This is the presentation of my 8th semester project on Application of Artificial Neural Network in Friction Stir Processing. We have used AA5052. The presentation starts from the basics of Aluminium and FSP process and then first we predict the properties of Hardness, Roughness and Tensile strength using Minitab16 and then use Minitab16 to create dummy outputs which are fed into the ANN to train it.
1. Application of Artificial Neural Network (ANN) in Friction Stir Processing (FSP)
Presented by
Under the guidance of
Dr. Arun Kumar Shettigar
Department of Mechatronics Engineering
Manipal Institute of Technology, Manipal
Yyyy
Department of Mechatronics Engineering
Manipal Institute of Technology, Manipal
March, 2017
Alok Tiwari 130929190
Nihal Shetty 120929138
Vansh Vardhan Jha 130929238
2. Contents
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 2
Introduction
Objectives
Methodology
Result and discussion
Conclusion
References
4. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 4
Aluminium
Friction Stir Processing (FSP)
FSP process parameters
Response Surface Methodology (RSM)
Artificial Neural Network (ANN)
5. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 5
Aluminium
1. 3rd most abundant element on earth (after oxygen and silicon) with 8% by weight.
2. Aluminum has relatively low density (2.7 g/cc as compared to 7.9 g/cc for steel)
3. It has FCC structure.
4. High electrical & thermal conductivity.
5. nonmagnetic and non sparking.
6. Resistance to corrosion
7. It is easy to cast (low melting point).
6. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 6
Limitations of Aluminium
1. Chief limitation is its low melting temperature (660 °C).
2. It is very soft, which restricts its application.
7. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 7
Aluminium Alloys
Aluminium
(molten)
Fe, Zn, Si, Cu, Mg, Mn
( up to 15% of weight)
Aluminium Alloy
( strength & durability )
8. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 8
Aluminium Alloys
Designation
Main alloying
element
Application
1xxx Pure 1100 for Food packaging trays.
1350 for power grids, electrical appliances.
2xxx Cu 2024 for aircraft alloy
3xxx Mn 3004 for Al beverage cans
3003 for heat exchangers
4xxx Si 4043 for welding wire and brazing alloys
5xxx Mg 5005 for architecture
5083 for tanks
6xxx Si, Mg 6061, 6063 for Automobile production, architectural and structural
7xxx Zn 7050, 7075 for Airlines industry
9. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 9
FSW FSP
Material 1 Material 2 Material 1
• FSW is a Solid State welding process.
• When we have to join 2 components we use FSW. It’s
joint efficiency is higher than most other Welding
techniques.
• For e.g. we want to make our material corrosion
resistant, 2 options
1. Coat the material.
2. Make the material hard using FSP.
• We use FSP to modify the microstructure and harden
the upper surface till a specific depth by using the
same FSW principle.
In FSP, a rotating tool with shoulder and pin is plunged into the surface
of material till the shoulder touches the surface of the base material.
This creates frictional heat and dynamic mixing of material area
underneath the tool.
• Material is mixed without changing the phase (by melting or
otherwise) and
• a microstructure with fine equiaxed grains is created.
11. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 11
FSP parameters
How to optimize FSP process?
1. By having knowledge of effect of all process variables of FSP.
2. Here we will be looking at the effect of 3 process variables
SR Process parameter Effect on FSP process
1 Tool rotational speed
(ω)
Determine the amount of heat input in the Stir Zone
Amount of heat affects the microstructure and resultant properties.
Tool rotation speed generates the heat.
Tool traverse speed supplies the amount of heat generated.
2 Tool traverse speed (𝜈
)
3 Tool probe geometry Circular pin Round edges
Lower tool wear rate than others.
Triangular
pin
It has sharp edges.
This results in better stirring of materials.
Square pin Produces more pulse/sec. than other pins.
Produce smaller grains with uniformly distributed fine precipitates
This in turn yield higher strength and hardness
12. Introduction
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 12
Artificial Neural Network
1. Artificial neural network is a sub category of AI system.
2. ANN technique learns and understands the relationship between the input and output patterns by training
the network.
3. It consists of number of interconnected neurons, where it stores the knowledge in the memory based on the
given set of input and output patterns.
14. Objectives
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 14
There are 3 objectives of this project
Investigation - Investigate the effects of FSP process parameters on the mechanical and metallurgical
properties of AA5052-O
Prediction - Prediction of surface roughness & mechanical properties (Ultimate tensile strength, Percentage
elongation, Vickers hardness) of FSPed alloys using
Response surface methodology (RSM)
Artificial neural network (ANN)
Optimization – Use Desirability approach to find the optimum range of process parameters
16. Methodology
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 16
Methodology can be organised into 3 parts
1. Initialization
2. Experimentation
3. RSM modelling
4. Desirability approach
5. ANN modelling
20. Methodology - initialization
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 20
Step 1.1 Selection of base material AA5052 -O
-O = annealed
Chemical composition
Properties
• Good workability,
• medium static strength,
• high fatigue strength, good weldability,
• very good corrosion resistance, especially in marine atmospheres.
• low density and excellent thermal conductivity
Physical properties
Property At Value unit
Density 20oC 2,680 kg/m3
Melting Range 607 –
650
oC
Mean
Coefficient
of Expansion
20oC 23.75 x 10-6 / oC
Thermal
Conductivity
25oC 138 W / m. oC
Electrical
resistivity
20oC 0.050 Micro-
ohm .m
Alloy Si Fe Cu Mn Mg Cr Zn
5052 0.25 0.40 0.10 0.10 2.2 – 2.8 0.15 – 0.35 0.10
22. Methodology - initialization
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 22
Need for FSP on AA5052-O
1. -O means soft material.
2. In some cases we might need
• Upper surface to have more hardness. In these cases
• Lower surface to have lower hardness. We go for FSP.
3. Based on application.
New hardened
upper surface
Lower surface
23. Methodology - initialization
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 23
Step 1.2 Selection of tool material
1. There are some criteria for selection of tool material.
a) It should be stronger than selected base material.
b) It should have a low wear rate.
c) It should be easy to manufacture.
d) No Manufacturing constraint.
2. Hence we select – molybdenum tungsten alloy
a) Molybdenum and Tungsten both are Refractory Metals – [ extraordinary resistance to heat and wear ]
b) Moly alloys - excellent strength, mechanical stability at high temperatures (up to 1900°C).
c) Their high ductility and toughness provide a greater tolerance for imperfections.
d) It has a Vickers hardness of 62 HRC.
24. Methodology - initialization
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 24
Step 1.3 Selection of tool profile
We have selected square pin profile as it
Produces more pulse/sec. than other pins.
Produce smaller grains with uniformly distributed fine
precipitates
This in turn yield higher strength and hardness
Figure 4.1 shows square pin profile with shoulder diameter of
33 mm, pin diameter of 10 mm and 5.7 mm height.
