This document describes a study on preparing nickel-coated aluminum through an electroless deposition technique. Sintered aluminum samples were developed using powder metallurgy. Nickel was deposited from an aqueous nickel chloride solution onto the sintered aluminum substrates without external electricity. The coating process was studied at different temperatures. Characterization of the coated samples found uniform nickel distribution at room temperature. XRD analysis confirmed the presence of both nickel and aluminum phases. Coating improved the surface properties by decreasing porosity and increasing hardness. The nickel-coated aluminum samples exhibited magnetic properties.