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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 151
Experimental investigation of microstructure and mechanical
characteristics of Al5083 & Fly ash composite.
K.Ganesh1
, I.Justin antony raj 2
, P.kamaraj3 ,J.Sebastin joyal4
1 2 3 4 Assistant Professor, Department of Mechanical Engineering, Vandayar engineering college ,
Thanjavur-613501-TN-india.
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract: Applications of this project is in ship building, rail
cars, vehicle bodies, tip truck bodies, mine skips ,cages and
pressure vessels. Present study is to investigate the
mechanical wear behaviour of Al5083 flyash composite
fabricated by the stir casting method with different volume
fraction of fly ash (5,10,15wt%).Mechanical test is about
hardness test and tensile test has been conducted by using
brinell Hardness Testing and universal testing machine
respectively. Microstructures of the specimens are analyzed
to understand the modes .
Keywords: Composite materials, Raw materials, Scanning
Electron microscope.
1.INTRODUCTION
Al5083 alloy matrix hybrid composites reinforced with
flyash particles are studied. Al5083 alloy matrix hybrid
composites can be synthesized by the stir casting method.
SEM review is studied . Uniform distribution of
reinforcement particles for cast composite is studied.
Project deal with interfacial bonding between the particles
and the matrix. Incorporation of flyash particles( upto
15wt% led ) are marked with improvements in the
resistance of the Al alloy.Wear test is studied.
2.LITERATURE SURVEY
A.P.S.V.R.Subrahmanyam. et.al(2015) Above researcher
conduct experiments on effect of rice husk ash and fly ash
of aluminium alloy (AlSi10Mg) Matrix composites.
Hussein Abdizadeh et al (2011). Above researcher
conduct experiments on study of metal matrix composites
(MMCs) and aluminium (Al)as the best metal for
producing these composites. Shailovekumar et al
(2010). Above researcher conduct experiments on study
the strength of composite depend primarily on the
amount. K.Kalaiselvan et al (2010). Above researcher
conduct experiments on studied this work focuses on the
fabrication of aluminium (6061-T6)matrix of B4C
particulates by modified stir casting route. Research Gap:
Above researchers are not done research with stir casting
method and not researched over the incorporation of
flyash particles upto 15wt% led are marked with
improvements in the resistance of the Al alloy without
much effect in tensile strength and hardness.
3. EXPERIMENTAL DETAILS:
3.1 CNC lathe settings
Fig.1.Schematic setup for fabrication of AMC Via stir
casting technique
A stir casting setup is as shown in figure 1 consisted of a
resistance muffle furnace and a stirrer assembly is used to
synthesize the composite . Variable speed vertical drilling
machine having range. Stirrer is made by cutting and
shaping a graphite block and three blades at an angle of
120 apart .5Kg capacity Graphite crucible is placed inside
the furnace .
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 152
Fig.2.Experimental setup of stir casting and poured
molten metal in the mould
Table .1. processing parameters
Processing temperature 8000C
Stirrer speed 640rpm
Feed rate of reinforcement 20 g/min
Stirring time after reinforcement 10minutes
Incubation time 3hours
Slag removing agent Scum powder
Degassing tablet Hexo chloro
ethane
Fig.3.Scum power and Degassing Tablets
Table .2. Chemical composition of A15083 alloy
Elem
ent
SiC F
e
Cu Mn Mg Ti Cr Zn Al
% 0.4 0.
1
0.4-1 4.0-
4.9
0.15 0.05-
0.25
0.05-
0.25
0.25 92.7
Table 3.Composition of matrix and reinforcement in
wt%.
Samples Al 5083in wt.% Fly ash in wt.%
1 95 5
2 90 5
3 85 10
4 80 15
MICROSTRUCTURE:
Fig.4.shows the experimental setup of Scanning electron
microscopy.The as cast composites are cut into required
size and which surface is prepared for microstructure
analysis .The emery papers grid sizes (-
100,300,600,1000,0/1,0/2,0/3,0/4) are used for making
the scratchless surface and then the fine scratches caused
by final grinding and fineness are used as polishing
abrasives .A mixture of powder , velvet cloth ,alumina
,magnesia and diamond powders are used as a material.
