used for gas-solid catalytic reactions, with a focus on packed bed reactors. It summarizes:
1) The main types of reactors are adiabatic packed beds, wall cooled tubular reactors, fluidized beds, and risers.
2) Key design considerations for adiabatic packed beds include controlling the adiabatic temperature rise, pressure drop, and explosion potential.
3) Wall cooled tubular reactors require plug flow and careful control of wall cooling to prevent hot spots from forming.
4) Scale up of these reactors aims to maintain the same conditions as the laboratory scale, such as space time and flow distribution. Novel designs and operation methods aim
Sequential Design – The Challenge Of Multiphase Systems PdJames Ward
The document outlines an approach to developing a robust process for producing a crystalline form of a drug using mechanistic understanding rather than statistical modeling alone. Key factors like temperature, solvent composition, and water content were identified through solubility studies and reaction monitoring, allowing a targeted design of experiments. The initial process worked well at scale but later required modification when a new solvate form appeared. Repeating the mechanistic work incorporating prior knowledge improved the process design and mitigated issues with particle size and form variability.
Enhancing the Kinetcs of Mill Scale Reduction: An Eco-Friendly Approach (Part 2)chin2014
This document summarizes a research paper on enhancing the kinetics of mill scale reduction using hydrogen gas as an eco-friendly approach. The document includes:
1. An introduction to mill scale, its composition, and issues with current techniques for treating it.
2. A literature review summarizing previous research on reducing iron oxide using hydrogen and production of sponge iron powder from mill scale.
3. The objectives of experimentally studying the reduction kinetics using hydrogen gas at different temperatures and times to efficiently produce iron powder.
Efficiency of biogas production - Jan LiebetrauEBAconference
This document discusses methods for measuring the efficiency of biogas production. It presents data on the energy balance of a biogas plant, showing inputs, outputs, and losses at each stage of the process. Mass balance is identified as the basis for calculating conversion efficiency. Challenges include a lack of standardized methods for characterizing substrates and determining biogas potential. The document concludes that developing standard methods and validating approaches for full-scale applications would advance the evaluation of biogas process efficiency.
Development of Dynamic Models for a Reactive Packed Distillation ColumnCSCJournals
This work has been carried out to develop dynamic models for a reactive packed distillation column using the production of ethyl acetate as the case study. The experimental setup for the production of ethyl acetate was a pilot scale packed column divided into condenser, rectification, acetic acid feed, reaction, ethanol feed, stripping and reboiler sections. The reaction section was filled with Amberlyst 15 catalyst while the rectification and the stripping sections were both filled raschig rings. The theoretical models for each of the sections of the column were developed from first principles and solved with the aid of MATLAB R2011a. Comparisons were made between the experimental and theoretical results by calculating the percentage residuals for the top and bottom segment temperatures of the column. The results obtained showed that there were good agreements between the experimental and theoretical top and bottom segment temperatures because the calculated percentage residuals were small. Therefore, the developed dynamic models can be used to represent the reactive packed distillation column.
The document discusses process intensification, including its history, components, methods, and case studies. Process intensification aims to shrink the size of chemical plants while increasing efficiency. It can reduce environmental impact and costs. Case studies on producing olefins from natural gas, water treatment, and power generation from waste were presented. Simulation of the waste to power process was described along with the thermodynamic packages used.
Understanding and Predicting CO2 Properties for CCS Transport, Richard Graham, University of Nottingham. Presented at CO2 Properties and EoS for Pipeline Engineering, 11th November 2014
This document discusses scaling up a process for producing paste-glue from the laboratory scale to the pilot and near-commercial scales. Two methods for synthesizing the paste-glue using corn-based starch are developed at the laboratory scale. For Method 1, starch is decomposed with water and enzyme and polymer is produced separately, then combined. For Method 2, monomer, catalyst and decomposed starch are combined directly. The laboratory scale reactions are then scaled up 1000x for pilot studies. The pilot reactions produce paste-glue but with poorer properties, likely due to excessive exothermic reaction not controllable at larger scale. Further modifications are needed to successfully scale up the process.