Figure 4.1 Square pin profile
25. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 25
Step 2.1 identify working range
• Trial experiments have been conducted to determine the working range of the parameters.
• The FSP area should be free from any visible external defects.
Table 4.2 Different combinations tried
26. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 26
Step 2.2 Perform FSP
• Total 9 experiments with 3 tool rotation speeds (700, 1000, 1300) RPM and 3 tool traverse speed (50, 65, 80) mm/min as
shown in Table 4.2, were selected as they had the least visible defects.
Figure 4.1 Friction stir processing setup
27. Methodology – experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 27
Step 2.3 Specimen cutting
Fig 9 Specimen before
Specimen cutting
Fig 10 Specimen after
28. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 28
Step 2.4 Perform tests
1. Surface roughness
2. Tensile strength
3. Vickers hardness
4. Microstructure
29. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 29
Step 2.4 Preform tests
Surface roughness
• It is a measure of the finely spaced surface irregularities.
Significance of roughness
• Rough surfaces usually wear more quickly
• Rough surfaces have higher friction coefficients than smooth surfaces.
• It is a predictor of the performance of a mechanical component, since irregularities in the surface may
form nucleation sites for cracks or corrosion.
• But, roughness may promote adhesion too.
• Measuring roughness – Roughness average Ra
• Ra is the most widely used parameter is the is the arithmetic average of the absolute values.
30. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 30
Surface roughness
Specimen cutting
TEST Specimen used Preparation
Surface
Roughness • The specimen can be used directly.
• Surface measurements was carried
out by using Surtronics 3+.
• In each sample 3 reading were taken
at points A, B and C. The mean was
then used for analysis.
31. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 31
Microstructure
Specimen cutting
TEST Specimen used and Preparation
Microstructure The specimen should be polished so that there are no scratches before we observe it in Scanning Electron
Microscope.
1. Polish
I. Polish the specimen using progressively finer emery paper (grades 100, 600, 1000, 2000) to
get near mirror finish
II. Diamond Polish
2. Etching using Keller's Etchant
32. 6/19/2017 Department of Mechatronics Engineering, MIT Manipal 32
Specimen cutting
Step 1 Step 2 Step 3 Step 4 Step 5 Step 6
Use Polishing Machine
RPM – 150-200 RPM
Use velvet cloth
as cover for disc
Drop few
drops of 3μ
diamond
paste
Polish for 5
min in 1
position
Rinse and
dry
Polish for 5 min in a position 90° to the original
Diamond polishing
33. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 33
Specimen cutting
Step 1 Step 2 Step 3 Step 4
Put few drops of Keller’s
etch.
(let bubbles appear)
Rinse it using
running water
Dry it using dryer See the sample in Optical Microscope.
If less scratches and grain boundaries
and orientations visible then OK.
Etching
34. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 34
Vickers Hardness test
Specimen cutting
TEST Specimen used Preparation
Vickers
Hardness
• The microstructure specimen was
used for Vickers hardness too.
• Tests were carried out at the cross
section of stir zone on surface
normal to the FSP direction.
• Samples were tested with a load of
100 g and duration of 15s using a
Vickers hardness tester.
35. Methodology - experimentation
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 35
Step 2.4 Perform tests
Specimen cutting
TEST Specimen used Preparation
Tensile
strength
• The tensile specimens were prepared
as per ASTM: E8/E8M-11 standard,
which was cut along the direction of
FSP.
• The tensile test is carried out on a
computer controlled horizontal
tensometer.
37. Methodology – RSM modelling
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 37
38. Methodology – RSM modelling
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 38
Step 3.2 Checking for adequacy of model using ANOVA
• The adequacy of the developed RSM model is tested using the analysis of variance (ANOVA) technique.
• Analysis of Variance (ANOVA) is a statistical method used to test differences between two or more means.
• In order to analyse the
• effect of design factors (namely tool rotational speed and traverse speed) and the
• interactions on the experimental data,
analysis of variance is performed at 95% level of confidence.
• Main effect plot was also plotted.
39. Methodology – RSM modelling
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 40
Step 3.3 Confirmation tests
• Confirmation tests are used to check the robustness of the model created.
• The process parameters for Experiments which are already done are fed into the RSM model and the response is
predicted and error calculated.
40. Methodology – RSM modelling
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 41
Step 3.4 Optimizing the process parameters
In order to determine the optimum process parameter values, contour plots and surface plots were used.
1. Contour plot = A contour plot is produced to visually display the region of optimal factor settings. They play very important
role in the study of the response surface.
• Minitab 16 software is used to optimize the process parameters for obtaining the maximum responses (mechanical
properties).
2. Surface plot = 3D wireframe plots are graphs that are used to explore the potential relationship between three variables.
• The predictor variables are displayed on the x- and y-scales, and the response (z) variable is represented by a smooth
surface (3D surface plot) or a grid (3D wireframe plot).
41. Methodology
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 42
Step 4 Desirability approach
The desirability method is a method used for determining the best conditions for process adjustment, making possible
simultaneous optimization of multiple responses.
According to Derringer and Suich (1980), the algorithm will depend on the optimization type desired for response
(maximization, minimization or normalization) of desired limits within the specification and the amounts (weights) of each
one response, which identifies the main characteristics of different optimization types
42. Methodology - ANN
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 43
Input Layer Hidden Layer 1 Output Layer
Tool rotational speed
Tool traverse speed
Tensile strength
Vickers Hardness
Figure 7 Skeleton of proposed ANN
Ultimate Tensile Strength
44. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 45
Macro structure analysis
Micro structure analysis
Mechanical properties
RSM Modelling
Desirability approach
ANN modelling
45. Results and discussions
46
1. Macro structure analysis
Top view of FSPed sample
• It can be seen that the surface is shiny, reflective
and is free of visible defects.
• No cracks are presents.
• But, in some samples small “ribbon flashes”
are visible. Defects like “surface lack of fill” and
“surface galling” are also not present.
.
46. Results and discussions
47
1. Macro structure analysis
Side view of FSPed sample
• The macro images of the AA5052-O FS processed with different combinations of traverse speeds of 50, 65, 80 mm/min
and rotational speeds of 700, 1000 and 1300 rpm, using Square Pin Profile have been presented in Table 5.1.
• The nugget region exhibited basin-shape for the all the cases of FSP using Square pin profile.
.
Table 5.1 Macro structural images of AA5052-O FS processed at different rotational speed and
traverse speeds, using square pin profile
47. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 48
2. Micro structure analysis
1. Analysis of base material
Figure 5.2 shows the SEM micrograph of as received AA5052 alloy.
• It shows uniform distribution of grains in all the direction.
• The approximate grain size is around 56±6 micrometer.