Fig.4.Scanning Electron microscopy
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 153
Fig.5.Specimen for Microstructure Analysis.
Brinell Hardness Test :
Test material is indented with a 5mm diameter hardened
tungsten carbide ball subjected to a weight of 250kg
applied for 20 seconds .The diameter of the indentation
left and hardness number is calculated by dividing the
load applied and the impression is the average of five
readings at right angles.
Fig.6.Brinell Hardness testing Machine
Tensile Test:
The room temperature tensile test is conducted using
Universal testing machine .The as cast Aluminium 5083
alloy composite samples for tensile test are prepared
using CNC lathe according to ASTM E8.
Fig.7.Tensile specimen ASTM E8
Fig.8.Specimen for Tensile Test and Tested specimen
The test is conducted trice to get the average response
value.
The schematic diagram of Universal Testing Machine is
given in the figure. 9.
Fig.9.Universal Testing Machine
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 154
4.METHODOLOGY
The experimental work is planned as per the flow chart
given in the figure 10.
Fig.10. Work flow chart
MATERIALS/MACHINES/EQUIPMENTS USED
For performing the experiment and testing of composites,
the following.
Materials/ machines/ equipment’s are used.
 Matrix(Al alloy 5083)
 Reinforcements(Fly ash)
 Digital control Electric resistance Muffle
Furnace
 Weighing Machine
 Graphite crucible
 Graphite stirrer
 Mild steel Mould
 Power hacksaw
 Lathe Machine
 Emery papers grid sizes-
100,300,600,1000,0/1,0/2,0/3,0/4
 Double disc polishing machine
 Scanning Electron Microscope (SEM)
 Hardness Testing Machine
 Computerized UTM
RAW MATERIALS:
 Matrix
Aluminium alloy 5083 is used as matrix in the synthesis of
composite in the form of ingots and then cut into smaller
pieces with the help of power hacksaw in order to keep
the alloy inside the crucible properly.
5. RESULT AND DISCUSSION
Fig.11. SEM Image of 5% Flyash composite
The scanning electron micro graphs are taken for
analyzing the bonding ,grain size of the reinforcement and
the formation of pores ,clusters and inter metallic
formation. Figure 11 shows the SEM image of the
composites of the different combinations for 250x zooms .
HARDNESS:
Fig.12.Brinell Hardness Test
Figure. 12.shows the hardness result in terms of BHN
along Y axis .The composite sample having 5 wt.% of Si3N4
have greater hardness value.The curve decreases on
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 155
further addition of Si3N4 and Fly ash particles.The
hardness value is seen increasing when 15 wt.% of Si3N4
and 5 wt.% flyash particles are added .
TENSILE STRENGTH:
Fig.13.Tensile strength graph.
Figure 13.shows the tensile curve for the composites
according to their combinations .Usually the tensile
property of the composite will get loose on the zircon sand
and Boron carbide reinforced composites .As compared to
the 10% Flyash & 15%Flyash composite ,the resultant
graph shows the peak value in the 5%flyash composites
having higher tensile strength over the flyash reinforced
composites.
Table.4.parameters
Load(N) Trac radius
(mm)
Speed
(rpm)
Time
(min)
Frictional
force (N)
Coefficient
of friction
15 60 520 30 1 0.08
The resultant graph shows the peak value in the 5% flyash
composites having higher tensile strength over the flyash
reinforced composites.
Fig. 14 .wear test result
6.CONCLUSION
1) Al5083 alloy matrix hybrid composites are
reinforced with flyash particles can be
successfully synthesized by the stir casting
method.
2) SEM reviews that the cast composite shows
uniform distribution of reinforcement particles.
3) Good interfacial bonding between the particles
and the matrix.
4) Incorporation of flyash particles (upto 15wt%
led) are marked with improvements in the
resistance of the Al alloy without much effect in
tensile strength and hardness.