multiphase flow modeling and simulation ,Pouriya Niknam , UNIFIPouriya Niknam
This document discusses modeling and simulation of multiphase flows using computational fluid dynamics (CFD). It begins with definitions of multiphase flow and discusses important types including bubbly, droplet, particle-laden, and annular flows. The document then provides tips on multiphase simulation including choosing appropriate modeling approaches such as Lagrangian, Eulerian, or volume of fluid methods depending on the problem. It concludes with discussions of challenges such as convergence difficulties and appropriate solver settings and techniques to address these challenges.
Fermentation
Scale up of fermentation
Steps in scale up
Scale up fermentation process
Optimizing scale up of fermentation process
Rules followed while doing scale up
Studies carried out during scale up
Reference
Big data is transforming terrestrial ecosystem science by enabling new approaches to model evaluation, development and prediction. Several examples are provided where large datasets on atmospheric measurements, remote sensing, and flux towers are integrated with models. This allows processes to be better understood from data analysis and provides opportunities to improve models. However, tools are still needed to easily facilitate comparison and assimilation of diverse data with models. The eMAST initiative aims to develop infrastructure for predictive ecosystem models that are fully informed by all relevant data.
Optimizing Hydrogel MW, Concentration, and ThicknessMatthew Sze
This document summarizes research optimizing the actuation of electroactive hydrogels by varying molecular weight, mass, thickness, and concentration. Testing found that higher molecular weight PEGDA, greater hydrogel thickness, and a concentration ratio of 8:1 acrylic acid to PEGDA facilitated the most movement. Future work could further vary concentration ratios and thickness to refine the optimal parameters.
Study of Heat Transfer Characteristics of Nanofluid as Coolant on a Single Cylinder Diesel Engine with Spiral Radiator.
Team Members: Sandeep Raj Kanth, Viral Hitenkumar Naik, Rudra Ranjan Swain
Guide: Dr. G. Naga Srinivasulu, Assistant Professor, Mechanical Engineering Department, NIT Warangal
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Model-based Optimization of a CompactCooking G2 Digesting Process Stage
1. Model-based Optimization of a CompactCooking™
G2 Digesting Process Stage
Master’s thesis presentation for the degree of M.Sc. (Tech.) in Process
Systems Engineering (Process Automation)
Igor Saavedra
Supervisor: Prof. Sirkka-Liisa Jämsä-Jounela
Advisor: Dr.-Ing. Aldo Cipriano
Instructor: D.Sc. Olli Joutsimo
Tuesday January 26, 2016
2.
3. Introduction
Pulp and Paper
• What is Pulp …
• Fibers sources
• Lignocellulosic
biomass
• Market pulp
• Softwood
• Hardwood
• and Paper?
• Paper products
• Fiber properties
Logs
Woodchips
Pulp
4. Introduction
Kraft Pulp Mill Process
Nueva Aldea Pulp Mill 1500+1500 Adt/d pine & euca, 91% ISO, 460MWth (95 MWe), 1000 L/s water inflow
5. Introduction
Problem Statement
• Digesting Stage Optimization
• Key area of the Kraft pulp mill
transforming woodchips into
brownstock and weak black
liquor by consuming steam and
white liquor
• Given an scenario of operating
costs and target production
rate: how do we cook pulp
optimally?
• CompactCooking G2 (Valmet),
digesting system found in the
mill, is a highly interacting
process that combines liquor
recycling and heat integration
6. Introduction
Goals, Scope and Novelty
• Main Goal
• Design a process optimizer able of minimizing cost or maximizing
profit rates of a CompactCooking G2 digesting stage.
• Specific Objectives
• Design and validate a dynamic model of the process stage.
• Design and perform a steady-state optimization routine based on
the previously validated model.
• Assess performance of theoretical optimal set-points versus current
mill set-points.
7. Introduction
Goals, Scope and Novelty
• Scope
• Development of an applied solution for the mill.