• The dark block spots represents the presences of intermetallic phases.
• These sports are Al-Mg phases, which were confirmed during spot
EDAX analysis.
Figure 5.2 SEM micrograph of Base material
Uniform grains
Al-Mg intermetallic phases
48. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 49
2. Micro structure analysis
Figure 5.4 SEM micrographs of AA5052-O FS processed at(a) 700 RPM and 65 mm/min
(b)1000 RPM and 65 mm/min (c)1300 RPM and 80 mm/min
2. Analysis of FS Processed material
49. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 50
2. Micro structure analysis
2. Analysis of FS Processed material
Figure shows the micro images of FS processed AA5052-O at different tool rotation speeds and tool traverse
speeds by using SEM.
• It is clear from the images that the grains of the alloys are further refined and uniformly distributed in all the
direction.
• The approximated average grain size is 2±0.5 microns.
• As the rotational speed increases, the grain size increases.
Rotational
speed
Effect Reason
700 RPM No ultrafine grain
Grain is refined
heat generated is not sufficient
Heat generated is sufficient for this.
1000 RPM ultrafine grains. Temperature at nugget zone sufficient.
1300 RPM Grain growth
Ultrafine grain
Temperature produced is more than required.
50. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 51
2. Micro structure analysis
• Figure (a) = SEM image for analysis.
• Figure (b)-(e) = represent the distribution of
Mg, Al, Cu and Si element in the stir zone,
respectively.
• Figure (f) = peaks presents
in the stir zone.
51. Results and discussions
Department of Mechatronics Engineering, MIT Manipal 52
• 3. Fracture analysis
The fracture surfaces exhibit dimple and tear ridges confirming the ductile fracture.
Figure 5.6 SEM micrograph showing the fracture surface of (a) FS processed at 1000 RPM, 80 mm/min (b) base material
Property Non FSP FSP
Dimples Shallow deeper
No. of dimples Less more
Inference % elongation is less % elongation is more
52. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 53
3. Mechanical properties
Vickers hardness (HV) UTS (MPa) % Elongation
68 HV 195 MPa 25
Table 5.2 Mechanical properties of base material
Property effect
Tool Rotational speed
(RPM)
• Tool rotation speed generates heat.
• Lower rotational speeds resulting in lesser heat generation causes improper mixing,
• High rotational speeds affect grain refinement due to heat input.
Tool traverse speed
(mm/min)
• Tool traverse speed supplies heat.
• Lower traverse speed results in higher quantity of heat supply.
Table 5.2 Mechanical properties of base material
53. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 54
0
1
2
3
4
5
6
7
700.0 1000.0 1300.0
SurfaceRoughness(Ra)
Rotational Speed (RPM)
Surface Roughness
50 65 80
RPM Ra
mm/min Ra
Further
mm/min Ra
Observation
Reason
This is due to increase in the
quantity of heat generated
during process.
.This is due to
• decrease in the quantity of
heat supplied to the processed
region &
• tool advancement is greater
than the previous case.
55. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 56
0
10
20
30
40
50
60
70
80
90
100
700.0 1000.0 1300.0
Vickershardness(HV)
Rotational Speed (RPM)
Vickers hardness
50 65 80
0
50
100
150
200
250
300
700.0 1000.0 1300.0
UTS(MPa)
Rotational Speed (RPM)
Ultimate tensile strength
(UTS)
50 65 80
Reason
@700 RPM
This is due to decrease in the quantity of heat supplied to the processed
region which resulted in insufficient mixing of the material lead to
decrease in the hardness.
@1000 RPM
This is due to proper generation and supply of heat at pressed region.
Further, increase in the traverse speed resulted in decrease in the
hardness. The reason behind the decrease in the hardness is due to
improper mixing of the material.
@1300 RPM
This is due to increase in the heat generation which results in turbulence
in the material flow and grain growth.
Observation
@700 RPM mm/min HV
@1000 RPM mm/min HV
@1300 RPM mm/min HV
56. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 57
30.5
31
31.5
32
32.5
33
33.5
34
34.5
35
700.0 1000.0 1300.0
%EL
Rotational Speed (RPM)
Percentage Elongation
50 65 80
Reason
As the rotation speed increases, quantity of heat
generated increases during process.
As the welding speed increases, quantity of heat supplied
decreases.
Observation
RPM %EL
mm/min %EL
57. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 58
4. RSM Modelling
RSM model was developed using the experimental data. The following is the analysis of the model.
4.1 Checking the adequacy of the model using ANOVA (analysis of variance)
• In order to analyse the effect of design factors namely rotational speed and welding speed and the interactions on the
experimental data, analysis of variance is performed at 95% level of confidence. The adequacy of the developed model is
tested using the analysis of variance (ANOVA)
• If the calculated value of Fisher ratio of the developed model is less than the standard Fisher ratio (from F-table) value at
a desired level of confidence 95%, then the model is said to be adequate within the confidence level.
• The value of P> F for three developed models is less than 0.05 (95% Confidence level), which indicates that the model is
significant and lack of fit is not significant, as desired. All the above considerations indicate an excellent adequacy of the
regression models.
58. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 59
4. RSM Modelling
4.2 Equations for prediction
All the regression coefficients were estimated and tested by applying “Response surface design” using Minitab 16 software
for their significance at a 95% confidence level. After determining the significant coefficients, the final model was developed
to predict the surface roughness, Vickers hardness, ultimate tensile strength and percentage elongation. The equations are as
follows.