5) Wear test result of co-efficient of friction is 0.08.
REFERENCE
[1] H.C Anil kumar ,”mechanical properties of fly ash
reinforced aluminium alloy (Al6061) composites
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 156
”,vol.06,Issue No:01,2011,pp.41-45.international journal of
mechanical & materials engineering (IJMME).
[2]N.V.Murthy,”A review on fabrication of aluminium alloy
based metal matrix nano composites through ultrasonic
assisted casting”,vol.01,Issue No:02,Dec 2015,pp.1-
8,Journal of metallurgical and materials
[3]Diju Samuel G,”Effect of process parameters on the
microstructure & mechanical properties of
Al6061/powdered activated carbon metal matrix
composite “,vol.10,Nov.27,2017,international journal of
control theory and applications.
[4]Rohit Sharma,”A review of the aluminium metal matrix
composite & it properties”,vol.02, Issue No: 02,feb
2017,International research journal of engineering &
technology.(IRJET).
[5]V.jaya Prasad,”A study of microstructure & tribological
properties of stir cast Al metal matrix composite”,vol. 04,
Issue No: 08, 2017, pp. 9264- 9271, materials today
proceedings .
[6]Shashi prakash Dwivedi,”comparison of microstructure
& mechanical properties of A356/SiC metal matrix
composites produced by two different melting routes
“,vol.2014,2014,international journal of manufacturing
engineering .
[7]G.Dijusamuel,”Influence of tool pin in friction stir
welding on activated carbon reinforced aluminium metal
matrix composite “,vol.247,material science &
Engineering.
[8]Abihilash A ,”Assessment of mechanical & corrosion
properties of aluminium reinforced with fly ash (ALFA)
metal matrix composites”,vol.04,Issue No:03,International
journal of engineering development & research.
[9]Jithin jose,”Studies on mechanical and wear properties
of Al7075/Zircon/Fly ash hybrid metal matrix
composites”,2016, International conference on current
research in engineering science & technology.
[10]Wang qingping ,”micro structural characterization and
mechanical property of flyash /Al-25mg composites “,oct
2014,Journal of wuhan university of technology –mater
.sci.Ed.

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IRJET-Experimental Investigation of Microstructure and Mechanical Characteristics of Al5083 & Fly Ash Composite

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 151 Experimental investigation of microstructure and mechanical characteristics of Al5083 & Fly ash composite. K.Ganesh1 , I.Justin antony raj 2 , P.kamaraj3 ,J.Sebastin joyal4 1 2 3 4 Assistant Professor, Department of Mechanical Engineering, Vandayar engineering college , Thanjavur-613501-TN-india. ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract: Applications of this project is in ship building, rail cars, vehicle bodies, tip truck bodies, mine skips ,cages and pressure vessels. Present study is to investigate the mechanical wear behaviour of Al5083 flyash composite fabricated by the stir casting method with different volume fraction of fly ash (5,10,15wt%).Mechanical test is about hardness test and tensile test has been conducted by using brinell Hardness Testing and universal testing machine respectively. Microstructures of the specimens are analyzed to understand the modes . Keywords: Composite materials, Raw materials, Scanning Electron microscope. 1.INTRODUCTION Al5083 alloy matrix hybrid composites reinforced with flyash particles are studied. Al5083 alloy matrix hybrid composites can be synthesized by the stir casting method. SEM review is studied . Uniform distribution of reinforcement particles for cast composite is studied. Project deal with interfacial bonding between the particles and the matrix. Incorporation of flyash particles( upto 15wt% led ) are marked with improvements in the resistance of the Al alloy.Wear test is studied. 2.LITERATURE SURVEY A.P.S.V.R.Subrahmanyam. et.al(2015) Above researcher conduct experiments on effect of rice husk ash and fly ash of aluminium alloy (AlSi10Mg) Matrix composites. Hussein Abdizadeh et al (2011). Above researcher conduct experiments on study of metal matrix composites (MMCs) and aluminium (Al)as the best metal for producing these composites. Shailovekumar et al (2010). Above researcher conduct experiments on study the strength of composite depend primarily on the amount. K.Kalaiselvan et al (2010). Above researcher conduct experiments on studied this work focuses on the fabrication of aluminium (6061-T6)matrix of B4C particulates by modified stir casting route. Research Gap: Above researchers are not done research with stir casting method and not researched over the incorporation of flyash particles upto 15wt% led are marked with improvements in the resistance of the Al alloy without much effect in tensile strength and hardness. 3. EXPERIMENTAL DETAILS: 3.1 CNC lathe settings Fig.1.Schematic setup for fabrication of AMC Via stir casting technique A stir casting setup is as shown in figure 1 consisted of a resistance muffle furnace and a stirrer assembly is used to synthesize the composite . Variable speed vertical drilling machine having range. Stirrer is made by cutting and shaping a graphite block and three blades at an angle of 120 apart .5Kg capacity Graphite crucible is placed inside the furnace .
