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Dynamic Tensile Testing of Fabric-Cement Composites
Deju ZHU, Barzin MOBASHER
Civil and Environmental Engineering, Arizona State University, USA
Flavio SILVA
Institute of Construction Materials – Technical University of Dresden, Dresden, Germany
Alva PELED
Structural Eng. Dept., Ben Gurion University, Israel
International Conference on Material Science and 64th RILEM Annual Week
Aachen, Germany, Sept. 6– 9, 2010
Outline
 Introduction
 Objectives
 Setup of dynamic tensile testing
 Specimen preparation and data analysis
 Failure behavior of composites
 Conclusions
Introduction
•HPFRCC, Strain-hardening behavior
•Cases for dynamic loading:
• blast explosions,
• projectiles,
• earthquakes,
• fast moving traffic,
• wind gusts, wind driven objects,
• machine vibrations.
•Inherent brittleness and low tensile strength,
dynamic loading can cause severe damage.
•mechanical properties at high strain rates for
analysis of structural components.
0 0.01 0.02 0.03 0.04
Strain, mm/mm
0
4
8
12
16
20
Stress,MPa
AR Glass Fabric
GFRC
Vf =5%
PE Fabric
E-Glass
Fabric
Mortar
ECC
Objectives
Study the role of fabric type on the tensile behavior of textile composites
 Study the strain rate effect on the mechanical material properties
 Investigate the failure behavior (cracking) of different composite system
under dynamic loading
High Speed Testing System at ASU
Servohydraulic system, Speed Up to 14 m/s, Load Capacity: 90 kN load
High Strain Rate Tensile Test
AR-Glass- bonded Carbon FabricPE- Knitted
Textile Materials
Alkali Resistant (AR)-Glass: Bonded fabric, multifilament impregnated with sizing
Polyethylene (PE): Knitted fabric, monofilament
Carbon Fabric: Fiber Bundle
5mm
Yarn type Yarn nature
Strength
(MPa)
Young’s Modulus
(MPa)
Filament size
(mm)
Bundle diameter
(mm)
PE Monofilament 240 1760 0.250 0.25
AR-Glass Bundle 1372 72000 0.014 0.30
Carbon Bundle 2200 240000 0.008 1.15
Table 1 Mechanical properties and geometry of the yarns used in the fabric manufacture
Composite Preparation: Pultrusion Process
Cement Composite
Laminates
Squeeze Rollers
Cement
Bath
Fabric
Mix design of the matrix
Cement: 42%
Silica fume: 0% and 5%
Super-plasticizer: 0.1%
water/cement ratio :0.4
Composite: 6 layer fabrics
Curing: in water at room
temperature for 28 days
Cut into specimens: 25mm
x150 mm (width x length).
Data Processing
Data Processing
Data Processing
Typical Response under high speed Tension
Videos of AR-Glass Fabric and Composites
AR-Glass CompositeAR-Glass Fabric
Failure of AR-Glass Composite
(a) (b) (c) (d) (e)
T= 0.4 ms T= 0.6 ms T= 0.8 ms T= 1.5 ms
Yarn
breakage
T= 4.0 ms
AR glass composites
(plain cement):
(a)-(c) multiple micro-
cracking,
(d) main crack widening
and other micro-cracks
closing,
(e) complete failure
(a) (b) (c) (d) (e)
T= 0.5 ms T= 5.8 ms T= 4.0 msT= 0 ms T= 1.5 ms
AR glass composites
(5%silica fume):
(a)-(c) multiple micro-
cracking,
(d) main crack widening
and other micro-cracks
closing,
(e) complete failure
Microstructure of AR-Glass Composite
Bundle
with
coating
Matrix
SEM micrographs of AR glass fabric embedded in
cement matrix, side view
Stress-Strain Curves of AR-Glass Fabric
and AR-Glass Composite
Stress-strain of AR-Glass
Composite(5% Silica Fume)
Stress-strain of AR-Glass
Fabric
0 0.01 0.02 0.03
Strain, mm/mm
0
2
4
6
8
10
Stress,MPa
Strain Rate, s-1
22
21
13
17
23
AR_Glass_SF
0 0.004 0.008 0.012 0.016
Strain, mm/mm
0
2
4
6
8
Stress,MPa
Strain Rate, s-1
21
15
17
15
AR_Glass_PC
Stress-strain of AR-Glass
Composite (plain cement)
0 0.02 0.04 0.06
Strain, mm/mm
0
1000
2000
3000
4000
Stress,MPa
Strain Rate, s-1
19
18
22
18
23
AR Glass Specimen
(4 yarns)
Videos of PE Fabric and PE Composite
PE Composite with Silica FumePE Fabric
Failure of PE Composite
(a) (b) (c) (d) (e)
T= 3.8 ms T= 5.8 ms T= 11.8 msT= 0 ms T= 9.8 ms
(a) (b) (c) (d) (e)
T= 0 ms T= 0.5 ms T= 1.0 ms T= 1.5 ms T= 3.5 ms
Crack
PE composites
(plain cement):
(a) intact,
(b) single cracking,
(c)-(d) crack widening,
(e) complete failure.