x = rotational speed (RPM)
y = traverse speed (mm/min)
Surface roughness
Vickers hardness
Ultimate tensile strength
Percentage elongation
59. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 60
4. RSM Modelling
Source DF Seq SS Adj SS Adj MS F P
1. Regression 5 15.6456 15.6456 3.12912 151.30 0.000
Linear 2 14.7215 0.81 0.40498 19.58 0.001
x 1 14.6922 0.7027 0.70265 33.98 0.001
y 1 0.0293 0.0314 0.03141 1.52 0.258 insignificant
Square 2 0.8565 0.8565 0.42826 20.71 0.001
x2 1 0.7764 0.4996 0.49964 24.16 0.002
y2 1 0.0801 0.0801 0.08013 3.87 0.090 insignificant
Interaction 1 0.0676 0.0676 0.06760 3.27 0.114 insignificant
xy 1 0.0676 0.0676 0.06760 3.27 0.114 insignificant
2. Residual Error 7 0.1448 0.1448 0.02068
Lack-of-Fit 3 0.1424 0.1424 0.04748 81.87 0.000
Pure Error 4 0.0023 0.0023 0.00058
Total 12 15.7904
Table 5.6 ANOVA for Surface roughness (surface quadratic model)
60. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 61
4. RSM Modelling
Table 5.6 ANOVA for Vickers hardness (surface quadratic model)
Source DF Seq SS Adj SS Adj MS F P
1. Regression 5 950.11 950.109 190.022 23.35 0.000
Linear 2 68.33 144.798 72.399 8.90 0.012
x 1 48.17 3.790 3.790 0.47 0.517 insignificant
y 1 20.17 144.778 144.778 17.79 0.004
Square 2 575.53 575.525 287.763 35.56 0.000
x2 1 254.82 62.996 62.996 7.74 0.027
y2 1 320.71 320.710 320.710 39.41 0.000
Interaction 1 306.25 306.25 306.250 37.63 0.000
xy 1 306.25 306.25 306.250 37.63 0.000
2. Residual Error 7 56.97 56.968 8.138
Lack-of-Fit 3 54.97 54.968 18.323 0.002 0.002
Pure Error 4 2.00 2.00 0.500
Total 12 1007.08
61. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 62
4. RSM Modelling
Table 5.6 ANOVA for UTS (surface quadratic model)
Source DF Seq SS Adj SS Adj MS F P
1. Regression 5 6282.58 6282.58 1256.52 60.86 0.000
Linear 2 576.15 1058.95 529.48 25.65 0.001
x 1 445.48 2.09 2.09 0.10 0.759 insignificant
y 1 130.67 1009.07 1009.07 48.88 0.000
Square 2 4142.23 4142.23 2071.11 100.32 0.000
x2 1 2100.42 633.05 633.05 30.66 0.001
y2 1 2041.81 2041.81 2041.81 98.90 0.000
Interaction 1 1564.20 1564.20 1564.20 75.77 0.000
xy 1 1564.20 1564.20 1564.20 75.77 0.000
2. Residual Error 7 144.51 144.51 20.64
Lack-of-Fit 3 141.92 141.92 47.31 73.00 0.001
Pure Error 4 2.59 2.59 0.65
Total 12 6427.09
62. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 63
4. RSM Modelling
Table 5.6 ANOVA for % Elongation (surface quadratic model)
Source DF Seq SS Adj SS Adj MS F P
1. Regression 5 37.0593 37.0593 7.4119 118.52 0.000
Linear 2 16.0651 8.9745 4.4873 71.75 0.000
x 1 15.1051 8.2143 8.2143 131.35 0.000
y 1 0.9600 0.1308 0.1308 2.09 0.191 insignificant
Square 2 18.8772 18.8772 9.4386 150.93 0.000
x2 1 18.2857 13.4012 13.4012 214.29 0.000
y2 1 0.5914 0.5914 0.5914 9.46 0.018
Interaction 1 2.1170 2.1170 2.1170 33.85 0.001
xy 1 2.1170 2.1170 2.1170 33.85 0.001
2. Residual Error 7 0.4378 0.4378 0.0625
Lack-of-Fit 3 0.4367 0.4367 0.1456 539.12 0.000
Pure Error 4 0.0011 0.0011 0.1456
Total 12 37.4970 0.0003
63. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 64
4. RSM Modelling
4.3 Confirmation tests
• Confirmation tests are used to check the robustness of the model created.
• The process parameters for Experiments which are already done are fed into the RSM model and the
response is predicted.
• The difference between the already Experimentally obtained data and newly predicted data is termed as
Error. The error must be below 10% for the model to be accepted.
66. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 67
4. RSM Modelling
4.4 Graphs and analysis
1. Surface roughness
2. Vickers hardness
3. Ultimate tensile strength
4. Percentage elongation
67. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 68
4.4.1 Surface roughness
13001000700
6.0
5.5
5.0
4.5
4.0
3.5
3.0
806550
Rotational speed (RPM)
Mean
Traverse speed (mm/min)
Main Effect plot for Surface roughness (Ra) • The reference line represents the overall mean.
• RPM line is not ||r to the X axis affects Ra
• Mm/min line is almost ||r to X axis has less
effect.
• However, in the middle (i.e., 60-70 mm/min) there is
mean effect.
• Optimum combination is - 1300 RPM and 65
mm/min.
68. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 69
4.4.1 Surface roughness
• The contours are band like.
• It can be inferred that for a Ra of less than 3µm,
• Tool rotation speed =1200 RPM to 1300 RPM
• Welding speed = 55 mm/min to 80 mm/min
Rotational speed (RPM)
Traversespeed(mm/min)
1300120011001000900800700
80
75
70
65
60
55
50
>
–
–
–
–
–
–
< 3.0
3.0 3.5
3.5 4.0
4.0 4.5
4.5 5.0
5.0 5.5
5.5 6.0
6.0
(Ra)
Roughness
Contour Plot for Surface Roughness (Ra)
70. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 71
(RPM) Mm/min Result Reason
a Low Low Highest Ra Tool rotation speed generates heat. This heat leads to localized plastic deformation which in
turn, is responsible for smoother surface.
• Hence, low tool speed less heat generated less plastic deformation rough
surface
Tool traverse speed supplies the heat generated.
• Less welding speed more heat supplied.
b Low high
c High Low Very less Ra High amount of heat generated. High amount of heat supplied.
A lot of plastic deformation. Hence, less surface roughness.
d High High Less Ra So, here high heat generated, less amount of heat supplied to the sample (but Welding
speed has less effect on Ra). High heat generated would be more than the optimum, hence,
more roughness
e High Medium Least Ra optimum values.
71. Results and discussions
4.4.2 Vickers hardness and UTS
13001000700
90.0
87.5
85.0
82.5
80.0
77.5
75.0
806550
Rotational speed (RPM)
Mean
Traverse speed (mm/min)
Main Effect plot for Hardness (HV)
13001000700
280
270
260
250
240
806550
Rotational speed (RPM)
Mean
Traverse speed (mm/min)
Main Effect plot for UTS (MPa)
• The reference line represents the overall mean.
• Both the Parameters have high degree of impact on the Vickers hardness and UTS . For both the parameters, it can be seen that
the graph peeks in the middle and hence the main effect plot showed maxima in the middle.
• For both the parameters, Vickers Hardness & UTS first increases with increase in the value of parameters, but then decreases
it the values are further increased.
• The optimum combination would be 1000 RPM and 65 mm/min.
72. Results and discussions
4.4.2 Vickers hardness and UTS
Rotational speed (RPM)
Traversespeed(mm/min)
1300120011001000900800700
80
75
70
65
60
55
50
>
–
–
–
–
–
< 65
65 70
70 75
75 80
80 85
85 90
90
(HV)
Hardness
Contour Plot for Surface Hardness (HV)
Rotational speed (RPM)
Traversespeed(mm/min)
1300120011001000900800700
80
75
70
65
60
55
50
>
–
–
–
< 220
220 240
240 260
260 280
280
UTS (MPa)
Contour Plot for UTS (MPa)
• This graph too indicates us that the central region has the maximum hardness when both Rotational Speed and Traverse
Speed are at median.