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 152 Fig.2.Experimental setup of stir casting and poured molten metal in the mould Table .1. processing parameters Processing temperature 8000C Stirrer speed 640rpm Feed rate of reinforcement 20 g/min Stirring time after reinforcement 10minutes Incubation time 3hours Slag removing agent Scum powder Degassing tablet Hexo chloro ethane Fig.3.Scum power and Degassing Tablets Table .2. Chemical composition of A15083 alloy Elem ent SiC F e Cu Mn Mg Ti Cr Zn Al % 0.4 0. 1 0.4-1 4.0- 4.9 0.15 0.05- 0.25 0.05- 0.25 0.25 92.7 Table 3.Composition of matrix and reinforcement in wt%. Samples Al 5083in wt.% Fly ash in wt.% 1 95 5 2 90 5 3 85 10 4 80 15 MICROSTRUCTURE: Fig.4.shows the experimental setup of Scanning electron microscopy.The as cast composites are cut into required size and which surface is prepared for microstructure analysis .The emery papers grid sizes (- 100,300,600,1000,0/1,0/2,0/3,0/4) are used for making the scratchless surface and then the fine scratches caused by final grinding and fineness are used as polishing abrasives .A mixture of powder , velvet cloth ,alumina ,magnesia and diamond powders are used as a material. Fig.4.Scanning Electron microscopy
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 153 Fig.5.Specimen for Microstructure Analysis. Brinell Hardness Test : Test material is indented with a 5mm diameter hardened tungsten carbide ball subjected to a weight of 250kg applied for 20 seconds .The diameter of the indentation left and hardness number is calculated by dividing the load applied and the impression is the average of five readings at right angles. Fig.6.Brinell Hardness testing Machine Tensile Test: The room temperature tensile test is conducted using Universal testing machine .The as cast Aluminium 5083 alloy composite samples for tensile test are prepared using CNC lathe according to ASTM E8. Fig.7.Tensile specimen ASTM E8 Fig.8.Specimen for Tensile Test and Tested specimen The test is conducted trice to get the average response value. The schematic diagram of Universal Testing Machine is given in the figure. 9. Fig.9.Universal Testing Machine
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 154 4.METHODOLOGY The experimental work is planned as per the flow chart given in the figure 10. Fig.10. Work flow chart MATERIALS/MACHINES/EQUIPMENTS USED For performing the experiment and testing of composites, the following. Materials/ machines/ equipment’s are used.  Matrix(Al alloy 5083)  Reinforcements(Fly ash)  Digital control Electric resistance Muffle Furnace  Weighing Machine  Graphite crucible  Graphite stirrer  Mild steel Mould  Power hacksaw  Lathe Machine  Emery papers grid sizes- 100,300,600,1000,0/1,0/2,0/3,0/4  Double disc polishing machine  Scanning Electron Microscope (SEM)  Hardness Testing Machine  Computerized UTM RAW MATERIALS:  Matrix Aluminium alloy 5083 is used as matrix in the synthesis of composite in the form of ingots and then cut into smaller pieces with the help of power hacksaw in order to keep the alloy inside the crucible properly. 5. RESULT AND DISCUSSION Fig.11. SEM Image of 5% Flyash composite The scanning electron micro graphs are taken for analyzing the bonding ,grain size of the reinforcement and the formation of pores ,clusters and inter metallic formation. Figure 11 shows the SEM image of the composites of the different combinations for 250x zooms . HARDNESS: Fig.12.Brinell Hardness Test Figure. 12.shows the hardness result in terms of BHN along Y axis .The composite sample having 5 wt.% of Si3N4 have greater hardness value.The curve decreases on