• Dynamic modeling of KPIs of stage such as
• Kappa number
• Production rates
• Temperatures and alkali concentrations
• Pulp intrinsic viscosity and cellulose DP
• “Cooking recipe” values:
• Liquor-to-wood ratios (L/W),
• Alkali charges (A/W),
• H-factor
• Dilution factor (DF) of the wash zone
• Phenomena to be modeled are chip bed compaction, cooking
reaction kinetics, and heat-exchanges within cooking liquors.
8. Introduction
Structure of the Thesis
Chapter 1 Introduction
LITERATURE PART
Chapter 2 The Kraft Pulp Mill
Chapter 3 Pulp Digesting Stage
Chapter 4 Mathematical Models on Pulp Digesters
EXPERIMENTAL PART
Chapter 5 Methods
Chapter 6 Process Description
Chapter 7 Mathematical Modeling
Chapter 8 Simulator Design
Chapter 9 Simulation Results
Chapter 10 Optimizer Design
Chapter 11 Optimization Results
Chapter 12 Conclusions
Appendix A Model-based Process Analysis
9. Literature Review
Mathematical Models on Pulp Digesters
• Review on first-principle modeling
Vroom (1957) H-Factor concept that describes the extent of delignification based on a
simple kinetic law using temperature and time as parameters
Hatton (1973; 1976) Equations relating cooking yield and kappa number with H-factor and
effective alkali for softwood and hardwood species. Later he applies this
work to Kraft cooking control.
Smith (1974) First version of the Purdue kinetic model. Wood solid is represented as 5
components, and parallel reaction kinetics are used to describe cooking
reactions.
Christensen (1982) Improved Purdue model by search algorithm to adjust kinetics parameters
for softwood and hardwood species. Liquor concentrations are also
calculated.
Gustafson et al. (1983) First version of the Gustafson kinetic model. Three stages cooking: initial,
bulk and residual. Wood solid is represented as 2 components: lignin and
carbs
Härkönen (1987) First 2D continuous digester model with emphasis on chips and fluid flow
dynamics with a simplified kinetic model. This contributed a framework for
bed compaction modeling used in almost all later developments.
10. Literature Review
Mathematical Models on Pulp Digesters
• Review on first-principle modeling
Saltin (1992) A dynamic, continuous digester model using the Purdue kinetics and a
simplified Härkönen bed compaction model. Implemented in GEMS.
Agarwal (1993) A steady-state, continuous digester model using Gustafson kinetics and
implemented by the single chip approach. It also incorporated a viscosity
model derived from Kubes et al. work and introduced the modelling of
diffusion and chip thickness by a sphere-equivalent chip model.
Implemented in GEMS.
Michelsen (1995) A dynamic, continuous digester model using a simplified Purdue-like
kinetics and a modified Härkönen bed compaction model that involves
solving a dynamic momentum balance for the chips phase. First modelling
approach of chip level variations. Implemented in MATLAB.
Wisnewski et al. (1997) A dynamic, continuous digester model with improved Purdue kinetics but
fixed bed compaction profile. It is also modelled the liquor concentration of
dissolved wood substance and the chip internal porosity. Implemented in
MATLAB.
He et al. (1999) First 3D model of a continuous digester based on Harkonen and
Michelsen fluid dynamics assumptions with a simplified kinetics model.
3D, dyn M&E&P balances
11. Literature Review
Mathematical Models on Pulp Digesters
• Review on first-principle modeling
Bhartiya et al. (2001) Continuation of Wisnewski et al. work incorporating advances made by
Michelsen. It also contributed a modelling approach for grade transition.
Implemented in MATLAB.
Andersson (2003) New kinetic model that combines Purdue and Gustafson approaches.
Wood substance is represented by 5x3 components.
Kayihan et al. (2005) A dynamic, continuous digester model based on Purdue kinetics, modified
Härkönen bed compaction, and Agarwal diffusion and chip thickness. It is
solved by a novel cinematic approach allowing to model chip level and
stochastic changes in chip size distribution. Implemented in MATLAB.