• It can be observed that the contours are in circular pattern. as compared to the bands like contours of Surface Roughness
• So an optimum range would be from 830-1130 RPM and around 55-70 mm/min.
73. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 74
4.4.2 Vickers hardness and UTS
No general trend can be observed here with respect to the individual parameters.
Tool Rotation Speed Traverse Speed Result
a low low High Hardness
b low high low hardness
c high low Least hardness
d high high High hardness
e median median Highest hardness
74. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 75
4.4.4 Percentage elongation
• The reference line represents the overall mean.
• RPM not ||r to the X axis affects %EL
• Mm/min line is almost ||r to X axis has less effect
• However, in the middle (i.e., 60-70 mm/min) there is mean
effect
• Observation
• % EL decreases sharply as both the parameters increase,
• but rebounds after a sharp dip which is when both
the parameters have median values.
• optimum for minimum %Elongation would be 1000 RPM
and 65 mm/min.13001000700
36
35
34
33
32
31
806550
Rotational speed (RPM)
Mean
Traverse speed (mm/min)
Main Effect plot for Percentage Elongation
75. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 76
4.4.4 Percentage elongation
• This graph indicates that the
central White region has the least %elongation
when both Rotational Speed and Traverse Speed are
a. at median
b. at high traverse and rotational speeds.
• It can be observed that the contours are in circular
pattern.
Rotational speed (RPM)
Traversespeed(mm/min)
1300120011001000900800700
80
75
70
65
60
55
50
>
–
–
–
–
< 32
32 33
33 34
34 35
35 36
36
%EL
Contour Plot for % Elongation
76. Results and discussions
6/19/2017 77
4.4.4 Percentage elongation
A general trend of decrease in % elongation can be
observed with
• RPM , mm/min %EL
• however the contribution both the parameters
towards %EL is observed to be different.
• At different points
Tool Rotation
Speed (RPM)
Traverse
Speed (mm/min)
Result
a low low High %EL
b low high High %EL
c high low Less %EL
d high high Least %EL
e median median Least %EL
77. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 78
5. Desirability approach
Composite Desirability (D)
It is the overall index calculated from combination of each response variables processed through a geometric
mean
• This index is responsible for showing the best condition to optimize all responses variables at the same
time.
• The goal is to obtain the highest possible value for D.
• Our goal is to get, Using Minitab 16’s Response Optimizer,
minimum roughness and % Elongation
maximum UTS and Hardness.
78. Results and discussions
Here Ra has an importance of 0.75. We did 4 iterations. For each response, the importance was varied while keeping others at 1.
Department of Mechatronics Engineering, MIT Manipal 79
Table 5.19 Specifications loaded in Response optimizer
79. Results and discussions
Cur
High
Low0.89014
D
Optimal
d = 0.82391
Minimum
Roughnes
y = 3.1035
d = 0.85161
Maximum
Hardness
y = 88.5482
d = 0.89631
Maximum
UTS (MPa
y = 276.3566
d = 1.0000
Minimum
%EL
y = 31.0861
0.89014
Desirability
Composite
50.0
80.0
700.0
1300.0
TraverseRotation
[1178.7879] [69.3939]Cur
High
Low0.89863
D
Optimal
d = 0.76704
Minimum
Roughnes
y = 3.2855
d = 0.87962
Maximum
Hardness
y = 89.3887
d = 0.92899
Maximum
UTS (MPa
y = 279.3961
d = 1.0000
Minimum
%EL
y = 31.0311
0.89863
Desirability
Composite
50.0
80.0
700.0
1300.0
TraverseRotation
[1130.3030] [68.4848] Cur
High
Low0.88416
D
Optimal
d = 0.80328
Minimum
Roughnes
y = 3.1695
d = 0.86278
Maximum
Hardness
y = 88.8835
d = 0.90934
Maximum
UTS (MPa
y = 277.5683
d = 1.0000
Minimum
%EL
y = 31.0509
0.88416
Desirability
Composite
50.0
80.0
700.0
1300.0
TraverseRotation
[1160.6061] [69.0909]Cur
High
Low0.89318
D
Optimal
d = 0.82391
Minimum
Roughnes
y = 3.1035
d = 0.85161
Maximum
Hardness
y = 88.5482
d = 0.89631
Maximum
UTS (MPa
y = 276.3566
d = 1.0000
Minimum
%EL
y = 31.0861
0.89318
Desirability
Composite
50.0
80.0
700.0
1300.0
TraverseRotation
[1178.7879] [69.3939]
(a) 0.75 importance to Ra (b) 0.75 importance to UTS (c) 0.75 importance to HV (d) 0.75 impt.to %EL
By looking at all the 4 graphs the inferences that can be drawn are
1. When Surface Roughness is given an importance of 0.75, it has
The maximum overall composite Desirablity
The maximum UTS
The minimum %EL
The maximum Hardness
2. This leads us to select the process parameters mentioned by the 1st approach as the
desirable optimization approach.
3. Hence, 1130.30 RPM and 68.48 mm/min is selected as the process parameter.
80. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 81
6. ANN Modelling
6.1 Architecture of ANN
Figure 5.14 shows the architecture of the ANN developed.
• 2 inputs (tool rotation speed and traverse speed)
• 2 hidden layers.
• The first hidden layer has 10 neurons while the second hidden layer has 3 neurons.
• 3 outputs, namely, Vickers hardness, UTS and %Elongation.
Figure 5.14 Architecture of the Artificial Neural Network
81. Results and discussions
6. ANN Modelling
6.2 Process parameters
2 Number of hidden layers 2
3 Number of hidden neurons 13
4 Transfer function used Logsig(sigmoid)
5 Number of patterns used for training 70%
6 Number of patterns used for testing 15%
7 Number of patterns used for validation 15%
8 Number of epochs 1000
9 Learning factor 0.01
10 Momentum factor 0.9
11 Training function Trainscg
12 Max_fail 60
13 Goal 0
14 Time infinity
15 Minimum gradient 0.000001
16 Show iteration till 250
17 sigma 0.00005
82. Results and discussions
83
6. ANN Modelling
6.3 Training of ANN
Figure shows the training of the Neural Network by 101 epochs, or, iterations.
Blue line
Input process parameters of already conducted
experimental data to train the neural network.
An output graph is created.
Red line
same input is again put in the neural network and
ANN’s response is recorded.
This tells how much the neural network was trained.
83. Results and discussions
84
6. ANN Modelling
6.3 Training of ANN
Figure shows the training of the Neural Network by 101 epochs, or, iterations.
Green line
After training, new experiments were conducted
now these process parameters were sent as input in order
to compare the Experimental data and the ANN predicted
output response.
Dotted line
The dotted line shows the best Validation performance.