PE composites
(5% silica fume):
(a)intact,
(b-d) developing of multiple
cracks,
(e) complete failure
Microstructure of PE Composite
(a) (b)
SEM micrographs of PE fabric in the cement matrix and (a) cross section
of reinforcing yarn, (b) top view of loop
Stress-Strain Curves of PE Fabric and PE
Composite
0 0.05 0.1 0.15 0.2 0.25
Strain, mm/mm
0
1
2
3
Stress,MPa
Strain Rate, s-1
22
21
22
21
23
PE_SF
Stress-strain of PE Composite
(5% Silica Fume)
Stress-strain of PE Composite
(plain cement)
0 0.01 0.02 0.03 0.04
Strain, mm/mm
0
0.4
0.8
1.2
1.6
Stress,MPa
Strain Rate, s-1
26
21
18
26
PE_PC
Videos of Carbon Fiber Bundle and
Carbon Composite
Carbon Composite (plain cement)Carbon Fiber Bundle
Failure of Carbon Composite
(a) (b) (c) (d) (e)
T= 0 ms T= 1.0 ms T= 1.5 ms T= 2.0ms T= 2.5 ms
Carbon composites:
(a)intact,
(b) few of cracks visible,
(c-e) yarn pullout
(a) (b) (c) (d) (e)
T= 0 ms T= 1.0 ms T= 2.0 ms T= 4.0 ms T= 6.0 ms
Carbon composites
(multiple cracking):
(a)intact,
(b) multiple cracking,
(c)-(e) multiple crack
widening
Microstructure of Carbon Composite
(a) (b)
Matrix
Embedded
filaments
SEM micrographs of carbon fiber bundle embedded in cement matrix:
(a) view of cross section and (b) side view
Stress-Strain Curves of Carbon Fiber and
Carbon Composite
0 0.005 0.01 0.015 0.02 0.025
Strain, mm/mm
0
400
800
1200
1600
Stress,MPa
Strain Rate, s-1
17
20
18
17
21
Carbon Fibre Bundle
0 0.04 0.08 0.12
Strain, mm/mm
0
4
8
12
16
20
Stress,MPa
Strain Rate, s-1
9
11
9
Carbon Composite
Stress-Strain of Carbon CompositeStress-Strain of Carbon Fiber Bundle
Comparison of Different Composites
0 0.02 0.04 0.06 0.08 0.1
Strain, mm/mm
0
4
8
12
16
20
Stress,MPa
Carbon Composite
PE Composite
AR Glass Composite
Comparison of typical stress-strain curves
of different composites (plain cement)
0 0.05 0.1 0.15 0.2 0.25
Strain, mm/mm
0
4
8
12
16
20
Stress,MPa
Carbon Composite
PE Composite
AR Glass Composite
Carbon Composite (plain cement)
AR-glass and PE composites (5% silica fume)
Summary Tables
Composites
Strain Rate
(1/s)
Young’s Modulus
(MPa)
Strength
(MPa)
Toughness
(MPa)
Maximum strain
(mm/mm)
PE 23 (4) 140 (24) 1.31(0.17) 0.016(0.007) 0.021(0.007)
AR-Glass 18(3) 1176(323) 5.56(0.51) 0.032(0.009) 0.01(0.002)
Carbon 10(1) 2247(463) 17.86(0.82) 1.21(0.14) 0.10(0.014)
Table 2- Composites Properties (plain cement) under High Rate Loading
Composites
Strain Rate
(1/s)
Young’s Modulus
(MPa)
Strength
(MPa)
Toughness
(MPa)
Maximum strain
(mm/mm)
PE 22 (1) 156 (15) 2.33(0.28) 0.343(0.101) 0.207(0.04)
AR-Glass 19(4) 919(164) 8.27(0.86) 0.127(0.024) 0.025(0.004)
Table 3- Composites Properties (5% silica fume) under High Rate Loading
(the values in parenthesis are standard deviation)
Deju Zhu, Alva Peled, Barzin Mobasher. Dynamic Tensile Testing of Fabric-Cement Composites.