Rantanen (2006) A dynamic, continuous digester model based on Gustafson kinetics, Saltin
simplified bed compaction, and Agarwal diffusion and chip thickness. It is
applied to describe a LoSolids™ process (two-vessel stage) with grade
transition. Implemented in MATLAB.
Nieminen et al. (2014a,
2014b)
New kinetic models of lignin and carbohydrates degradation.
Delignification can be described with varying degrees of sophistication
(including Donnan equilibrium); and carbs degradation is modelled based
on the reaction mechanism of peeling, stopping and alkaline hydrolysis.
Reactions dependence on [OH-], [HS-] and [Na+] is considered.
12. Literature Review
Process Control and Optimization
• LP optimization
• Objective function as
• Cost or profit rate
• Cost or profit per unit of
product or educt
• Constraints on
• Flow rates, temperatures,
compaction pressures,
concentrations, etc.
• Linear input-output models
of the process
• SP-MV ( u=u(r) )
• PV-MV ( y=y(u) )
13. Process Description
CompactCooking G2 System
• Physical input
streams:
• Woodchips
• MP-steam
• White liquor
• Wash liquor
• Physical output
streams:
• Cooked pulp
Weak black
liquor
14. Simulator Design
Methodology
• The simulator aims to capture the
dynamic behavior of the system with
emphasis on interaction effects
• Changes in one input variable affect several
outputs in a non-linear form
• Some bias on the output is acceptable, but
poor correlation between measured and
simulated outputs is not.
• Simulator code builds upon parts of the Pulp
Mill Benchmark Model, updating it to
represent current cooking technologies
• CompactCooking G2 is a highly
interacting process, thus simulation of
the whole is a must for a rigorous
optimization effort
Start
Process flowsheet
abstraction
Conceptual model
IO variables
Conceptual model
states variables
Data acquisition and
conditioning for
testing
Test criteria are
met?
Testing runs and
parameter
adjustment
NO
End
Data acquisition and
conditioning for
validation
Validation run
Validation
criteria are met?
Validity domain
definition
NO
YES
YES
Model
implementation
Process
historian
P&ID, PFD, DCS
visualizations
Literature
submodels
Open source
models, code
libraries
Validated
simulation
model
Process
historian
ModelValidationModelTesting
Castro, J. J., & Doyle, F. J. (2004). A pulp mill benchmark problem for control: problem description.
Journal of Process Control, 14(1), 17–29.
18. Mathematical modeling
Main assumptions
• Vessels are tubular moving bed reactors
• Fixed levels
• Although levels were tried to be dynamically modeled, computation times
increase too much and numerical stability of the model is compromised
• Two-phases reacting system