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 155 further addition of Si3N4 and Fly ash particles.The hardness value is seen increasing when 15 wt.% of Si3N4 and 5 wt.% flyash particles are added . TENSILE STRENGTH: Fig.13.Tensile strength graph. Figure 13.shows the tensile curve for the composites according to their combinations .Usually the tensile property of the composite will get loose on the zircon sand and Boron carbide reinforced composites .As compared to the 10% Flyash & 15%Flyash composite ,the resultant graph shows the peak value in the 5%flyash composites having higher tensile strength over the flyash reinforced composites. Table.4.parameters Load(N) Trac radius (mm) Speed (rpm) Time (min) Frictional force (N) Coefficient of friction 15 60 520 30 1 0.08 The resultant graph shows the peak value in the 5% flyash composites having higher tensile strength over the flyash reinforced composites. Fig. 14 .wear test result 6.CONCLUSION 1) Al5083 alloy matrix hybrid composites are reinforced with flyash particles can be successfully synthesized by the stir casting method. 2) SEM reviews that the cast composite shows uniform distribution of reinforcement particles. 3) Good interfacial bonding between the particles and the matrix. 4) Incorporation of flyash particles (upto 15wt% led) are marked with improvements in the resistance of the Al alloy without much effect in tensile strength and hardness. 5) Wear test result of co-efficient of friction is 0.08. REFERENCE [1] H.C Anil kumar ,”mechanical properties of fly ash reinforced aluminium alloy (Al6061) composites
  • 6. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 01 | Jan-2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 156 ”,vol.06,Issue No:01,2011,pp.41-45.international journal of mechanical & materials engineering (IJMME). [2]N.V.Murthy,”A review on fabrication of aluminium alloy based metal matrix nano composites through ultrasonic assisted casting”,vol.01,Issue No:02,Dec 2015,pp.1- 8,Journal of metallurgical and materials [3]Diju Samuel G,”Effect of process parameters on the microstructure & mechanical properties of Al6061/powdered activated carbon metal matrix composite “,vol.10,Nov.27,2017,international journal of control theory and applications. [4]Rohit Sharma,”A review of the aluminium metal matrix composite & it properties”,vol.02, Issue No: 02,feb 2017,International research journal of engineering & technology.(IRJET). [5]V.jaya Prasad,”A study of microstructure & tribological properties of stir cast Al metal matrix composite”,vol. 04, Issue No: 08, 2017, pp. 9264- 9271, materials today proceedings . [6]Shashi prakash Dwivedi,”comparison of microstructure & mechanical properties of A356/SiC metal matrix composites produced by two different melting routes “,vol.2014,2014,international journal of manufacturing engineering . [7]G.Dijusamuel,”Influence of tool pin in friction stir welding on activated carbon reinforced aluminium metal matrix composite “,vol.247,material science & Engineering. [8]Abihilash A ,”Assessment of mechanical & corrosion properties of aluminium reinforced with fly ash (ALFA) metal matrix composites”,vol.04,Issue No:03,International journal of engineering development & research. [9]Jithin jose,”Studies on mechanical and wear properties of Al7075/Zircon/Fly ash hybrid metal matrix composites”,2016, International conference on current research in engineering science & technology. [10]Wang qingping ,”micro structural characterization and mechanical property of flyash /Al-25mg composites “,oct 2014,Journal of wuhan university of technology –mater .sci.Ed.