Construction and Building Materials, 2010, in press.
Strain Rate Effect on Composites with
plain cement
0 0.005 0.01 0.015
Strain, mm/mm
0
2
4
6
8
Stress,MPa
Strain rate = 2.2x10-5 s-1
Strain rate = 18 s-1
(a) AR Glass composite
0 0.01 0.02 0.03
Strain, mm/mm
0
0.3
0.6
0.9
1.2
1.5
1.8
Stress,MPa
Strain rate = 2.2x10-5 s-1
Strain rate = 23 s-1
(b) PE composite
0 0.02 0.04 0.06 0.08 0.1
Strain, mm/mm
0
5
10
15
20
25
Stress,MPa
Strain rate = 2.2x10-5 s-1
Strain rate = 10 s-1
(c) Carbon composite
Composite
High speed loading
(1000 mm/s)
Quasi-static loading
(0.004 mm/s)a
Strain Rate
(1/s)
Young’s
Modulus (MPa)
Strength
(MPa)
Toughness
(MPa)
Max.
strain
(mm/mm)
Strength
(MPa)
Max. strain
(mm/mm)
PE
23
(4)
140
(24)
1.31
(0.17)
0.016
(0.007)
0.021
(0.007)
1.36
(0.12)
1.98
(0.97)
AR Glass
18
(3)
1176
(323)
5.56
(0.51)
0.032
(0.009)
0.01
(0.002)
5.11
(0.25)
1.03
(0.07)
Carbon
10
(1)
2247
(463)
17.86
(0.82)
1.21
(0.14)
0.10
(0.014)
26.63
(2.87)
0.03
(0.01)
Applied Velocity
X (Warp Yarn)
Z
Y (Fill Yarn)
Micromechanical modeling of Textile Dry
fabrics
29
•modeling fill and warp yarns and capturing yarn to yarn interaction.
•modeling of contact surfaces as well as mass scaling.
•BCs: Left end of the fabric is fixed and velocity is applied on right end.
• Both contact types (SOFT = 1 & 2) were used
Design of Textile Containment system
30
LG689 Experimental
(47%) Single Layer
(37%)
Multi Layer
(31%)
Projectile Capture
31
LG657 Experimental
(100%) Single Layer
(100%)
Multi Layer
(100%)
Conclusions
 High speed tensile tests of three types of fabric-cement composites
were performed. A fairly uniform tensile behavior was clearly observed
of all composite systems, demonstrating the reliability of the high
speed test method for testing cement-based composites.
 A good correlation was found between the properties of the
composites and the fabrics. The fabric with the highest performance
provides the best composite behavior in the high-rate tensile test, in
this study it is carbon fabric. Differences in tensile behavior of the
various composites were recorded indicating differences in the role of
each fabric as reinforcements under high speed loading.
 A multiple cracking behavior was observed for all the fabric-cement
composites except the PE composite with the matrix of plain cement.
Acknowledgements
The authors would like to thank Nippon Electric Glass Co., Ltd. USA,
SAERTEX GmbH & Co. KG, Germany and Polysack Ltd., Israel for their
cooperation for providing the fabrics used in this study. The US Federal
aviation administration, FAA, National Science Foundation NSF, and the
BSF (United States Israel Bi-national Science Foundation) program
2006098 acknowledged for the financial support in this research.