• Concentrations on entrapped liquor are the same as on the free liquor
phase, thus total number of states is lowered
• 1D description on the axial direction of bed compaction and reaction
kinetics phenomena
• Heat-exchangers are perfectly mixed tanks
• Heat exchange occurs between hot and cold side at a given total heat
transfer coefficient UA
• Liquor densities are held constant, although composition is
dynamically modeled
• Liquor compositions vary solely due to retention times, no reaction
kinetics take place into heat-exchangers
19. Mathematical modeling
Main assumptions
• Woochips are composed of six mass entities
• Fast lignin, slow lignin, cellulose, (galacto)glucomanan,
(arabino)xylan, and extractives
• Extractives are represent as instantaneously leached when
entering the Impbin
• Liquor is composed of seven mass entities
• Sodium hydroxide NaOH(aq), sodium hydrosulfide NaSH(aq),
dissolved lignin, dissolved cellulose and so on
• Consumed NaOH and NaSH are accounted for density calculations
in order to keep mass balance consistency
𝜌𝑖 𝑤ℎ𝑒𝑟𝑒 𝑖 ∈ 𝐿 𝑓, 𝐿 𝑠, 𝐶, 𝐺𝑀, 𝑋, 𝐸
𝐶𝑗 𝑤ℎ𝑒𝑟𝑒 𝑗 ∈ 𝑁𝑎𝑂𝐻, 𝑁𝑎𝑆𝐻, 𝐷𝐿, 𝐷𝐶, 𝐷𝐺𝑀, 𝐷𝑋, 𝐷𝐸
20. Mathematical modeling
Bed Compaction
• Equations based on Härkönen model
𝜌 𝑐,𝑏 =
𝑖
𝜌𝑖 𝑧, 𝑡
𝑑𝑃𝑙
𝑑𝑧
= 𝑹 𝟏
1 − 𝜂 2
𝜂3 𝑢𝑙 + 𝑹 𝟐
1 − 𝜂
𝜂3 𝑢𝑙
2
𝑑𝑃𝑐
𝑑𝑧
= 𝜌𝑐,𝑤 − 𝜌𝑙 1 − 𝜂 𝑔 − 𝝁
𝑃𝑐,𝑒𝑥𝑡
𝐷
−
𝑑𝑃𝑙
𝑑𝑧
𝜂 = 𝒌 𝟎 +
𝑃𝑐 kPa
10
𝒌 𝟏
−𝒌 𝟐 + 𝒌 𝟑ln 𝜅
𝜄 = 1 − 𝜂 1 −
𝜌 𝑐,𝑏
𝝆 𝒘𝒐𝒐𝒅
𝜌𝑙 = 𝜌 𝑤 +
𝑗
𝐶𝑗 𝑧, 𝑡 𝜌𝑐,𝑤 =
𝜌 𝑤𝑜𝑜𝑑 1 − 𝜂 − 𝜄 + 𝜌𝑙 𝜄
1 − 𝜂
𝜂
𝜀
1 − 𝜂
1 − 𝜀
𝑃𝑐 𝑃𝑙
𝑑𝑉
Volumen fractions
𝜂 free liquor
𝜀 entrapped liquor
1 − 𝜂 woodchips
(1 − 𝜂)(1 − 𝜀) solid wood
Härkönen, E. J. (1984). A Mathematical Model for Two-Phase Flow (Doctoral dissertation). Helsinki University of Technology.
Härkönen, E. J. (1987). A mathematical model for two-phase flow in a continuous digester. Tappi Journal, 70(12), 122–126.
21. Mathematical modeling
Bed Compaction
• Experimental values from literature
Lee, Q. F. (2002). Fluid flow through packed columns of cooked wood chips (Master’s thesis). University of British Columbia.
22. Mathematical modeling
Reaction kinetics
• Equations based on Purdue model
𝜌𝑖 = 𝜌𝑖 𝑧, 𝑡 𝑖 ∈ 𝐿 𝑓(1), 𝐿 𝑠(2), 𝐶(3), 𝐺(4), 𝐴(5), 𝐸 6
𝐶𝑗 = 𝐶𝑗 𝑧, 𝑡 𝑗 ∈ 𝑁𝑎𝑂𝐻 1 , 𝑁𝑎𝑆𝐻 2 , 𝐷𝐿 3 , 𝐷𝐶 4 , 𝐷𝐺 5 , 𝐷𝐴 6 , 𝐷𝐸 7
𝑅𝑖 = −𝒆 𝒇 𝑘 𝑎𝑖 𝐶 𝑁𝑎𝑂𝐻
1
2 + 𝑘 𝑏𝑖 𝐶 𝑁𝑎𝑂𝐻
1
2 𝐶 𝑁𝑎𝑆𝐻
1
2 𝜌𝑖 − 𝝆𝒊
∞
𝑘 𝑎𝑖 = 𝑘 𝑎0𝑖exp
−𝐸 𝑎𝑖
𝑅𝑇
𝑘 𝑏𝑖 = 𝑘 𝑏0𝑖exp
−𝐸 𝑏𝑖
𝑅𝑇
𝑅 𝑁𝑎𝑂𝐻 =
1 − 𝜂
𝜂 + 𝜄
𝜷 𝑬𝑨𝑳
𝑖=1
2
𝑅𝑖 + 𝜷 𝑬𝑨𝑪
𝑖=3
5
𝑅𝑖
𝑅 𝑁𝑎𝑆𝐻 =
1 − 𝜂
𝜂
𝛽 𝐻𝑆𝐿
𝑖=1
2
𝑅𝑖
𝑅𝑗 =
1 − 𝜂
𝜂
𝑅𝑖
Wisnewski, P. A., Doyle, F. J., Kayihan, F. (1997). Fundamental Continuous Pulp-Digester Model for Simulation and Control. AIChE Journal, 43 (12), 3175-3192
Christensen, T. (1982,). A Mathematical Model of the Kraft Pulping Process (Doctoral Dissertation). Purdue University.