The best performance is at 41 epochs, i.e.,
After 41 iterations of the 9 experimental data the
best results can be found.
84. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 85
6. ANN Modelling
6.4 Learning using scaled conjugate gradient algorithm
• This graph shows the gradient value. The minimum
gradient we selected was 0.000001. That is not visible
in graph (a). Here the gradient value which we get is
1.7834
• For graph (b) 101 iteration took place.
The best performance was 60 after 101 iterations.
88. Conclusions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 89
Objective 1. Investigation of effect of FSP parameters
What we have been able to achieve is
6.37
68
228
25
2.93
93
284
31.3
-54.00313972
36.76470588
24.56140351
25.2
-100 -50 0 50 100 150 200 250 300 350
Ra
HV
UTS
%EL
Effect of FSP on AA 5052-O
%change after FSP original
89. Conclusions
Optimum RPM Optimum mm/min Contribution of parameters
Ra 1300 (high) 65 (median) Tool rotation speed has highest influence
HV &
UTS
1000 (median) 65-70 (median) Both
%EL 1350 (high)
1000 (median)
80 (high)
60 (median)
Tool rotation speed has highest influence
Objective 2. Build a prediction model
Using RSM
a. The model developed is robust as it passes ANOVA and Confirmation tests with less than 5% error between the
experimental and predicted values.
• We have been able to pin point
• optimum range of values
• Effect of process parameters
90. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 91
Using ANN
a. A robust ANN model using Scale conjugate gradient was developed which could be trained in 41
iterations to give a validation performance of 8.866. This model can be used to predict Vickers Hardness,
UTS and %Elongation with high accuracy.
91. Results and discussions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 92
6. ANN modelling
The desirability method is a method used for determining the best conditions for process adjustment, making possible
simultaneous optimization of multiple responses.
According to Derringer and Suich (1980), the algorithm will depend on the optimization type desired for response
(maximization, minimization or normalization) of desired limits within the specification and the amounts (weights) of each
one response, which identifies the main characteristics of different optimization types
92. Conclusions
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 93
Objective 3. Desirability approach
1. For simultaneous responses, we have been able to build a composite desirable model with 0.75 importanc eto Surface
roughness, which would give us
Property Value
Ra 3.2855 µm
UTS 279.39 MPa
HV 89.388 HV
%EL 31.03
93. Scope for future work
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 94
In the FSF process, a modified friction stir welding tool is plunged into the top work piece,
• simultaneously creating frictional heat, stirring, and forming the work material into a new shape.
• The new shape has many possible applications.
Figure 6.1 Illustration of new friction stir processes
Currently, for depositing Monel for corrosion protecting of Steel
• electroplating is done.
• However, this process is very problematic and inconsistent
INSTEAD
In the friction surfacing process, a consumable, usually a softer material is rotated and forced into the stronger substrate
material. As the frictional heat builds, the spinning work material softens and is deposited onto the surface.
• FSD = FSF + friction surfacing.
• The transferred material forms to the shape where it is deposited.
The future of this technology is the capability to friction stir deposit material in situ for coating, reduction of stress
concentration at joints and welds, crack filling, etc.
.
95. References
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 96
1. Asadi, P., Faraji, G., Besharati, M.K., 2010. Producing of AZ91/SiC composite by friction stir processing (FSP). Int. J. Adv. Manuf. Technol. 51, 247–260, http://dx.doi.org/10.1007/s00170-
010-2600
2. Azizieh, M., Kokabi, A.H., Abachi, P., 2011. Effect of rotational speed and probe profile on microstructure and hardness of AZ31/Al2O3nanocomposites fabricated by friction stir processing.
Mater. Design 32, 2034–2041, http://dx.doi.org/10.1016/j.matdes.2010.11.055
3. Barmouz, M., Givi, M.K.B., Seyfi, J., 2011a. On the role of processing parameters in producing Cu/SiC metal matrix composites via friction stir processing: Investigating microstructure,
micro hardness, wear and tensile behavior. Mater. Charact. 62,108–117, http://dx.doi.org/10.1016/j.matchar.2010.11.005
4. Dolatkhah, A., Golbabaei, P., Givi, M.K.B., Molaiekiya, F., 2012. Investigating effects of process parameters on micand mechanical properties rostructural of Al5052/SiC metal matrix
composite fabricated via friction stir processing. Mater. Design 37,458–464, http://dx.doi.org/10.1016/j.matdes.2011.09.035
5. Elangovan, K., Balasubramanian, V., Valliappan, M., 2007. Influences of tool pin pro-file and axial force on the formation of friction stir processing zone in AA6061aluminium alloy. Int. J.
Adv. Manuf. Technol. 38, 285–295, http://dx.doi.org/10.1007/s00170-007-1100-2
6. Faraji, G., Dastani, O., Mousavi, S.A.A.A., 2011. Effect of process parameters on microstructure and micro-hardness of AZ91/Al2O3surface composite produced by FSP. J. Mater. Eng.
Perform. 20, 1583–1590, http://dx.doi.org/10.1007/s11665-010-9812-0
7. Farias, A., Batalha, G.F., Prados, E.F., Magnabosco, R., Delijaicov, S., 2013. Tool wear evaluations in friction stir processing of commercial titanium Ti-6Al-4 V. Wear302, 1327–1333,
http://dx.doi.org/10.1016/j.wear.2012.10.025
8. Gandra, J., Miranda, R., Vilac¸ a, P., Velhinho, A., Teixeira, J.P., 2011. Functionally graded materials produced by friction stir processing. J. Mater. Process. Tech.211, 1659–1668,
http://dx.doi.org/10.1016/j.jmatprotec.2011.04.016
96. References
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 97
9. Ghasemi-Kahrizsangi, A., Kashani-Bozorg, S.F., 2012. Microstructure and mechanical properties of steel/TiC Nano-composite surface layer produced by friction stir processing. Surf. Coat.
Tech. 209, 15–22, http://dx.doi.org/10.1016/j.surfcoat.2012.08.005
10. Heidarzadeh, A., Jabbari, M., Esmaily, M., 2014. Prediction of grain size and mechanical properties in friction stir welded pure copper joints using a thermal model. Int. J. Adv. Manuf.
Technol., 1–11, http://dx.doi.org/10.1007/s00170-014-6543-7
11. Kapoor, R., Kumar, N., Mishra, R.S., Huskamp, C.S., Sankaran, K.K., 2010. Influence of fraction of high angle boundaries on the mechanical behavior of an ultrafine grained Al-Mg alloy.