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High speed tensile testing of textile composites 2a

  • 1. Dynamic Tensile Testing of Fabric-Cement Composites Deju ZHU, Barzin MOBASHER Civil and Environmental Engineering, Arizona State University, USA Flavio SILVA Institute of Construction Materials – Technical University of Dresden, Dresden, Germany Alva PELED Structural Eng. Dept., Ben Gurion University, Israel International Conference on Material Science and 64th RILEM Annual Week Aachen, Germany, Sept. 6– 9, 2010
  • 2. Outline  Introduction  Objectives  Setup of dynamic tensile testing  Specimen preparation and data analysis  Failure behavior of composites  Conclusions
  • 3. Introduction •HPFRCC, Strain-hardening behavior •Cases for dynamic loading: • blast explosions, • projectiles, • earthquakes, • fast moving traffic, • wind gusts, wind driven objects, • machine vibrations. •Inherent brittleness and low tensile strength, dynamic loading can cause severe damage. •mechanical properties at high strain rates for analysis of structural components. 0 0.01 0.02 0.03 0.04 Strain, mm/mm 0 4 8 12 16 20 Stress,MPa AR Glass Fabric GFRC Vf =5% PE Fabric E-Glass Fabric Mortar ECC
  • 4. Objectives Study the role of fabric type on the tensile behavior of textile composites  Study the strain rate effect on the mechanical material properties  Investigate the failure behavior (cracking) of different composite system under dynamic loading
  • 5. High Speed Testing System at ASU Servohydraulic system, Speed Up to 14 m/s, Load Capacity: 90 kN load
  • 6. High Strain Rate Tensile Test
  • 7. AR-Glass- bonded Carbon FabricPE- Knitted Textile Materials Alkali Resistant (AR)-Glass: Bonded fabric, multifilament impregnated with sizing Polyethylene (PE): Knitted fabric, monofilament Carbon Fabric: Fiber Bundle 5mm Yarn type Yarn nature Strength (MPa) Young’s Modulus (MPa) Filament size (mm) Bundle diameter (mm) PE Monofilament 240 1760 0.250 0.25 AR-Glass Bundle 1372 72000 0.014 0.30 Carbon Bundle 2200 240000 0.008 1.15 Table 1 Mechanical properties and geometry of the yarns used in the fabric manufacture
  • 8. Composite Preparation: Pultrusion Process Cement Composite Laminates Squeeze Rollers Cement Bath Fabric Mix design of the matrix Cement: 42% Silica fume: 0% and 5% Super-plasticizer: 0.1% water/cement ratio :0.4 Composite: 6 layer fabrics Curing: in water at room temperature for 28 days Cut into specimens: 25mm x150 mm (width x length).
  • 12. Typical Response under high speed Tension
  • 13. Videos of AR-Glass Fabric and Composites AR-Glass CompositeAR-Glass Fabric
  • 14. Failure of AR-Glass Composite (a) (b) (c) (d) (e) T= 0.4 ms T= 0.6 ms T= 0.8 ms T= 1.5 ms Yarn breakage T= 4.0 ms AR glass composites (plain cement): (a)-(c) multiple micro- cracking, (d) main crack widening and other micro-cracks closing, (e) complete failure (a) (b) (c) (d) (e) T= 0.5 ms T= 5.8 ms T= 4.0 msT= 0 ms T= 1.5 ms AR glass composites (5%silica fume): (a)-(c) multiple micro- cracking, (d) main crack widening and other micro-cracks closing, (e) complete failure
  • 15. Microstructure of AR-Glass Composite Bundle with coating Matrix SEM micrographs of AR glass fabric embedded in cement matrix, side view
  • 16. Stress-Strain Curves of AR-Glass Fabric and AR-Glass Composite Stress-strain of AR-Glass Composite(5% Silica Fume) Stress-strain of AR-Glass Fabric 0 0.01 0.02 0.03 Strain, mm/mm 0 2 4 6 8 10 Stress,MPa Strain Rate, s-1 22 21 13 17 23 AR_Glass_SF 0 0.004 0.008 0.012 0.016 Strain, mm/mm 0 2 4 6 8 Stress,MPa Strain Rate, s-1 21 15 17 15 AR_Glass_PC Stress-strain of AR-Glass Composite (plain cement) 0 0.02 0.04 0.06 Strain, mm/mm 0 1000 2000 3000 4000 Stress,MPa Strain Rate, s-1 19 18 22 18 23 AR Glass Specimen (4 yarns)