Smith, C. C. & Williams T. J. (1974). Mathematical Modeling, Simulation and Control of the Operation of Kamyr Continuous Digester for Kraft Process,
Tech. Rep. 64, PLAIC, Purdue University.
23. Mathematical modeling
Reaction kinetics
• Experimental values from literature
Wisnewski, P. A., Doyle, F. J., Kayihan, F. (1997). Fundamental Continuous Pulp-Digester Model for Simulation and Control. AIChE Journal, 43 (12), 3175-3192
Christensen, T. (1982). A Mathematical Model of the Kraft Pulping Process (PhD’s thesis). Purdue University.
26. Simulation Results
Testing (Pine)
DCS
estimate.
NO
SENSOR
Cooking and
bleaching
yield are
actually set
point
parameters
Prod. rate is
assumed
based on
yield set
points
Manipulated variable (simulated)
Disturbance (simulated)
Output (simulated)
Mill data (measured)
29. Simulation Results
Assessment
• In general, simulated outputs capture the main dynamic trends
with reasonable agreement
Model is operationally validated
• Simulated temperature signals show higher variability than
measured ones
• Improvements in the simulated heat-exchanger networks is required,
but this demands implementing several TI at the mill in order to
estimate U coefficients for each heat-exchanger (or to estimate U
within the model and to have output signals for comparison)
• Simulated blowline flow rate shows higher variability than
measured
• This might be generating a bias in the wash zone dilution factor
calculation
• One way to fix this involves using the signal as a logical input
(manipulated variable) and changing the model structure for bed
compaction calculation Long-term effort
30. Optimizer Design
Methodology
• The routine tries to find a new cooking recipe that
optimize process economics by changing following
DCS setpoints:
Liquor to wood ratio (L/W) for Impbin (bottom), Digester
cook zone 1 and 2
Alkali charge (EA/W) for the whole area, fresh charge to
Impbin, and fresh charge to Digester
Alkali splitting as white liquor flow distribution
Cooking temperature (for H-Factor setpoint)
Digester wash zone dilution factor (DF)
• Decision variables are taken as manipulated
variables, thus optimization outputs continue to be
the same as in the simulation model
• A previously validated model is a critical factor to
judge the optimization results
32. Optimization Results
Raw Results (Pine)
U0
U profit
heuopt
U cost
heuopt
Chipmeter speed rpm 15.93 15.93 15.93
MP steam flow rate kg/s 10.27 7.23 11.05
White liquor flow rate l/s 65.05 78.87 43.00
Wash liquor flow rate l/s 151.41 116.56 111.18
Filter reject flow rate l/s 35.15 96.94 8.78
Middle extraction flow rate l/s 35.58 138.33 8.89
Transfer liquor flow rate l/s 232.52 58.13 341.89
Upper extraction flow rate l/s 114.11 527.65 266.82
Lower extraction flow rate l/s 126.10 31.52 45.70
White liquor split fraction 1 0.0922 0.2499 0.1068
White liquor split fraction 2 0.3995 0.0999 0.0999
White liquor split fraction 3 0.0000 0.0000 0.2362
Transfer liquor split fraction 1 0.2300 0.0575 0.0575