Mater. Sci. Eng. A 527, 5246–5254, http://dx.doi.org/10.1016/j.msea.2010.04.086
12. Khayyamin, D., Mostafapour, A., Keshmiri, R., 2013. The effect of pro-cess parameters on microstructural characteristics of AZ91/SiO2com-posite fabricated by FSP. Mater. Sci. Eng. A 559,
217–221, http://dx.doi.org/10.1016/j.msea.2012.08.084
13. Kurt, A., Uygur, I., Cete, E., 2011. Surface modification of aluminium by friction stir processing. J. Mater. Process. Tech. 211, 313–317,
http://dx.doi.org/10.1016/j.jmatprotec.2010.09.020Kwon
14. McNelley, T.R., Swaminathan, S., Su, J.Q., 2008. Recrystallization mechanisms during friction stir welding/processing of aluminum alloys. Scripta Mater. 58, 349–354,
http://dx.doi.org/10.1016/j.scriptamat.2007.09.064
15. Mishra, R.S., Ma, Z.Y., 2005. Friction stir welding and processing. Mater. Sci. Eng. R50, 1–78, http://dx.doi.org/10.1016/j.mser.2005.07.001
97. References
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 98
16. Mishra, R.S., Ma, Z.Y., Charit, I., 2003. Friction stir processing: a novel technique for fabrication of surface composite. Mater. Sci. Eng. A 341, 307–310, http://dx.doi.org/10.1016/S0921-
5093(02)00199-5
17. Moghaddas, M.A., Kashani-Bozorg, S.F., 2013. Effects of thermal conditions on microstructure in nanocomposite of Al/Si3N4 produced by friction stir processing. Mater. Sci. Eng. A 559,
187–193, http://dx.doi.org/10.1016/j.msea.2012.08.073
18. Nandan, R., Debroy, T., Bhadeshia, H., 2008. Recent advances in friction-stir welding-Process, weldment structure and properties. Prog. Mater. Sci. 53, 980–1023,
http://dx.doi.org/10.1016/j.pmatsci.2008.05.001
19. Padmanaban, G., Balasubramanian, V., 2009. Selection of FSW tool pin profile, shoulder diameter and material for joining AZ31B magnesium alloy-An experimental approach. Mater. Design
30, 2647–2656, http://dx.doi.org/10.1016/j.matdes.2008.10.021
20. Palanivel, R., Koshy Mathews, P., Murugan, N., Dinaharan, I., 2012. Effect of tool rotational speed and pin profile on microstructure and tensile strength of dissimilar friction stir welded
AA5083-H111 and AA6351-T6 aluminum alloys. Mater. Design 40, 7–16, http://dx.doi.org/10.1016/j.matdes.2012.03.027
21. Rai, R., De, A., Bhadeshia, H.K.D.H., DebRoy, T., 2011. Review: friction stir welding tools. Sci. Technol. Weld. JOI 16, 325–342, http://dx.doi.org/10.1179/1362171811y.0000000023
22. Shamsipur, A., Kashani-Bozorg, S.F., Zarei-Hanzaki, A., 2011. The effects of friction-stir process parameters on the fabrication of Ti/SiC nanocomposite surface layer. Surf. Coat. Tech. 206,
1372–1381, http://dx.doi.org/10.1016/j.surfcoat.2011.08.065
23. Valiev, R.Z., Korznikov, A.V., Mulyukov, R.R., 1993. Structure and properties of ultrafine-grained materials produced by severe plastic deformation. Mater. Sci.Eng. A 168, 141–148,
http://dx.doi.org/10.1016/0921-5093(93)90717-S
24. Xu, N., Ueji, R., Fujii, H., 2014. Enhanced mechanical properties of 70/30 brass joint by rapid cooling friction stir welding. Mater. Sci. Eng. A 610, 132–138,
http://dx.doi.org/10.1016/j.msea.2014.05.037
98. References
6/19/2017 Department of Mechatronics Engineering, MIT Manipal 99
26. Xue, P., Xiao, B.L., Ma, Z.Y., 2014. Achieving ultrafine-grained structure in a pure nickel by friction stir processing with additional cooling. Mater. Design 56,848–851,
http://dx.doi.org/10.1016/j.matdes.2013.12.001
27. You, G.L., Ho, N.J., Kao, P.W., 2013a. In-situ formation of Al2O3nanoparticles during friction stir processing of AlSiO2composite. Mater. Charact. 80, 1–8,
http://dx.doi.org/10.1016/j.matchar.2013.03.004
28. 28. You, G.L., Ho, N.J., Kao, P.W., 2013b. The microstructure and mechanical properties of an Al-CuO in-situ composite produced using friction stir processing. Mater. Lett. 90, 26–29,
http://dx.doi.org/10.1016/j.matlet.2012.09.028
29. 29. Yu, Z., Zhang, W., Choo, H., Feng, Z., 2011. Transient heat and material flow modeling of friction stir processing of magnesium alloy using threaded tool. Metall. Mater.Trans. A 4
2010.07.024
30. 30. Zhang, Q., Xiao, B.L., Ma, Z.Y., 2013. In situ formation of various intermetallic particles in Al-Ti-X (Cu, Mg) systems during friction stir processing. Intermetallics40, 36–44,
http://dx.doi.org/10.1016/j.intermet.2013.04.003 3, 724–737, http://dx.doi.org/10.1007/s11661-011-0862
Editor's Notes
Add results, conclusion at endIntroduction
Review of literature
Objectives
Methodology
Timeline
Budget
Result
conclusion
References
Grain morphology - Two of the key microstructural parameters in the as-cast microstructure of an alloy are the grain size and the secondary dendrite arm spacing (SDAS).
Fundamentally, these parameters can be used to describe the morphology of a grain.
Where the grain size is large and the dendrite arm spacing is small, the grains are dendritic; when the grain size is only a little greater than the dendrite arm spacing then a rosette or cellular grain morphology is observed, and if the grains are spherical or globular then no dendrites are observed. The grain size, SDAS and grain morphology affect various properties of the alloy including their castability,1,2) especially hot tearing resistance,3) their mechanical properties,4) and are especially important in semi-solid processing.5–7)
1. g/cc =1 g per centimeter cube
2. Fcc = face centred cubic. 1/8* 8 corner atoms + 1/2*6 face atoms = 12 coordination no.,, tightly packed. .. 8 tetrahedral void, 4 octahedral void.
3.
Low MP -- restricts the maximum temperature at which it can be used. Hence aircraft में ya space में high temp. so cannot be used. 4.5% copper is added to overcome this.
Soft – why not usable ? (where lightweight and stronger materials are required).
Solid State welding process – it will not melt the material.
Laser welding – it will melt the material.
Why FSP needed ?
Q1) feed forward architecture? input will go in 1 direction… ek direction में aage badhega. Input
Error back propagation? kuch o/p aaya, 0.5, we need 0.6, hence 0.1 will be used to modify the weights. How did you calculate error ? summed square method ?