  • 17. Videos of PE Fabric and PE Composite PE Composite with Silica FumePE Fabric
  • 18. Failure of PE Composite (a) (b) (c) (d) (e) T= 3.8 ms T= 5.8 ms T= 11.8 msT= 0 ms T= 9.8 ms (a) (b) (c) (d) (e) T= 0 ms T= 0.5 ms T= 1.0 ms T= 1.5 ms T= 3.5 ms Crack PE composites (plain cement): (a) intact, (b) single cracking, (c)-(d) crack widening, (e) complete failure. PE composites (5% silica fume): (a)intact, (b-d) developing of multiple cracks, (e) complete failure
  • 19. Microstructure of PE Composite (a) (b) SEM micrographs of PE fabric in the cement matrix and (a) cross section of reinforcing yarn, (b) top view of loop
  • 20. Stress-Strain Curves of PE Fabric and PE Composite 0 0.05 0.1 0.15 0.2 0.25 Strain, mm/mm 0 1 2 3 Stress,MPa Strain Rate, s-1 22 21 22 21 23 PE_SF Stress-strain of PE Composite (5% Silica Fume) Stress-strain of PE Composite (plain cement) 0 0.01 0.02 0.03 0.04 Strain, mm/mm 0 0.4 0.8 1.2 1.6 Stress,MPa Strain Rate, s-1 26 21 18 26 PE_PC
  • 21. Videos of Carbon Fiber Bundle and Carbon Composite Carbon Composite (plain cement)Carbon Fiber Bundle
  • 22. Failure of Carbon Composite (a) (b) (c) (d) (e) T= 0 ms T= 1.0 ms T= 1.5 ms T= 2.0ms T= 2.5 ms Carbon composites: (a)intact, (b) few of cracks visible, (c-e) yarn pullout (a) (b) (c) (d) (e) T= 0 ms T= 1.0 ms T= 2.0 ms T= 4.0 ms T= 6.0 ms Carbon composites (multiple cracking): (a)intact, (b) multiple cracking, (c)-(e) multiple crack widening
  • 23. Microstructure of Carbon Composite (a) (b) Matrix Embedded filaments SEM micrographs of carbon fiber bundle embedded in cement matrix: (a) view of cross section and (b) side view
  • 24. Stress-Strain Curves of Carbon Fiber and Carbon Composite 0 0.005 0.01 0.015 0.02 0.025 Strain, mm/mm 0 400 800 1200 1600 Stress,MPa Strain Rate, s-1 17 20 18 17 21 Carbon Fibre Bundle 0 0.04 0.08 0.12 Strain, mm/mm 0 4 8 12 16 20 Stress,MPa Strain Rate, s-1 9 11 9 Carbon Composite Stress-Strain of Carbon CompositeStress-Strain of Carbon Fiber Bundle
  • 25. Comparison of Different Composites 0 0.02 0.04 0.06 0.08 0.1 Strain, mm/mm 0 4 8 12 16 20 Stress,MPa Carbon Composite PE Composite AR Glass Composite Comparison of typical stress-strain curves of different composites (plain cement) 0 0.05 0.1 0.15 0.2 0.25 Strain, mm/mm 0 4 8 12 16 20 Stress,MPa Carbon Composite PE Composite AR Glass Composite Carbon Composite (plain cement) AR-glass and PE composites (5% silica fume)
  • 26. Summary Tables Composites Strain Rate (1/s) Young’s Modulus (MPa) Strength (MPa) Toughness (MPa) Maximum strain (mm/mm) PE 23 (4) 140 (24) 1.31(0.17) 0.016(0.007) 0.021(0.007) AR-Glass 18(3) 1176(323) 5.56(0.51) 0.032(0.009) 0.01(0.002) Carbon 10(1) 2247(463) 17.86(0.82) 1.21(0.14) 0.10(0.014) Table 2- Composites Properties (plain cement) under High Rate Loading Composites Strain Rate (1/s) Young’s Modulus (MPa) Strength (MPa) Toughness (MPa) Maximum strain (mm/mm) PE 22 (1) 156 (15) 2.33(0.28) 0.343(0.101) 0.207(0.04) AR-Glass 19(4) 919(164) 8.27(0.86) 0.127(0.024) 0.025(0.004) Table 3- Composites Properties (5% silica fume) under High Rate Loading (the values in parenthesis are standard deviation) Deju Zhu, Alva Peled, Barzin Mobasher. Dynamic Tensile Testing of Fabric-Cement Composites. Construction and Building Materials, 2010, in press.