Transfer liquor split fraction 2 0.0223 0.0056 0.1674
Upper liquor split fraction 1 0.1397 0.0349 0.0349
Upper liquor split fraction 2 0.2406 0.8101 0.8101
Y0
Y profit
heuopt
Y cost
heuopt
Blowline flow rate l/s 148.47 152.10 137.39
Top liquor flow rate l/s 151.63 174.80 140.26
Bottom liquor flow rate l/s 198.67 276.57 313.93
Cooking Kappa 27.87 28.10 28.49
Blowline consistency w/v% 11.11 10.89 12.01
WBL consistency w/v% 11.06 11.48 12.46
Impbin top temp. C 98.93 112.47 106.44
Top liquor temp. C 127.74 141.99 140.31
Transfer liquor temp. C 119.26 134.58 133.86
Digester top temp. C 151.89 148.81 159.51
Upper extraction temp. C 157.99 151.62 165.13
Lower extraction temp. C 151.11 154.69 159.35
Blowline temp. C 100.99 100.70 101.32
White liquor hot temp. C 144.49 143.32 148.19
Lower extraction cold temp. C 146.08 145.20 150.17
Top liquor EA conc. g/l 32.39 28.44 22.37
Transfer liquor EA conc. g/l 14.21 15.13 8.77
Upper extraction EA conc. g/l 17.10 20.42 9.31
Lower extraction EA conc. g/l 10.09 13.32 4.55
Cooked pulp prod. rate ADt/d 1582.82 1589.45 1583.77
WBL prod. rate tDS/d 2120.25 2337.34 2027.56
Cooking yield % 46.37 46.55 46.38
Cooking wood sp. cons. m3sub/ADt 5.07 5.05 5.07
EA/W total % 22.29 24.66 18.51
EA/W impbin fresh % 8.08 5.10 5.64
EA/W digester fresh % 12.15 15.34 11.03
L/W impbin top m3/BDt 5.60 6.25 5.28
L/W impbin bottom m3/BDt 4.60 3.81 4.66
L/W digester top m3/BDt 6.09 11.21 7.38
L/W digester bottom m3/BDt 2.79 2.06 1.92
DF digester wash zone m3/ADt 0.67 0.14 0.45
Impbin max Pc kPa 13.88 14.92 12.99
Digester max Pc kPa 23.37 31.50 23.99
Blowline carryover kgDS/BDt 1.96 1.46 2.08
WBL heating value HHV MJ/kg dry 15.03 13.66 15.68
Technically feasible?
Digester hang?
Lignin precipitation risk?
33. Optimization Results
EconomicAssessment
• For each objective
function a new cooking
recipe has been
identified
• But “how much”
optimal are these
recipes?
Y0
Y profit
heuopt
Y cost
heuopt
Constraint set-points
Bleached pulp prod. rate ADt/d 1535
Cooking kappa κ 28
Computed set-points
EA/W total % 20.05 21.97 18.83
EA/W impbin fresh % 8.02 5.77 6.70
EA/W digester fresh % 12.03 16.20 12.13
L/W impbin top m3/BDt 5.58 5.98 5.18
L/W impbin bottom m3/BDt 4.58 3.44 4.22
L/W digester cook zone 1 m3/BDt 5.89 5.33 6.56
L/W digester cook zone 2 m3/BDt 2.86 3.30 2.62
DF digester wash zone m3/ADt 1.24 0.60 0.99
H-factor H 631.41 714.71 703.77
Simulated variables
Cooking kappa κ 28.66 28.62 28.62
Digester top temp. C 151.63 153.06 152.88
MP steam flow rate kg/s 10.27 8.07 9.40
Cooked pulp prod. rate ADt/d 1663.88 1689.62 1662.80
Cooking yield % 48.74 49.49 48.71
Cooking wood sp. cons. m3sub/ADt 4.82 4.75 4.83
34. Optimization Results
EconomicAssessment
Steady-state Optimization
380
400
420
440
460
Profit rate
USD/min
250
260
270
280
290
Cost rate
USD/min
360
370
380
390
400
Profit per ADt
USD/ADt
225
230
235
240
245
Cost per ADt
USD/ADt
0 500 1000 1500 2000
72
74
76
78
80
82
Profit per m3
sub
USD/m
3
sub
min
0 500 1000 1500 2000
47.5
48
48.5
49
49.5
Cost per m3
sub
min
USD/m
3
sub
Profit rate as o.f.