What is the contribution of error in modifying each weight ? use gradient descent method. Mechanical properties - strength, hardness..Elastic deformation. Plastic deformation. Yield point. Yield stress. Tensile strength. Ductility. Resilience. .Toughness.
Metallurgical properties – defects, phase, strength
Literature review kar rhe hai all time yeh भी bolo.
Before may 9 you have to submit.
W4 – you have done fsp. Now you have to do tests for microstructure, tensile strength, hardness prepare the specimen. 2 weeks.
W5 – if you don’t see then again polish, etch. Polish – make the surface smooth and shiny.Etching - use strong acid or mordant to cut into the unprotected parts of a metal surface to create a design in intaglio (incised) in the metalSEM – scanning electron microscope.
Kuch papers में SEM chahiye kuch में Optical microscope. Hence we are using both.Difference b/w SEM and Optical microscope optical microscope uses light to illuminate specimen while SEM uses a beam of electrons. Also SEM resolution is very high (50000x). SEM is available in MIT.
W6 – VHT में indent banao on the test material using diamond indenter. Then measure the indent and compare to table to get hardness.
Multiple measurement lena hoga.
W7 – why UTM naam ? The "universal" part of the name reflects that it can perform many standard tensile and compression tests on materials, components, and structures
W10 – Confirmation tests.. Now you have prediction model, so it will give o/p like hardness, tensile strength for any input tool speed, feed speed and probe you enter.
W11 – Validation test - Now you will perform the above test manually and check. And get the error.
W12 – write thesis till submission.
Annealing - heat treatment that alters the physical and sometimes chemical properties
increase its ductility and reduce its hardness, making it more workable
Annealing involves heating steel to a specified temperature Tempering involves heating the metal to a precise temperature below the critical point, and is often and then cooling at a very slow and controlled rate. done in air, vacuum or inert atmospheres.
Annealing is commonly used to:
Soften a metal for cold working
Improve machinability
Enhance electrical conductivity
Why FSP needed ?
See reference 3 for more properties.
Other considered – HSS – High speed steel.
The Rockwell scale is a hardness scale based on indentation hardness of a material.
The Rockwell test determines the hardness by measuring the depth of penetration of an indenter
under a large load compared to the penetration made by a preload
Ra =1/n * sigma of all roughness
Polishing - Polishing is the process of creating a smooth and shiny surface by rubbing it or using a chemical action, leaving a surface with a significant specular reflection (still limited by the index of refraction of the material according to the Fresnel equations.)[1] In some materials (such as metals, glasses, black or transparent stones) polishing is also able to reduce diffuse reflection to minimal values.
Emery paper type of abrasive paper or sandpaper, that can be used to abrade (remove material from) surfaces or mechanically finish a surface. Operations include deburring, polishing, paint removal, corrosion removal, sizingBy the successive use of progressively finer mesh emery paper, near-mirror finishes can be obtained.
Difference between different grit paper - When using sandpaper, the key consideration is grit size, or relative smoothness of the sandpaper. The rule is that you go from coarse to progressively finer smoothness
Etching
Etching is traditionally the process of using strong acid or mordant to cut into the unprotected parts of a metal surface to create a design in intaglio (incised) in the metal.
Keller’s etchKeller's reagent is a mixture of nitric acid, hydrochloric acid, and hydrofluoric acid, used to etch aluminum alloys to reveal their grain boundaries and orientations
Keller reagent will eat the side edges of the grain, so that you would be able to see the grain structure.
HV – Vickers pyramid number
The solid-state nature of the FSW process, combined with its unusual tool shape and asymmetric speed profile, results in a highly characteristic microstructure. The microstructure can be broken up into the following zones:
The stir zone (also nugget, dynamically recrystallised zone) is a region of heavily deformed material that roughly corresponds to the location of the pin during welding. The grains within the stir zone are roughly equiaxed and often an order of magnitude smaller than the grains in the parent material.[11] A unique feature of the stir zone is the common occurrence of several concentric rings which has been referred to as an "onion-ring" structure.[12] The precise origin of these rings has not been firmly established, although variations in particle number density, grain size and texture have all been suggested.
The flow arm zone is on the upper surface of the weld and consists of material that is dragged by the shoulder from the retreating side of the weld, around the rear of the tool, and deposited on the advancing side.[citation needed]
The thermo-mechanically affected zone (TMAZ) occurs on either side of the stir zone. In this region the strain and temperature are lower and the effect of welding on the microstructure is correspondingly smaller. Unlike the stir zone the microstructure is recognizably that of the parent material, albeit significantly deformed and rotated. Although the term TMAZ technically refers to the entire deformed region it is often used to describe any region not already covered by the terms stir zone and flow arm.[citation needed]
The heat-affected zone (HAZ) is common to all welding processes. As indicated by the name, this region is subjected to a thermal cycle but is not deformed during welding. The temperatures are lower than those in the TMAZ but may still have a significant effect if the microstructure is thermally unstable. In fact, in age-hardened aluminium alloys this region commonly exhibits the poorest mechanical properties.[13]
ASTM: E8/E8M-11 – it is a standard test method for tensile test testing.
computerized tensometer experimental setup for tensile test
Fixture setup for tensile test
Schematic of tensile specimen draw as per your diagram
Tensile test specimens
Regression -
a measure of the relation between the mean value of one variable (e.g. output) and corresponding values of other variables (e.g. time and cost).
Variance mean nikalo, (each no – mean ) ka square / total
Square root of variance std. deviation.
How to select 1 hidden layer or 2 hidden layer ? agar ek se o/p aa gya toh 1 hidden layer, bad results then 2 hidden layer.
What is hidden layer ?
#DUCTILE FRACTURE
In ductile fracture, extensive plastic deformation (necking) takes place before fracture.
The terms rupture or ductile rupture describe the ultimate failure of ductile materials loaded in tension.
Rather than cracking, the material "pulls apart," generally leaving a rough surface. In this case there is slow
propagation and an absorption of a large amount energy before fracture.
The ductility of a material is also referred to as toughness.The basic steps in ductile fracture are: void formation, void coalescence (also known as crack formation),
crack propagation, and failure, often resulting in a cup-and-cone shaped failure surface
#BRITTLE FRACTURE
In brittle fracture, no apparent plastic deformation takes place before fracture. In brittle crystalline materials,
fracture can occur by cleavage as the result of tensile stress acting normal to crystallographic planes with low bonding
(cleavage planes). In amorphous solids, by contrast, the lack of a crystalline structure results in a conchoidal fracture,
with cracks proceeding normal to the applied tension.
The confidence level assumed for this project was 95%. So, anything above 0.05 is insignificant.
DF =
The confidence level assumed for this project was 95%. So, anything above 0.05 is insignificant.
The confidence level assumed for this project was 95%. So, anything above 0.05 is insignificant.
The confidence level assumed for this project was 95%. So, anything above 0.05 is insignificant.