  • 27. Strain Rate Effect on Composites with plain cement 0 0.005 0.01 0.015 Strain, mm/mm 0 2 4 6 8 Stress,MPa Strain rate = 2.2x10-5 s-1 Strain rate = 18 s-1 (a) AR Glass composite 0 0.01 0.02 0.03 Strain, mm/mm 0 0.3 0.6 0.9 1.2 1.5 1.8 Stress,MPa Strain rate = 2.2x10-5 s-1 Strain rate = 23 s-1 (b) PE composite 0 0.02 0.04 0.06 0.08 0.1 Strain, mm/mm 0 5 10 15 20 25 Stress,MPa Strain rate = 2.2x10-5 s-1 Strain rate = 10 s-1 (c) Carbon composite Composite High speed loading (1000 mm/s) Quasi-static loading (0.004 mm/s)a Strain Rate (1/s) Young’s Modulus (MPa) Strength (MPa) Toughness (MPa) Max. strain (mm/mm) Strength (MPa) Max. strain (mm/mm) PE 23 (4) 140 (24) 1.31 (0.17) 0.016 (0.007) 0.021 (0.007) 1.36 (0.12) 1.98 (0.97) AR Glass 18 (3) 1176 (323) 5.56 (0.51) 0.032 (0.009) 0.01 (0.002) 5.11 (0.25) 1.03 (0.07) Carbon 10 (1) 2247 (463) 17.86 (0.82) 1.21 (0.14) 0.10 (0.014) 26.63 (2.87) 0.03 (0.01)
  • 28. Applied Velocity X (Warp Yarn) Z Y (Fill Yarn)
  • 29. Micromechanical modeling of Textile Dry fabrics 29 •modeling fill and warp yarns and capturing yarn to yarn interaction. •modeling of contact surfaces as well as mass scaling. •BCs: Left end of the fabric is fixed and velocity is applied on right end. • Both contact types (SOFT = 1 & 2) were used
  • 30. Design of Textile Containment system 30 LG689 Experimental (47%) Single Layer (37%) Multi Layer (31%)
  • 31. Projectile Capture 31 LG657 Experimental (100%) Single Layer (100%) Multi Layer (100%)
  • 32. Conclusions  High speed tensile tests of three types of fabric-cement composites were performed. A fairly uniform tensile behavior was clearly observed of all composite systems, demonstrating the reliability of the high speed test method for testing cement-based composites.  A good correlation was found between the properties of the composites and the fabrics. The fabric with the highest performance provides the best composite behavior in the high-rate tensile test, in this study it is carbon fabric. Differences in tensile behavior of the various composites were recorded indicating differences in the role of each fabric as reinforcements under high speed loading.  A multiple cracking behavior was observed for all the fabric-cement composites except the PE composite with the matrix of plain cement.
  • 33. Acknowledgements The authors would like to thank Nippon Electric Glass Co., Ltd. USA, SAERTEX GmbH & Co. KG, Germany and Polysack Ltd., Israel for their cooperation for providing the fabrics used in this study. The US Federal aviation administration, FAA, National Science Foundation NSF, and the BSF (United States Israel Bi-national Science Foundation) program 2006098 acknowledged for the financial support in this research.