Cost rate as o.f.
Base case (ss)
Base case (dyn)
35. Optimization Results
EconomicAssessment
• Process economics can be evaluated from several point
of views. This work considers 3 definitions of profit/cost:
• per unit of time,
• per unit of actual cooked ADt
• per unit of actual woodchips m3sub consumed
• Optimized recipe for cost reduction results more attractive
economically than the profit recipe
• Savings per actual cooked ADt up to 4 USD/ADt
• For a line aiming to produce 1500 ADt/d, this represent up to 2.19
MM annual savings
36. Conclusions
Main Conclusions
• CompactCooking G2 system has been dynamically
modeled with fairly good results although high uncertainty
on process disturbance signals.
• An LP task can be formulated around an identified mill’s
steady state, thus permitting to calculate a new optimized
cooking recipe (optimization direction for mill setpoint
changes).
• Potential savings based on the model prediction may
reach up to 4 USD/ADt, what for a modern mill (1500 –
2000 ADt/d) represent savings in the order of 1 – 3 MM/y.
41. Simulated Contribution
Case study: CompactCooking G2 analysis
… i.e., temperature control scheme must be
improved in order to reduce cooking kappa
variability
Editor's Notes
First of all, I would like to start this presentation from a reflection that motivates the subject of the thesis. It is about the forest industry, our consumption habits, and the role of the engineers. We are probably producing much more paper products than what we really need, and this is putting a huge burden on our natural resources. As engineers, we are far from being to able to solve this problem, but we can do our best with the aim of optimizing our production processes. In this sense, we should minimize the consumption of energy, water, and chemicals, as well as the generation of environmental emissions. This is certainly not an easy task. However, today we have amazing tools in the field of process modeling & simulation that must leveraged if we really want to arrive to better solutions for the pulp & paper industry.
OK. But, what is pulp and paper?
Types of fiber sources: primary and secondary
Lignocellulosic biomass: softwood and hardwood
Fiber properties: tensile, tear, burst indices among several others (density, opacity, brightness, etc)
Fiberization and lignin fraction -> kappa number
White liquor: sodium hydroxide and sodium sulphide (Na2S) turn into effective alkali and sodium hydrosulphide (NaHS)
Kraft cooking, white liquor composition, temperature and residence time –> H-factor
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)
In a rigorous model structure, flow rate of the cooked pulp stream should be a logical input for the model, and vessel levels would be outputs instead. However, due to the difficulty of modeling vessel levels, these are fixed and cooked pulp stream is seen as an output signal.
Original DCS visualization has an error as it doesn’t show one more black liquor split point, for this reason one circle seems to be pointing to no-split.
Except for 3 signals (Temp Woodchips, Temp MP-Steam, and Pressure MP-Steam) all the rest are highly uncertain since there is no online instrument available.
Instrumentation could be installed demanding low capital investment for measuring several of these signals.
Grey signals are covered by simulated signals, i.e., the model takes input signals identical to actual mill as measured data (except for noise filtering)
Blue plots: Inputs – Manipulated Variables
Green plots: Inputs - Disturbances
Red plots: Outputs
Grey plots: Mill data
Blue plots: Inputs – Manipulated Variables
Green plots: Inputs - Disturbances
Red plots: Outputs
Gray plots: Mill data
Grey signals are covered by simulated signals, i.e., the model takes input signals identical to actual mill as measured data (except for noise filtering)
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)
Blue plots: MV
Green plots: DV
Black plots: estimated signal e.g. woodchips flow is estimated from chip meter rpm and woodchip bulk density as seen by DCS (not shown)